M 03
M 03
M 03
Method 1.
1.1 Analytes.
Analyte CAS No. Sensitivity
Oxygen (O2) 7782-44-7 2,000 ppmv
Nitrogen (N2) 7727-37-9 N/A
Carbon dioxide (CO2) 124-38-9 2,000 ppmv
Carbon monoxide (CO) 630-08-0 N/A
analysis.
4.0 Interferences.
314
5.0 Safety.
all components of the gas stream, may be used for the probe.
will not remove O2, CO2, CO, and N2, to remove excess
flow rate.
Install a small surge tank between the pump and rate meter
is suggested.
train leak-check.
analyzer.
14 to 18 percent CO2.
Transport.
by the Administrator.
the outlet at the quick disconnect, and then turning off the
Next, connect the bag, and make sure that all connections
are tight.
with, and for the same total length of time as, the
Figure 3-3.
321
Quality Control
Section Measure Effect
8.2 Use of Fyrite to Ensures the accurate
confirm Orsat results. measurement of CO2 and
O2.
10.1 Periodic audit of Ensures that the
analyzer and operator analyzer is operating
technique. properly and that the
operator performs the
sampling procedure
correctly and
accurately.
11.3 Replicable analyses of Minimizes experimental
integrated samples. error.
manufacturers specifications.
Section 10.1.
minutes.
4-minute interval.
12.1 Nomenclature.
(lb/lb-mole).
100.
100 percent.
16.0 References.
326
15219. 1951.
Filter
(Glass Wool)
Flexible Tubing To Analyzer
Probe
Squeeze Bulb
Rate Meter
Surge
Filter Tank
Valve
(Glass Wool)
Probe
Quick
Disconnect
Air-Tight
Pump
Air-Cooled
Condenser
Bag
Average
a
%Dev. = [(Q - Qavg)/Qavg] x 100 (Must be < + 10 %)