Manual Julabo
Manual Julabo
Manual Julabo
Operating manual
EH-13
EH-33
EH-19
EH-39
JULABO GmbH
77960 Seelbach / Germany
Tel. +49 (0) 7823 / 51-0
Fax +49 (0) 7823 / 24 91
info@julabo.de
www.julabo.de
1.951.0257-V2
19510257-V2.doc
06/13
Print date: 11.07.13
Congratulations!
You have made an excellent choice.
JULABO thanks you for the trust you have placed in us.
This operating manual has been designed to help you gain an understanding of the operation
and possible applications of our circulators. For optimal utilization of all functions, we
recommend that you thoroughly study this manual prior to beginning operation.
Printed in Germany
EH
TABLE OF CONTENTS
Operating manual .................................................................................................................... 4
1.
2.
4.
5.
Preparations ..................................................................................................................14
5.1. Installation ................................................................................................................. 14
5.2. Bath fluids .................................................................................................................. 15
5.3. Filling / Draining ......................................................................................................... 17
5.4. Temperature application to external systems ............................................................ 18
5.4.1. Tubing ............................................................................................................... 18
5.5. Adjusting the pump flow ............................................................................................ 19
5.6. Countercooling .......................................................................................................... 20
6.
7.
8.
9.
Operating manual
Operating manual
1.
Intended use
JULABO circulators have been designed to control the temperature of specific fluids in a bath
tank. The units feature pump connections for temperature control of external systems (loop
circuit).
JULABO circulators are not suitable for direct temperature control of foods,
semi-luxury foods and tobacco, or pharmaceutical and medical products.
Direct temperature control means unprotected contact of the object with the
bath medium (bath fluid).
1.1.
Description
The circulators are operated via the splash-proof keypad. The implemented
microprocessor technology allows to set and to store the setpoint that can
be indicated on the LED temperature display.
The PID temperature control adapts the heat supplied to the thermal
requirements of the bath.
PID1
80
40
0
120
160
Electrical connection:
Alarm output for external alarm message or control of JULABO refrigerating
baths.
2.
The products of JULABO ensure safe operation when installed, operated, and maintained
according to common safety regulations. This section explains the potential dangers that may
arise when operating the circulator and also specifies the most important safety precautions to
preclude these dangers as far as possible.
The operator is responsible for the qualification of the personnel operating the units.
The personnel operating the units should be regularly instructed about the dangers involved
with their job activities as well as measures to avert these dangers.
Make sure all persons tasked with operating, installing, and maintaining the unit have read
and understand the safety information and operating instructions.
When using hazardous materials or materials that could become hazardous, the circulator
may be operated only by persons who are absolutely familiar with these materials and the
circulator. These persons must be fully aware of possible risks.
4
EH
If you have any questions concerning the operation of your unit or the information in this
manual, please contact us!
Contact:
JULABO GmbH
Eisenbahnstrae 45
77960 Seelbach / Germany
info@julabo.de
www.julabo.de
Appropriate operation
Only qualified personnel is authorized to perform configuration, installation, maintenance and
repairs of the circulator.
Routine operation can also be carried out by untrained personnel who should however be
instructed by trained personnel.
Use:
The bath can be filled with flammable materials. Fire hazard!
There might be chemical dangers depending on the bath medium used.
Observe all warnings for the used materials (bath fluids) and the respective instructions (safety
data sheets).
Insufficient ventilation may result in the formation of explosive mixtures. Only use the unit in
well ventilated areas. The unit is not for use in explosive atmosphere.
Only use recommended materials (bath fluids). Only use non-acid and non corroding materials.
or
Semi S1-0701 Table A1-2 #9
Carefully read the user information prior to beginning operation.
Scope: USA, NAFTA
Particular care and attention is necessary because of the wide operating range.
There are thermal dangers:
Burn, scald, hot steam, hot parts and surfaces that can be touched.
Warning label W26: Colors: yellow, black
Hot surface warning.
(The label is put on by JULABO)
Observe the instructions in the manuals for instruments of a different make that you connect to
the circulator, particularly the respective safety recommendations. Also observe the pin
assignment of plugs and technical specifications of the products.
2.1.
