Is 1489 1 1991 PDF
Is 1489 1 1991 PDF
Is 1489 1 1991 PDF
( am @mJr )
Indian Standard
PORTLAND-POZZOLANACEMENT-
SPECIPICATION
PART 1 FLY ASH BASED
( Third Revision)
First Reprint MARCH 1993
Q BIS 1991
FOREWORD
This Indian Standard ( Part 1 ) ( Third Revision .) was adopted by the Bureau of Indian Standards,
after the draft finalized by the Cement and Concrete Sectional Committee had beenapproved by
the Civil Engineering Division Council.
Portland-pozzolana cement can be produced either by grinding together Portland cement clinker
and pozzolana with addition of gypsum or calcium sulphate, or by intimately and uniformly
blending Portland cement and fine, pozzolana. While grinding of the two materials together
presents no difficulty, the mixing of dry powders intimately is extremely difficult. The blending
method should, therefore, be resorted to only when the grinding method is impossible or proves
uneconomical, in a particular case. Where blending method is adopted, every care should be taken
to see that the blending is as intimate as possible. Generally, if the blending is not uniform, it is
reflected in the performance tests. The Sectional : Committee responsible for the preparation of
this specification is of the opinion that the blending method should be confined to such factories/
works where intimate and uniform blending is feasible with the employment of requisite
machinery so as to ensure uniformity of product and its guaranteed performance.
Portland-pozzolana cement produces less heat of hydration and offers greater resistance to the
attack of aggressive waters than normal Portland cement. Moreover, it reduces the leaching of
calcium hydroxide liberated during the setting and hydration of cement. It is particularly useful
in marine and hydraulic construction and other mass concrete structures. Portland-pozzolana
cement can generally be used wherever 33 grade ordinary Portland cement is usable under normal
conditions. However, it should be appreciated that all pozzolanas need not necessarily contribute
to strength at early ages. In view of this fact, this specification has been prepared to enable
manufacturers to produce PortJand-pozzolana cement equivalent to 33 grade ordinary Portland
cement on ihe basis of the 3, 7 and 2%days compressive strength.
For construction of structures using rapid construction methods like slipform construction,
Portland-pozzolana cement shall be used with caution since 4 to 6h strength of concrete is
considered significant in such construction.
This standard was first published in 1962 and subsequently revised in 1967 and 1976. In this
revision the standard has been split into two parts based on the pozzolana used in the manufacture
of such cements in view of the special needs of some hydraulic structures which require pozzolana
cement manufactured only with fly ash pozzolana, This would also enable the user to identify
the pozzolana used in the manufacture of cement. Part I of this standard covers pozzolana cement
manufactured by using only fly ash pozzolana and Part 2 covers pozzolana cement manufac-
tured by using either calcined clay or a mixture of calcincd clay and fly ash as pozzolana.
In this revision both chemical and physical requirements have been kept the same as was given
in 1976 version of this standard as amended. Various rcquiremrnts of Portland-pozzolana
cement given in 1976 version oi this standard had been modified from time to time by
issuing amendments based on the experience gained with the use of the standard and the
requirements of the users and also 1teepin.g in view raw materials and fuel available in the
country for manufacture of cement. The Important amendments include lowering the value
of compressive strength in lime reactivity test from 5 MPa to 4 MPn, incorporating a value of
3-days compressive strength as 16 MPa, modifying the requirement of sulphuric anhydride (SOS)
and insoluble residue, deleting the requirement of pozzolanicity test, increasing the value of 28-
days compressive strength from 31 MPa to 33 MPa, making autoclave soundness test compulsory
irrespective of the magnesia content in cement, incorporating a provision for retest in respect of
autoclave soundness test after aeration of the cement, incorporating a clause on false set of cement
and permitting packaging of cement in 25 kg bags. All these amendments have been taken care
of in this revision.
Mass of cement packed in bags and the tolerance requirements for the mass of cement packed in
bags shall be in accordance wrth the relevant provisions of the Standards of Whghts and Measures
( Packaged Commodities ) Rules, 1977 and B-l.2 (see Annex B ). Any modification in these rules
in respect of tolerance on mass of cement would apply automatically to this standard.
