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Manual Flash Pasteurizacion

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OPERATION MANUAL

FLASH
PASTEURIZATION
(FP & UFP SYSTEMS)
Keg cleaner, keg cleaning, Sankey keg, semi-automatic keg washing, sanitizing & filling, semi-automatic keg washing, sanitizing and filling, automatic keg washing, sanitizing & filling, semi-automatic keg washing, sanitizing and filling, stainless steel Sankey keg, American Sankey, European Sankey, Flash Pasteurizer, Flash Pasteurize, Flash Pasteurization, Brewing System, Brew House, Brewery, Micro Brewer, Keg Washer, Fill By Weight, Wine on Tap, Winemaker, Fill By Weight Keg Filling, Fill By Weight Beer, Fill By Weight Wine

Keg cleaner, keg cleaning, Sankey keg, semi-automatic keg washing, sanitizing & filling, semi-automatic keg washing, sanitizing and filling, automatic keg washing, sanitizing & filling, semi-automatic keg washing, sanitizing and filling, stainless steel Sankey keg, American Sankey, European Sankey, Flash Pasteurizer, Flash Pasteurize, Flash Pasteurization, Brewing System, Brew House, Brewery, Micro Brewer, Keg Washer, Fill By Weight, Wine on Tap, Winemaker, Fill By Weight Keg Filling, Fill By Weight Beer, Fill By Weight Wine

Keg cleaner, keg cleaning, Sankey keg, semi-automatic keg washing, sanitizing & filling, semi-automatic keg washing, sanitizing and filling, automatic keg washing, sanitizing & filling, semi-automatic keg washing, sanitizing and filling, stainless steel Sankey keg, American Sankey, European Sankey, Flash Pasteurizer, Flash Pasteurize, Flash Pasteurization, Brewing System, Brew House, Brewery, Micro Brewer, Keg Washer, Fill By Weight, Wine on Tap, Winemaker, Fill By Weight Keg Filling, Fill By Weight Beer, Fill By Weight Wine

PROCESS & PACKAGING, INC.


5450 Tech Circle, Moorpark, CA 93021

Tel: (805) 529-9890 Fax: (805) 529-9282

TABLE OF CONTENTS

TITLE

SECTION

Table of contents
What is Pasteurization
Preface
Disclaimer
Confidentiality and Copyrights
Operational Safety Notes

EMERGENCY STOP

Training
Specifications
Start-up and Shut-down Procedure
C.I.P. Procedures
Machine Layout
Electrical Section
Mechanical Section
Pneumatics Section
I/O List
Oxine
Planned Prevenative Maintenance Schedule
Dimensions
Spares
Services
Cycle Times
Flow Diagram
Control Philosophy
Appendix Section

PROCESS & PACKAGING, INC.

A
a
B
C
D
E
F
G
H
I
J
K
L
M
N
O
P
R
S
T
V
W
X
Z

PREFACE

The SYSTEM has been designed as a self contained and reliable automatic Flash
Pasteurization system.
The following instructions and information have been prepared to clarify operational and
maintenance procedures and should ensure long, reliable service from the machine if
followed carefully.
Proper maintenance and use of approved spare parts will extend the life of the system and
it's reliability.
The use of any non approved spare parts may void any warrants or guarantees, actual or
implied.

DISCLAIMER

The customer assumes all responsibility for the SYSTEM once delivered. The SYSTEM is
tried and tested equipment. As such IDD Processing & Packaging will not be held
responsible for alterations and modifications carried out by the customer without the written
approval of IDD Processing & Packaging.

CONFIDENTIALITY & COPYRIGHT


All information within is confidential and the copyright of IDD Process & Packaging, Inc.
No portion of this data shall be released, disclosed, used or duplicated for use in
procurement or manufacturing without the express written permission from IDD Process &
Packaging, Inc.

PROCESS & PACKAGING, INC.

OPERATIONAL SAFETY NOTES E


WEAR SAFETY GOGGLES
Wear Safety Goggles approved for use by your Safety and Operational Procedures
Committees when operating or observing this system.

WEAR CHEMICAL-RESISTANT GLOVES


Wear Chemical-Resistant Gloves approved for use by your Safety and Operational
Procedures Committees.

WEAR BACK SUPPORT EQUIPMENT


Wear Back Support Equipment approved for use by your Safety and Operational Procedures
Committees and use proper lifting technique approved for use by your Safety and
Operational Procedures Committees.

VENTILATION
Area should have adequate ventilation approved for use by your Safety and Operational
Procedures Committees.
Respirators should be used during cleaning and operations where fumes are present.

EMERGENCY STOP
MANUAL STOP
In an emergency use the RED mushroom button to isolate the power and stop the process
sequence at any time. The Emergency Stop Button is located on the Main Control Panel.

PROCESS & PACKAGING, INC.

TRAINING

SPECIFICATIONS

.
On-site training is available from our technical staff at the customers request.

Output parameters.
Note: Insert your specific optimum and acceptable values into this chart for your internal
reference. This chart is the be used as a bench mark in the future of your production.
Change in operating personnel, valves, wash sequences and mechanical integrity can be
tracked with this bench-marking.
Date:

Temperatures:

Chase Times:

Special Notes:

PROCESS & PACKAGING, INC.

Flow Rate:

START UP AND SHUT DOWN PROCEDURES

SEE CONTROL PHILOSOPHY


SECTION FOR DETAILS

PROCESS & PACKAGING, INC. 1999

C.I.P. PROCEDURES

See the 'Control Philosophy' section


and the following notes to suit the
specific plant requirements

PROCESS & PACKAGING, INC. 1999

MACHINE LAYOUT

PROCESS & PACKAGING, INC. 1999

ELECTRICAL SECTION

PLEASE NOTE:
Customer to supply local disconnect and ground fault device

PROCESS & PACKAGING, INC. 1999

MECHANICAL SECTION

SEE SUPPLEMENTAL
TECHNICAL DATA MANUAL
FOR ADDITIONAL INFORMATION
IF PROVIDED

PROCESS & PACKAGING, INC. 2003

BUTTERFLY VALVES

F.lli TASSALINI s.p.a.

F.lli TASSALINI S.p.A.

Application

Features

BUTTERFLY VALVES

Butterfly valves are universal and economical on/off routing valves


used for isolation and control in food processing pipelines.

They are sanitary valves that offer low flow resistance and
reversible flow direction providing gentle treatment of product.
Valve maintenance is easy and valves have long service life.
All flanges with the same diameter are interchangeable thus
allowing any combination of outlets as well as combinations
between different standards.
Valves can be operated manually or pneumatically.
Manual valves are available with a wide choice of handles that lock
in intermediate positions, so that the flowrate can be regulated.
Pneumatic valves are available with a full range of accessories,
including horizontal and vertical single-, double-acting and flow
control actuators, control tops and electrical components.
All handles and actuators are fitted onto the valve with the same
connection. This allows for great flexibility and increased savings
during extensions or modifications of processing lines.

Components

PARTS LIST

1
2
3
4
11

Butterfly
Seal
Screw
Flange
Bush

Aisi 316L
Silicone, EPDM, FTM, PTFE-coated FTM, PTFE + silicone
Aisi 304L
Aisi 304L/Aisi 316L
PTFE

Page 1

F.lli TASSALINI S.p.A.

Technical Data

BUTTERFLY VALVES

Max. product pressure: 700 kPa (7 bar); for valves with PTFE seals
max 200 kPa (2 bar).
Recommended working pressure: 600 kPa (6 bar).
General temperature range: -10C +95C (+15F +205F).
Seals temperature range:
!

silicone: -50C +200C (-60F +390F);

EPDM: -30C +140C (-20F +280F);

FTM: -15C +220C (+5F +430F);

PTFE-coated FTM: -10C +150C (+15F +300F);

PTFE + silicone: -10C +150C (+15F +300F).

Finish: 120 grit (max Ra 1.01-1.14 m, 40-45 ).


Production range:
!

manual butterfly valves from DN 10 to DN 250 and to


10;

pneumatic butterfly valves from DN 25 to DN 100 and 1


to 4.

Connections: welding end, expanding end, threaded end, liner +


nut, bend, flange, ferrule end.
Standards: DIN, SMS, RJT BS, IDF ISS, BSP, Eno, Macon, Clamp.
Steel grades: Aisi 304L, Aisi 316L.

Torque Ratings

Butterfly valves with silicone seal:


OPEN

DIAMETER

[90]

1
1
2
2
3

1
1
2
5
6

Page 2

NW
NW
NW
NW
NW

CLOSE

[0]
5 NW
5 NW
17 NW
28 NW
32 NW

F.lli TASSALINI S.p.A.

p (kPa)

Butterfly valves DIN:

Flowrate Q = m3/h

Butterfly valves SMS, RJT BS, IDF ISS, Clamp:

p (kPa)

Pressure Drop

BUTTERFLY VALVES

Flowrate Q = m3/h

For further technical information, section and dimensional


drawings and range of models available please refer to our series
of product brochures, technical catalogues and valve manuals.

Page 3

API Schmidt-Bretten

Plate Heat Exchangers


Plate Pack Arrangement

Contract Number:
Plate Grouping:

NP111012-101

Document Number: 4-026-GBF-086-001.PA

SECT 1

1/1*3SH

Left Side (Beer)

HEATING

1/1*3SH

Right Side (Water)

SECT 2

8/8*4SH

Left Side (Beer)

REGEN

8/6*4SH+2*4SW

SECT 3
COOLING

1/1*7SH
2/2*3SH

Plate Summary:

Part Number
3-026-B5HM-00F23
3-026-B6HM-00F01
3-026-B6HM-00F02
3-026-B5HM-00F03
3-026-B6HM-00F04
3-026-B6HM-00F05
3-026-B6HM-00F06
3-026-B6HM-00F11
3-026-B6HM-00F12
3-026-B6HM-00F16
3-026-B6HM-00F26
3-026-B6HM-00F29
3-026-B5WM-00F03
3-026-B6WM-00F05
3-026-B6WM-00F06

Right Side (Beer)


Left Side (PG 25%)
Right Side (Beer)
Qty
1
5
5
48
1
3
3
6
5
1
1
1
4
1
1
86

Arrangement:

Plate No.

Part Number

1
2
3
4
5
6
7

3-026-B5HM-00F23
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F04
3-026-B6HM-00F16
INTERMEDIATE GRID
3-026-B6HM-00F26
3-026-B6HM-00F12
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F02
3-026-B6HM-00F05
3-026-B6HM-00F11
3-026-B5HM-00F03

8
9
10
11
12
13
14
15
16
17
18
19

Plate Pack Dimension:


22.423 inches Maximum
21.756 inches Minimum

Total

Figure

R
L
R
L
R
L
R

ACR/ECR
CL
CR
CL
CR
DL
PR

L
R
L
R
L
R
L
R
L
R
L
R

AFL/EFL
KR
CL
CR
CL
CR
CL
CR
BL
FR
KL
CR

Gaskets face fixed head.

Page 1 of 3

API Schmidt-Bretten
Arrangement:

Plate No.
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70

Plate Heat Exchangers


Part Number

3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F01
3-026-B6HM-00F06
3-026-B6HM-00F12
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F02
3-026-B6HM-00F05
3-026-B6HM-00F11
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F01
3-026-B6HM-00F06
3-026-B6HM-00F12
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F02
3-026-B6HM-00F05
3-026-B6HM-00F11
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F01
3-026-B6HM-00F06
3-026-B6HM-00F12
3-026-B5HM-00F03
3-026-B5WM-00F03
3-026-B5HM-00F03
3-026-B5WM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F02
3-026-B6WM-00F05
3-026-B6HM-00F11
3-026-B5HM-00F03
3-026-B5WM-00F03
3-026-B5HM-00F03
3-026-B5WM-00F03

Figure
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L
R
L

Gaskets face fixed head.

CL
CR
CL
CR
AL
ER
LL
CR
CL
CR
CL
CR
BL
FR
KL
CR
CL
CR
CL
CR
AL
ER
LL
CR
CL
CR
CL
CR
BL
FR
KL
CR
CL
CR
CL
CR
AL
ER
LL
CR
CL
CR
CL
CR
BL
FR
KL
CR
CL
CR
CL

Page 2 of 3

API Schmidt-Bretten
Arrangement:

Plate Heat Exchangers

Plate No.

Part Number

71
72

3-026-B6HM-00F01
3-026-B6WM-00F06
INTERMEDIATE GRID
3-026-B6HM-00F29
3-026-B6HM-00F11
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F02
3-026-B6HM-00F12
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B5HM-00F03
3-026-B6HM-00F01
3-026-B6HM-00F11

73
74
75
76
77
78
79
80
81
82
83
84
85
86

Figure
R
L

BR
FL

R
L
R
L
R
L
R
L
R
L
R
L
R
L

AJR/EJR
KL
CR
CL
CR
CL
AR
LL
CR
CL
CR
CL
BR
KL

Gaskets face fixed head.

Page 3 of 3

TOLLERANZE OVE NON INDICATE

SECONDO ISO-2768 CL.-C- (grossolana)

535

da

da

SEZIONE A-A

M 20

da

da

0,5

120

400

1000

4000

fino a

fino a

fino a

fino a

fino a

fino a

fino a

fino a

30

120

400

1000

2000

4000

0,2

0,3

da

da

30

0,5

0,8

da

1,2

da

2
3

12
239

1
10

100

579

435

6
A
VITE TCEI M10X20

A2

95423

ANELLO ELAST. D18,5

A2

94042

VOLANTINO VI/190

AISI 304

97062

RONDELLA 44X20 SP 3

NYLON

71085

TRAVERSINO

97210

BUSSOLA PER SNODO

AISI304

97285

SNODO

AISI 304

71017

BRACCIO

9604

GUARNIZIONE G/200LKD

7CA0801

COPERCHIO 200LKD

7TA0802

TELAIO C/SUPP.