Disposal
The product may be used with oil as bath fluid. These oils fully or partially consist of mineral oil
or synthetic oil. For disposal, observe the instructions in the safety data sheets.
Valid in EU countries
See the current official journal of the European Union WEEE directive.
Directive of the European Parliament and of the Council on waste electrical
and electronic equipment (WEEE).
This directive requires electrical and electronic equipment marked with a
crossed-out trash can to be disposed of separately in an environmentally
friendly manner.
Contact an authorized waste management company in your country.
Disposal with household waste (unsorted waste) or similar collections of
municipal waste is not permitted!
EH
2.2.
EC Conformity
The products described in the operating instructions conform to the
requirements of the following European guidelines:
Directive of the European Parliament and of the Council on the
approximation of the laws of the Member States relating to machinery.
EMC guideline with respect to legal harmonization of the member countries
concerning electromagnetic compatibility.
JULABO GmbH
Eisenbahnstr. 45
77960 Seelbach / Germany
2.3.
Warranty conditions
JULABO GmbH warrants its products against defects in material or in workmanship, when used
under appropriate conditions and in accordance with appropriate operating instructions
for a period of ONE YEAR.
Extension of the warranty period free of charge
With the 1PLUS warranty the user receives a free of charge extension to the warranty of up to
24 months, limited to a maximum of 10 000 working hours.
To apply for this extended warranty the user must register the unit on the JULABO web site
www.julabo.de, indicating the serial no. The extended warranty will apply from the date of
JULABO GmbHs original invoice.
JULABO GmbH reserves the right to decide the validity of any warranty claim. In case of faults
arising either due to faulty materials or workmanship, parts will be repaired or replaced free of
charge, or a new replacement unit will be supplied.
Any other compensation claims are excluded from this guarantee.
Technical specifications
kW
kW
Circulating pump:
discharge, max.at 0 bar
pressure, max. at 0 l
l/min
bar
2.0
1.0
15
0.35
Vdc/mA
Ambient temperature
Mains power connection 230 V/50 Hz
Current input (208V / 230 V)
Mains power connection 230 V/60 Hz
Current input (208V / 230 V)
Mains power connection 115 V/60 Hz
Current input (at 115 V)
Mains power connection 100 V/60 Hz
Current input (at 100 V)
digital
LED
0.1
1-point
PID1
Electrical connections:
External alarm device
EH
20 ... 150
0.03
C
C
5 ... 40
V/ Hz
A
V/ Hz
A
V/ Hz
A
V/ Hz
A
190-253 / 50
8/9
190-253 / 60
8/9
103-127 / 60
9
90 ... 110 / 60
9
cm
cm
liters
cm
kg
EH-5
15x15
15
3 ... 4.5
17x33x36
7.0
EH-13
18x30
15
8 ... 13
39x33x37
8.0
EH-19
36x30
15
14 ... 19
57x33x37
11.0
EH
Open Bath Circulators
Bath opening (WxL)
Bath depth
Filling volume from ... to
Overall dimensions (WxDxH)
Weight
EH-27
36x30
20
21 ... 27
57x37x42
13.0
cm
cm
liters
cm
kg
EH-33
67x30
15
24 ... 33
91x33x38
20.0
EH-39
36x30
30
33 ... 39
54x34x52
19.0
IP21
Overvoltage category
Pollution degree
II
2
Caution:
The unit is not for use in explosive atmosphere
Standards for interference resistance according to EN 61326-1
This unit is an ISM device classified in Group 1 (using high frequency for internal purposes)
Class A (industrial and commercial range).
Operating instructions
Operating instructions
3.
3.1.
3.2.
3.3.
Safety recommendations
Follow the safety recommendations to prevent damage to persons or property. Further, the
valid safety instructions for working places must be followed.
10
Only connect the unit to a power socket with an earthing contact (PE
protective earth)!
The power supply plug serves as a safe disconnecting device from the line
and must always be easily accessible.
Place the unit on an even surface on a base made of nonflammable
EH
material.
Do not stay in the area below the unit.
Make sure you read and understand all instructions and safety precautions
listed in this manual before installing or operating your unit.
Never operate the unit without bath fluid in the bath.
Set the excess temperature safety installation at least 25 C below the fire
point of the bath fluid.
