Mini-Pour/Cloud Point Tester

Model MPC-102A/102L
Instruction Manual
Ver.2.21 090120

Read this manual thoroughly before using the product,

and store in a safe place for future reference.

TANAKA SCIENTIFIC LTD, TOKYO, JAPAN

 FOREWORD

Thank you for purchasing the Mini-Pour/Cloud Point Tester Model MPC-102A/102L from
Tanaka Scientific Limited.
This instruction manual provides necessary information for using the MPC-102A/102L.
Read this manual thoroughly before use and ensure that you have understood its
contents.
This manual employs the following precautionary notation. For your safety, ensure that
you understand these precautions and heed them at all times.

! WARNING：・・・・・・・・・・
Warnings indicate a significant risk of death or serious
physical injury if the information is ignored.
! CAUTION：・・・・・・・・・・
Cautions indicate a significant risk of physical injury or
property damage if the information is ignored.

USES

! Warning: Use the product only to measure pour points and cloud
points as prescribed under ASTM D6749 "Standard Test
Method for Pour Point of Petroleum Products (Automatic
Air Pressure Method)" and ASTM D2500 "Standard Test
Method for Cloud Point of Petroleum Products".

The product has automated test processes corresponding to those prescribed in ASTM
D6749 "Standard Test Method for Pour Point of Petroleum Products (Automatic Air
Pressure Method)" and ASTM D2500 "Standard Test Method for Cloud Point of
Petroleum Products" for the purpose of obtaining pour points and cloud points only. This
product is not to be used for any other purpose.
 ABOUT THIS INSTRUCTION MANUAL

● This manual is intended for all operators of the MPC-102A/102L.

The reader is assumed to have sufficient knowledge of ASTM procedures and
standards as well as knowledge of the correct handling procedures for hazardous
materials.

● The content this manual is subject to change without notice due to enhancements to
the performance and functionality of the instrument.

● If this manual is lost or damaged, contact Tanaka Scientific Limited or an authorized

distributor for a replacement copy.

● The contents of this manual have been thoroughly reviewed. If any pages are
missing, out of order, or the manual contains spelling, grammatical or descriptive
errors, please contact Tanaka Scientific Limited or an authorized distributor.

BEFORE USE

● Before using the product, ensure that you have read this manual thoroughly and
have understood all of the content. If you have any questions, be sure to contact
Tanaka Scientific Limited or an authorized distributor

● Keep this manual in a safe, easily accessible place.

● This product is to be used for its intended purpose only. Adhere strictly to all
procedures given in this manual.

● Ensure that you understand and abide by all warnings and cautions given in this
manual.

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 WARNINGS AND CAUTIONS FOR SAFE USE

Failure to follow all of the warnings and cautions listed below may result in
damage to the instrument and/or serious personal injury. Tanaka Scientific
Limited will not assume any responsibility for faults or accidents arising from
failure to adhere to these instructions.

Installation Environment

! Warning: The instrument must be installed on a flat, sturdy surface

to prevent the instrument from falling over.

Coolant Circulation Piping

! Caution: Ensure that each joint in the coolant circulation piping is
securely fastened to prevent coolant leakage, as this may
result in instrument failure.

! Caution: Do not use methanol as cooling medium. O-ring of

solenoid valve may have damage and the unit will not work
correctly.
70% of ethylene glycol and 30% of distilled water mixture
will be the best for this unit.

Electrical Connection

! Warning: Observe the following instructions when handling power

cables and electric connections:

・Do not connect or disconnect any cables or electrical

connections when the mains power is ON.
・Do not handle any cables or electrical connections with
wet hands.
・Be sure to use the plug to remove cables. Never use
the cord to pull a plug from an outlet.
・Do not place heavy items on cords or cable.

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 ・Do not use force to bend any cords or cables.
・Ensure that all electric connections (plugs, sockets,
connectors, etc.) are free of dust.
・Keep all cables and electrical connections free of water
and other liquids.

・Failure to adhere to the above precautions may result in

electric shock, damage to the instrument, cords and/or
cables, and/or fire due to overheating.

! Warning: Ensure that supply voltage meets the specifications of the

product. Do not turn the power on until all electric
connections are secured. Incorrect power supply
specifications or loose electric connections may damage
the instrument and result in electric shock and/or other
electrical accidents.

! Warning: Ensure all ground wires are securely grounded.

Loose or disconnected ground wires may result in electric
shock.
Never connect ground wires to gas pipes, as this may
result in fire or an explosion.
Ground wires may be connected to one of the following:

・Ground terminal of a power outlet

・Copper bar buried 65 cm or more underground
・Water pipes as authorized by your local water bureau
as a grounding object

Handling Precautions

! Caution: Never press the START key unless coolant is circulating

normally. Starting the unit with no coolant present may
damage the thermo-module that cools and heats the bath.