This siandard contains clauses 4.1.4, 4.2 and 12.4.1 which permit the purchaser to use his option
and 10.2. 1 and 10. 3 call for agreement between the purchaser and the manufacturer.
The composition of the technical committee responsible for the formulation of this standard is
given in Annex C.
For the purpose of deciding whether a particular requirement of this standard is complied with,
the final value, observed or calculated, rressing the result of a test, shall be rounded off in
accrdance witn IS 2 : 1960 ‘Rules for rounding off numerical values ( revised )‘. The number
of significant places retained in the rounded off value should be the same as that of the specified
value in this standard.
IS 1489 ( Part 1 ) : 1991
Indian Standard
PORTLAND-POZZOLANA CEMENT -
SPECIFICATION
PART 1 FLY ASH BASED
( Third Revision )
1 SCOPE 4.1.2 Fineness and average compressive strength
in lime reactivity of fly ash that is to be blended
This standard ( Part 1 ) covers the manufacture, with finished Portland cement to produce
physical and chemical requirements of Portland- Portland-pozzolana cement, when tested in
pozzolana cement using only fly ash pozzolana. accordance with the procedure specified in
IS 1727 : 1967, shall not be less than 320 mq/kg
2 REFERENCES and 4’0 MPa respectively. Average compressive
strength in lime reactivity test of such fly ash
The Indian Standards listed in Annex A are shall be carried out at the fineness at which
necessary adjuncts to this standard. pozzolana has been received for blending.
3 TERMINOLOGY 4.1.3 Average compressive strength in lime
reactivity of fly ash that is to be interground
For the purpose of this standard, the definitions with Portland cement clinker for manufacture
given in IS 4845 : 1968 and the following shall of Portland-pozzolana cement shall not be less
apply. than 4’0 .MPa when tested at the fineness of
Portland-pozzolana cement manufactured out of
3.1 Pozzolma it or at the fineness in ‘as-received’ condition,
whichever is greater, in accordance with the
An essentially silicious material which while in
procedure specified in IS 1727 : 1967.
itself possessing little or no cementitious pro-
perties will, in finely divided form and in the 4.1.4 The purchaser shall have the right, if he
presence of water, react with calcium hydroxide so desires to obtain samples of fly ash used in
at ambient temperature to form compounds the manufacture of Portland-pozzolana cement
possessing cementitious properties. The term for purposes of checking its conformity to the
includes natural volcanic material having requirements specified in 4.1.1 to 4.1.3.
pozzolanic properties as also other natural and
artificial materials, such as diatomaceous earth, 4.2 Portland Cement Clinker
calcined clay and fly ash.
The Portland cement clinker used in the
3.2 Portland Clinker manufacture of Portland-pozzolana cement
shall comply in all respects with the chemical
Clinker, consisting mostly of calcium silicates, requirements of IS 269 : 1989 and the purchaser
obtained by heating to incipient fusion, a pre- have the right, if he so desires to obtain
determined and homogeneous mixture of sample of the clinker used in the manufacture
materials princi ally containing lime ( CaO ) for purposes of checking its conformity to
and silica ( SiOl 7 with a smaller proportion of IS 269 : 1989.
alumina ( AlsOI ) and iron oxide ( Fe,O* ). 4.3 Portland Cements
3.3 Portland-Pozzolaoa Cement Portland cement for blending with fly ash shall
conform to IS 269 : 1989.
An intimately interground mixture of Portland
clinker and pozzolana with the possible addition 4.4 Other Admixtares
of gypsum ( natural or chemical ) or an intimate When Portland-pozzolana cement is obtained
and uniform blending of Portland cement and by grinding fly ash with Portland cement clinker,
fine pozzolana. no material other than gypsum ( natural or
chemical ) or water or both, shall be added.