Pos

N doc.

Descrizione

11

VARIANTI
P. MAX (bar)
MESCOLE
4,8
NBR
EPDM
SILICONE
FPM

ZORZINI S.p.A.

Modifica

95020

10

Ind.

11

1
V.MESCOLE

1
1
1

Materiale

Q.t

note

NOME
TITOLO

MOD.200 LKD

Disegnato

SERIE 201LKD
ISO

DATA

26/04/2007

Controllato
Peso

Scala

27,4
GRUPPO

ORSARIA

1:5

Firma

Orsaria
Cl.

Materiale

14404-14301

CODICE

FA08-100

Revisione

Ai sensi delle vigenti leggi, la Zorzini spa si riserva la propiet di questo disegno con il divieto di riprodurlo e/o renderlo noto
a terzi senza autorizzazione

TOLLERANZE OVE NON INDICATE

SECONDO ISO-2768 CL.-C- (grossolana)

H1

da

da

120

400

1000

4000

fino a

fino a

fino a

da

fino a

fino a

fino a

fino a

30

120

400

1000

2000

4000

0,2

0,3

da

30

0,5

0,8

da

1,2

da

SP

da

0,5
fino a

da

440

SP2
457
A

SEZIONE A-A

498

334

5
7

94053

VOLANT. MEC/90 M16

97008

RONDELLA 16X30

71080

TRAVERSINO

95421

ANELLO ELAS.10

93012

SPINA TESTA TORNITA

71031

BRACCIO

V.MESCOLE

H
60
80
60
80

1
14404-EN10028-7

AISI 304

A2

AISI 304

1
1

7CA0400

COPERCHIO FINITO

7TA0400

TELAIO C/SUPPORTI

Pos

N doc.

Descrizione

Materiale

Q.t

note

H1
166
186
166
186

ZORZINI S.p.A.

GUARNIZIONE G/170

Modifica

9621

Ind.

SP
6
6
8
8

VARIANTI
SP 2
1,5
1,5
2
2

P. MAX (bar)
1,3
1,3
1,3
1,3
NOME

TITOLO

PORTELLA 180
GRUPPO

SERIE 180
ISO

Disegnato

ORSARIA

MESCOLE
NBR
EPDM
SILICONE
FPM
DATA

Firma

26/04/2007

Controllato
Peso

Scala

CODICE

FA04

Materiale

Revisione

Ai sensi delle vigenti leggi, la Zorzini spa si riserva la propiet di questo disegno con il divieto di riprodurlo e/o renderlo noto
a terzi senza autorizzazione

TOLLERANZE OVE NON INDICATE

SECONDO ISO-2768 CL.-C- (grossolana)

547

da

da

da

0,5

120

400

1000

4000

fino a

fino a

fino a

fino a

fino a

fino a

fino a

fino a

30

120

400

1000

2000

4000

0,2

0,3

da

60
8

440

da

30

0,5

0,8

1,2

da

NOTE
P. MAX (bar)
MESCOLE
0,5
NBR
EPDM
SILICONE
FPM

180

da

da

332

SEZIONE A-A

9
10
345

13
11

452
A
14

97257

TUBO DIST. L=123

AISI 304

13

91030

TIRANTE M12X166

AISI 304

12

71005

BRACCIO di CHIUSURA

11

94031

VOL. VI165A C/CODOLO

10

97044

RONDELLA 34 SP 3

91009

TIRANTE M16 L=120

14301/7-EN10028-7

95421

ANELLO ELAS.10

A2

93006

SPINA 12X30

AISI 304

95210

DADO CIECO M12

A2

97031

RONDELLA M12 GROWER

A2 ARM.

95031

VITE TE M12X50

A2

9620

GUARNIZIONE G/R165

V.MESCOLE

7CA2700

COPERCHIO FINITO

7TA2700

TELAIO C/SUPPORTI

Pos

N doc.

Descrizione

14

1
AISI 304

1
1

Materiale

Q.t

ZORZINI S.p.A.

note

Ind.

Modifica

12

3
NOME

TITOLO

PORTELLA 165
GRUPPO

SERIE 165

Disegnato

ORSARIA

DATA

Firma

26/04/2007

Controllato
Peso

12,8

Scala

Materiale

1:5

14404-14301

CODICE

FA27

Ai sensi delle vigenti leggi, la Zorzini srl si riserva la propriet di questo disegno con il divieto di riprodurlo e/o renderlo noto a terzi senza autorizzazione.

Revisione

Materiale
Moteriol

I Temperatura
I Peso
I Temperature
lWeight

ffiffi

ffire
ffire

Guarnizione
Gosket
Montaggio
sulcoperchio,
senza
cnllante
Fixedon the cover,withoutglue

Temperatura
Temperature

ffiffi

Guarnizione
Gosket
senza
Montaggio
sulcoperchio,
collante
Fixedon the cover,withoutglue

Materiale
Moteriol

I Temperatura
I Pesokg
I Tenperoture
lWeightkg

Guarnizione
Gosket
Montaggio
sulcoperchio,
concollante
Fixedon the covenwith glue

Materiale
Moteriol

I Temperatura
I Pesokg
I Temperoture
lWeightkg

Guarnizione
Gosket
Montaggio
sulcoperchio,
senza
cnllante
Fixedon the cover,withoutglue

=N

Materiale
Moteriol

<s

e=

I Temperatura
I eesotg
I Temperature
lWeightkg

Guarnizione
Gosket
Montaggio
senza
sulcoperchio,
collante
Fixedon the cover,withoutglue

rJ.Jtr

==

Eg

Guarnizione
Goskef
Montaggio
sulcoperchio,
senza
collante
Fixedon the cover,withoutglue

Guarnizione
Gosket
Montaggio
sulcoperchio,
senza
collante
Fixedon the cover,withoutglue

Guarnizione
Gosket
Montaggio
sulcoperchio,
concollante
Fixedon the cover,with glue

Temperatura Pesokg
,TemperotureWeightlq

Guarnizione
Gosket
Montaggio
sulcoperchio,
concollante
Fixedon the cover,with glue

=H

<s

e=
rJ.Jtr

za

Guarnizione
Goskef

tx

Montaggio
sulcoperchio,
senza
collante
Fixedon the cover,withoutglue

S=
z.i.

ffiffi
ffiffi
ffiffi

Dimensions and Weights


5SV Series 3500 RPM

All dimensions are in inches (mm).

Pump
Type
5SV-02
5SV-03
5SV-04
5SV-05
5SV-06
5SV-07
5SV-08
5SV-09
5SV-10
5SV-11
5SV-12
5SV-13
5SV-14
5SV-15
5SV-16
5SV-17
5SV-18
5SV-20
5SV-21
5SV-23
5SV-25
5SV-26
5SV-27

Motor
NEMA Frame
HP ODP TEFC ODP TEFC L1 ODP
1 1 3 3
1
0.75
12.85 10.79
1
13.84 10.66
14.82 10.67
1.5
15.8 10.67
56C
16.78 11.18
2
17.77 11.18
18.75 11.57
3
19.73 11.57
20.71 11.57
22.45 13.93
23.43 13.93
24.42 13.93
5
184TC 182TC
25.4 13.93
26.38 13.93
27.37 13.93
184TC 28.55 13.93
29.28 13.88
31.64 13.88
32.23 13.88
7.5
213TC 184TC
34.2 13.88
36.17 13.88
37.23 13.88
10
215TC 213TC 215TC 38.22 16.63

GOULDS PUMPS
Commercial Water

Dimensions (in)
L2
TEFC ODP
1 3
9.91 9.16
11.19 9.16
11.19 10.66
11.19 10.66
12.06 11.16
12.06 11.16
13.44 11.18
13.44 11.18
13.44 11.18
15.43 12.55
15.43 12.55
15.43 12.55
15.43 12.55
15.43 12.55
15.43 12.55
15.43 12.55
15.53 13.93
15.53 13.93
15.53 13.93
15.53 13.93
15.53 13.93
15.53 13.93
16.68 15.55

TEFC
3
9.29
9.29
9.91
9.91
10.79
10.79
11.16
11.16
11.16
13.93
13.93
13.93
13.93
13.93
13.93
13.93
15.43
15.43
15.43
15.43
15.43
15.43
15.51

L3

L4

L5

L6

15.87
16.85
18.23
19.21
20.2
21.18
22.17
23.15
24.13
25.12
26.1
27.48
29.44
30.43
32.4
34.37
35.35
36.33

9.53
10.51
11.5
12.48
13.46
14.45
15.43
16.42
17.4
18.39
19.37
20.35
22.31
23.31
25.28
27.24
28.22
29.2

9.57
10.55
11.54
12.91
13.9
14.88
15.87
17.24
18.23
19.21
20.2
21.18
22.17
23.15
24.13
25.11
26.5
28.46
29.45
-

9.57
10.55
11.54
12.91
13.9
14.88
15.87
17.24
18.23
19.21
20.2
21.18
22.17
23.15
24.13
25.11
26.5
28.46
29.45
31.42
33.39
34.37
35.35

M ODP
(Ref.) 1
5.19 6.20
5.19 6.19
5.74 6.20
5.74 6.20
5.74 7.19
5.74 7.19
5.75 6.50
5.75 6.50
5.75 6.50
6.87 8.88
6.87 8.88
6.87 8.88
6.87 8.88
6.87 8.88
6.87 8.88
6.87 8.88
8.05 8.89
8.05 8.89
8.05 8.89
8.05 8.89
8.05 8.89
8.05 8.89
8.77 10.62

D1 (max.)
TEFC ODP
1 3
6.19 6.19
6.19 6.19
7.19 6.19
7.19 6.19
7.19 6.20
7.19 6.20
7.19 7.16
7.19 7.16
7.19 7.16
8.86 9.02
8.86 9.02
8.86 9.02
8.86 9.02
8.86 9.02
8.86 9.02
8.86 9.02
10.62 8.88
10.62 8.88
10.62 8.88
10.62 8.88
10.62 8.88
10.62 8.88
10.18 10.18

TEFC
3
6.19
6.19
6.19
6.19
6.19
6.19
7.19
7.19
7.19
8.86
8.86
8.86
8.86
8.86
8.86
8.86
8.86
8.86
8.86
8.86
8.86
8.86
10.28

D2 Pump ODP
1
4.13 27 21
4.13 28 27
4.13 30 32
4.13 32 32
4.72 33 43
4.72 35 43
5.51 35 49
5.51 37 49
5.51 37 49
5.51 41 81
5.51 42 81
5.51 44 81
5.51 45 81
5.51 46 81
5.51 47 81
5.51 49 81
5.51 50 100
5.51 53 100
5.51 54 100
5.51 56 100
5.51 58 100
5.51 59 100
4.13 60 132

Weight (lbs.)
Motor
TEFC ODP TEFC ODP
1 3 3 1
21 19
19 48
29 21
21 55
40 23
23 62
40 23
23 64
51 32
33 76
51 32
33 78
64 41
44 84
64 41
44 86
64 41
44 86
92 62
69 122
92 62
69 123
92 62
69 125
92 62
69 126
92 62
69 127
92 62
69 128
92 62
69 130
120 75
85 150
120 75
85 153
120 75
85 154
120 75
85 156
120 75
85 158
120 75
85 159
145 107 122 192

Pump/Motor
TEFC ODP
1 3
48
46
57
49
70
53
72
55
84
65
86
67
99
76
101 78
101 78
133 103
134 104
136 106
137 107
138 108
139 109
141 111
170 125
173 128
174 129
176 131
178 133
179 134
205 167

TEFC
3
46
49
53
55
66
68
79
81
81
110
111
113
114
115
116
118
135
138
139
141
143
144
182

28

5SV Curve 3500 RPM

Q [m3/hr]
TOTAL STAGES
27
26
25

5SV 60Hz
3500 RPM

23
21
20
17
15
14
13
12
11
10
9
8
7
6
5
4
3
2

110 psi

MINIMUM FLOW RATE: 7 GPM [1.6 m3/hr]

GOULDS PUMPS
Commercial Water

29

TOP-FLO TF-C Series Centrifugal


Capacity Curves

Model: C114

Based on water at 70F (22C)

60 Hz
3500 RPM
Size: 1-1/2 x 1-1/2 x 4

CUBIC METERS PER HOUR

HEAD IN FEET

HEAD IN METERS

30 psi

US GALLONS PER MINUTE

FEET

METERS

CUBIC METERS PER HOUR

US GALLONS PER MINUTE


1

NOTES:
)MPELLERDIAMETERSAVAILABLEIN INCHINCREMENTS

.03(2ISSHOWNFORMAXIMUMIMPELLERDIAMETER

PSI = (EADIN&EET83PECIlC'RAVITY
2.3

Office: 0/"OXs"RADFORD 0!


Plant:
6ALLEY(UNT$RIVEs,EWIS2UN 0!
Phone:   s  sFAX   

+GCM2 = (EADIN-ETERS83PECIlC'RAVITY

(0X+W

PROCESS EQUIPMENT COMPANY


17

TOP-FLO TF-C Series


Close-Coupled Pump Dimensions

$$)-%.3)/.&!#%/&).,%44/#%.4%2/&#/.$5)4/0%.).'