! Caution: Ensure that an approximate pour/cloud point is entered

prior to every test run. If an appropriate estimation is not

-3-
 entered or the value entered is much greater than the
actual pour/cloud point, the testing procedure may be
prolonged or produce incorrect results.

Operational Precautions

! Warning: If the instrument makes any abnormal noises or exhibits

any abnormal behavior, stop operation immediately, turn
the power off at the mains, and contact Tanaka Scientific
Limited or an authorized distributor.

Consumables, Accessories and Replacement Parts

! Caution: Use only Tanaka Scientific Limited genuine consumables,

parts and accessories or such parts as recommended by
Tanaka Scientific Limited.

Repairs, Alterations and Maintenance

! Warning: Do not make any modifications or alterations to the

instrument without the approval of Tanaka Scientific
Limited.

! Warning: Do not attempt to repair the instrument yourself. In the

event that the instrument exhibits any abnormal behavior
whatsoever, contact Tanaka Scientific Limited or an
authorized distributor.

! Warning: Only Tanaka Scientific Limited service personnel or

authorized representatives are to repair or maintain the
instrument.

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 Contents
FOREWORD.................................................................................................................................. 0
ABOUT THIS INSTRUCTION MANUAL ........................................................................................ 1
BEFORE USE ................................................................................................................................ 1
WARNINGS AND CAUTIONS FOR SAFE USE ............................................................................ 2
Contents......................................................................................................................................... 5
1. Section Names and Functions ............................................................................................. 6
2. Operational Principles.......................................................................................................... 8
3. Installation............................................................................................................................ 9
3.1. Installation Site .......................................................................................................................... 9
3.2. Connection of the Coolant Circulation Device (MPC-102L Only) .................................... 10
3.3. Electric Connections (See Fig. 4 on page 12) .................................................................... 10
4. Routine Daily Inspection .................................................................................................... 13
5. Prior to Testing .................................................................................................................. 14
5.1. Turning the Power on ............................................................................................................. 14
5.2. Setting the Coolant Temperature (MPC-102L Only) ......................................................... 15
5.3. Specimen Preparation............................................................................................................ 15
5.4. Test Mode Selection ............................................................................................................... 17
5.5. Setting the Expected Pour/Cloud Point ............................................................................... 18
5.6. Preheating Selection .............................................................................................................. 18
5.7. Entering Sample Names ........................................................................................................ 18
6. Test Procedure .................................................................................................................. 20
6.1. Starting a Test ......................................................................................................................... 20
6.2. Automatic Testing Process.................................................................................................... 20
7. Data Storage Functionality................................................................................................. 27
8. Maintenance and Post-sales Servicing .............................................................................. 28
8.1. Periodic Maintenance ............................................................................................................. 28
8.2. Consumables and Accessories............................................................................................. 28
8.3. Troubleshooting....................................................................................................................... 29
8.4. Period of Warranty .................................................................................................................. 29
8.5. Period of Availability of Maintenance Tools ........................................................................ 29
9. Post-delivery Notes............................................................................................................30
9.1. Long Periods of Dormancy .................................................................................................... 30
9.2. Lost Instruction Manuals ........................................................................................................ 30
9.3. Transfer .................................................................................................................................... 30
9.4. Disposal .................................................................................................................................... 30
10. Specifications..................................................................................................................... 31
Product Warranty ......................................................................................................................... 34

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1. Section Names and Functions

Cloud Point Sensor Pour Point Sensor

(Vinyl Tube)
Temperature
Sensor

Detector

Insulator

Display

Control Panel Main Switch

Fig. 1: General View of Model MPC-102A/102L

Main Switch: Turns the instrument on or off.

Control Panel: Keys and switches for operating the device (See Fig. 2 on page 7)
Display: Displays test conditions, instrument state and test results (See Fig. 2 on page
7)
Temperature sensor: Two sensing elements for pour point and cloud point measurements
Pour Point Sensor: Detects flow changes due to changes in pressure on the surface of a specimen.
Cloud Point Sensor: Detects changes in the intensity of light reflected from the bottom of the
specimen cup
Detector: Compound detector assembly containing temperature, PP and CP sensors
Insulator: Prevents condensation around the detector.

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 ④ ⑥

FUNC
① TION
⑨

RUN

COOL
MODE START RESET CHECK ⑪
WARM

② ③ ⑤ ⑦ ⑧ ⑩

Fig. 2: Model MPC-102A/102L Control Panel

① Fluorescent Display: Displays test mode, specimen temperature, pour/cloud point results
(when flashing), and Expected flow point.
② MODE Key: Changes test mode.
③ START Key: Starts testing.
④ RUN Lamp: Indicates when testing is in progress. (Green)
⑤ COOL/WARM Key: Heats the bath.
Note: the device does not provide a cooling function, only a heating function.
⑥ WARM Lamp: Indicates when heating is in progress. (Orange)
⑦ RESET Key: Immediately stops all testing and heating operations.
⑧ CHECK Key: Applies air pressure to the specimen.
⑨ FUNCTION Key: Accesses the function menu.
⑩ Left-Right Arrow Keys: Used to select menu items.
⑪ Up-Down Arrow Keys: Increment or decrement numeric values or to change the value of an item.

