DatosDestilacionC (LS)

Descargar como xlsx, pdf o txt
Descargar como xlsx, pdf o txt
Está en la página 1de 19

%v/v Propiedades Densidad[kg/m3]

Alimentancion 15 Etanol 789


Destilado (1) 95 Agua 997
Fondos (1) 8

Alimentacion Destilado Fondos


V sln [m3] 0.005 0.00004 0.0002
V etanol [m3] 0.00075 0.000038 0.000016
V Agua [m3] 0.00425 0.000002 0.000184

Fracciones teoricas a P = 1 atm


x y 1

0 0 0.9
0.019 0.17 0.8

Fraccion mol etanol vapor (y)


0.0721 0.3891 0.7
q>1
0.0966 0.4375 0.6
0.1238 0.4704 0.5
0.1661 0.5089 0.4
0.2337 0.5445 0.3
0.2608 0.558
0.2
0.3273 0.5826
0.1
0.3965 0.6122
0
0.5079 0.6564 0 0.1 0.2 0.3 0.4 0.5 0.6
0.5198 0.6599 Fraccion mol etanol liquid
0.5732 0.6841
0.6763 0.7385
Datos tomados de :
0.7472 0.7815 HADRICH, B., BOUDHRIOUA, N., & KECHAOU, N. ID
0.8943 0.8943 BEST MODEL AND PARAMETERS FOR TYX EQUILIBR
1 1 ETHANOL-WATER MIXTURE.
Linea donde y =x
x y
0 0
0.019 0.019
1
0.0721 0.0721
0.9
0.0966 0.0966
0.8
Fraccion mol etanol vapor (y)

0.1238 0.1238
0.1661 0.1661 0.7

0.2337 0.2337 0.6


0.2608 0.2608 0.5
0.4
0.3
0.2
0.1
0.8

Fraccion mol etanol vapor (


0.7
0.6
0.5
0.3273 0.3273 0.4
0.3965 0.3965 0.3
0.5079 0.5079 0.2
0.5198 0.5198 0.1
0.5732 0.5732 0
0.6763 0.6763 0 0.1 0.2 0.3 0.4 0.5 0.
0.7472 0.7472 Fraccion mol etanol liqu
0.8943 0.8943
1 1
PM[g/mol]
46.07
18

Alimenatacion Destilado
Compuesto masa [kg] moles[mol] Fraccion molar masa [kg] moles[mol]
Etanol 0.59175 12.8445843 0.051741070758 0.029982 0.65079227263
Agua 4.23725 235.402778 0.948258929242 0.001994 0.11077777778
Total 4.829 248.247362 1 0.031976 0.76157005041

REFLUJO MINIMO

Intercepto Rmin
0.285 1.99838689

0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1


Fraccion mol etanol liquido (x)

de :
OUDHRIOUA, N., & KECHAOU, N. IDENTIFICATION OF THE
ND PARAMETERS FOR TYX EQUILIBRIUM DATA OF
ER MIXTURE.

REFLUJO MAXIMO

Intercepto Rmax
0.1 7.54540265
0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
Fraccion mol etanol liquido (x)
Destilado Fondos
Fraccion molar masa [kg] moles[mol] Fraccion molar
0.854540264919 0.012624 0.2740178 0.026182779453952
0.145459735081 0.183448 10.1915556 0.973817220546049
1 0.196072 10.4655734 1

NUMERO DE ETAPAS MINIMAS


%v/v Propiedades Densidad[kg/m3]
Alimentancion 15 Etanol 789
Destilado (1) 92 Agua 997
Fondos (1) 10

Alimentacion Destilado Fondos


V sln [m3] 0.005 0.00006 0.0001226
V etanol [m3] 0.00075 0.0000552 0.00001226
V Agua [m3] 0.00425 0.0000048 0.00011034

Fracciones teoricas a P = 1 atm xD(18 min) 0.780498262429261


x y xD(70 min) 0.854540264918946
0 0
0.019 0.17 Xd (70 min) b
0.0721 0.3891 0.8545402649189 0.854540264918946
0.0966 0.4375 0 0.213635066229737
0.1238 0.4704
0.1661 0.5089 xD(18 min) b
0.2337 0.5445 0.7804982624293 0.780498262429261
0.2608 0.558 0 0.195124565607315
0.3273 0.5826
0.3965 0.6122
0.5079 0.6564
0.5198 0.6599
0.5732 0.6841
0.6763 0.7385
0.7472 0.7815
0.8943 0.8943
1 1 EFICIENCIA
Linea donde y =x

