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Requirements for Bituminous Material

(Grade 60-70)
Penetration Grade
Test 60-70 Designation Sampling and Testing Frequency
Min Max
Specific gravity - - AASHTO T-228 2 per Shipment

3 per week of plant operation. Samples


Penetration at 25ºC (77ºF) 100 g.. 5 s 60 70 AASHTO T-49 taken from heating tank at staggered
intervals.

Flash point. Cleveland Open Cup ºC (ºF) 232 (450) - AASHTO T-48
Ductility at 25 ºC (77ºF) 5 cm per min. cm 100 - AASHTO T-51
Solubility in trichloroethylene percent 99 - AASHTO T-44
Thin-film oven test. 3.2 mm (1/8 in.) 163ºC (325ºF)
5 hour
Loss on heating. percent - 0.8 AASHTO T-179
Penetration. of residue. percent of original 54 - AASHTO T-49
Ductility of residue at 25 ºC (77ºF) 5 cm per min. cm 50 - AASHTO T-51
Spot test ( when and as specified ( see Note1) with):
Standard naphtha solvent
Naphtha-xylene solvent. percent xylene Negative for all grades AASHTO T-102
Heptane-xylene solvent. percent xylene
Note - The use of the spot test is optional. When it is specified. The Engineer shall indicate whether the standard naphtha solvent. The naptha-xylene solvent.
Or the heptane-xylene solvent will be used in determining compliance with the requirement. And also. in the case of the xylene solvents. the percentage of
xylene to be used.

Ref. AASHTO M20-70

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Requirements for Prime Coat
Cationic Emulsified Bitumen (CSS-1)
Slow-Setting
Test CSS-1 Designation Sampling and Testing Frequency
Min Max
Test on emulsions:
Viscosity, Saybolt Furol at 25ºC (77ºF). s 20 100 AASHTO T-59
Viscosity, Saybolt Furol at 50ºC (122ºF). s - - AASHTO T-59
b
Storage stability test, 24 h. percent - 1 AASHTO T-59
Demulsibility. 35 mL 0.8 percent
Sodium dioctyl sufosucinate. percent - - AASHTO T-59
Coating, ability and water resistance:
Coating, dry aggregate - - -
Coating, after spraying - - -
Coating, wet aggregate - - -
Coating, after spraying - - -
Particle charge test Positive AASHTO T-59
Sieve test, percent - 0.10b AASHTO T-59
Cement mixing test, percent - 2.0 AASHTO T-59
Distillation:
Oil distillate, by volume of emulsion percent - - AASHTO T-59
Residue, percent 57 - AASHTO T-59
Test on residue from distillation test:
Specific gravity - - AASHTO T-228 2 per Shipment
3 per week of plant operation. Samples
Penetration at 25ºC (77ºF) 100 g. 5 s 100 250 AASHTO T-49 taken from heating tank at staggered
intervals.
Ductility, 25 ºC (77ºF) 50 mm/min. mm 40 - AASHTO T-51
Solubility in trichlorethylene, percent 97.5 - AASHTO T-44
b
This test requirement on representative samples may be waived, if successful application of the material has been achieved in the field.

Ref. AASHTO M208-96

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Requirements for Tack Coat
Cationic Emulsified Bitumen (CRS-2)
Rapid-Setting
Test CRS-2 Designation Sampling and Testing Frequency
Min Max
Test on emulsions:
Viscosity, Saybolt Furol at 25ºC (77ºF). s - - AASHTO T-59
Viscosity, Saybolt Furol at 50ºC (122ºF). s 100 400 AASHTO T-59
b
Storage stability test, 24 h. percent - 1 AASHTO T-59
Demulsibility. 35 mL 0.8 percent
Sodium dioctyl sufosucinate. percent 40 - AASHTO T-59
Coating, ability and water resistance:
Coating, dry aggregate - - -
Coating, after spraying - - -
Coating, wet aggregate - - -
Coating, after spraying - - -
Particle charge test Positive AASHTO T-59
Sieve test, percent - 0.10b AASHTO T-59
Cement mixing test, percent - - AASHTO T-59
Distillation:
Oil distillate, by volume of emulsion percent - 3 AASHTO T-59
Residue, percent 65 - AASHTO T-59
Test on residue from distillation test:
Specific gravity - - AASHTO T-228 2 per Shipment
3 per week of plant operation. Samples
Penetration at 25ºC (77ºF) 100 g. 5 s 100 250 AASHTO T-49 taken from heating tank at staggered
intervals.
Ductility, 25 ºC (77ºF) 50 mm/min. mm 40 - AASHTO T-51
Solubility in trichlorethylene, percent 97.5 - AASHTO T-44
b
This test requirement on representative samples may be waived, if successful application of the material has been achieved in the field.

Ref. AASHTO M208-96

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