TO&RAME-OTORS

AND&RAME-OTORS

Pump Dimensions (Easy-Clean totally-enclosed motor)


Pump
Model
Suction
4& #  
4& #

4& #

4& #

Discharge
 
 
 

X*
 
 
 

X**
 
 
 

Y*
 
 
 

Y**
 
 
 

Z
 
 
 



 

 

 

 

 



Pump and Motor Dimensions with Easy-Clean Totally Enclosed Motors


Pump
Model Frame

A1

B1

#

 

 

 

 

4#

 

 

#

 

 

4#

 

4#

 

 

4#

 

 

TF-C114

TF-C216

C*

C1 *

C**

C1**

D*

D**

HD

AA

AB

       

 

 

 



 

 

 

   





 

 

 

 

 

 



 



 

 

 

 

   





 

 

 

   

 



 

   

   



 

 

 



 

 



 





4#

 

 

 

 

 

 

 

 

4#

 

 

 

 

TF-C218

4#

 

 

 

     

4#

 

 

 

 

4#

 

 



     

 

 

4#

 

 

 

 

 

 

 



4#

 

 

 

 

   

TF-C328

4#

 

 

 

 

   

4#

 

 

 

 

   

4#

 

 

 

 

4#

 

 

 

 

   
 

 



 

 

 

 



 





 

 



 

 

 



   

 

 

 

   

 

 

 

   



 
 

 

$IMENSIONSAREAPPROPRIATEANDFORGUIDANCEONLY/.APPLICATIONSWHEREEXACTDIMENSIONS
AREREQUIRED REQUESTACERTIlEDPRINTFROM4OP,INE
./4%3 $IMENSIONSFORSINGLEPHASEFRAMEMOTORS LONGER

4HESEDIMENSIONSAREFORPUMPSUSINGSTANDARD#&LANGE-OTORS
4& #3ERIESPUMPSWILLNOTACCEPT43#&RAME-OTORS

7ITHCLAMPCONNECTIONS

7ITHTHREADEDBEVEL SEATCONNECTIONS

27
25

Performance Curves 60 Hz, 3500 RPM


Curvas de Funcionamiento 60 Hz, 3500 RPM

METERS
METROS

Model NPE / 2ST Size (Tamao) 11c4 x 11c2-6


RPM 3500 Curve (Curva) CN0235R02

FEET
PIES

5'

NPSH R FEET (PIES)


40

50

130

G 5 c16" DIA.

120
TOTAL DYNAMIC HEAD (CARGA DINAMICA TOTAL) H

110
100

NOTE: Not recommended for operation beyond printed HQ curve.


NOTA: No se recomienda para funcionamiento superior al
impreso en la curva H-Q.

10'

15' 20'
60

A 51c4"

62

55 EFF %
64

C 47c8"

80

30 psi

66

D 45c8"

70
E 41c4"

20
60
15

50

F 37c8"

40
10

c4

HP

HP
1

20
10

20

40

60
10

2
11
HP
c2 H
P

HP

80

100

120

20

15

378

458

478

5116

51516

NOTE: Although not


recommended, the pump
may pass a 316 sphere.
NOTA: Si bien no se
recomienda, la bomba puede
pasar una esfera de 316.

HP

30

Ordering Standard
Code,
HP Rating, Imp.
Cdigo Estndar HP Dia.
de Pedido Potencia

58

B 51c16"

90
25

58

H 51c2"

35

30

7'
55

15

Impeller Selections for ODP & TEFC Motors


Selecciones del Impulsor para
Motores ODP & TEFC

140

25

30

160
35

U.S. GPM
m3c hr

CAPACITY (CAPACIDAD) Q

METERS
METROS

Model NPE / 2ST Size (Tamao) 11c4 x 11c2-6 Impeller Selections for Exp. Proof Motors
RPM 3500 Curve (Curva) CN0235R01
Selecciones del Impulsor para Motores Exp. Proof

FEET
PIES

NPSH R FEET (PIES)

NOTE: Not recommended for operation beyond


printed H-Q curve.
NOTA: No se recomienda para funcionamiento
superior al impreso en la curva H-Q.

5'
50

TOTAL DYNAMIC HEAD (CARGA DINAMICA TOTAL) H

110
30

100

7'
55
58 60 62

B 51c16" DIA.

10'
64

90
25

15'

66
64

80

D 45c8"

20'

70

58

E 41c4"

6
50

55 EFF %

3
3
c4

30

HP

1H

11
c2 H

378

458

5116

20

40

60
10

80
15

HP

HP

20
10

F 37c8"

40
10

NOTE: Although not


recommended, the pump
may pass a 316 sphere.
NOTA: Si bien no se
recomienda, la bomba puede
pasar una esfera de 316.

62
60

20

15

Ordering Standard
Code,
HP Rating, Imp.
Cdigo Estndar HP Dia.
de Pedido Potencia

100
20

120
25

140
30

160

U.S. GPM
m3c hr

CAPACITY (CAPACIDAD) Q

GOULDS PUMPS
Commercial Water

NPE Close Coupled Dimensions, Weights and Specifications


NPE Acople Cerrado Dimensiones, Pesos y Especificaciones
Clockwise Rotation Viewed from Drive End
Rotacin en Direccin de las Agujas del Reloj Visto desde el Extremo del Motor
DISCHARGE
DESCARGA
41c4

C MAX.

FILL AND VENT


CARGA Y VLVULA

1 PHASE UNITS ONLY


UNIDADES MONOFSICAS
SOLAMENTE

2 3c4

SUCTION
SUCCIN

6 5c16 MAX.
30o
TYP.

41c4

311/16
MAX.
(4) 13c32 DIA. MOUNTING HOLES
(4) 13c32 DIA. AGUJEROS DE MONTAJE

DRAIN PLUG 3c8


ENCHUFE DE DRENAJE 3c8

215c16

215c16
3

67c8

c16

3c4

6 1c2

ODP and TEFC , and 1 HP (standard), ODP y TEFC , y 1 HP (estndar)


41 c4

DISCHARGE
DESCARGA

C MAX.
1 PHASE ONLY
MONOFSICA
SOLAMENTE

FILL AND VENT


CARGA Y VALVULA

23c4

X
SUCTION
SUCCIN
61c2 MAX.

30
TYP

MOTOR CRADLE
HORQUILLA DEL MOTOR

41 c4

311c16
4 MAX.
13 c 32 DIA.

DRAIN
DRENAJE

215c16

215c16
81c8

131c32

5
81c4

HOLE
4-MOUNTING HOLES
13c32 DIA. 4-AGUJEROS
DE MONTAJE

ODP and TEFC 1, 2 and 3 HP (standard), ODP y TEFC 1, 2 y 3 HP (estndar)

Specifications
Especificaciones
Capacities to:
85 GPM (322L/min) at 1750 RPM
170 GPM (643L/min) at 3500 RPM
Heads to:
39 feet (12 m) at 1750 RPM
150 feet (46 m) at 3500 RPM
Working pressures to:
125 PSIG (9 bars)
Maximum temperatures to:
250 F (121 C)
Direction of rotation:
Clockwise when viewed from
motor end.

Motor specifications:
NEMA 56J frame, 1750 RPM,
HP. 3500 RPM through
5 HP. Open drip-proof, totally
enclosed fan-cooled or explosion
proof enclosures. Stainless steel
shaft with ball bearings.
Single phase: Voltage 115/230
ODP and TEFC. (3 and 5 HP model
230 V only) Built-in overload
with auto-reset provided.
Three phase: Voltage 208230/460 ODP, TEFC and EX
PROOF.
NOTE: For three phase motors,
overload protection must be
provided in starter unit. Starter
and heaters must be ordered
separately.

Capacidades:
85 GPM (322L/min) a 1750 RPM
170 GPM (643L/min) a 3500 RPM
Cargas:
39 pies (12 m) a 1750 RPM
150 pies (46 m) a 3500 RPM
Presin de trabajo:
125 PSIG (9 baras)
Temperatura mxima:
250 F (121 C)
Direccin de rotacin:
En direccin de las agujas del reloj
visto desde el extremo final del
motor.

Motores:
Armazn 56J NEMA, 1750 RPM
HP. 3500 RPM a 5 HP.
Cubiertas abiertas resguardadas,
totalmente encerradas enfriadas
por ventilador o a prueba de explosiones. Eje de acero inoxidable
con balineras de bolas.
Monofsicos: Voltaje 115/230
ODP y TEFC. (modelo 3 y 5 HP
230 voltios solamente) Se
proporciona proteccin trmica
contra sobrecarga construida con
reseteo automtico.
Trifsicos: Voltaje 208-230/460
ODP, TEFC y EX PROOF.
NOTA: Para motores trifsicos se
debe de proporcionar la proteccin
trmica contra sobrecarga en la unidad
de arranque. El arrancador y los calentadores se deben pedir por separado.

GOULDS PUMPS
Commercial Water

12

NPE Close Coupled with Footed Motor, Explosion-proof and 5 HP Motors


NPE Acople Cerrado con Motor con Patas, Motores a Prueba de Explosin Y 5 HP
All Explosion Proof Motors and 5 HP ODP and TEFC
Todos los motores son a prueba de explosiones, 5 HP, ODP
(abiertos resguardados) y TEFC (totalmente encerrados con
enfriamiento forzado)

FILL AND VENT


CARGA Y VLVULA
SUCTION
SUCCIN

DISCHARGE
DESCARGA

81/2
Y

41/4

C. MAX.

61/2 DIA.
31/2
41/4
1/3

7/8

3
33/4

47/8
61/2

DRAIN PLUG 3/8


ENCHUFE DE DRENAJE 3/8

Dimensions Determined by Pump,


Dimensiones Determinadas por la Bomba
Pump,
Bomba

Suction,
Succin

1ST

2ST

Discharge,
Descarga

HP

3 516

3
3

4 8

Motor Weights, Pesos del Motor


1 Phase, Monofsicos
3 Phase, Trifsicos

3ST

15

438

4916

7516

218

5 18

7 78

7 78

2 8

5 8

Available Motor Weights and Dimensions,


Pesos y Dimensiones Disponibles del Motor

ODP

TEFC

EXP

ODP

TEFC

EXP

C Max.
Length,
(Longitud)

16

21

47

19

18

27

91516

19

24

41

21

21

30

10

22

26

49

23

21

30

11

28

35

56

27

27

37

11516

33

39

60

32

33

44

12116
7

HP

40

43

41

37

12 16

42

42

45

14

Dimensions in inches, weights in pounds.


Dimensiones en pulgadas, pesos en libras.

NOTES:
1. Pump will be shipped with top
vertical discharge position as
standard. For other orientations,
remove casing bolts, rotate
discharge to desired position,
replace and tighten 6mm bolts
to 5 6 lbs.-ft.
2. Motor dimensions may vary with
motor manufacturers.
3. Dimensions in inches, weights
in pounds.
4. For explosion proof motor
dimensions consult factory for
information.
5. Not to be used for construction
purposes unless certified.

NOTAS:
1. Las bombas se transportarn
con la descarga vertical superior
como estndar. Para otras orientaciones, retirar los tornillos de
la carcasa, rotar la descarga a la
posicin deseada, y reemplazar y
apretar los tornillos de 6mm a 5
6 libras-pies.
2. Las dimensiones del motor
puede que varen con los
fabricantes.
3. Dimensiones en pulgadas, pesos
en libras.
4. Para las dimensiones de los
motores a prueba de explosin
consultar con la fbrica para
informacin.
5. No usar para propsitos de
construccin sin certificar.

GOULDS PUMPS
Commercial Water

13

PNEUMATICS M

PROCESS & PACKAGING, INC. 2003

I/O LIST

PROCESS & PACKAGING, INC. 1999

PROCESS & PACKAGING, INC.

FLASH PASTUERIZER 11FP353


I/O LISTING SHORTS BREWING CO. 6/09/11
INPUTS
I:0.0/0
I:0.0/1
I:0.0/2
I:0.0/3
I:0.0/4
I:0.0/5
I:0.0/6
I:0.0/7
I:0.0/8
I:0.0/9
I:0.0/10
I:0.0/11
I:0.0/12
I:0.0/13
I:0.0/14
I:0.0/15
I:0.0/16
I:0.0/17
I:0.0/18
I:0.0/19

OUTPUTS

FLOW METER (PULSE)


SLT HL PROBE
SLT LL PROBE
AV1 CLOSED
AV2 CLOSED
AV3 CLOSED (JB1)
AV4 CLOSED (JB1)
AV5 CLOSED (JB1)
SEQUENCE STOP
MBP RUNNING
BBP RUNNING
HWR RUNNING
BBP CONTROL MK1 (REMOTE)
BBP CONTROL MK2 (REMOTE)
FEED PROTECT PROBE (OPT)
SPARE
SPARE
SPARE
SPARE
SPARE

O:0.0/0
O:0.0/1
O:0.0/2
O:0.0/3
O:0.0/4
O:0.0/5
O:0.0/6
O:0.0/7
O:0.0/8
O:0.0/9
O:0.0/10
O:0.0/11
O:1.0/0
O:1.0/1
O:1.0/2
O:1.0/3
O:1.0/4
O:1.0/5

(P1) MBP STARTER


(P2) BBP VFD STARTER
(P3) HWR STARTER
SPARE
CIP FLOW VALVES
AV1 OPEN
AV2 OPEN
AV3 OPEN
AV4 OPEN
AV5 OPEN
AV6 OPEN
SEQUENCE STOP LAMP
AUDIBLE ALARM
RED STACK LAMP - UHL SPT
CLEAR STACK LAMP - HL SPT
AMBER STACK LAMP - ML SPT
GREEN STACK LAMP - LL SPT
BLUE STACK LAMP - ULL SPT

NOTE: FOR CIP MODE, BLINK BLUE


STACK LAMP, O:1.0/1

ANALOG INPUTS
ANALOG OUTPUTS
I:0.0/V0+ SPT DIFF. PRES. TRANS. (DP1)
I:0.0/V1+ BEER PRES. TRANSDUCER

RTD INPUTS
I:3.0/0
I:3.0/1
I:3.0/2

RTD 1 HOLDING TUBE TEMP.