Eficiencia O'conell
x y (70 min)
0 0 0.597901
0.019 0.019 0.596161
0.0721 0.0721 0.594415
0.0966 0.0966 0.592631
0.1238 0.1238 0.590775
0.1661 0.1661 0.588806
0.2337 0.2337 0.586678
0.2608 0.2608 0.584329
0.3273 0.3273 0.581674
0.3965 0.3965 0.578594
0.5079 0.5079 0.574911
0.5198 0.5198 0.570334
0.5732 0.5732 0.56436
0.6763 0.6763 0.556001
0.7472 0.7472 0.542979
0.8943 0.8943 0.518445
1 1 0.457302
0.391057
Promedio 0.559297388888889
PM[g/mol]
46.07
18

Alimenatacion Destilado
Compuesto masa [kg] moles[mol] Fraccion molar masa [kg] moles[mol]
Etanol 0.59175 12.8445843 0.051741070758 0.0435528 0.94536140656
Agua 4.23725 235.402778 0.948258929242 0.0047856 0.26586666667
Total 4.829 248.247362 1 0.0483384 1.21122807322

0.9

0.8
Fraccion mol etanol vapor (y)

0.7

0.6

0.5
18 min
0.4 70 min

0.3

0.2

0.1

0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
Fraccion mol etanol liquido (x)

Eficiencia
O'conell (18
min)
0.579112
0.571262
0.561935
0.549535
0.530147
0.490862
0.418298
0.384502
0.378777
0.377951
0.377831
0.377814
0.377812
0.377811
0.377811
0.377811
0.377811
0.377811
0.4369385
Destilado Fondos
Fraccion molar masa [kg] moles[mol] Fraccion molar
0.780498262429 0.00967314 0.20996614 0.033214207008703
0.219501737571 0.11000898 6.11161 0.966785792991297
1 0.11968212 6.32157614 1
PERFIL DE TEMPERATURA

t [min] TB [°C] TD [°C] Ts1 [°C] Ts2 [°C] Ts3 [°C] Ts4 [°C]
10 79.9 76.7 70.6 63.8 63.4 62.4
14 77.1 76.7 71.3 63.8 63.6 62.6
21 77.7 76.7 70.5 72.5 70.5 67.8
28 78.1 76.7 72.8 70.3 69 60.6
36 78.5 76.7 73.4 73 67.3 64.5
41 79 76.7 73.3 73.7 72.8 70.3
46 79.5 76.7 73.2 74.3 73.6 71.2
64 80.7 76.7 75 76.5 66.3 63.7

90

80

70

60
Temperatura [°C]

TB
50 TD
40 TS1
TS2
30 TS3
20 TS4
TS5
10

0
0 10 20 30 40 50 60 70
Tiempo [min]
Ts5 [°C]
63.8
63.9
67.1
66.2
64.8
67.2
64.5
64
Metodo grafico
xD xW 1/(xD-xW) I
0.78049826 0.05174107 1.37219915 0.03296262
0.85454026 0.02618278 1.20720826

F 248.247362
W 240.190749
D 8.04925053
xd 0.81440402

VOLATILIDAD RELATIVA

K-value profiles

Etapa Etanol Agua α


1 1.0344 0.877736 1.17849 Ec. Rayleigh α=cte
2 1.0556 0.842271 1.25331 Ln(F/W) 0.03299228
3 1.0847 0.808062 1.34235 xf 0.05174107
4 1.1278 0.772675 1.45963 xw 0.04139658
5 1.2001 0.733237 1.63674 α 11.49
6 1.3493 0.685249 1.96901 Ec. Rayleigh 0.00015534
7 1.8150 0.622614 2.91506 (xD)avg 0.36014008
8 3.9412 0.601946 6.54745
9 7.1649 0.693239 10.33538
10 8.3037 0.734164 11.31044
11 8.5018 0.741528 11.46527
12 8.5313 0.742629 11.48796
13 8.5356 0.742788 11.49125
14 8.5362 0.742812 11.49171
15 8.5363 0.742815 11.49178
16 8.5363 0.742815 11.49180
17 8.5363 0.742815 11.49180
18 8.5363 0.742815 11.49180
19 8.5363 0.742815 11.49181
20 8.5363 0.742815 11.49181

También podría gustarte