2 1 Extrusion
2 1 Extrusion
2 1 Extrusion
SPRING 2015
VI Semester BE (Chemical Engineering Plastics)
EXTRUSION INTRODUCTION
Extruders are the heart of polymer processing industry.
Extrude means to push or to force out. (eg., toothpaste is squeezed out of a tube, it
is extruded).
The part of the machine containing the opening through which the material is
forced is referred to as extruder die.
As the material passes through the die, the material acquires the shape of the die
and the extruded product is referred to as extrudate.
Materials can be extruded in the molten state or in the solid state.
Generally, polymers are extruded in the molten state, but in some applications
involve solid state extrusion of polymers.
If the polymer is fed to the extruder in the solid state and the material is melted as
it is conveyed by the extruder screw from the feed port to die is called plasticating
extrusion. In this case, it performs additional function namely melting besides
regular extrusion function.
Extruder is fed with molten polymer and called melt fed extrusion and it purely
acts as a pump developing the necessary pressure to force the polymer melt
through the die.
EXTRUSION HISTORY
First machine for extrusion of thermoplastic materials was built around 1935 by
Paul Troester in Germany.
After 1935, extruders evolved to electrically heated screw extruders.
Around this time, the basic principle of intermeshing co-rotating twin screw
extruder was developed by Roberto Colombo.
Then, Pasquetti developed a different concept of intermeshing counter-rotating
twin screw extruder.
TYPES OF EXTRUDER
In polymer industry, extruders come in many different designs.
Main difference between various extruders is their mode of operation; continuous or
discontinuous.
Continuous extruder are capable of developing steady, continuous flow of material. It
utilizes a rotating member for transport of material.
The batch type or discontinuous extruder operates in a cyclic fashion and it generally have
a reciprocating member for the transport of material.
CLASSIFICATION OF POLYMER EXTRUDERS
Screw Extruder (Continuous)
Single screw extruder Melt fed or plasticating, single stage or Multi stage.
Multi screw extruder Twin screw extruder, Gear pump.
Disk or Drum Extruder (Continuous)
Viscous drag type extruder Spiral disk, drum, diskpack and stepped disk extru.
Elastic melt extruder Screwless extruder and screw/disk extruder
Reciprocating Extruder (Discontinuous)
Ram extruder melt fed and plasticating extruder
Reciprocating screw extruder plasticating unit in molding m/cs and
compounding extruder
BASIC OPERATION
Material enters from the feed hopper by gravity down into the extruder barrel. Some
materials will not flow easily in dry form and special care have to be taken to prevent
bridging of the material in the feed hopper.
In the barrel, it is situated in the annular space between the extruder screw and barrel
where the barrel is stationery and the screw is rotating. As a result, frictional forces will
act on the material. These frictional forces are responsible for the forward transport of
the material, atleast as long as the material is in the solid state.
As the material moves forward, it will heat up as a result of frictional heat generation
and heat conduction from barrel heaters.
The depth of the screw channel is reduced along the length of the screw so as to
compact the material.
Temp. of the mtl. exceeds the melting point, a melt film will be form at the barrel
surface where the plasticating zone starts.
As the material moves forward, the amount of solid mtl. at each location will reduce as
a result of melting. When all solid polymers disappeared, the end of plasticating zone
has been reached.
Next, in melt conveying zone, the polymer melt is simply pumped to the die to produce
an extrudate of the desired cross-sectional shape.
BASIC OPERATION
Since the die exerts a resistance to flow, a pressure is required to force the material
through the die. It is termed as die head pressure.
The die head pressure is determined by the shape of the die, the temp. of the polymer
melt, flow rate through the die and the rheological properties of the polymer melt.
The pressure build-up which occurs along a screw
The lengths of the zones on a particular screw depend on the material to be extruded.
With nylon, for example, melting takes place quickly so the compression of the melt
can be performed in one pitch of the screw.
PVC on the other hand is very heat sensitive and so a compression zone which covers
the whole length of the screw is preferred.
VENTED EXTRUDER
Some extruders also have a venting zone.
Some plastics are hygroscopic in nature - they absorb moisture from the atmosphere, hence
vented extruders are necessary.
If these materials are extruded wet in conventional equipment the quality of the output is not
good due to trapped water vapour in the melt.
Vented barrels were developed to overcome these problems.
In the first part of the screw, the granules are taken in and melted, compressed and homogenised
in the usual way.
The melt pressure is then reduced to atmospheric pressure in the decompression zone.
This allows the volatiles to escape from the melt through a special port in the barrel.
The melt is then conveyed along the barrel to a second compression zone which prevents air
pockets from being trapped.