4 RAW MATERIAL Such air-entraining agents or surfactants which
have been proved harmless may be added in
4.1 Pozzolrna quantities not exceeding one percent.
4.1.1 Fly ash used in the manufacture of 5 MANUFACTURE
Portland-pozzolana cement shall conform to
IS 3812 : 1981 subject to the requirements Porland-pozzolana cement shall be manufactured
specified in 4.1.2 and 4.1.3. either by intimately mtergrinding Portland
1
IS 1489 ( Part 1) : 1991
cement clinker and fly ash or by intimately and total period of 7-days. The expansion of cement
uniformly blending Portland cement and fine so aerated shall be not more than 5 mm and
fly ash. For blending of Portland cement and 0’6 percent when tested by ‘Le-Chatelier’ method
fly ash, the metbod and equipment used shall be and autoclave test respectively as described in
the one well accepted for achieving a complete IS 4031 ( Part 3 ) : 1988.
uniform and intimate blending. The blending
operation shall be a prcperly designed and well 7.3 Setting Time
defined unit operation in approved blenders. The setting time of Portland-pozzolana cement,
Gypsum ( natural or chemical ) may be added if when testpd by the Vicat apparatus method
the Portland-pozzolana cement is made by described in IS 4031 ( Part 5 ) : 1988, shall be
intergrinding Pcrtland cement clinker with fly as follows:
ash. The fly ash constituent shall not be less
tban 10 percent and not more than 25 percent Initial setting time 30 min, Min
by mass of Portland-pozzolana cement. The Final setting time 600 min, MUX
homogeneity of the mixture shall be guaranteed
within A3 percent in the same consignment. 7.3.1 If cement exhibits false set, the ratio of
final penetration measured after 5 min of com-
6 CHEMICAL REQUIREMENTS pletion of mixing period to the initial penetra-
tion measured exactly after 20 s of completion
6.1 Portland-pozzolana cement, shall comply of mixing period, expressed as percent, shall be
with the cbcmical requirements given in Table 1. not less than 50 when tested by the method
described in IS 4031 ( Part 14 ) : 1989. In the
Table 1 Chemical Requirements of Portland- event of cement exhibiting false set, the initial
Pozzolana Cement and final setting time of cement when tested by
the method described in IS 4031 ( Part 5 ): 1988,
Characteristic Reqnirement Method of after breaking the false set, shall conform to 7.3.
Test Ref
to IS
7.4 Compressing Strength
(1) (2) (3) (4)
i) LOSSon ignition, percent 5.0 4032 : 1985 7.4.1 The average compressive strength of not
by mass, Max
less than three mortar cubes ( area of face
ii) Magnesia ( MgO ), per- 6’0 4032 : 1985
50 cm* ) composed of one part of cement, three
cent by mass, Max
iii) Sulpburic anhydride 3’0 4032 : 1985 parts of standard sand ( see Note 2 ) by mass,
( SOS ), percent by and P/4 + 3.0 percent ( of combined mass of
mass. Max cement and sand ) water, and prepared, stored
iv) Insoluble material, X+4*0 ( 100-x ) 4032 : 1985 and tested in the manner described in IS 4031
percent by mass, 100 ( Part 6 ) : 1988 shall be as follows:
Max
where x is the declared per- a) At 72 f 1h I6 MPa, Min
centage of flyash in the given
Portland-pozzolana cement b) At 168 =t 2 h 22 MPa, Min
c) At 672 rt 4 h 33 MPa, Min
7 PHYSICAL REQUIREMENTS
NOTES
7.1 Fineness 1 P is the percentage of water required to produce
a paste of standard consistency ( see 12.3 ).
When tested by the air permeability method 2 Standard sand shall conform to IS 650 : 1966.
described in IS 4031 ( Part 2 ) : 1988, the specific
surface of Portland-pozzolana cement sball be 7.4.2 Notwithstanding the cubes satisfying the
not less than 300 ml/kg. strength requirements specified in 7.4.1, they
shall also show a progressive increase in strength
7.2 Soundness from the strength at 72 h.
7.2.1. When tested by ‘Le Cbatelier’ method and 7*5 Dr@g Sbrinkage
autoclave test described in IS 4031 ( Part 3 .) ; The average drying shrinkage of mortar bars
1988, unaerated Portland-pozzolana cement prepared and tested in accordance with IS 4031
shall not have an expansion of more than 10 mm ( Part 10 ) : 1988 &all not be mOre than o.15
and 0’8 percent respectively. percent.
