Pinturas y Barniz Prueba Dobles-T ISO 17132
Pinturas y Barniz Prueba Dobles-T ISO 17132
Pinturas y Barniz Prueba Dobles-T ISO 17132
net)
DEUTSCHE NORM January 2008
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DIN EN ISO 17132
ICS 87.040
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Paints and varnishes –
T-bend test (ISO 17132:2007)
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English version of DIN EN ISO 17132:2008-01
Beschichtungsstoffe –
T-Biegeprüfung (ISO 17132:2007)
Englische Fassung DIN EN ISO 17132:2008-01
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National foreword
This standard falls in the domain of Technical Committee CEN/TC 139 “Paints and varnishes” (Secretariat:
DIN, Germany). It is identical with International Standard ISO 17132 which was prepared by ISO/TC 35/SC 9
“General test methods for paints and varnishes” (Secretariat: BSI, United Kingdom).
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The responsible German body involved in its preparation was the Normenausschuss Beschichtungsstoffe
und Beschichtungen (Coatings and Coating Materials Standards Committee), Technical Committee
NA 002-00-07 AA Allgemeine Prüfverfahren für Beschichtungsstoffe und Beschichtungen.
The DIN Standards corresponding to the International Standards referred to in the EN are as follows:
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ISO 1513 DIN EN ISO 1513
ISO 1514 DIN EN ISO 1514
ISO 1519 DIN EN ISO 1519
ISO 1520 DIN EN ISO 1520
ISO 2808 DIN EN ISO 2808
ISO 6272-1
ISO 6272-2
ISO 6860
ISO 15528
IEC 60454-2
DIN EN ISO 6272-1
DIN EN ISO 6272-2
DIN EN ISO 6860
DIN EN ISO 15528 xw
DIN EN ISO 60454-2 (VDE 0340-2)
National Annex NA
(informative)
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Bibliography
DIN EN 60454-2 (VDE 0340-2), Specification for pressure-sensitive adhesive tapes for electrical purposes —
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DIN EN ISO 1513, Paints and varnishes — Examination and preparation of samples for testing
DIN EN ISO 1514, Paints and varnishes — Standard panels for testing
DIN EN ISO 1519, Paints and varnishes — Bend test (cylindrical mandrel)
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DIN EN ISO 6272-1, Paints and varnishes — Rapid-deformation (impact resistance) tests — Part 1: Falling-
weight test, large-area indenter
DIN EN ISO 6272-2, Paints and varnishes — Rapid-deformation (impact resistance) tests — Part 2: Falling-
weight test, small-area indenter
DIN EN ISO 6860, Paints and varnishes — Bend test (conical mandrel)
DIN EN ISO 15528, Paints, varnishes and raw materials for paints and varnishes — Sampling
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NORME EUROPÉENNE
EUROPÄISCHE NORM October 2007
ICS 87.040
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English Version
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Peintures et vernis - Essai de pliage en T (ISO 17132:2007) Beschichtungsstoffe - T-Biegeprüfung (ISO 17132:2007)
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
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Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the
official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,
Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,
Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
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© 2007 CEN All rights of exploitation in any form and by any means reserved worldwide Ref. No. EN ISO 17132:2007: E
for CEN national Members.
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Contents Page
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Foreword ........................................................................................................................................................... 3
Introduction ...................................................................................................................................................... 4
1 Scope ................................................................................................................................................... 5
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2 Normative references ......................................................................................................................... 5
3 Terms and definitions ........................................................................................................................ 5
4 Principle ............................................................................................................................................... 5
5 Apparatus ............................................................................................................................................ 6
6 Sampling .............................................................................................................................................. 6
7
7.1
7.2
7.3
8
8.1
8.2
8.3
8.4
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Test panels ..........................................................................................................................................
Substrate .............................................................................................................................................
Preparation and coating .....................................................................................................................
Thickness of the coating ....................................................................................................................
Procedure ............................................................................................................................................
Conditioning of the test panels .........................................................................................................
Test conditions ...................................................................................................................................
Bending ................................................................................................................................................
Evaluation ............................................................................................................................................
