Fluids and Proppants Selection Qa&Qc in Hydraulic Fracturing
Fluids and Proppants Selection Qa&Qc in Hydraulic Fracturing
Fluids and Proppants Selection Qa&Qc in Hydraulic Fracturing
SELECTION
QA&QC IN HYDRAULIC FRACTURING
ALBERTO MENDOZA ROJAS
ECOPETROL S.A.-ICP
CONTENT
FLUIDS
AND
SELECTION
PROPPANTS
QA&QC IN FIELD
PROBLEMS FOUNDS IN FIELD
Flitrate controller
GEL STABILITY
Fresh Gel
GEL BREAKING
INTERFACIAL TENSION
SISTEMA
Brine A-Crude oil
Brine B-Crude oil
FF A-Crude oil
FF B- Crude oil
Organic Treatment A-FW
Organic Treatment B-FW
IT (Dinas/cm)
32.8
0.71
4.76
1.12
32.17
0.95
10
Gel stability/BREAKING
Gel stability/BREAKING
Regain Permeability
Prepare and Restore plugs
Prepare fluids and fracturing fluid
Set P & T
Measure brine Ke
Measure oil Ke
Measure brine Ke
Inject organic treatment
Inject Fracturing fluid (eventually static leak-off test)
Shut in for x hs.
Measure brine Ke
Measure oil Ke
Regain Permeability
FF-1
FF-2
FF-1
14
PROPPANTS
Hexion: Ceramax I, E, SB Excel.
Carboceramics: CarboLite, Carboprop, Econoprop,
Hydroprop.
Santrol: Resin Coated sands:
9 Curables and Tempered
9 Sand: Jordan & Ottawa types.
Saint Gobain: Bauxitas:
9 Versaprop, Econoprop, Valuprop, Interprop.
National sands
BHCP(psi)
H (ft)
Yarigui
Cantagallo
Llanito
Cardales
Piedemonte
Acae
Loro
Casabe
Sardinata
Bonanza
Lisama
Orito
Gala
Santa Clara
PG
4060-6654
2980
4800-8500
5600-7237
6760-9750 / 10650-13392
7400
5800
2200-2500
8500
1450-2045
4593
6500
7300-7880
1800
4050-5050
5500
5770
6900-7800
8070-8132
13700-17200
10500
10500
3500
5352
2400-2600
4200
5050-7600
7300-7800
2500-2670
6000-6500
Proppant Tests
Sieve test
Mnimum 90% of tested sample: Between
designed sieves sizes.
Not over 0.1 % total sample larger than the first
sieve.
Not over 1% smaller than the last sieve.
20/40: 16, 20, 30, 35, 40, 50.
GOOD
BAD
Crushing Test
Sieve test
Crushing:
Stress: 7500-10000-12500-15000 psi
Sieve test
Sieve
16/20
20/40
Fines Max.
(Wt %)
25
10
Proppant Flowback
Prepare Fluid and mix with proppant
Break the fluid
Drain excess of fluid.
Pack rubber slevee and install endcaps.
Confine the system
Displace fluids at increasing flow rates
Measure proppant recovered
PC
Oven
Proppant core
Confining P
Pump
CONSOLIDATION : at 5 Days
4500 psi - 120 oC
CONDITIONS
Proppant CONSOLIDATION
Fluid
Propant: 6 ppg
Resin: 3 y 6 gpt
Confine at P & T
T: 6 & 12 h
Resin
Concentratin
Cure time
(hrs)
Overburden
(kN)
Stress resistance
(psi)
3 gpt
0.50
13.8
3 gpt
12
0.37
10.1
5 gpt
0.36
9.94
5 gpt
12
0.37
10.1
pH Effect
QA&QC In Field
QA&QC in Field
Equipments
Cleanness
Materials
Inventory
Storage
Additive Quality control
Proppant size
QA&QC In Field
Fluids
> Water:
Suspended slids, bacterias
Turbidity, Fe++, pH, Conductivity
> Gel
Disolucition
Viscosity (Fann 35A)
Breaking
Compatibility
Wetabbility: Formation sand.
QA&QC in Field
During Pumping
Fluid Formation
Fluid Density (In lab)
Eyefishes Presence.
SOME PROBLEMS
PROBLEMS
PROBLEMS
PROBLEMS
Brines with high
suspend solids,
iron and crude
oil content.
PROBLEMS
Filtration
PROBLEMS
Wrong Additives dosification
Wrong materials storage
PROBLEMS
Poor polymer hydration: Fisheyes
PROBLEMS
BACTERIAS
Anaerobios totales
Biota total aerobia
Microorganismos Gram (-)
MUESTRA
8139-1
8139-2
Pseudomonas
Recuento de
Recuento de
Recuento de
Aislamiento de
microorganismos microorganismos microorganismos
Hongos
Bacterias/mL
Bacterias/mL
Bacterias/mL
Bacterias
BSR
Agar Malta
Productoras de Caldo Tioglicolato
cido
1
108
107
Negativo
10 (parcial)
6
9
9
10
10
Negativo
10 (parcial)
PROBLEMS
PROBLEMS
CRUSHING
PROBLEMS
Dirty pipes