RTD 2 PRODUCT OUT TEMP.
RTD 3 CIP RETURN TEMP. (OPT)

O:0.0/OV0
O:0.0/OV1
O:2.0/0
O:2.0/1
O:2.0/2
O:2.0/3

PROCESS & PACKAGING, INC. 1996

CHART REC. HOLD TUBE TEMP.


CHART REC. PROD. OUT TEMP.
STEAM I/P CONVERTER
GYLCOL I/P CONVERTER
CHART REC. CIP RETURN TEMP
VFD SPEED CONTROL

PROCESS & PACKAGING, INC.

FLASH PASTUERIZER 11FP353


I/O LISTING SHORTS BREWING CO. 6/2/11
6 CORE COLOR CODE - JUNCTION BOX (JB1)
ADDRESS
I:0.0/5
I:0.0/6
I:0.0/7

INPUTS
AV3 CLOSED
AV4 CLOSED
AV5 CLOSED

COLOR
BLUE
GREEN
WHITE

24VC

24VDC CONTROL

RED

0VC

0VDC CONTROL

BLACK

PROCESS & PACKAGING, INC. 1996

PROCESS & PACKAGING, INC.

FLASH PASTUERIZER 11FP353


I/O LISTING SHORTS BREWING CO. 6/02/11
12 CORE COLOR CODE - JUNCTION BOX (REMOTE)
ADDRESS
I:0.0/12
I:0.0/13
24VDC

INPUTS
BBP CONTROL MK1
BBP CONTROL MK2

COLOR (CABLE)
ORG
(REMOTE INPUTS)
YEL
(REMOTE INPUTS)

CONTROL +

VIOLET

(REMOTE INPUTS)

RED STATUS LAMP


CLEAR STATUS LAMP
AMBER STATUS LAMP
GREEN STATUS LAMP
BLUE STATUS LAMP

RED
WHITE
BROWN
GREEN
BLUE

(REMOTE OUTPUTS)
(REMOTE OUTPUTS)
(REMOTE OUTPUTS)
(REMOTE OUTPUTS)
(REMOTE OUTPUTS)

COM

BLACK (REMOTE OUTPUTS)

OUTPUTS
O:1.0/1
O:1.0/2
O:1.0/3
O:1.0/4
O:1.0/5
0VS

PROCESS & PACKAGING, INC. 1996

PROCESS & PACKAGING, INC.

FLASH PASTUERIZER 11FP353


SHORTS BREWING CO. 6/09/11
TWISTED PAIR 4 COND. - JUNCTION BOX (REMOTE)
ADDRESS
I:0.0/V1+

24VDC
0VDC

INPUTS
COLOR (CABLE)
SPT DIFF. PRES. TRANS PAIR TWO - RED

ANALOG +
ANALOG -

PAIR ONE - RED


PAIR ONE - BLACK

PROCESS & PACKAGING, INC. 1996

OXINE

PROCESS & PACKAGING, INC. 1999

Manual Oxine Dilution & Use


Useful figures to have available if you are diluting Oxine manually without a titration kit. These
figures are applicable with Oxine that has been activated within 48 hours of dilution with a food
grade acid at 2.5 to 3 pH .
For keg sanitizing and use with the Super King, Mini King or Squire series machines:
It is recommended that you start by using approximately 100 ppm of activated Oxine for keg
sanitizing until you can determine through your own QC procedures whether you need to
increase or decrease the amount based upon microbial results obtained. Experience indicates
that normal usage will be in the range of 20 to 100 ppm.
1. Take a one gallon container with a screw lid and drill a hole in the cap to suit the dosing unit
siphon tube.
2. Take 0.6 liter (20 ounces) of Oxine, add food grade acid to lower the pH to approximately 2.5
to 3.0 pH to activate the Oxine and stir. This will give you approximately 20,000 ppm of
activated Oxine. CAUTION Do so in a well ventilated area and do NOT breathe the fumes
given off during activation. See the MSDS in this section for more details.
3. When activated (after 5 to 10 minutes) add 3 liters (101 ounces) of water to the activated
Oxine (5:1 ratio). This will give you approximately 4,000 ppm of activated Oxine. Stir and
replace cap with siphon tube into Oxine.
4. Using the chart supplied with the Oxine doser venturi kit select the colored venturi that will
then give you a 40:1 reduction ratio. This will give you approximately 100 ppm of activated
Oxine being supplied as your rinse and sanitizing water to the keg for pre and post rinse.
5. This can be verified with the Oxine test kit or Oxystix attainable from IDD Process &
Packaging, Inc.

Other ratios of Oxine for general sanitizing purposes


One unit of manually activated Oxine at 20,000ppm and you:
Add 1 unit of water, the concentration reduces to 10000ppm Ratio of water to Oxine 1:1.
Add a further 2 units of water, the concentration reduces to 5000ppm Ratio of water to Oxine 3:1.
Add a further 4 units of water, the concentration reduces to 2500ppm Ratio of water to Oxine7:1.
Add a further 8 units of water, of the concentration reduces to 1250ppm Ratio of water to Oxine 15:1.
Add a further 16 units of water, the concentration reduces to 625ppm Ratio of water to Oxine 31:1.
Add a further 32 units of water, the concentration reduces to 312.5ppm Ratio of water to Oxine 63:1.
Add a further 64 units of water, the concentration reduces to 156.5ppm Ratio of water to Oxine 127:1.
Add a further 128 units of water, the concentration reduces to 78ppm Ratio of water to Oxine 255:1.
Add a further 256 units of water, the concentration reduces to 39ppm Ratio of water to Oxine 511:1.
Add a further 512 units of water, the concentration reduces to 19.5ppm Ratio of water to Oxine 1023:1.
Add a further 1024 units of water, the concentration reduces to 9.5ppm Ratio of water to Oxine 2047:1.
Add a further 2048 units of water, the concentration reduces to 5ppm Ratio of water to Oxine 4095:1.
Add a further 4096 units of water, the concentration reduces to 2.5ppm Ratio of water to Oxine 8191:1.
Add a further 8192 units of water, the concentration reduces to 1.25ppm Ratio of water to Oxine 16382:1.

OXINE & PUROGENE SANITIZER

The following information is offered as suggested uses of Oxine and Purogene and is
not intended to be definitive or accurate for all applications. IDD Process & Packaging,
Inc. do not accept any liability for the use or application of Oxine or Purogene.
OXINE AND PUROGENE...THE SANITIZERS FOR ALL REASONS. For years it has
been known that chlorine dioxide gas is a powerful anti-microbial agent. However, this
gas is toxic and unstable in an aqueous solution. Modern technology has overcome
these problems with Oxine and Purogene. Today, stabilized chlorine dioxide (ClO2) is
available in a concentrated stable form with very low toxicity. As a powerful oxidant,
stabilized ClO2 is virtually unaffected by organic load and hard water. These technical
advances have resulted in the FDA, EPA and USDA approving stabilized ClO2 as an
acceptable sterilant for numerous applications within the brewery, dairy and food
processing plants. Properties which make stabilized ClO2 most attractive to the
brewer, maltster and other beverage plant operators are:
LOW ODOR - Unlike typical sanitizers such a hypochlorites, quaternary ammonium, or
even peroxy-acetic acid, stabilized ClO2 has an almost undetectable odor while
surpassing the bacteriocidal efficacy of these other compounds. Hypochlorites can
form chlorophenols (a medicinal flavor compound) when combined with organic
material in beer: Quaternary ammonia compounds have well known negative effects on
flavor; the end product of the reduction of peroxy-acetic acid is acetic acid, with its
typically "vinegar-like" character. Even small amounts remaining in a tank and having
the opportunity of coming in contact with beer, can have a deleterious effect on beer
flavor.
LOW CORROSIVITY - Stabilized ClO2 is not harmful to vessels or piping systems
when used at the recommended dosages. Typically, brewers like the effectiveness of
hypochlorites but a major drawback is hypochlorites role in causing stress corrosion
fatigue in stainless steel, particularly at weld joints. Stabilized ClO2 while actually being
4 to 7 times more effective as a sanitizer than hypochlorite, does not enhance or
contribute to stress corrosion fatigue in the metal. Stabilized ClO2 is only slightly
more corrosive than tap water at and much of this is due to the acid used in the
activation of the product. When it is used as a final rinse in vessels, or piping systems,
it is perfectly safe to leave a 10 ppm solution un-rinsed in a tank, pipe network or piece
of process equipment, (i.e. bottle fillers, keg racking machines, sheet or pressure leaf
filters, etc.).
EASE OF HANDLING - While idophors, peroxy-acetic acid and hypochlorites are
popular sanitizers for tanks, fillers and other equipment, they have some handling
drawbacks. Iodophors are really only effective at low pH, thus they are typically carried
as a concentrate in a solution of phosphoric or nitric acid. This makes them hazardous
to handle. Iodophors also have a tendency to stain equipment (and people). Pereoxy-

PROCESS & PACKAGING, INC. 2003

OXINE & PUROGENE SANITIZER


acetic acid is actually quite volatile at moderately elevated temperatures (120_F/50_C)
and can cause spontaneous explosions. It is also corrosive in its concentrated form.
Hypochlorites as chlorine gas have a short-term exposure limit slightly higher than that
of stabilized ClO2 (1.0 ppm versus 0.3 ppm respectively). However, since stabilized
ClO2 is 4 to 7 times more effective than hypochlorites at normal use levels, it is less
hazardous.
NO ENVIRONMENTAL IMPACT - Stabilized ClO2 does not form the highly
carcinogenic trihalomethanes as do hypochlorites in the presence of organic materials.
Oxine is environmentally and user friendly and has been accepted by the EPA has
having no environmental impact upon disposal. It is not corrosive nor is it volatile in its
concentrated (2%) form.
EFFICACY - Stabilized ClO2 does not act by chlorination but by oxidation and has
proven effective against all common brewery, winery and beverage plant microorganisms. It is an effective bacteriostat at use rates as low as 5 to 20 ppm against
such common pests as Lactobacillus and Pediococcus sp. and at 50 ppm against Wild
Yeasts and Mold strains.
As with all gaseous products such as stabilized ClO2, Oxine can be monitored by
using a standard gas monitoring system such as those supplied by LAB SAFETY
SUPPLIES COMPANY. Toll free telephone number 800-356-0722. It is necessary to
take extra care with good ventilation during the "activation" process of Oxine. If it is
considered necessary to monitor gas levels at this time for your safety records, we
recommend that the chlorine "low range" (0.05 to 16ppm) tube be used to monitor gas
levels. These tubes readily detect and measure all types of inorganic chlorine.
MALTHOUSE:
Stabilized ClO2 is an effective wash down sanitizer for walls and floors, germination
areas and steep tanks. At 100 to 500 ppm it will kill and bleach out mold and mildew
common to these high-humidity areas. Stabilized ClO2 is successfully used in barley
steep waters to inhibit microbial growth of all types. Typically at 10 to 50 ppm
depending on the microbial load, one can assure a safe re-cyling of the steep water
into subsequent batches. Stabilized ClO2's strong oxidizing capability actually reduces
B.O.D. loads for disposal.
BREWHOUSE:
Safe for all vessels and piping systems, whether copper or stainless steel, stabilized
ClO2 can ensure a microbially free environment in coppers/kettles, mash filters or
lauter tuns, swirl tanks, settlers and wort cooling systems when used at 50 to 100 ppm.
The related piping systems for wort transfer to fermentation areas can be sanitized at
100 ppm. A 50 ppm solution is also safe to leave in the pipelines during periods of nonuse, to keep them sanitized.

PROCESS & PACKAGING, INC. 2003

OXINE & PUROGENE SANITIZER


FERMENTATION/STORAGE AREAS:
A 50 ppm solution is adequate to sanitize tank walls and related piping systems.
Since low levels of contact with finished product do not effect final beer flavor, one can
safely use stabilized ClO2 in a final rinse and be able to obtain some residual
bacteriostatic value. It is recommended that boots, gloves, yeast-handling tools and the
like be sanitized at 100 ppm. Stabilized ClO2 at 100 ppm is ideal for foot baths at or
near tank entry areas.
FILTRATION:
Stabilized ClO2 is particularly useful for stabilizing and sanitizing filter systems. It can
be used to shock sanitize activated carbon and sand/gravel filters in the water
treatment facility. Typically, a 50 to 100 ppm solution is run slowly through these type
filters. Stabilized ClO2 will not be absorbed significantly by the active carbon. Once the
bed is sanitized it is then possible to dose Oxine into the water stream prior to the filter
bed at a concentration of 1 to 5 ppm in order to prevent future contamination.
Plate-and-frame filters can be sanitized with a 10 to 50 ppm solution without the
typical water flush/rinse required by acid-sanitizers and the like. A standing solution of
up to 10 ppm can be left in a filter during periods of non-use with no harm to the filter
frame or the sheets.
It is recommended that this procedure be carried out after any normal beer filter use to
inhibit the growth of yeasts and bacteria, since residual beer on the sheets makes for
an ideal growth media. A solution of the same strength sprayed over the outer exposed
edges of the filter sheets will prevent mold growth when standing.
PACKAGING:
Stabilized ClO2 provides a safe sanitization and soaking solution for keg washer
rackers, bottle and can fillers. Sanitize at 50 ppm and soak or stand filler bowls in cold
water at 10 ppm.
Aseptic keg, bottle and can rinsing immediately prior to filling with beer is enhanced
when 20 to 50 ppm of stabilized ClO2 is used as a final cold rinse.
The use of stabilized ClO2 as an aseptic "fog" spray around aseptic bottle and can
fillers is highly effective as a sanitizer and microbial preventative at 10 to 20 ppm.
The non-corrosive nature of stabilized ClO2 makes it an ideal growth inhibitor in tunnel
pasteurizers. Stabilized ClO2 is most effective in the moderate temperature zones
(warm-up and cool-down fresh water zones) of the pasteurizer. A 20 to 30 ppm solution
is normally adequate and quite safe to the equipment.