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6
6
6
6
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7
9
8.5 T-bend test as a pass/fail test ........................................................................................................... 9
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9 Supplementary information ............................................................................................................... 9
10 Expression of results ......................................................................................................................... 9
11 Precision ........................................................................................................................................... 10
11.1 General .............................................................................................................................................. 10
11.2 Repeatability, r ................................................................................................................................. 10
11.3 Reproducibility, R ............................................................................................................................. 10
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Foreword
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This document (EN ISO 17132:2007) has been prepared by Technical Committee ISO/TC 35 "Paints and
varnishes" in collaboration with Technical Committee CEN/TC 139 "Paints and varnishes", the secretariat of
which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an identical
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text or by endorsement, at the latest by April 2008, and conflicting national standards shall be withdrawn at the
latest by April 2008.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
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Sweden, Switzerland and the United Kingdom.
Endorsement notice
The text of ISO 17132:2007 has been approved by CEN as a EN ISO 17132:2007 without any modification.
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Introduction
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This International Standard is one of five standards which specify empirical test procedures for assessing the
resistance of coatings of paints, varnishes and related products to cracking and/or detachment from the
substrate under different conditions of deformation. The other International Standards are ISO 1519,
ISO 1520, ISO 6272 and ISO 6860.
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The T-bend test has already been standardized in the USA (ASTM D 4145), Europe (EN 13523-7) and Japan
(JIS G 3312). The test methods in these standards are basically the same, but differ from each other in details
such as
⎯ whether the coated test panel is folded back on itself or is bent round a mandrel or a test panel used as a
spacer;
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the way in which the test result is expressed.
In this International Standard, the basic contents common to the US, European and Japanese standards have
been adopted, but details in which the US, European and Japanese standards differ, in particular the use of a
mandrel or spacer panels, have been made subject to agreement between the interested parties.
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1 Scope
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This International Standard describes a method of evaluating the flexibility and adhesion of an organic coating
on a metallic substrate by observing the cracking or loss of adhesion when a coated test panel is bent.
The method can be used to confirm whether paints, varnishes or related products meet a given test
requirement in a pass/fail test, or to determine the minimum bending diameter at which cracking does not
occur.
2 Normative references
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The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
ISO 1513, Paints and varnishes — Examination and preparation of samples for testing
IEC 60454-2, Specification for pressure-sensitive adhesive tapes for electrical purposes — Part 2: Methods of
test
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3.1
T-bend test
test designed to determine the flexibility of a paint coating by bending a coated test panel through 180°
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3.2
T-bend rating
minimum number of spacers of defined thickness around which a coated test panel can be bent (or, if bent
around a mandrel, the number of spacers equivalent to the diameter of the mandrel) without cracking or loss
of adhesion (flaking) of the coating occurring
4 Principle
Coated panels are bent back on themselves to 180°, with the coated surface on the outside of the bend, at
progressively less severe radii of curvature, the radii of curvature being defined by spacers or mandrels. After
bending, each panel is examined with a magnifying glass for cracking of the coating and by a tape pull-off test
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for loss of adhesion of the coating. The minimum diameter to which the test panel can be bent without
cracking or loss of adhesion, i.e. when failures no longer occur, is taken as the T-bend rating.
Visual examination with a magnifying glass can also be used to determine whether there is any loss of
adhesion.
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5 Apparatus
5.1 Vice, with flat and smooth jaws. This is used to hold one end of the test piece firmly in place at the start
of the bending test.
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If the test panel is not bent around itself, a series of bending mandrels with smoothly rounded ends may be
used as guides around which the test panel is bent (see Figure 1).
By agreement between the interested parties, one or more uncoated panels may also be used as mandrels.
6 Sampling
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5.3 Adhesive tape, with an adhesive strength between 6 N/25 mm width and 10 N/25 mm width when
determined in accordance with IEC 60454-2.
Examine and prepare each sample for testing, as described in ISO 1513.
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7 Test panels
7.1 Substrate
Unless otherwise agreed, use rectangular steel test panels. The panel surfaces shall be plane.
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Unless otherwise agreed, prepare each test panel in accordance with ISO 1514 before coating it using the
specified application method (see Clause 9) and drying, curing or stoving.
Determine the thickness, in micrometres, of the dry coating by one of the procedures given in ISO 2808.