7.2.1.1 In the Went of cement f’ailing to COrnply 8 STORAGE
with any or both the requirements specified
in 7.2.1, further tests in respect of each failure The Portland-pozzolana cement shall be stored
shall be made as described in IS 4031 ( Part 3 ) ; in such a manner as to permit easy access for
1988 from another portion of the same sample proper inspection and identification, and in a
after aeration. The aeration shall be done by suitable weather-proof building to protect the
spreading out the sample to a depth of 75 mm cement from dampness and to minimize ware-
at a relative humidity of 50 to 80 percent for a house deterioration.
2
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3
Is 1489 ( Part 1) : 1991
ANNEX A
( Chuse 2 )
LIST OF REFERRED INDIAN STANDARDS
4
IS 1489 ( Part 1) : 1991
ANNEX B
( czfzuse 10.2 )
TOLERANCE~REQUIBEMENTS FOR THE MASS OF CEMENT PACKED IN BAGS
B-1 The average net mass of cement packed in minus-error in none of such bags in the sample
bags at the plant in a sample shall be equal to shall exceed 4 percent of the specified net mass
or more than 50 kg. The number of bags in of cement in the bag.
aample shall be as given below: NOTE-The matter given in B-l and B-l.1 are
Batch Size Sample Size extracts based pn the Standards of Weights and
Measures ( Packaged Commodities ) Rules, 1977 to
100 to 150 20 which reference shall be made for full details. Any
151 ,, 280 modification made in these Rules and other related
:: Acts and Rules would apply automatically.
281 ,, 500
1200 B-l.2 In case of a wagon/truck load of 20 to
1% ” 3 200 1;: 25 tonnes, the overall tolerance on net mass of
3 201 &d above 200 cement shall be 0 to +0’S percent.
The bags in a sample shall be selected at random NOTE - The mass of a jute sacking bag coaform-
(see IS 4905 ; 1968 1. ing to IS 2580 : 1982 to bold 50 kg of cement is
531 g. the mass of a double hessian bituminized
B-l.1 The number of bags in a sample showing ( CR1 type ) bag to bold 50 kg of cement is 630 g,
the mass of a 6-Ply Paper bag to hold 50 kg of
a minus error greater than 2 percent of the cement is approximately 400 g and the mass of a
specified net mass ( 50 kg ) shall be not more polyethylene lined ( CR1 type 1 jute bag to bold
than 5 percent of the bags in the sample and the 50 kg of cement is approximately 480 g.
ANNEX C
( Foreword,)
COMPOSITION OF THE TECHNICAL COMMITTEE
Cement and Concrete Sectional Committee, CED 2
Chairman Representing
m H. c. VlsvasvARAYa In Personal Capacity ( University of Roorkee,
Roorkee-247667 )
Members
SKI H. BI~AITACHARYA Orissa Cement Limited, New Delhi
@R A. K. CHATTERJEE The Associated Cement Companies Ltd, Bombay
SHRI S. H. SUBRAMANIAN ( Alternate )
CHIRP ENCIINEER( DESI~NB) Central Public Works Department, New Delhi
SUPERINTENDINOENOINEER( B&S ) ( Alternate )
CHIRPENQINEER. NAVAOAM DAM Sardar Sarovar Narmada Nigam Ltd, Gandhinagar
( Supma ) ENGINEER. QCC ( Alternate )
CHIRPENGINEER( RESEARCH-CUM-DIRECTOR ) Irrigation and Power Research Institute, Amritsar
RESEARCH OFFICER( CONCRETE-TECHNOLOC+Y ) ( Alternate )
DIRECTOR A.P. Engineering Research Laboratories, Hyderabad
JOINT DIRECTOR( Alternate )
DIN~~OR( C&MDD)( N&W) Central Water Commission, New Delhi
DEPUTYDIRECTOR ( C dt MDD ) ( NW & S ) ( Alternate )
Senx K. H. GANOWAL Hyderabad Industries Limited, Hyderabad
Srlax V. PA~ABHI ( Alternate )
SHRI V. K. GHANEKAR Structural Engineering Research Centre ( CSIR ),
Ghaziabad
SHRI S. GOPIN~TH The India Comments Ltd, Madras
SHRI R. TAMILAKARAN ( Alternate )
SHRI S. K. GUHA THAKURTA Gennon Dunkerley & Company Limited, Bombay