PROCESS & PACKAGING, INC. 2003

OXINE & PUROGENE SANITIZER


TANK-TRUCK WASHING:
As in the typical use for tank washing and sanitizing, stabilized ClO2 can be used for
the sanitization and cleanup of bulk tankers and their related piping and hoses. Wash
down tank internals, pumps and hoses at 100 ppm, externals at 250 to 500 ppm. This
will prevent transfer of micro-organisms to or from the connecting systems.
MOLD AND MILDEW CLEANUP AND CONTROL:
Clean off walls and floors as well as air handling units and machinery using a 200 to
500 ppm solution of stabilized ClO2. This effectively kills mold and mildew spores while
still retaining some bleaching ability to remove tough black stains. This is good
procedure prior to painting, or prior to the application of a mold and slime growth
inhibitor such as Alltech's Mold-Zap.
PROCESS WATER TREATMENT:
The FDA has approved stabilized ClO2 for process water sanitization at between 100
to 200 ppm available ClO2. Potable water treatment is approved for human
consumption at 4 ppm available ClO2.
ACTIVE CARBON BED (ACB):
Infected ACB's can be back flushed and soaked in a 100 ppm solution of ClO2 for 15
to 60 minutes, after which time a forward flush-out of 15 to 30 minutes with the process
water can take place. It is then advisable to inject 1 to 3 ppm of activated ClO2 into the
process water stream thereafter prior to the ACB to prevent future infections.
GLASS WASHING/RINSING:
Even at the final stage of the brewer's trade, where bars and pubs have a need for an
effective and safe drinking-glass sanitizer, stabilized ClO2 can fill the need. Since
stabilized ClO2 can be safely consumed at 4 ppm, it makes an ideal glass rinse. Unlike
typical quaternary ammonium rinses, it will not have any deleterious effect on beer
flavor, nor on beer foam quality. Use at 20 to 50 ppm in final rinse water.
WASHING OF YEAST SLURRY WITH STABILIZED ClO2 (OXINE):
Stabilized ClO2 (Oxine) will effectively kill unwanted bacteria in yeast at 20 to 40 ppm,
while leaving the culture yeast unharmed. Because of stabilized ClO2's unique action,
it does not have the drawbacks of phosphoric acid. It does not form chlorophenols
(which contribute to a much feared medicinal character in beers) in the presence of
organic materials.
METHOD:
Normally, an initial washing at 20 to 40 ppm (20 ppm for homogenous yeast, 40 ppm
for "clumpy" or highly flocculant strains) is effective against most Lactobacilli and
Pediococci species. This "wash" is done by adding stabilized ClO2 directly to yeast
slurry on a volume/ppm basis. It does not need to be activated as the pH of the yeast
slurry is low enough to convert to ClO2.

PROCESS & PACKAGING, INC. 2003

OXINE & PUROGENE SANITIZER


Stabilized ClO2 is supplied at a concentration of 20,000 ppm or 2% Chlorine Dioxide
when activated. Therefore, on a volume basis, one could essentially make up with one
gallon of stabilized ClO2 concentrate, one thousand gallons of solution at 20 ppm. By
this method, we can also assume with one gallon of concentrate to make up one
thousand gallons of yeast slurry at 20 ppm.
It is impractical to measure the
concentration of ClO2 in the presence of yeast, so the dilution must be made based on
the strength of the concentrate (20,000 ppm).
Yeast slurry should be thin enough to allow for homogeneous mixing, usually 20 to
40% solids. The killing action of stabilized ClO2 is very fast compared to the traditional
phosphoric acid wash. Only 15 to 30 minutes need be allowed for effective bactericidal
effect of stabilized ClO2, with no resultant stress on yeast cells.
DOSING RATE:
NORMAL WASH: For regular washing of homogenous recycled brewers yeast, a 20
to 40 ppm wash for a minimum 30 minutes to 5 hours prior to pitching. Mix 1 to 2 ml of
stabilized ClO2 concentrate with each liter of yeast slurry. Agitate thoroughly during the
process.
ACTIVATION OF CONCENTRATE:
Since the ClO2 is in a stabilized form in concentrate, it must be "activated" before
using. To activate Oxine add acid to lower the pH in a well ventilated area to below 5
pH. Activation can be verified by a corresponding color change of the concentrate from
clear to yellow/green. Any number of acids will activate the stabilized ClO2, however,
food grade Citric or Phosphoric acid is recommended for this application.
Normally it requires up to 200 grams of Citric Acid to activate one gallon of stabilized
ClO2 concentrate (up to 50 grams per liter of stabilized ClO2 concentrate).
Following are the details for replacement chemicals for your Oxine Test Kits.
10% Potassium Iodide - 100 g diluted to 1,000 ml with distilled water.
0.2N Hydrochloric Acid - Add 16.6 ml Concentrated HCL (39%) to 800 ml water. Bring
to 1,000 ml with water.
0.00564N PAO (Phenylarsine Oxide).
Oxine is available from IDD in 1, 5, 30, 55 gallon and tote containers. Test kits and
replacement materials can also be purchased from IDD.

PROCESS & PACKAGING, INC. 2003

OXINE & PUROGENE SANITIZER


STORAGE:
Concentrated ClO2 can be stored in a dry area away from acids for up to 3 years
under standard conditions.
Activated ClO2 has a half-life of approximately 48 hours under standard conditions.
Activated ClO2 can be added to cold water at 4,000 ppm. Under such conditions a
half-life of up to 2 weeks is possible under standard conditions.
AUTOMATIC ACTIVATION SYSTEMS:
A series of low cost, hands free, automated activation systems are available to provide
a continuous volume of activated ClO2 into a storage reservoir as needed. These
systems eliminate the need for manual mixing, measuring and dispensing.

PROCESS & PACKAGING, INC. 2003

INTERNATIONAL,

INC.

MATERIAL SAFETY DATA SHEET


I

SECTION 1: CHEMICAL PRODUCT AND COMPANY IDENTIFICATION


PRODUCT NAME
Oxine
CHEMICAL FAMILY
Mixture of Oxychlorine Compounds

MANUFACTURER
Bio-Cide International, Inc., 2845 Broce Drive, Norman, OK 73072 U.S.A. (800.323.1398)

EPA REGISTRATION NUMBER:


9804-1

EFFECTIVE DATE:
June 2004

SUPERSEDES:
April 2002

SECTION 2: COMPOSITIONIINFORMATION

ON INGREDIENTS

Chemical Name

C.A.S. No.

% by Wt.

Sodium Chlorite

7758-19-2

3.35%

SECTION 3: HAZARDS IDENTIFICATION


EMERGENCY OVERVIEW
Clear liquid with very faint chlorinous odor
May cause skin reaction. May cause eye irritation.

POTENTIAL HEALTH EFFECTS


INHALATION:

Prolonged inhalation of fog or mist may be irritating to nose and throat.

SKIN:

Based on rabbit studies, product is listed as "practically not an irritant".


Prolonged exposure may produce localized irritation, contact dermatitis, mild
erythema and edema.

EYE:

Based on rabbit studies, product has been given an EPA Category III rating as a
mild irritant. Exposure can produce slight irritation of conjunctiva, cornea and
eyelid.

INGESTION:

Ingestion may produce gastric discomfort, nausea, vomiting and diarrhea. Intake
of large quantities may produce methemoglobinemia.

SYSTEMS OF OVER EXPOSURE


Skin and eye irritation. Exposures to chlorine dioxide from activation can produce coughing.

MEDICAL CONDITIONS AGGRAVATED BY EXPOSURE


Skin disorders, such as dermal allergies and dermatitis. Exposure to chlorine dioxide produced
by activation can aggravate pulmonary disorders, such as emphysema.

- 1-

CHRONIC EXPOSURE EFFECTS


May cause localized irritation to areas exposed to product.
,

SECTION 4: FIRST AID MEASURES


The following procedures are recommended as emergency first aid only. They are not intended to
replace or supplant the treatment advice of a physician or other authorized health care specialist.

Inhalation:
Move person to fresh air. If person is not breathing, call 911 or an ambulance, and then
give artificial respiration, preferably mouth-to-mouth if possible. Call a poison control center or doctor for
further treatment advice.
Skin Contact:

Take off contaminated clothing. Rinse skin immediately with plenty of water for 15-20
minutes. Call a poison control center or doctor for further treatment advice.

Eye Contact:
Hold eye open and rinse slowly and gently with water for 15-20 minutes. Remove
contact lenses, if present, after the first 5 minutes, then continue rinsing eye. Call a poison control center
or doctor for further treatment advice.
If Swallowed:
Call a poison control center or doctor immediately for treatment advice. Have person
sip a glass of water if able to swallow. Do not induce vomiting unless told to do so by a poison control
center of doctor. Do not give anything by mouth to an unconscious person.
NOTES TO PHYSICIAN
Chlorine dioxide vapors are emitted when this product contacts acids or chlorine. If these vapors
are inhaled, monitor patient closely for delayed development of pulmonary edema which may
occur up to 48-72 hours post inhalation.

SECTION 5: FIRE FIGHTING MEASURES


FLAMMABLE PROPERTIES
Autoignition temperature
Flash Point
Flammable Limits - LEL
Flammable Limits - UEL

Not
Not
Not
Not

Applicable
Applicable
Applicable
Applicable

EXTINGUISHING MEDIA
Water unless contraindicated by other materials involved in the fire.

FIRE-FIGHTING EQUIPMENT
Standard protective gear with self-contained breathing apparatus.

SPECIAL FIRE-FIGHTING PROCEDURES


Do not allow product to evaporate to dryness.
atmosphere. Open or vent any large containers.

If chlorine dioxide gas is produced, vent to

UNUSUAL FIRE OR EXPLOSIVE HAZARDS


The sodium chlorite in dried Oxine~ is a strong oxidizer, which supports combustion. Chlorine
dioxide, which may evolve from Oxine'" solutions, is explosive in the gaseous phase at
concentrations greater than 10% by volume. Do not allow chlorine dioxide gas to accumulate
within a confined space.

Note: See STABILITY AND REACTIVITY (SECTION 10) for hazardous combustion and
thermal decomposition information.

-2 -

SECTION 6: ACCIDENTAL RELEASE MEASURES


ENVIRONMENTAL NOTIFICATION
All spills and leaks involving more than 10 gallons should be reported to the nearest regional EPA
office or designated state emergency response office with 24 hours. Spills from ocean vessels or
which may contaminate U.S. costal waterways should be reported to the nearest Coast Guard
office within 24 hours.

SPILL OR LEAK PROCEDURE


Small spills, involving less than 10 gallons, may be flushed to a designated and permitted sewer
system with the amount of water that is about 10 times the amount of the spill.
Large spills, involving more than 10 gallons, should be contained and neutralized using anyone
of the three neutralizers: i) sodium sulfite, ii) sodium bisulfite, or iii) sodium thiosulfate. The
neutralization reaction can be extremely exothermic, and therefore, care should be taken to add
the neutralizer in small increments. Sodium sulfite is the most preferred (least exothermic)
neutralizer that can be used in the ratio of 1 Ib per gallon of spilled material. Sodium thiosulfate
can be used in the ratio of 2 Ibs of anhydrous salt or 3 Ibs of pentahydrate salt per estimated
gallon of the spilled material. The neutralized solution can then be flushed to a designated and
permitted sewer system with double the amount of water. The product that is not neutralized may
be disposed of as chemical waste in the manner indicated below. The vicinity of the spill should
be thoroughly flushed with water after clean-up. At no time should the spilled material be allowed
to dry to a crystalline salt. Do not discharge this product to storm drains or to any surface or
groundwater source unless specifically allowed under a valid NPDES permit.
If the neutralizer is not available, volumes larger than 10 gallons should be carefully transferred
into a container and taken to an authorized chemical disposal site (Class I or landfill) in
accordance with all federal, state, and local regulations. Consult with selected facility regarding
the need for prior neutralization of waste.

SECTION 7: HANDLING AND STORAGE


HANDLING
Use product only as directed by the label. Avoid contact with skin and eyes; avoid breathing any
vapors or fumes resulting from product activation. Wash thoroughly after handling. Thoroughly rinse
all protective gear and handling equipment, such as transfer pumps and lines, with water prior to
reuse or storage. Keep away from children, animals, and unauthorized personnel.