DISKPACK EXTRUDER
These type of extruders do not utilize an screw for transport of the material.
These are referred to as screwless extruders.
These m/cs employ some kind of disk or drum to extrude the material.
Material drops in the axial gap b/w relatively thin disks mounted on a rotating shaft.
The mtl. will move with the disk almost a full turn, then it meets the channel block.
The channel block deflects the polymer flow to either an outlet channel or to transfer channel in
the barrel.
DRUM EXTRUDER
Mtl. Is fed by a feed hopper into an annular space b/w rotor & barrel.
By the rotation of the rotor, the mtl. Is carried along the circumference of the barrel.
Before the mtl. Reaches the hopper, it encounters a wiper bar, this deflects the polymer flow into
a channel that leads to the extruder die.
RAM EXTRUDER
Ram or plunger extruders are simple in design & discontinuous in their mode of operation.
They are able to generate very high pressures.
Limitations for switch to reciprocating screw extruders are: limited melting capacity, poor temp
uniformity of polymer melt.
Used in relatively small shot size molding machines and outstanding pressure generation
capability is needed.
Two types of ram extruders are: Single ram and Multi Ram.
SINGLE and MULTI RAM EXTRUDER
It is used in small general purpose molding m/c but also in some special polymer processing
operations such as Ultrahigh molecular weight polyethylene & polytetrafluoroethylene (PTFE).
These polymers are not considered to be melt processable on conventional melt processing
equipment.
Ram are used to mold UHMWPE under very high pressure. The m/c uses a reciprocating plunger
that densifies the cold incoming mtl with a pressure upto 300 Mpa.
The mtl is forced to heated channels into the heated cylinder where final melting takes place.
The mtl is then injected into the mold by injection ram.
Another application is the extrusion of PTFE material with very high pressure is required.
The main disadvantage are discontinuous o/p. Hence multi ram extruder are developed.
RAM EXTRUDER
In this type, the two rams discharge mtl into a common barrel in which plasticating shaft is
rotated.
The m/c is able to extrude but the throughput uniformity is poor.
EXTRUDER DRIVES
Extruder drives are used to turn the extruder screw at the desired speed.
It should be able to maintain a constant screw speed because fluctuations in screw speed will
result in throughput fluctuations which in turn cause fluctuations in the dimensions of the
extrudate.
The drive also able to supply the required amount of torque to the shank of the extruder.
Another requirement is the ability to vary the speed over a relatively wide range from almost
zero to maximum screw speed.
Main drive systems employed on extruders are: AC motor drive system, DC motor drive system
and hydraulic drives.
AC motor drive system used on extruders are adjustable transmission ratio drive and adjustable
frequency drive.
Adjustable transmission ratio drive can be either mechanical adjustable speed drive using belt or
chain drives or electric friction clutch drive.
Adjustable frequency drive uses an AC squirrel cage induction motor connected to a solid state
power supply capable of providing an adjustable frequency to the AC motor.
DC motor drive uses fixed AC motors to drive DC generators that produce the variable voltage
for the DC motor.
Hydraulic drive generally consists of a constant speed AC motor driving a hydraulic pump
which in turn drives hydraulic motor and associated controls.
EXTRUDER SCREW
Extruder screw is the heart of the machine.
The rotation of the screw causes forward transport, contributes to a large extent to the heating of
the polymer, and causes homogenization of the material.
Simply, Screw is a cylindrical rod of varying diameter with a helical flights wrapped around it.
The outside diameter of the screw is constant on most extruders.
Clearance between screw and barrel is usually small, generally the ratio of radial clearance to
screw diameter is around 0.001.
Common screw material is 4140 steel, which is medium carbon and relatively low cost. Some of
other materials are Low carbon steel, Stainless steel, Tool steel, Nickel base and hardfacing
material (stellite).
MODIFICATIONS OF SCREW
Standard screw with additional flight in feed section: Forces acting on the screw are
balanced, thus screw deflection is less likely to occur.
To smooth out the pressure fluctuations caused by the flight interrupting the inflow of material
from feed hopper every revolution of the screw.
Negative side is reduces the cross sectional area thus solid conveying rate will be reduced.
Variable pitch extruder with increasing pitch: Pitch increases with axial distance of the
screw.
The varying pitch allows the use of locally optimum helix angle, ie. Helix angle for solid
conveying and helix angle for melt conveying.
Used for high sensitive material. As well as power consumption is reduced by increasing the
helix angle.
Negative side is deflection of screw is more.
MODIFICATIONS OF SCREW
Variable pitch screw with reducing pitch: Pitch decreased with axial distance.