Do not drain the bath fluid while it is hot!
Check the temperature of the bath fluid prior to draining (e.g., by switching
the unit on for a short moment).
Pay attention to the thermal expansion of bath oil during heating to avoid
overflowing of the fluid.
Prevent water from entering the hot bath oil.
Use suitable connecting tubing.
Make sure that the tubing is securely attached.
Avoid sharp bends in the tubing, and maintain a sufficient distance from
surrounding walls.
Regularly check the tubing for material defects (e.g., for cracks).
Never operate damaged or leaking units.
Always turn off the unit and disconnect the mains cable from the power
source before performing any service or maintenance procedures, or before
moving the unit.
Always turn off the unit and disconnect the mains cable from the power
source before cleaning the unit.
Always empty the bath before moving the unit.
Transport the unit with care.
Sudden jolts or drops may cause damage in the interior of the unit.
Observe all warning labels.
Never remove warning labels.
Never operate units with damaged mains power cables.
Repairs are to be carried out only by qualified service personnel.
Some parts of the bath cover and the pump connections may become
extremely warm during continuous operation. Therefore, exercise particular
caution when touching these parts.
11
Notice:
Check the safety installations at least twice a year!
Excess temperature protection according to IEC 61010-2-010.
With a screwdriver turn back the adjustable excess temperature protection
until the shut-down point (actual temperature).
Caution:
The temperature controlling i.e. of fluids in a reactor constitutes normal circulator
practice.
We do not know which substances are contained within these vessels.
Many substances are:
inflammable, easily ignited or explosive
hazardous to health
environmentally unsafe
i.e.: dangerous
The user alone is responsible for the handling of these substances!
The following questions shall help to recognize possible dangers and to reduce
the risks to a minimum.
Are all tubes and electrical cables connected and installed?
Note:
sharp edges, hot surfaces in operation, moving machine parts, etc.
Do dangerous steams or gases arise when heating?
Is an exhaust needed when working?
What to do when a dangerous substance was spilled on or in the unit?
Before starting to work, obtain information concerning the substance and
determine the method of decontamination.
12
EH
4.
Front view
Rear view
Edit keys
Setpoint increase or decrease
Press keys shortly for step-by-step changes,
Keep the keys pressed for fast change of setpoint
OK key (store)
120
160
10
11
15
A
M
P
13
Preparations
5.
5.1.
Preparations
Installation
Top view
A
B
14
EH-5
The circulator (A) mounted on a stainless steel bridge is
placed on the back of bath tank.
Close the bath tank with the bath cover (B).
EH
5.2.
Bath fluids
Caution:
Carefully read the safety data sheet of the bath fluid used, particularly with
regard to the fire point!
If a bath fluid with a fire point of 65 C is used, only supervised operation is
possible.
Water:
The quality of water depends on local conditions.
Due to the high concentration of lime, hard water is not suitable for
temperature control because it leads to calcification in the bath.
Ferrous water can cause corrosion - even on stainless steel.
Chloric water can cause pitting corrosion.
Distilled and deionized water is unsuitable. Their special properties cause
corrosion in the bath, even in stainless steel.
Recommended bath fluids:
Bath fluid
soft/decalcified water
JULABO
Description
Order Number
Temperature range
Flash point
Fire point
Color
10 liters
5 liters
C
C
C
Temperature range
5 C to 80 C
Thermal
H10
8 940 114
8 940 115
-20 ... 180
190
216
clear
15
Preparations
Caution:
Fire or other dangers when using bath fluids that are not recommended:
Please contact JULABO before using other than recommended bath fluids.
Use only nonacidic and noncorrosive bath fluids.
JULABO assumes no liability for damage caused by the selection of an
unsuitable bath liquid.
Unsuitable bath fluids are fluids which, e.g.,
are highly viscous
(much higher than 30 mm2 x s-1 at the respective working temperature)
have a low viscosity and have creep characteristics
have corrosive characteristics or
tend to crack.
No liability for use of other bath fluids!
16
EH
5.3.
Filling / Draining
Notice:
Pay attention to the thermal expansion of bath oil during heating to avoid
overflowing of the liquid.
Do not drain the bath fluid while it is hot!
Check the temperature of the bath fluid prior to draining (by switching the
unit on for a short moment, for example).