PRODUCT STORAGE
Store in a cool, dry, well-ventilated location away from acids, chlorine and chlorine compounds,
hypochlorites
(bleach), organic solvents, sulfur and sulfite compounds,
phosphorus,
combustiblelflammable materials, and direct sunlight. Keep containers tightly closed when not in
use and open carefully to prevent spillage.
Storage on wooden floors and pallets is not
recommended. Do not contaminate water, food or feed by storage or disposal.

SECTION 8: EXPOSURE CONTROLS/PERSONAL PROTECTION


ENGINEERING CONTROLS
VENTILATION
Open air or good room ventilation is normally adequate for safe use of this product. Avoid
breathing any vapors or fumes resulting from acid activation.

-3 -

PERSONAL PROTECTIVE EQUIPMENT (PPE)


Eye/Face Protection
Good manufacturing practice recommends use of chemical safety goggles for all applications
involving chemical handling.

Skin Protection
Good manufacturing practice recommends that, at a rmrumurn, rubber, neoprene, or other
chemically impervious gloves be worn for all applications involving chemical handling.

Respiratory Protection
In accordance with OSHA regulations (29 CFR 1910.134 and 29 CFR 1910.1000), fogging or
spraying applications may require worker respiratory protection, such as: (1) NIOSH/MSHA
approved air-purifying respirators, or (2) NIOSH/MSHA approved canister/cartridge facial
respirators rated for chlorine/acid vapors or specified for chlorine dioxide.

General
Product should be stored and applied in close proximity to a safety shower, chemical eyewash
station or other fresh water source.

SECTION

9: PHYSICAL

Odor, Color, Grade


General Physical Form
Volatile Organic Compounds
Flash Point
Evaporation Rate
Solubility in Water
Boiling Point
Vapor Density
Vapor Pressure
Specific Gravity
pH
Melting point:

SECTION

AND CHEMICAL

PROPERTIES

Clear liquid with very faint chlorinous odor


Liquid
<0.1% by weight
Not applicable
Comparable to water
Complete
213F (100.5C)
0.02 kglm3
23.7 mm Hg (25C)
1.03 glml (200C)
8.0 - 8.5
Not determined.

10: STABILITY

AND REACTIVITY

CHEMICAL STABILITY
Stable

Materials and Conditions to Avoid:


Avoid storing product under conditions in which it could evaporate to crystalline salt. Avoid
accidental contact of concentrate with acids, chlorine compounds, hypochlorites (bleach), sulfur
and sulfite compounds, phosphorous, organic solvents and combustiblelflammable material

Hazardous

Reaction and Decomposition

Products:

Exposure to acids or chlorine compounds can produce uncontrolled generation of chlorine dioxide
gas.

Hazardous Polymerization:
Hazardous polymerization will not occur

-4-

SECTION

11: TOXICOLOGICAL

INFORMATION

ANIMAL TOXICOLOGY
Inhalation LC50:
Dermal LD50:
Oral LD50:

>5.61 mg/I
>2,020 mg/kg (rabbit)
4,360 mg/kg (rat)

CARCINOGENICITY
Active ingredients are not listed by ROTECS, OSHA, IARC, NTP or EPA. No evidence to date
implicating product as a carcinogen or tumor promoter.

MUTAGENICITY
Though product active ingredient is a chemical oxidant, no evidence to date for mutagenicity from
whole animal or in vitro studies.

REPRODUCTIVE/DEVELOPMENTAL

TOXICITY

No known effects to date.

SECTION

12: ECOLOGICAL

INFORMATION

ECOTOXICOLOGICAL INFORMATION
This product is toxic to fish and aquatic organisms. Do not discharge effluent containing this
product into lakes, streams, ponds, estuaries, oceans or other waters unless in accordance with
the requirements of a National Pollutant Discharge Elimination System (NPDES) permit and the
permitting authority has been notified in writing prior to discharge. Do not discharge effluent
containing this product to sewer systems without previously notifying the sewage treatment plant
authority. For guidance, contact your State Water Board or Regional office of the EPA.

SECTION

13: DISPOSAL

CONSIDERATIONS

CONTAINER DISPOSAL
Triple rinse. Then offer for recycling or reconditioning; or puncture and dispose of in a sanitary
landfill; or by incineration; or, if allowed by state and local authorities, by burning. If burned, stay
out of smoke.

PESTICIDE DISPOSAL
Wastes resulting from the use of this product may be disposed of on site or at an approved waste
disposal facility.

DISPOSAL PROCEDURE
Small quantities, less than 10 gallons, may be flushed to an authorized and permitted sewer with
copious amounts of water. Larger volumes should be taken to an authorized chemical disposal
site (Class I or landfill) in accordance with all federal, state and local regulations. Consult with
selected facility regarding the need for prior neutralization of waste.

SECTION

14: TRANSPORT

Not DOT Regulated

-5 -

INFORMATION

SECTION 15: REGULATORY INFORMATION


US FEDERAL REGULATIONS
TSCA
All product ingredients are in inventory

SARA TITLE 312/313


Neither the product nor its constituent ingredients are listed under SARA reporting requirements.
Chlorine dioxide produced from activation is listed under SARA 313.

RCRA
Not considered a hazardous waste either categorically or by chemical listing.

FIFRA
Oxine" is an EPA registered sanitizer (EPA No. 9804-1)

FEDERAL OSHA REGULATIONS


Neither product nor constituent ingredients is classified as an acute or chronic health hazard by
OSHA. Chlorine dioxide produced by activation is regulated with an air exposure limit of 0.1 ppm
TL V and 0.3 ppm STEL.

STATE LAWS
CALIFORNIA: Not regulated under the provisions of Proposition 65 (Safe Drinking Water and
Toxic Enforcement Act of 1986)
NEW JERSEY:

Sodium Chlorite is listed under New Jersey's Chemical Inventory Notification


Requirement (NJAC 7:1Z). Estimated release notification, however, is not required.

NOTE: Regulatory requirements are subject to change and may vary from one location to
another. It is the user's responsibility to ensure compliance with all applicable federal, state and
local regulations pertaining to the purchase, transport, storage, use and disposal of this product.
CHEMICAL INVENTORIES
This material contains one or more substances listed on the TSCA Inventory. Commercial use of
this material is regulated by the EPA.
This MSDS has been prepared to meet the U.S. OSHA Hazard Communication

Standard,

29 CFR 1910.1200

SECTION 16: OTHER INFORMATON


NFPA Hazard Classification
Health: 1
Flammability:

Reactivity:

Special Hazards:

None

National Fire Protection Association (NFPA) hazard ratings are designed for use by emergency response
personnel to address the hazards that are presented by short-term, acute exposure to a material under
conditions of fire, spill, or similar emergencies. Hazard rating primarily based on the inherent physical
and toxic properties of the material but also include the toxic properties of combustion or decomposition
products that are known to be generated in significant quantities.

NOTICE: Manufacturer believes the information contained herein is accurate; however we make no
guarantees with respect to such accuracy and assume no liability in connection with the use of the
information contained herein by any party. Any party using this product should review all such laws, rules
or regulations prior to use.
Product may bleach clothing and fabric materials, such as draperies and carpets.

NO WARRANTY IS MADE, EXPRESS OR IMPLIED FOR A PARTICULAR PURPOSE


OR OTHERWISE

-6 -

PLANNED PREVENTATIVE MAINTENANCE

PROCESS & PACKAGING, INC. 1999

PLANNED PREVENTATIVE MAINTENANCE FOR


SQUIRE, MINI KING, SUPER KING & EMPEROR
SERIES KEGGING & FLASH PASTEURIZATION
SYSTEMS
DAILY:
1. Clean machine after use, with low pressure hose and warm soapy water.
DO NOT HOSE DOWN THE ELECTRICAL PANELS
2. Check and monitor service pressures and temperatures prior to and during operation in line with
operations manual recommendations.
3. Change caustic and/or acid detergents hourly and monitor pH levels as necessary.
4. Check the connection head spear adapters for damage. Change if necessary. Any damage may be
transferred to the keg valve seal.

WEEKLY:
1.
2.
3.
4.

Check connection head seals and O rings for wear and damage. Replace if necessary.
Check for leaks on all service lines and unions. Replace seals and/or tighten as necessary.
Check for loose nuts and bolts. Tighten as necessary.
Check for loose wire terminations. Tighten as necessary.

MONTHLY:
1. Check dosing units for accuracy and operation in line with operations manual recommendations.
Adjust if necessary.
2. Check fiber optic, I.R. and/or fiber optic probes for cleanliness and operation. Clean and/or replace if
necessary.
3. Clean out all airline filters and drain out condensate.
4. Check all push button switches and indicator lamps for damage. Replace is necessary.
5. Clean out all steam strainers.
6. Check all spare parts inventory levels in line with operations manual. Order if necessary.

THREE MONTHLY:
1. Check pressure gauges for accuracy. Adjust and/or replace if necessary.
2. Check the transfer system alignment and keg placement over the connection heads. Adjust and/or
replace worn parts and lubricate if necessary.
3. Check all hoses for leaks and/or wear. Replace if necessary.
4. Check tri-clover seals for wear and/or damage. Replace if necessary.
5. Check pressure switch calibrations and adjust according to the manual if necessary.
6. Check all reject functions are operational on all process heads.
7. Check all electrical power connections and motor overload settings. Reset if necessary.

YEARLY:
1.
2.
3.
4.
5.
6.
7.

Inspect all wearing strips. Replace if necessary.


Check process valve, seats, O rings and seals for wear. Replace if necessary.
Inspect pump seals for wear or damage. Replace if necessary.
Inspect all air cylinder seals for wear and/or damage. Replace if necessary.
Check nylon air lines for leaks and flexibility. Replace if necessary.
Check all solenoid valves for proper operation. Replace if necessary.
Replace seals on all process valves.
PROCESS & PACKAGING, INC. 1996

DIMENSIONS

PROCESS & PACKAGING, INC. 2003

RECOMMENDED SPARES PARTS

PROCESS & PACKAGING, INC. 1999

SERVICES

PROCESS & PACKAGING, INC. 2003

SERVICE REQUIREMENTS FOR 50 HL/HR FLASH PASTEURIZATION SYSTEM


NOTATION

LOCATION

SERVICE

1
2
3

BEER
CO2
STEAM

9
10
11

PASTEURIZER
S. P. TANK
HOT WATER
SET
C.I.P./S.L. TANK
HEAT
EXCHANGER
HEAT
EXCHANGER
C.I.P./S.L. TANK
HOT WATER
SET
PASTEURIZER
PASTEURIZER
C.I.P./S.L. TANK

12
13

C.I.P./S.L. TANK
PASTEURIZER

14

PASTEURIZER

4
5
6
7
8

PRESSURE
BAR
1
1
2.1

CONSUMPTION

FLOW RATE

TERMINATION COMMENTS

50 HL/HR
----70 KG/HR

50 HL/HR
0.1 M3/HR
120 KG/HR

1.5 O/D TUBE


N/B PIPE
1.5 N/B PIPE

STEAM
GLYCOL
IN
GLYCOL
OUT
WATER
WATER

2.1
3.0

-----70 HL/HR

100 KG/HR
100 HL/HR

1 N/B PIPE
1.5 N/B PIPE

-2.2 DEG C

2.4

70 HL/HR

50 HL/HR

1.5 N/B PIPE

3.3 DEG C

2.8
2.8

-----------

50 HL/HR
------

1 N/B PIPE
N/B PIPE

TOP UP

AIR
POWER
C.I.P.
RETURN
CAUSTIC
PRODUCT
OUT
C.I.P.
RETURN

5.7
480-3-60
------

-----20 AMP
------

0.3 M3/HR

N/B PIPE

-------

1.5 O/D TUBE

-----1

-----50 HL/HL

-----50 HL/HR

N/B PIPE
1.5 O/D TUBE

-------

------

------

1 DEG C

FROM
FILLER
DOSING

1.5 O/D TUBE BEER SUPPLY


MAIN

An Air Dryer will remove moisture from compressed air to a certain degree of dryness and this is referred
to as pressure dew point. Different types of dryers can achieve different dew points and, for the most part,
the drier the air needs to be, the more expensive it is to dry
Refrigerated Dryers condense the moisture out of the air and drain it away as liquid. They are limited to
about 35 F because the water would freeze if it got any colder.
Desiccant Dryers adsorb the moisture in the compressed air and remove it while still suspended as vapor.
They are typically applied at about -40 F, but can get to -100 and below.
Membrane Dryers use permeability to separate the moisture from the air and can also achieve low dew
points.
The selection is made on personal preference, the dryness required, and cost, which should include
operating and electrical or utility costs.

Reproduced in part from the web site of:


Gulf Atlantic Equipment, Co., Jacksonville, Florida. 904-636-8555 Fax: 904-636-8554 2006

CYCLE TIMES

SEE FP PROGRAM &


CONTROL PHILOSOPHY
SECTIONS FOR INFORMATION

PROCESS & PACKAGING, INC. 2003

FLOW DIAGRAM

PROCESS & PACKAGING, INC. 2003

CONTROL PHILOSOPHY

PROCESS & PACKAGING, INC. 2003

CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

AUTOMATIC FLASH PASTEURIZATION SYSTEM


CONTROL PHILOSOPHY

Project:

Automatic Flash Pasteurization System

Customer:
Job Number:
Revision:
Originator......................... Name:
Title:

Jeffrey Gunn
President

Generic

This is an unpublished work, the copyright of which vests in IDD Process & Packaging
Inc. All rights reserved. This document and the information contained herein is supplied
without liability for errors or omissions and no part may be reproduced, used or disclosed
except as authorized by contract or IDDs written permission. The copyright and the
foregoing restrictions and/or reproduction, use and disclosure extend to all media in which
this information maybe embodied.

