Convenient Functions of GC-2014: Gas Chromatography

LAAN-A-G-E001
SHIMADZU APPLICATION NEWS

● GAS CHROMATOGRAPHY
No. G233
Convenient Functions of GC-2014
The GC-2014, melding the performance and ease-of- market. Here we introduce the convenient functions
operation of our flagship model GC-2010 and the and options of the GC-2014.
flexibility of the GC-14 series, is now available in the
■ Automatic System Startup and Shutdown

The GC-2014 is equipped with AFC as standard, Procedure, the detector gasses are stopped and the
providing automatic control of carrier gas supply in flame is extinguished at automatic shutdown, and
either capillary or packed column analysis, and the following the sleep time interval, the GC can be
temperature of each unit and carrier gas control can started automatically. Additionally, the gas supply is
be started up and shut down automatically. Although a stopped when the detector is turned off or when the
manual flow controller is provided as standard for system is turned off, so that when power is
detector gases, an optional accessory is required to interrupted, such as during a power outage or other
provide automatic flame ignition and extinction at contingency, the solenoid valve closes automatically to
automatic startup and shutdown, respectively. (A shut off the gas supply.
filament for automatic flame ignition is provided as
standard for FID and FPD, however, the detector
gases must be flowing beforehand.)
If detector gas log management is required, installing
APC as in the GC-2010 enables automatic setting of
all gas controls, to say nothing of automatic flame
ignition and extinction. If detector gas flow rate log
management is not required but automatic startup and
shutdown are desired, this can be achieved at very
low cost by connecting a gas shut-off solenoid valve
unit (P/N 221-70782-91) upstream from the detector
gas manual flow controller, as shown in Fig.1. The gas
shut-off solenoid valve unit can control the supply and
shutoff of 2 types of gases (e.g., hydrogen, air). If the
gas shutoff solenoid valve unit is installed, by setting
[Detector=ON], [Auto Ignition=ON] in the GC Startup
Procedure, gas supply is started and ignition is
performed when all the parameters reach their set
values. By setting the [Stop time], [Flow off time] and
[Sleep time] parameters in the GC Shutdown Fig.1 Gas Shutdown Solenoid Valve Unit
Fig.2 GC Startup Procedure, GC Shutdown Procedure

No.G233
To conduct capillary analysis using the model DET

equipped with an injection unit for packed column and
an injection unit for capillary column, a branch tube
Adaptor for Detector Side
adapter can be connected inside the column oven to (with Makeup Gas Line)
the packed column injection unit and the detector Graphite Ferrule
without performing complex tubing changes, as shown Packed
Backring
in Fig.3, and by changing the AFC settings (see Fig.4) INJ
for the unused packed column injection unit, the AFC Washer
can be used for the makeup gas. With this change, not
only can the gas supply be switched on and off, digital Nut
setting of the makeup gas flow rate also becomes
possible. To once again conduct analysis using the
packed column, care must be taken to return the AFC
settings to their original state using the reverse
procedure of that shown in Fig.4, or the packed Fig.3 Structure of Branch pipe
column injection unit will not be included in the LINE
setting.
Press the [FUNC] key on the GC main unit to display the Function screen, and select “6. System Configuration”. In the Configuration screen, select “9. Other System
Configuration” to display the left-hand screen shown above. Use the ' key to move the cursor to the “DAFC Unit” item, and change the setting from [DAFC]→[AMC.LR].
(Right-hand screen above. This changes the dual AFC operation setting from carrier gas flow controller to makeup gas flow controller.)
- Setting parameters from GC Main Unit
In the screen displayed after pressing the [OPTION] key, set the adapter-connected packed column injection port channel (L or R) to ON, and set the flow rate. Then set the
unused channel to OFF.
- Setting parameters using GCsolution
After changing the settings on the GC main unit screen shown above, add the packed column injection port channel (AMC.L or R) to the additional flow of the instrument using
[System Configuration].
Settings and monitoring can be made from the Additional Flow tab.
The packed column injection unit cannot be used in its current condition to conduct packed column analysis. The DAFC unit setting must be returned from AMC.L or R to
DAFC using the reverse procedure of that in the above screen, and then select DAFC as an injection unit for the analysis line. Only one injection unit (AFC) can be selected
for one analysis line. To perform capillary analysis using AFC for SPL to control the carrier gas, two AFCs cannot be selected simultaneously, even if the makeup gas is to be
controlled using DAFC. For that reason, if DAFC is to be used for controlling the makeup gas, set “Not using DAFC as AFC” as in the above screen so that simultaneous
selection can be performed in exceptional cases.
Fig.4 Changing Dual AFC Control Mode
■ Exhaust Duct, High Speed Cooling Unit

One of the installation requirements for the GC-2014 exhausted hot air can be directed upward. With a
is to provide a distance of at least 40cm between the space of 5cm between the rear of the exhaust duct
rear of the instrument and the wall, for a total space and the wall, the required instrument installation space
requirement of about 1m. becomes about 80cm. To improve the cooling
If sufficient space between the rear of the instrument efficiency when the exhaust duct is installed and to
and the wall cannot be secured, there may be a slight shorten the analysis cycle when performing
reduction in cooling speed. However, by using an temperature-programmed analysis, the high speed
exhaust duct (P/N 221-70675-91) (see Fig.5), cooling unit (P/N 221-70676-38) is an effective option.
Fig.5 Exhaust Duct Fig.6 High Speed Cooling Unit
SHIMADZU CORPORATION. International Marketing Division

3. Kanda-Nishikicho 1-chome, Chiyoda-ku, Tokyo 101-8448, Japan Phone: 81(3)3219-5641 Fax. 81(3)3219-5710
Cable Add.:SHIMADZU TOKYO
Printed in Japan 3100-04501-10A-IK

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LAAN-A-G-E001

SHIMADZU APPLICATION NEWS

■ Automatic System Startup and Shutdown

Fig.2 GC Startup Procedure, GC Shutdown Procedure

To conduct capillary analysis using the model DET

Fig.4 Changing Dual AFC Control Mode

■ Exhaust Duct, High Speed Cooling Unit

Fig.5 Exhaust Duct Fig.6 High Speed Cooling Unit

SHIMADZU CORPORATION. International Marketing Division

Printed in Japan 3100-04501-10A-IK

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