Store and dispose the used bath fluid according to the laws for
environmental protection.
Filling
Take care that no liquid enters the interior of the circulator.
Recommended maximum filling level with water as bath fluid:
20 mm below the tank rim
Recommended maximum filling level with bath oils:
30 mm below the tank rim
After filling, immerse the samples in the bath or place the lid on
the bath, in case the opening is not to be used.
Draining
Press the mains switch to turn the circulator off.
Remove the circulator from the bath tank.
Empty the bath tank.
17
Preparations
5.4.
If the circulator is operated without external system, close the pump connector
(14a) with the cap nut.
The circulator is used for temperature application to external,
closed systems (loop circuit).
The circulator is used for temperature application to external, closed
systems (loop circuit) with simultaneous temperature application in
the circulator bath.
EH-5
14a
14b
EH-13 / EH-19 / EH-27 / EH-33 / EH-39
5.4.1. Tubing
Recommended tubing:
Order No.
Length
Temperature range
8 930 008 1 m
CR tubing
8 mm inner dia.
-20 C to 120 C
8 930 010 1 m
CR tubing
10 mm inner dia.
-20 C to 120 C
8 930 108 1 m
Viton tubing
8 mm inner dia.
-50 C to 200 C
8 930 110 1 m
Viton tubing
10 mm inner dia.
-50 C to 200 C
8 930 410 1 m
Insulation for tubing
8 mm or
-50 C to 100 C
10 mm inner dia.
8970480
2 Tubing clamps, size 1 for tubing 8 mm ID
8970481
2 Tubing clamps, size 2 for tubing 10 or 12 mm ID
EH
Warning:
Tubing:
At high working temperatures the tubing used for temperature application and
cooling water supply represents a danger source.
A damaged tubing line may cause hot bath fluid to be pumped out within a short
time.
This may result in:
Burning of skin
Difficulties in breathing due to hot atmosphere
Safety recommendations
Employ suitable connecting tubing.
Make sure that the tubing is securely attached.
Avoid sharp bends in the tubing, and maintain a sufficient distance from
surrounding walls.
Regularly check the tubing for material defects (e.g. for cracks).
Preventive maintenance: Replace the tubing from time to time.
5.5.
A
B
intern 100 %
intern 20 %
extern 80 %
D
Examples:
Internal applications in the bath
A 100 % internal bath circulation (for large bath tanks)
B Reduced internal bath circulation
(for smooth surface of bath fluid)
External/internal applications
C 40 % external discharge,
60 % internal circulation
(for large bath tanks)
D 80 % external discharge,
20 % internal circulation
(for small bath tanks)
19
Preparations
5.6.
Countercooling
Notice:
Securely attach all tubing to prevent slipping.
Observe the laws and regulations of the water distribution company valid in the
location where the unit is operated.
For applications near the ambient temperature, the cooling coil
must be connected to the water mains.
Using tubing, connect the cooling coil (25a) to the tap water
supply, and lead the tap water in a sink through the return
connector (25b).
25a
A specific water flow rate of 45 ml/minute is sufficient
25b
to compensate for the characteristic temperature.
15
A
M
P
15
A
M
P
Cooling coil
EH-5
25a
25b
NOTE: Immersion coolers are used for countercooling instead of tap water in
applications below room temperature.
Order No.
Description
9 650 820
FT200
9 650 840
FT400
8 970 400
Clamp for cooler probe for stainless steel or
plexiglass bath tanks
NOTE:
Flow-through cooler
Order No.
Description
9 655 825
FD200
The FD200 is suitable as cooling device for liquids in closed circuits (loops).
This unit is integrated in the return flow circuit from the external system
connected to a circulator, and continuously withdraws heat from the liquid.
20
EH
6.
6.1.
Operating procedures
Power connection
Caution:
Only connect the unit to a power socket with earthing contact (PE
protective earth)!
The power supply plug serves as safe disconnecting device from the line and
must be always easily accessible.
Never operate equipment with damaged mains power cables.
Regularly check the mains power cables for material defects (e.g. for cracks).
We disclaim all liability for damage caused by incorrect line voltages!
Check to make sure that the line voltage matches the supply voltage
specified on the identification plate.