PROCESS & PACKAGING, INC. 2008


1 of 15

CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER


INDEX:
Startup Sequence ------------------------------------------- Page 3
Alarm Sequence 1 ----------------------------------------------- Page 5
- Product over temperature on holding tube (RTD1)
- Flow Meter (FM1) low flow
- SPT HL probe condition

Alarm Sequence 2 ------------------------------------------ Page 7


- SPT UHL Condition (DP Failure)

Alarm Sequence 3------------------------------------------- Page 8


- Under temperature alarm
- Flow Meter (FM1) high flow

Alarm Sequence 4 ------------------------------------------ Page 9


- SPT ULL probe becomes uncovered
during production forward flow

Runoff Sequence ------------------------------------------- Page 10


Shutdown Sequence --------------------------------------- Page 12
Abbreviation descriptions --------------------------------- Page 14
Flow Diagram ---------------------------------------------- Page 15

PROCESS & PACKAGING, INC. 2008


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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

START UP SEQUENCE:
Start-Up to be commenced only after CIP and Hot Water
and/or Oxine Water Sterilize sequence
NOTE: All sequences described below are automatic unless preceded with Operator
Reference attached Flow Diagram

Open V7 until water exits through PRV1 to drain.

Open AV6 to fill SL/CIP Tank

Operator - select MENU then VALVE SCREEN and turn on AV2 & AV4. Select MENU
then PUMPS SCREEN and turn on Main Product Pump (P1), and Hot Water Pump (P3) to
place pasteurizer into water recirculation.

Operator - select MENU then TEMP. SELECT SCREEN and select either target
pasteurize or target CIP temperature. If necessary adjustment of setpoint can be made by
selecting the TEMPERATURE ADJUST SCREEN and adjusting the appropriate target
temperature.

When AV2 & AV4 are shown open, Main Product Pump (P1) running, FM1 flow indication,
Hot Water Recirculation Pump (P3) running & SL Tank LL probe is covered. System waits 1
min. to check system stability; Main Screen STATUS displays UNSTABILIZED or
STABILIZED depending on temperature stability.

NOTE: A STABILIZED condition must be shown for system to be ready for automatic startup.
NOTE: Flow rate and chase times are preset at time of commissioning.

Operator - select MENU then STARTUP.

AV1 opens.

When AV1 is open;

AV2 closes.

When AV2 is closed;

Start Product chase of water to SL/CIP Tank timer.

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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

Main screen displays PROD/WTR TO SLT.

When the timer times out;

AV5 opens.

When AV5 is open;

AV4 closes.

When AV4 is closed;

Start Product chase of water/product interface to Drain timer.

Main screen displays PROD/WTR TO DRAIN.

When the timer times out;

AV3 opens.

When AV3 is open;

AV5 closes.

When AV5 is closed;

Main screen displays FORWARD FLOW

NOTE: Manual valve V9 on AV5 drain line is partially closed and set to control flow rate to equal
the resistance of the SPT back pressure of 13 to 15 PSIG

When Low Level point in SPT is reached;

Product Boost Pump (P2) starts. (Operator must first turn Product on at the PUMPS screen)

If CIP/SL Tank LL probe is uncovered AV6 opens.

AV6 closes when CIP/SL Tank HL probe becomes covered.

PROCESS & PACKAGING, INC. 2008


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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

ALARM SEQUENCE 1
DURING PRODUCTION / FORWARD FLOW.
Alarm Conditions: Product over temperature on holding tube (RTD 1).
Flow Meter low flow (FM1).
SPT High Level Alarm condition.

Audible alarm on.

Operator to press ALARM ACCEPT and confirm type of alarm under ALARMS on the
Main Display Screen.

AV2 opens.

When AV2 is open;

AV1 closes.

When AV1 is closed;

Main screen displays WTR/PROD TO SPT.

Start water chase timer of product to the SPT

When the timer times out;

AV5 opens.

When AV5 is open;

AV3 closes.

Main screen displays WTR/PROD TO DRAIN.

Start water flush timer.

Product/Water interface flushed to drain.

Water flush timer times out.

AV4 opens.

When AV4 is open;

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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

AV5 closes.

When AV5 is closed;

Main screen displays WATER RECIRCULATION.

When the alarm has cleared and the system has stabilized for 1 min., remain in water
recirculation until the level in the SPT falls below low level.

AV1 opens.

When AV1 is open;

AV2 closes.

When AV2 is closed;

Start Product chase of water to CIP/SL Tank timer.

Main screen displays PROD/WTR TO SLT.

When the timer times out;

AV5 opens.

When AV5 is open;

AV4 closes.

When AV4 is closed;

Start product chase of water to drain timer.

Product chases Water/Product interface to drain.

Main screen displays PROD/WTR TO DRAIN.

When the timer times out;

AV3 opens

When AV3 is open;

PROCESS & PACKAGING, INC. 2008


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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

When AV5 closes.

When AV5 is closed;

Main screen displays FORWARD FLOW.

If C I P/S L Tank LL Probe in uncovered AV6 opens until it is covered

ALARM SEQUENCE 2
DURING PRODUCTION / FORWARD FLOW.
Alarm Condition: SPT - DP Cell Failure Alarm.

Audible alarm on.

Operator to press ALARM ACCEPT and confirm type of alarm under ALARMS on the
Main Display Screen.

AV5 opens.

When AV5 is open;

AV3 closes.

When AV3 is closed;

AV2 opens.

When AV2 is open;

AV1 closes.

When AV1 is closed;

Main screen displays WTR/PROD TO DRAIN.

Start water chase timer of product to drain.

When the timer times out;

AV4 opens.

When AV4 is open;


PROCESS & PACKAGING, INC. 2008
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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

AV5 closes.

When AV5 is closed.

Main screen displays WATER RECIRCULATION.

Operator to wait until SPT empties below ULL point.

Operator to go to MENU screen then press SHUTDOWN to repair DP Cell failure.

When problem is resoved repeat startup sequence.

ALARM SEQUENCE 3
DURING PRODUCTION / FORWARD FLOW.
Alarm Conditions: Under temperature alarm (RTD 1)
Flow Meter (FM1) high flow.

Audible alarm on.

Operator to press ALARM ACCEPT and confirm type of alarm under ALARMS on the
Main Display Screen.

The Glycol proportional valves close.

Operator to close glycol manual isolation valve & open glycol vent V30.

AV5 opens.

When AV5 is open;

AV3 closes.

When AV3 is closed;

AV2 opens.

When AV2 is open;

AV1 closes.

When AV1 is closed;

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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

Main screen displays WTR/PROD TO DRAIN.

Start water chase of product to drain timer.

When the timer times out;

AV4 opens.

When AV4 is open;

AV5 closes.

When AV5 is closed;

Interrupt AV6 top up of CIP/SLT during this sequence:

Main screen displays WATER RECIRCULATION.

Operator selects MENU then SHUTDOWN

Operator to repair alarm condition.

Operator commences with manual re-sterilize and CIP procedure.

ALARM SEQUENCE 4
DURING PRODUCTION / FORWARD FLOW.
Alarm Condition: SPT Ultra Low Level (ULL) reached during production/forward flow.

Product Boost Pump (P2) stops.

Audible alarm on.

Operator to press ALARM ACCEPT and confirm type of alarm under ALARMSon the
Main Display Screen.

P2 re-starts when level in SPT reaches Low Level.

PROCESS & PACKAGING, INC. 2008


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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

RUNOFF SEQUENCE:
At any time during production forward flow the operator can run out the remaining product in the
pipework to the SPT for the end of production, brand change or temporary interrupt of pasteurizing
as follows:

Operator to select MENU then RUNOFF from the display.

AV2 opens.

When AV2 is open;

AV1 closes.

When AV1 is closed;

Main screen displays WTR/PROD to SPT.

Start water chase timer of product to the SPT

When the timer times out;

AV5 opens.

When AV5 is open;

AV3 closes.

When AV3 is closed;

Start water flush timer.

Product/water interface flushed to drain; main screen displays WTR/PROD TO DRAIN.

Water flush timer times out.

AV4 opens.

When AV4 is open;

AV5 closes.

When AV5 is closed.

PROCESS & PACKAGING, INC. 2008


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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

Main screen displays RUNOFF. (This means system is water recirculation)

NOTE: If desired at this point, the operator can shut down the system by pressing SHUTDOWN,
or press RE-START to continue with production. If SHUTDOWN is selected please see
Shutdown, end of production & flush out sequence.
NOTE: To re-start production / forward flow the operator can, at any time complete the following:

From the MENU screen press RE-START

When the CIP/SL Tank LL probe is covered;

AV1 opens.

When AV1 is open;

AV2 closes.

When AV2 is closed;

Start Product chase of water to CIP/SL Tank timer.

Main screen displays PROD/WTR TO SLT.

When the timer times out;

AV5 opens.

When AV5 is open;

AV4 closes.

When AV4 is closed;

Product/water interface chased to drain.

Start Product chase of water to Drain timer.

Main screen displays PROD/WTR TO DRAIN.

When the timer times out;

AV3 opens.

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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

When AV3 is open;opens

AV5 closes.

When AV5 is open;

Main screen displays FORWARD FLOW.

SHUTDOWN SEQUENCE:
End of production & flush out.
NOTE: All Sequences below are manual and are performed by the Operator.
NOTE: System must indicate WATER RECIRCULATION" on Main Screen.

From the MENU screen select SHUTDOWN. The Hot Water Recirculation Pump (P3) will
stop. The steam and glycol proportional valves will be driven closed.

Close the steam and glycol supplies to the HWS and PHE respectively.

NOTE: Selecting shutdown on the display will produce the CIP screen which is for manual control
of all auto valvesAV and pumps from this point on.

Turn off the CO2 supply to the SPT

Slowly open SPT valve V13 to drain and de-pressurize the tank and pipework.

Open SPT valve V11.

Partially open SPT valve V10.

Set filling line equipment up for CIP

Close CIP/SL Tank valve V15.

Open CIP/SL Tank valve V14.

Check the CIP/SL Tank is full; if not open AV6 until the tank is full.

Open and close AV5 several times to rinse the valve.

Open AV3.

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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

Close AV4

When the level in the S.P.T reaches Low Level

Open V12

Start the Product Boost Pump (P2)

When clean water is detected at the CIP/SL Tank V14 drain

Open CIP/SL Tank V15

Close CIP/SL Tank V14

Stop all pumps and close all auto valves.

End of Flush Out and Shut Down sequence.

PROCESS & PACKAGING, INC. 2008


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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

ABBREVIATION DESCRIPTION
SPT ----------------- STERILE PRODUCT TANK
CIP/SL Tank ------- CLEANING IN PLACE / STERILE LIQUOR TANK
HWR ---------------- HOT WATER RECIRCULATION
P1 -------------------- MAIN PRODUCT PUMP (MPP)
P2 -------------------- PRODUCT BOOST PUMP (PBP)
P3 -------------------- HOT WATER RECIRCULATION PUMP (HWRP)
AV ------------------- AUTO VALVES (1 THRU 6)
V --------------------- MANUAL VALVES (7 THRU 18)
FM1 ----------------- FLOW METER
RTD1 ---------------- RESISTANCE THERMOMETER (PASTEURIZATION TEMP)
RTD2 ---------------- RESISTANCE THERMOMETER (PASTEURIZER OUTLET TEMP)
PHE ------------------ PLATE HEAT EXCHANGER
CIP ------------------- CLEAN IN PLACE
PRV ------------------ PRESSURE RELIEF VALVE (HWR)
PRV/AVV ----------- PRESSURE RELIEF/ANTI-VACUUM VALVE (SPT)
FCV1 ----------------- FLOW CONTROL VALVE (MPP OUTLET)
FCV2 ----------------- FLOW CONTROL VALVE (PHE OUTLET)
PCV1 & 2 ------------ PROPORTIONAL CONTROL VALVES (STEAM AND GLYCOL)
TCV1 ----------------- THERMOSTATIC CONTROL VALVE (STEAM)
LL --------------------- CIP/SL TANK LOW LEVEL PROBE
HL --------------------- CIP/SL TANK HIGH LEVEL PROBE

PROCESS & PACKAGING, INC. 2008


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CONTROL PHILOSOPHY AUTOMATIC FLASH PASTEURIZER

PROCESS & PACKAGING, INC. 2008


15 of 15

PROGRAM LISTING

Program Loaded into PLC


& Fully Tested
Program Listing Copy is on File

PROCESS & PACKAGING, INC. 1999

APPENDIX

PROCESS & PACKAGING, INC. 2003

What is Pasteurization
and how is it defined ?
Louis Pasteur (1822 - 1895), the father of microbiology and pasteurization, found
that heating wine would kill micro-organisms without damaging the wine.
In a paper entitled Thermal Death Time Studies on Beer Spoilage Organisms,
Del Vecchio et al (ASBC, Proc. 45, 1951), produced data to plot a Thermal
Death Time Curve
Benjamin later chose and suggested in an unpublished study at the American Can
Companys laboratory, that one Pasteurization Unit (P.U.) be defined as 140F
(60C) for 1 minute.
Ball went on to designate the Z factor as the number of degrees Fahrenheit
traversed by the curve in passing through one log cycle.
The Z factor is equal to 12.5F (7C) and 5.6PUs.