SHRI S. P. SANKARANARAYANAN ( Alternate )
DR IRSHADMASOOD Central Building Research Institute ( CSIR ), Roorkee
DR MD KHALID( Alternate )
JOINTDIRBCTOR,STANDARDS( B & S ) ( CB-I ) Research, Desigris 8 Standards Organization ( Ministry of
JOINT DIRFXTOR,STANDARDS ( B & S ) ( CB-II ) Railways ), Lucknow
( Alternate )
SHRI N. 0. JOSHI Indian Hume Pipes Co Ltd, Bombay
SHRI P. D. KELKAR( Alternate )
SARI D. K. KANUN~O National Test House, Calcutta
SXRI B, R. MEENA( Alternate )
5
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6
IS 1489 ( Part 1) : 1991
Members Representing
SARI G. K. hhlVMDAR Hospital Services Consultancy Corporation ( India j Lid,
New Delhi
DR IRSHAD MASOOD Central Building Research Institute ( CSIR ). Roorkee
SHRI K. P. MOHIDEEN Central Warehousing Corporation, New Delhi
SHRI M. K. MIJICHERJEE Roads Wing, Department of Surface Transport ( Ministry
SHRI M. K. GHOSH ( Altcrnute ) of Transport ), New Delhi
DR A. K. MVLLICK National Coun&l for Cement and Building Materials,
DR ( SMT ) S. LAXMI ( AIrernute ) New Delhi
SHRI K. NARANAPPA Centrzl Electricity Authority, New Delhi
SHRI D. P. KEWALRAMANI ( Afrernore )
SHRI NIRMAL StNoti Development Commissioner for Cement Industry
SHRI S. S. MtotANr ( AkernaSe ) ( Ministry of Industry )
SHRI Y. It. PHVLL Central Road Research Institute ( CSIR ), New Delhi
SHRI S. S. SEFHRA ( Alternate )
SHRt A. v. RAMANA Dalmia Cement ( Bharat ) Ltd, New Delhi
DR K. C. NARAN~ ( A/ternatc )
COL V. K. RAO Engineer-in-Chief’s Branch, Army Headquarters
SHRI N. S. GALANDE ( Altrrnare )
SHRI S. A. REDDI Gammon India Limited. Bombay
SHRI A. U. RIIHSINQHANI Cement Corporation of India Limited, New Delhi
SHRI M. P. SIN~H Federation of Mini Cement Plants, New Delhi
SVPERINTENDINOENGINEER( D ) Public Works Department, Government of Tamil Nadu
SENIOR DEPUTY CHIEF ENGINEER ( GENERAL) ( Alternate )
SHRI S. B. SVRI Central Soil and Materials Research Station, New Delhi
SHRI N. CHANDRASEKARAN ( AIIernote )
SHRI L. SWAROOP Orissa Cement Limited, New Delhi
SH~I H. BHA~ACHARYA ( Alternare )
SHRI V. M. WAD Bhilai Steel Plant, Bhilai
Standard Mark
The use of the Standard Mark is governed by the provisions of the Bureau of Indian
Standards Act, 1986 and the Rules and Regulations made thereunder. The Standard Mark on
products covered by an Indian Standard conveys the assurance that they have been produced
to comply with the requirements of that standard under a well defined system of inspection,
testing and quality control which is devised and supervised by BEG and operated by the
producer. Standard marked products are also continuously checked by BIS for conformity
to that standard as a further safeguard. Details of conditions under which a licence for the
use of the Standard Mark may be granted to manufacturers or producers may be obtained
from the Bureau of Indian Standards.
Bureau of Indian Standards
BIS is a statutory institution established under the Bureau of hdian Standards Act, 1986 to promote
harmonious development of the activities of standardization, marking and quality certification of
goods and attending to connected matters in the country.
Copyright
BIS has the copyngnr of all its publications. No part of these publications may be reproduced in
any form without the prior permission in writing of BIS. This does not preclude the free use, in the
course of implementing the standard, of necessary details, such as symbols and sizes, type or grade
designations. Enquiries relating to copyright be addressed to the Director (Publications), BIS.