8 Procedure
Unless otherwise agreed, condition the coated test panels for at least 16 h at (23 ± 2) °C and (50 ± 5) %
relative humidity before carrying out the test.
Unless otherwise agreed, carry out the test at (23 ± 2) °C and (50 ± 5) % relative humidity.
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8.3 Bending
8.3.1 General
The bending shall be performed in accordance with one of the procedures given in 8.3.2, 8.3.3 and 8.3.4, as
agreed between the interested parties.
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Unless otherwise agreed, the bend shall be across the direction of rolling of the panel, except for coil coatings
in which case the test panel shall be bent parallel to the direction of rolling.
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8.3.2 T-bend test around a mandrel
Clamp a coated test panel and a mandrel in the vice. Then bend the panel 180° around the mandrel (see
Figure 1) in a smooth and uniform manner with the coated side of the panel on the outside of the bend.
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Figure 1 — Bending around a mandrel
Examine the bend for cracking and for loss of adhesion as described in 8.4. Repeat the bending procedure,
using a new test panel and a different size of mandrel each time, to determine the minimum mandrel thickness
at which no cracking or loss of adhesion occurs.
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Express the T-bend rating, Tm, as the number of panel thicknesses equivalent to the thickness of the
narrowest mandrel around which the test panel could be bent without cracking or loss of adhesion occurring,
reporting the result as 1 Tm for one panel thickness, 2 Tm for two panel thicknesses, etc. (see also Table A.1).
Clamp one end of a coated test panel in the vice and bend it with the coated side of the panel on the outside
of the bend. Remove the panel from the vice and bend it further with the fingers until it can be placed in the
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vice again. Insert one or more uncoated panels as spacers inside the bent panel as shown in Figure 2, fasten
the assembly in the vice and bend it quickly to an angle of 180°. Each spacer panel shall have the same
thickness as the test panel.
Examine the bend for cracking and loss of adhesion as described in 8.4. Repeat the bending procedure, using
a new test panel and a different number of spacers each time, to determine the smallest number of spacers at
which no cracking or loss of adhesion occurs.
Express the T-bend rating, Tp, as the minimum number of spacers around which the test panel could be bent
without cracking or loss of adhesion occurring, reporting the result as 1 Tp for one spacer, 2 Tp for two
spacers, etc. (see also Table A.1).
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a) 1 Tp b) 2 Tp
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8.3.4 T-bend test with test panel repeatedly folded back on itself (folding method)
Clamp one end of a coated test panel in the vice and bend it through 90° in a smooth and uniform manner
with the coated side of the panel on the outside of the bend. Continue to bend the panel until the bent end can
be inserted in the jaws of the vice (see Figure 3). Tighten the vice to complete the 180° bend. Take care to
tighten the vice sufficiently so that the surfaces on the inside of the bend are as closely in contact as possible.
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Examine the bend for cracking and loss of adhesion as described in 8.4. If cracking or loss of adhesion has
occurred, repeat the bending procedure, as shown in Figure 3, until no cracking or loss of adhesion occurs.
Express the T-bend rating, Tf, as the number of bends, after the initial bend, which could be made in the test
panel before no cracking or loss of adhesion occurred, reporting the result as 0 Tf for no bends after the initial
one, 1 Tf for one bend after the initial one, etc. (see also Table A.1).
If it is agreed to use test panels in the shape of a right-angled triangle, the lengths of two sides should
preferably be equal and in the range 10 cm to 15 cm. This shape leaves part of each bend exposed for later
examination and for a permanent record.
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a) 0 Tf b) 1 Tf
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c) 2 Tf d) 3 Tf
e) 4 Tf
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8.4 Evaluation
Examine the bend, using the magnifying glass (5.2), immediately after bending for any cracking. Disregard
those parts of the bend within 5 mm of each edge of the panel.
Unless otherwise agreed, also examine each bend for loss of adhesion by the following test. Place a piece of
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adhesive tape (5.3) on the coating at the bend in the test panel. Rub the tape flat to ensure good contact with
the coating. Then pull off the tape with a rapid movement. If no coating residues can be seen on the adhesive
tape, there is no loss of adhesion.
If agreed, the magnifying glass (5.2) can be used instead to examine the bend for loss of adhesion of the
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coating.