It causes a lateral compression of the material in the screw channel, so normal compression in
the screw is eliminated.
Same channel depth throughout the entire length of the screw.
Negative side is reducing the helix angle, so increases the power consumption.
It works on high clearance b/w flight and barrel, hence it reduces the melting capacity.
Zero meter screw: Used to reduce the temp. build up in the material.
Disadvantage is pressure generating capability of the screw will be affected. (not a major
concern in the injection molding)
It is more appropriate for an injection molding machine.
MODIFICATIONS OF SCREW
Zero feed Zero meter screw: It consists of only a compression section.
Hence gradual compression of the material takes place.
Used especially for Nylon processing.
It also reduces air entrapment, pressure and output fluctuations and improved extrudate quality.
Rapid compression screw: Length of compression zone is generally less than 1D in these
screws.
Unfortunately, it is referred to as Nylon screw.
This is a major misconception in screw design and the success of zero feed zero meter with
nylon should make that quite clear.
Nylon has a narrow melting range and relatively low viscosity.
MODIFICATIONS OF SCREW
Decompression screw: Final portion of screw has a deep channel section following a
decompression section.
Channel depth is constant over the last screw section.
Effective power reduction can be obtained by changing the channel depth, helix angle, flight
width and radial clearance.
Negative side is pressure generating capability will reduce.
MODIFICATIONS OF SCREW
Multi-flighted screw: Increase the melting performance.
Reduce the screw deflection.
Adversely affects the solid conveying and melt conveying rate, so multiple flights to be
incorporated only a particular section of the screw.
Negative side is power consumption is more.
EXTRUDER DIE
The flow of polymer melt through the die requires knowledge of the viscoelastic behavior of the
polymer melt.
Polymer melt can no longer be considered a purely viscous fluid because elastic effects in the
die region are very important.
The objective of the extrusion die is to distribute the polymer melt in the flow channel such that
the material exists from the die with a uniform velocity.
The actual distribution will be determined by the flow properties of the polymer, flow channel
geometry, flow rate through the die, and the temp field in the die.
Flow channel geometry is optimized for one polymer under one set of conditions, a simple
change in flow rate or in temp can make the geometry non-optimum.
For this reason, adjustment capabilities into the die are generally incorporated by which the
distribution can be changed externally while the extruder is running.
The flow distribution is generally changed in two ways: by changing the flow channel geometry
by means of choker bars, restrictor bars, valves etc., and by changing the die temp.
In die design, problems often occur because the product designer has little or no appreciation for
the implications of product design on the ease or difficulty of extrusion.
Small changes in design can drastically improve the extrudability of the product.
EXTRUDER DIE
Basic guidelines in profile design to minimize extrusion problems are:
Use internal and external radii on all corners
Maintain uniform wall thickness
Avoid very thick walls
Minimize the use of hollow sections
The extrusion dies will be divided into Film & sheet dies, pipe and tubing dies, blown film dies,
profile dies and coextrusion die.
Design of the extrusion head, regardless of its purpose, should take into account the following
general requirements:
Ensuring proper polymer flow in the flow channels so as to obtain required shape and
dimensions of the extrudate,.
Preventing polymer stagnation areas in the extrusion head by ensuring proper shape and
geometric characteristics of the flow channels and ensuring adequate polymer flow resistance,
Ensuring adequate strength of specific design elements of the extrusion head and their
connections in high pressure and temperature conditions,
Protecting surfaces of the flow channels against aggressive impact of some polymers,
Providing the possibility of adjustment of polymer flow rate from the extrusion head die.
Considering the polymer flow direction with regard to the axis of the extrusion head main body,
the types of extrusion heads are: longitudinal, angular, transverse and spiral extrusion heads. The
spiral extrusion heads can be made as longitudinal as well as transverse ones.
EXTRUSION TROUBLESHOOTING
.
Problems
Possible Causes
Surging
Bubbles
Bubbles uniformly
distributed through
extrudate
Melt fracture
Rough surface
Incompatible additive
Die land too long
Melt temperature too low
EXTRUSION TROUBLESHOOTING
.
Problems
Possible Causes
Flow lines
Bridging in feed
zone
Screw overheated
Rear zone temperature too high
Screw speed too low
Poor shut down procedure
Hopper dryer temperature too high
Extruder surging
Takeoff variable
Temperature control inadequate
High moisture content
Carbon specks
Dirty equipment
Improper resin handling
Extruder run dry at shut down and not cooled
Problems
Possible Causes
Tube is sagging
between die and
cooling trough
Tubing is out of
round
Blocking
Problems
Possible Causes
Poor gloss or
transparency
Increase cooling
Blocking