Pasteurization
the Pasteurization Unit (PU)
1 PU = 1.3932

(T - 60)

Hold Time (secs.)


60 secs.
Where: T = Pasteurization Temperature in C.
-----------------------------------------------

Beer pasteurization can be confirmed by using the ASBC invertase test


detailed in Proc. (1960) page 63.
NOTE: The invertase test only determines that the beer is pasteurized,
NOT by how much.
Dallyn & Fallons work (The Brewer 1976, 62, 354.) indicated that
2 PU will approximate a 1 log reduction in beer spoilage organisms.
Therefore, 10 PU should effectively reduce organisms by a factor of 105

Pasteurization Options
In the brewery packaging environment
two methods of pasteurization have evolved for beer:
Tunnel Pasteurization for cans and bottles - Hot water immersion at 165F (74C)
of cans and bottles for 20 to 40 P.U.s.
A late 19th century comfort level approach for brewers. Widely used today but
still restricted by the physical limitations of heat transfer to and from the bottle!
Flash Pasteurization for kegs - The rapid and even temperature rise of beer
to 160.7F (71.5C) for 20 seconds for American Lagers ( 15PU) and 161.6F
(72C) for 30 seconds for European Ales and Lagers ( 26PU).
The way that virtually all keg beer is packaged and shipped great distances.
Relatively new to North American brewers where glass, PET bottles and can
beer is concerned.

The typical heat transfer coefficient ratio of


Flash to Tunnel Pasteurization is 24:1.
Taken from an unpublished study by Mr. Paul Kidger of Allied Breweries
(Study carried out through the 1970s).

Tunnel Pasteurization
Heat Transmission
of bottled beer

Hot Spot
12 min. to reach 140F

When the bottle size, shape


and thickness is conducive to
tunnel pasteurization and
the average volume is at
15 PU. The hot and cold spots
will be at least 30% above and
below the desired PUs
respectively.

Thermal Convection

MBAA Packaging Course


Presented by Barry-Wehmiller

Cold Spot
25 min. to reach 140F

Average Volume

Tunnel Pasteurization
SYSTEM PROs and CONs
PROs

CONs

Pasteurization of the beer in

Over pasteurization is common in 65%

the sealed package - High


assurance of pasteurization.

of the beer volume due to lack of thermal


convection in the bottle or can.
Difficult to control PU input when the
system is in a stop and start mode.
Flavor change - Over pasteurization.
Virtually impossible to handle PET
bottles.
Large foot print.
High energy usage.
High maintenance.

Flash Pasteurization
System Examples

Skid Mounted,
Fully Automatic
PurePass Systems
with
Sterile Product &
CIP/Sterile Liquor
Tanks

PurePass System Features


Sterile Product
Tank PR/AVV

Control Panels

Sterile Product
Tank
CIP/Liquor
Tank

Valve Manifold

Hot Water
System &
Control

Flow Meter
Glycol Control
(Optional)

Holding Tube

Product
Pump

Hot Water
Recirculating
Pump
Plate Heat Exchanger

PurePass
Flash Pasteurization
System Features

Flash Pasteurization
Control philosophies
There are TWO basic flash pasteurization system control philosophies:
THE STEADY STATE PHILOSPHY - Where flow, pressure and temperature stay

constant at all times during beer pasteurization.


- Pasteurized water is re-circulated within the system once the Sterile Beer Tank
(SBT) has filled, thus maintaining a constant controlled operating state.
THE VARIABLE PHILOSOPHY - Where flow, pressure and temperature are

varied to maintain a controlled beer level within the Sterile Beer Tank (SBT).
- As the SBT fills, the flow rate automatically slows down. The temperature and
pressure balance within the system are also automatically adjusted to maintain PU
and CO2 in solution balance.
- Conversely, as the SBT empties, the flow rate increases and the system parameters
revert back.

The Steady State Philosophy is a personal preference from


years of operating and auditing of both system types.

Flash Pasteurization
Star Points for the
Plate Heat Exchanger (PHE) Design
FLOW - The beer flow rate should not exceed 6 feet per second and the CIP rate
should be at least 150% that of the beer flow rate but not lower than 8 feet per
second in order to achieve optimal CIP in adjacent product lines and temperature
holding tube.
PRESSURE - To keep the CO2 in solution during the pasteurization process,
pressure at 10% above the vapor point release pressure of the CO2 is required.
PRESSURE DROP (P) - The plate heat exchanger (PHE) plate pack design must
optimize the pressure drop to retain CO2 in solution through all sections without
sacrificing the flow rate during CIP when the higher flow rates are required.
TEMPERATURE - Today it is standard practice to achieve an economical heat
exchange efficiency (regeneration) of 92% to 96% during pasteurization with
heating and optional cooling loads being maintained at approximately 10% of
regeneration.

Flash Pasteurization
Star Points for the
System Design
HOLDING TUBE

- The holding tube should be of constant diameter to maintain


the ratio of mean to peak values in the velocity distribution across the tube diameter
as defined by Coulson & Richardson (Chemical Engineering, Vol. 1, Pergamon
Press, 1965-66). A constant Reynolds Number (Re) helps to maintain a PU constant
for all product passing through the holding tube.

MINIMUM RECIRCULATION OF BEER - A control philosophy that prevents the


over-pasteurization of beer and reduces recirculated (spoilt) beer loss to drain is
preferable.

HEATING SYSTEM - The controlled heating of water and then using the hot water
as an indirect medium through the PHE plates to the beer is the most accurate
method of PU control.
Virtually all known damage to PHEs is due to the presence of chloride in the form of
sodium hypochlorite bearing compounds. Free chlorides should not exceed 150 ppm.

Flash Pasteurization
SYSTEM PROs and CONs
PROs
Constant flow, pressure and temperature

CONs
Microbial contamination possible with

control system. (Personal Preference).


bottle or can filling systems due to open
PU control within 0.2 at all times when
package.
processing beer.
Might require a hot air knife or bottle
0 to 1000 PU possible for varying products.
warmer to cut down sweating and allow
Small footprint and skid mounted.
label application.
Low energy use with a minimum 92%
operating efficiency.
PET sterile packaging possible.
Low maintenance.
Modem system support.
Fully automated control interface via PLC,
touch screen control and trending software.

Flash Pasteurization
CO2 Equilibrium Chart
: Operating pressure 10% above vapor point pressure

Flash
Pasteurization
Heating and Cooling
loads at
92% regeneration

Flash Pasteurization
Typical IDD Flow Diagram

How do we maintain bottle, cap or crown,


filler sterility and product integrity?
We use;

Stabilized Chlorine Dioxide (ClO2)


Chelated at 8.4 pH in an aqueous solution and activated with a
food grade acid (typically phosphoric) at 4 pH.
The active concentrate is then mixed with cold water providing
4,000 ppm of available active ClO2 for dilution and distribution
through chemical proportioning unit(s) to the bottle line rinser.
Fogging nozzles are also mounted in conveyor tunnel(s), between
the rinser and filler, at the filler head feed point, valve cam lifter,
crowning heads and crowns.

What is Stabilized Chlorine Dioxide

Stabilized chlorine dioxide in the form of Oxine is a patented process available in


a concentrated and stable form with very low toxicity. As a powerful oxidant, it is
virtually unaffected by organic load and hard water.
It is a highly refined, two percent modified chlorite ion containing liquid product
and is 7 times more effective than chlorine. It is NOT a simple solution of tech
grade sodium chlorite.
Chlorine Dioxide gas (ClO2) was discovered in 1811 by Sir Humphrey Davey, three
years after he discovered chlorine.
It wasnt until the 1970s that aqueous phase generators were developed to allow
the dry chlorine gas to be produced in water based solutions of precursor compounds,
normally sodium chlorite and a mineral acid.
Hypochlorite solutions were later added to further drive the reaction as completely
as possible to chlorine dioxide.
These technical advances have resulted in the FDA (reference CFR P-1, 3-D and G-5)
EPA, USDA, Health & Welfare and the majority of international authorities
approving stabilized ClO2 as a direct contact sanitizer for numerous applications
within the brewery, winery, soft drink, juice, dairy and food (meat, fish, fruit and
vegetable) processing plants.

Comparison with Other Sanitizers


Concentration (PPM)of biocide required for > 5 log reduction in 60 seconds
Sanitizer
P. aeruginosa
S. aureus S. cerevisiae E. Coli
(O157: H7)
Oxine

30

30

Tech grade Sodium Chlorite

310

1300

640

Sodium Hypochlorite

200

200

400

600

Peracetic Acid

30

60

300

20

Dodecylbenzenesulfonic
Acid & Phosphoric Acid

40

80

600

90

Octanoic Acid, Decanoic


Acid, Citric Acid &
Phosphoric Acid

80

150

200

60

Source: Tanner, et al.; Dept. of Microbiology, University of


Oklahoma, Norman, OK, J. Indst. Micro. 1989, 4, 145-154.

Bio-Cide International, 2001

Comparison with Other Sanitizers


Concentration (PPM) of biocide required for > log 5 reduction in 60 seconds

Sanitizer
Oxine
Acidified Quat
Phenolic Compound
Iodophor
Glutaraldehyde

P. aeruginosa

S. aureus

S. cerevisiae

30

30

150

1,200

300

1,500

380

190

440

440

450

1,600

2,200

18,000

Source: Tanner, et al.; Dept. of Microbiology, University of


Oklahoma, Norman, OK; J. Indst. Micro. 1989, 4, 145-154.
Bio-Cide International, 2001

Comparison of Oxine with Chlorine


Property

Chlorine Dioxide

Chlorine

Primary Chemical
Reaction

Oxidation only, no other


chlorinated by-products.

Produces THMs and


chlorinated by-products

Corrosion

Low

High

Taste & Odor

None at use concentrations

Produces chemical taste

Effective pH Range

1-10

6.8-7.6

Reaction in Water

Does not hydrolyze

Hydrolyzes in water

Reaction to Organic
Load

Resists neutralization

Readily neutralized

Reaction to Biofilms

Highly reactive

Largely ineffective

Oxine Activation
Oxine

Activator

ClO2 gas

free ClO2

Oxy Chloro
species
unactivated
component

Total Available Chlorine Dioxide (TACD)


= Free ClO2 + unactivated component.
Percentage of activation = (Free ClO2 / TACD) x 100

Typical activation with phosphoric acid is about 15 to 25 %.


1 PPM activated Oxine is approx. 0.6 PPM Chlorite

Chlorite is an anion determined by ion chromatography.


Chlorite unlike Bromate will dissipate over approximately 48 hours.

An IDD Oxine
Activation &
Dosing System
for Rinsing &
Fogging

Stabilized Chlorine Dioxide


A bottling line sanitizing system schematicunlocks the limitations
of flash pasteurization for bottle and can products
This image cannot currently be displayed.

STABILIZED
ClO2
4,000 PPM

Flash Pasteurization

A 72 valve CC&S PET bottle filling line with a


Flash Pasteurization System

Stabilized Chlorine Dioxide


PROs

CONs

A strong oxidant and very powerful

Activated concentrate is a yellow/green

toxic gas, similar to chlorine.


antimicrobial agent active from 1 to 10 pH.
Unlike chlorine it does not form chlorinated The gas can explode in high air
concentrations 12%.
by products (salt residues).
It is highly soluble in water (similar to CO2 ).
It can be produced, stored, handled and
applied safely.
Does NOT require a potable water rinse
after application.
Approved by FDA, USDA, EPA, Health &
Welfare for use in potable water (4ppm)
and as a direct food contact sanitizer.
No discernible taste, odor or corrosivity.
No environmental impact (as defined by
the EPA).
Multiple uses in the brewery environment.

Flash Pasteurization &


Bottling Line Field Results
Samples are cells/ml/100ml samples - 7 day anaerobic & 5 day aerobic UBA incubations.
Results are a count average taken prior to flash pasteurization and after bottling over
approximately 150 days of operations unless otherwise stated.
Yeasts Lactobacilli Pediococci Non-Lactic
35
1

15
1

1
1

50
1

Before
After

Carolina Beer & Beverage 40


71.5C/20 secs.= 15PU
1

20
1

20
1

N/A
N/A

Before
After

Spoetzl Brewery.
50,000
68.0C/20 secs.= 4.8PU 1

3
1

N/A
N/A

N/A
N/A

Before
After

1.8 mill
1

N/A
1

1.8 mill
6

Before
After

Sprecher Brewing Co.


71.5C/20 secs.= 15PU

Brewery Trial
73.0C/20 secs.= 25PU

N/A
N/A

Test carried out with with infected beer at 1.8 million cells/ml.
Immobilizing yeast prior to introducing a new strain into bottled wheat beer.

Flash Pasteurization for keg & bottled beer.


CONCLUSIONS
1. Flash Pasteurization PU input is finite and under closer control over that of
tunnel pasteurization.
2. Product is evenly pasteurized resulting in no perceptible flavor change (with DO2
below 0.02ppm)
3. A lower overall PU input to obtain a 5 or 6 log kill.
4. Carbonated and non-carbonated products can be handled on the same system.
5. Flash pasteurization provides cross utilization for glass and PET bottles, cans
and keg products.
6. Significant reduction in capital equipment cost, space and maintenance and
higher overall operating efficiencies are realized.
7. The use of stabilized ClO2 in conjunction with the correct CIP and sanitizing
regimes can provide a microbially stable environment for, cans, glass and PET
bottled products.
8. Microbial stability of at least 9 months is a practical possibility.

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