(Thid Revision)
(CED2)
Printed at Simco Printinp Press. Delhi, India
AMI~NI)MILN’J’ NO.2 ,IUNJ!: 1993
TO
IS 1489 ( Part 1) : 1991 PORTLAND-POZZOLANA
CEMENT - SPECIFICATION
PART1 FLY ASH BASED
“10.2.2 When cement is intended for export and if tbe purchaser so requires,
packing ol crmcnt may be done in bags or in drums with an average net mass of
ccmcnt per bag or drum as agreed to between the purchaser and the
nianu~aclurcr.
10.2.2.1 For this purpose the permission of the certifying authority shall be
ob~aincd in ;I~V:IIICC for each rxport order.
Itl.2.2.2 The words ‘I~OH 11:XI’OH’I” and the average net mass of cement per
bag/drum shalt he clearly marked in indelible ink on each bag/drum.
10.2.2.4 The tolerance requirements for the mass of cement packed in bags/drum
shaII bc as given in 10.2.1.1 rxccpt the average net mass which shall be equal to
or more than llic quantity in 10.2.2.”
(CED2)
ReprograpllyUnit, BIS, New Delhi. India
AMENDMENT NO. 3 JULY 2000
TO
IS 1489 ( Part i ) : 1991 PORTLAND-POZZOLANA
CEMENT - SPECIFICATION
PART 1 FLY ASH BASED
( Third Revision)
Substitute ‘netmass’for ‘nominal average net mass’ and ‘average net mass’
wherever these appear in the standard.
( Page 2, clause 5, lusf but one senrence ) - Substitute the following for
the existing sentence:
‘The fly ash constituent shall be not less than 15 percent and not more than
35 percent by mass of Portland-pozzolana cement.’
(CED2)
Reprography Unit, BIS, New Delhi, India
AMENDMENTNO. 4 MAY 2005
TO
IS 1489 (PART 1): 1991 PORTLAND-POZZOLANA
CEMENT — SPECIFICATION
PART1 FLY ASH BASED
( Third Reviswn )
( Page 1, clause 4.1.1, line 3 ) — Substitute ‘IS 3812 (Part 1)’ jiw
‘IS 3812:1981’.
( Page 1, clause 4.1.2, line 7 ) — Substitute ‘4.5 MPa’ for ‘4.0 MPa’.
( Page 1, clause 4.1.3, line 5 ) — Substitute ‘4.5 MPa’ for ‘4.0 MPa’.
( Page 1, clause 4.1.3) — Insert the following note at the end
‘NOTE — Fly ash of fineness 250 m2/kg, A4irr is also permitted to be used in the
manufacture of Portland pozzolana cement by inter ~dirrg it with Portland cement clinker
if the fly ash when ground to fineness of 320 m /kg or to the fineness of the resultant
Portland pozzolana cement whichever is tower, meets all the requirements specified in 6
arrd70f IS3812 (Part l).’
( Page 3, clause 9.2, Notes) — Substitute the following for the existing
‘NOTES
1 Total chloride content in cement shall not exceed 0.1 percent by mass for cement used in
structures other than prestressed coneretc. For determination of chloride content in cement,
1S 12423 maybe referred.
2 For use in special structures like prestressed cxmerere, where chloride is a critical
parameter, the chIoride content shall not exeeed 0.05 percent and shall be required to be
measured if desired by the purchaser.’
(CED2)
Reprography Unit, BIS, New Delhi, India
s
AMENDMENT NO. 5 JUNE 2009
TO
IS 1489 (PART 1) : 1991 PORTLAND-POZZOLANA CEMENT —
SPECIFICATION
( Third Revision )
(Page 3, clause 10.2.1) ― Substitute the following for the existing clause:
‘The net mass of cement per bag may also be 25 kg, 10 kg, 5 kg, 2 kg and 1 kg subject to tolerances as
given in 10.2.1.1 and packed in suitable bags as agreed to between the purchaser and the manufacturer.’
(Page 3, clause 10.2.1.1, last sentence) ― Substitute the following for the existing:
‘However, the average of net mass of cement in a sample shall be equal to or more than 25 kg, 10 kg, 5 kg,
2 kg or 1 kg, as the case may be.’
(CED 2)