6.2.
Press the
21
Operating procedures
6.3.
key and
AUTOSTART on.
AUTOSTART off.
NOTE:
The circulator has been configured and supplied by JULABO
according to N.A.M.U.R. recommendations. This means for the start
mode, that the unit must enter a safe operating state after a power
failure (non-automatic start mode). This safe operating state is
indicated by OFF on the LED temperature display. A complete
shutdown of the main functional elements such as heater and
circulating pump is effected simultaneously.
Should such a safety standard not be required, the AUTOSTART
function (automatic start mode) may be activated, thus allowing the
start of the circulator directly by pressing the mains power switch or
using a timer.
Warning:
For supervised or unsupervised operation with the AUTOSTART function, avoid
any hazardous situation to persons or property.
The circulator does no longer conform to N.A.M.U.R. recommendations.
Please make sure that all safety devices of the unit have been set properly.
6.4.
Factory setting:
25C
Press
to set a lower value.
Keep the keys depressed for the value to change fast.
3. Press the
22
EH
6.5.
Working temperature
range refer to page 8
1-point calibration:
The temperature sensor can be calibrated at any value within
the working temperature range.
Set the high temperature cut-off / safety temperature to a
value above the desired adjustment value (Example: 80 C).
80
40
120
160
48.87
Press
to set a lower value.
Keep the keys depressed for the value to change fast.
Press the
Notice:
If the determined value is bigger than the tolerance limit of
5 C, the value is ignored for the input!
Error message: -Err
23
Operating procedures
6.6.
Timer function
With the timer function the operating time can be limited to an
allowed time.
2.
Max. time:
Activate key
to set a lower value .
Activate the key shortly for single step, hold the key pressed for
quick enumeration.
33 h 19 min.
3.
key .
shortly.
Timer operation
24
EH
6.7.
Check the safety installations at least twice a year! See page 12.
6.7.1. Excess temperature protection
Warning:
The excess temperature protection should be set at least 25 C below the fire
point of the bath fluid used.
In the event of wrong setting there is a fire hazard!
We disclaim all liability for damage caused by wrong settings!
This safety installation is independent of the control circuit. When the
temperature of the bath fluid has reached the safety temperature, a
complete shutdown of the heater and pump is effected.
The alarm is indicated by optical and audible signals (continuous
tone) and on the LED-DISPLAY appears the error message "Error
14".
Setting range:
0 C to 170 C
Recommendation:
Set the excess temperature protector at 5 to 10 C above the
working temperature setpoint.
Turn off the unit with the mains switch, refill bath fluid and turn
the unit on again!
Warning:
For refill always use the same bath fluid type that is already in the bath.
Bath oils must not contain any water contaminants! Explosion hazard at higher
temperatures!
Recommendation:
Refill bath oils only at a bath temperature below 70 C!
25
7.
After eliminating the malfunction, press the mains power switch off and
on again to cancel the alarm state.
If the unit cannot be returned to operation, contact an authorized
JULABO service station.
26
EH
Disturbances that are not indicated.
The electronic pump motor is overload-protected by an electronic current
limiter. If viscosity of the bath fluid is or becomes too high, the motor
stops running.
15
A
M
P
8.
Electrical connections
Notice:
Use shielded cables only.
The shield of the connecting cable is electrically connected to the plug housing.
/ Control output
The connector may be used for control of JULABO refrigerated
circulators or as output for alarm messages.
4
1
Circuit:
Operation
Alarm
= relay powered
= relay not powered
Pin assignment:
Pin
Signal
1
+24 V (I max. current 25 mA)
2
0V
3
Alarm relay
4
Reserved - do not use!
5
Reserved - do not use!
27
9.
Cleaning
For cleaning the bath tank and the immersed parts of the circulator,
use low surface tension water (e.g., soap suds).
Clean the outside of the unit using a wet cloth and low surface
tension water.
The circulator is designed for continuous operation under normal
conditions. Periodic maintenance is not required.
The tank should be filled only with a bath fluid recommended by
JULABO. To avoid contamination, it is essential to change the bath
fluid from time to time.
Repairs
Before asking for a service technician or returning a JULABO
instrument for repair, please contact an authorized JULABO
service station.
28