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    Analysis of Acquatic Vegetation

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    Frank
    The document analyzes aquatic vegetation samples of chlorella and sargassum using an ICPE-9000 instrument. It describes the sample preparation process, analytical conditions, and provides a table with the quantitative results of various elements in the samples as well as figures showing the spectral profiles. The results obtained from the ICPE-9000 analysis agree well with the certified values for most elements in the samples.

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    Analysis of Acquatic Vegetation

    Uploaded by

    Frank
    25 views3 pages
    The document analyzes aquatic vegetation samples of chlorella and sargassum using an ICPE-9000 instrument. It describes the sample preparation process, analytical conditions, and provides a table with the quantitative results of various elements in the samples as well as figures showing the spectral profiles. The results obtained from the ICPE-9000 analysis agree well with the certified values for most elements in the samples.

    Original Description:

    Analysis of seaweed by ICP-OES

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    The document analyzes aquatic vegetation samples of chlorella and sargassum using an ICPE-9000 instrument. It describes the sample preparation process, analytical conditions, and provides a table with the quantitative results of various elements in the samples as well as figures showing the spectral profiles. The results obtained from the ICPE-9000 analysis agree well with the certified values for most elements in the samples.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    25 views3 pages

    Analysis of Acquatic Vegetation

    Uploaded by

    Frank
    The document analyzes aquatic vegetation samples of chlorella and sargassum using an ICPE-9000 instrument. It describes the sample preparation process, analytical conditions, and provides a table with the quantitative results of various elements in the samples as well as figures showing the spectral profiles. The results obtained from the ICPE-9000 analysis agree well with the certified values for most elements in the samples.

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    You are on page 1of 3

    LAAN-H-CP001

    ICPE-9000 Data Collection Aquatic Vegetation/Environment


    Page:1

    Analysis of Aquatic Vegetation /ICPE-9000

     Description After letting the sample cool, adjust the volume to


    25 mL, and use this as the analytical sample.
    The ICPE-9000 was used to perform quantitative
    analysis of aquatic vegetation (chlorella,  Analytical Conditions
    sargassum). Table 1 shows the quantitation results, Instrument : ICPE-9000
    and Fig. 1 and 2 show the spectral profiles. Nearly
    Radio Frequency Power : 1.2 (kW)
    all of the elements agree with the certified values in
    Plasma Gas : 10 (L/min)
    the obtained results.
    Auxiliary Gas : 0.6 (L/min)
     Sample Carrier Gas : 0.8 (L/min)
    Sample Introduction : Coaxial Nebulizer
    Powdered chlorella standard NIES No.3
    Sample Aspiration : 1.0 (mL/min)
    Powdered sargassum standard NIES No. 9
    Misting Chamber : Cyclone Chamber
     Pretreatment Attached Instruments : Mini Torch
    View Direction : Axial/Radial
    Perform heat-digestion after adding nitric acid,
    hydrochloric acid and a small amount of
    hydrofluoric acid to 1 g of each of the samples.

    Table 1 Quantitation Results of Aquatic Vegetation (µg/g)

    Sample Chlorella Sargassum


    Element Quantitation Value Certified Value Quantitation Value Certified Value
    Al 129 210 (215)
    As 1 121 128
    Ba 14 .0 19 .7
    Ca 4740 4900±300 12900 13400±500
    Cd 0 .02 0 .16 0.15
    Cr 0 .97 0 .18 ( 0.2 )
    Cu 3 .2 3.5±0.3 4 .7 4.9±0.2
    Fe 1855 1850±100 182 187±6
    K 12200 12400±600 59500 60900±2000
    Mg 3210 3300±200 6320 6500±300
    Mn 65 .5 69±5 20 .5 21.2±1.0
    Ni 0 .85 1 .15
    P 17700 (17000) 2540 (2600)
    Pb 0 .5 (0.6) 1 .2 1.35±0.05
    Sr 39 .5 40 0 .109 0.101
    V 0 .75 1 .11 1
    Zn 19 .5 20.5±1.0 16 .0 15.6±1.2

    *Values in parentheses are reference values

    1
    LAAN-H-CP001
    ICPE-9000 Data Collection Aquatic Vegetation/Environment
    Page:2
    Al 396.153 As 189.042
    条件1 条件1

    400
    75000
    350
    Intensity

    Intensity
    50000 300

    250
    25000
    200

    Ca 315.887 Best Cd 214.438 Best


    条件2 条件1

    75000 425
    Intensity

    Intensity
    50000
    400

    25000
    375

    Cr 267.716 Best Cu 327.396 Best


    条件1 条件1

    900

    875
    5000
    850
    Intensity

    Intensity

    825 4000
    800

    775 3000

    750
    2000

    Fe 259.940 K 766.490
    条件1 条件2
    60000
    400000
    50000
    300000
    Intensity

    40000
    Intensity

    30000 200000
    20000
    100000
    10000

    0 0

    Fig. 1 Spectral Profiles of Aquatic Vegetation (Sargassum)

    2
    LAAN-H-CP001
    ICPE-9000 Data Collection Aquatic Vegetation/Environment
    Page:3
    Mg 285.213 Best Mn 257.610 Best
    条件2 条件1

    40000

    30000 50000

    Intensity
    Intensity

    20000
    25000
    10000

    0 0

    Ni 231.604 Best P 178.287


    条件1 条件1

    500
    600
    400

    Intensity
    Intensity

    575
    300
    550

    200
    525

    100

    Pb 220.353 Best Sr 421.552 Best


    条件1 条件2

    600000
    390
    500000
    Intensity
    Intensity

    380 400000

    300000
    370
    200000

    100000
    360
    0

    V 290.882 Zn 206.200
    条件1 条件1

    1250
    2750

    1000
    Intensity

    Intensity

    2500
    750

    2250 500

    250

    Fig. 2 Spectral Profiles of Aquatic Vegetation (Sargassum)

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