The T-bend tests described in 8.3.2, 8.3.3 and 8.3.4 can also be used as a pass/fail test, the bend being
evaluated, as before, in accordance with 8.4.
9 Supplementary information
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If the results of several determinations differ, additional tests shall be carried out.
For any particular application of the test method specified in this International Standard, the following
information needs to be specified, in addition to that given in the preceding clauses, to enable the method to
be carried out. The information required should preferably be agreed between the interested parties and may
be derived, in part or totally, from an international or national standard or other document related to the
coating material under test.
a) The material, shape, thickness and surface preparation of the test panels.
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b) The method of application of the coating material under test to the panels, including duration and
conditions of drying between coats in the case of a multi-coat system.
c) The duration and conditions of drying (or stoving) and ageing (if applicable) of the coating before testing.
d) The temperature and relative humidity of conditioning of the coated panels before starting the test, if
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e) The thickness, in micrometres, of the dry coating and the method of measurement used, and whether it is
a single coat or a multi-coat system.
f) The test temperature and relative humidity, if different from those indicated in 8.2.
g) The type of test to be carried out, i.e. whether it is a classification test or a pass/fail test.
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10 Expression of results
Report the test result as the greatest extent to which the test panel can be bent without cracking or loss of
adhesion, expressed as specified in 8.3.2, 8.3.3 or 8.3.4 for the method used and indicating, in addition, if
cracking took place without loss of adhesion or vice versa.
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11 Precision
11.1 General
The precision statements below are based on results obtained from round-robin testing using spacers (i.e. the
method described in 8.3.3). The test conditions were (20 ± 1) °C and (65 ± 5) % RH and the bends were
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evaluated visually both with and without a magnifying glass.
11.2 Repeatability, r
The repeatability r is the value below which the absolute difference between two single test results, each the
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mean of duplicates, can be expected, with 95 % probability, to lie when this method is used under repeatability
conditions, i.e. same material, same operator, same apparatus and results obtained within a short interval of
time. For examination with a magnifying glass, r was found to be ± 0,66; for unaided visual examination, r was
found to be ± 0,57.
11.3 Reproducibility, R
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The reproducibility R is the value below which the absolute difference between two single test results, each
the mean of duplicates, can be expected, with 95 % probability, to lie when this method is used under
reproducibility conditions, i.e. same material but operators in different laboratories. For examination with a
magnifying glass, R was found to be ± 1,09; for unaided visual examination, R was found to be ± 1,12.
12 Test report
The test report shall contain at least the following information:
c) the items of supplementary information referred to in Clause 9, including a reference to the international
or national standard, product specification or other document supplying the information referred to;
f) the results of the test, including the results of the individual determinations, expressed as specified in
Clause 10;
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Annex A
(informative)
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Table A.1 — Correlation between the ISO rating system and the European,
American and Japanese systems
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ISO T-bend
European T-bend American T-bend Japanese T-bend
(subscripts m, p and f used to
(EN 13523-7) b (ASTM D 4145) b (JIS G 3312) b
indicate the method) a
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2 Tm/Tp/Tf
3 Tm/Tp/Tf
4 Tm/Tp/Tf
5 Tm/Tp/Tf
It is recommended that a subscript be added to the symbol T if the result is measured in accordance with a
method other than one of those in this International Standard, viz:
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EN for the European T-bend test;
ASTM for the American T-bend test;
JIS for the Japanese T-bend test.
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Bibliography
[1] ISO 1519, Paints and varnishes — Bend test (cylindrical mandrel)
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[2] ISO 1520, Paints and varnishes — Cupping test
[3] ISO 6272-1, Paints and varnishes — Rapid-deformation (impact resistance) tests — Part 1: Falling-
weight test, large-area indenter
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[4] ISO 6272-2, Paints and varnishes — Rapid-deformation (impact resistance) tests — Part 2: Falling-
weight test, small-area indenter
[5] ISO 6860, Paints and varnishes — Bend test (conical mandrel)
[6] ASTM D 4145, Standard Test Method for Coating Flexibility of Prepainted Sheet
[7]
[8]
(T-bend test)
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EN 13523-7, Coil coated metals — Test methods — Part 7: Resistance to cracking on bending
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