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2. Operational Principles

The MPC Series employs Tanaka Scientific's unique air pressure system (certified as U.S. standard
ASTM D 6749) to detect pour points (solidification points). Air pressure is applied to the surface of a
specimen, with subsequent motion of the sample surface measured to detect sample flow.

［System Outline］
The specimen chamber and specimen surface are divided into inner and outer regions by the pressure
conducting tube. Air pressure is applied to the specimen by a pressurizing syringe connected to the
outer region, creating a pressure differential between the inner and outer surfaces of the sample. Two
outcomes are then possible.

Detector
Pressure sensor Head Pressurizing
Syringe
Pressure
conducting
tube
Pressure
Switch Bath
Specimen Specimen
Cup

1. Specimen flow
The pressure differential causes the specimen to flow,
with the surface level inside the pressure conducting Pressure rise detected

tube rising (principle of the U-tube), causing a change in

pressure that is detected by the pressure sensor inside.
Upon a pre-determined pressure change, the pressure ON
switch is activated, indicating to the instrument that the
specimen is still flowing.
<Flow detected ⇒ Test continues>

2. No specimen flow
When the specimen is not flowing, the specimen surface
levels do not change despite the pressure differential. No pressure rise

Thus, the pressure inside the pressure conducting tube

remains unchanged and the pressure switch is not
activated. Specimen flow is assumed to have stopped if OFF
the pressure switch is not activated within five seconds.
<<Non-Flow (solid) detected ⇒ Test completes>

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3. Installation

3.1. Installation Site

! Warning: The instrument must be installed on a flat, sturdy surface

to prevent the instrument from falling over.

Install the instrument on a strong, level bench in a ventilated place.

Do not expose the instrument to any of the following:
・ High temperatures or high humidity
・ Direct sunlight
・ Dust
・ Rapid temperature changes

The instrument is divided into two sections, a test unit and a control unit, with the test unit designed
to sit on top of the control section. However, the units may be separated to allow, for example, the
test unit to be located in a draft chamber (1).
When stacking the measuring and control units, the dripping tray (standard accessory, MPC-102L
only) should be installed between the units. The drip tray protects the control unit and electrical
connections from any water leaking from the test unit or any hose connections.
Ensure that the drip tray is installed in the correct orientation. The side of the tray with no wall
should be located at the rear of the unit. The four protrusions on the bottom of the test unit align
with the four indentations in the top surface of the control unit (see Fig. 3).

Note (1): When operating the units in separate locations, the optional 3-m connection cable
should be used instead of the standard accessory connection cable (0.6 m).

Test unit

Front Rear

Protrusions from drip

Water flows from here

Indentations in control unit

Fig. 3: Drip tray installation (MPC-102L Only)

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3.2. Connection of the Coolant Circulation Device (MPC-102L Only)

! Caution: Do not use methanol as cooling medium. O-ring of

solenoid valve may have damage and the unit will not
work correctly.
70% of ethylene glycol and 30% of distilled water
mixture will be the best for this unit.

! Caution: Do not use methanol as cooling medium. O-ring of

solenoid valve may have damage and the unit will not
work correctly.
70% of ethylene glycol and 30% of distilled water
mixture
will be the best for this unit.

Connect the coolant inlet on the back of the test unit to the pump discharge port of the coolant
circulation device and the coolant outlet to the coolant return side of the coolant circulation device
using the standard accessory coolant circulation hose (with insulation pipe). Secure each connection
port with a hose belt.

3.3. Electric Connections (See Fig. 4 on page 12)

! Warning: Observe the following instructions when handling power

cables and electric connections:

・Do not connect or disconnect any cables or electrical

connections when the mains power is ON.

・Do not handle any cables or electrical connections with

wet hands.

・Be sure to use the plug to remove cables. Never use

the cord to pull a plug from an outlet.
・Do not place heavy items on cords or cable.
・Do not use force to bend any cords or cables.
・Ensure that all electric connections (plugs, sockets,
connectors, etc.) are free of dust.
・Keep all cables and electrical connections free of water
and other liquids.
・Failure to adhere to the above precautions may result

- 10 -
 in electric shock, damage to the instrument, cords
and/or cables, and/or fire due to overheating.

! Warning: Ensure that supply voltage meets the specifications of

the product. Do not turn the power on until all electric
connections are secured. Incorrect power supply
specifications or loose electric connections may damage
the instrument and result in electric shock and/or other
electrical accidents.

! Warning: Ensure all ground wires are securely grounded.

Loose or disconnected ground wires may result in
electric shock.
Never connect ground wires to gas pipes, as this may
result in fire or an explosion.
Ground wires may be connected to one of the following:
・Ground terminal of a power outlet
・Copper bar buried 65 cm or more underground
・Water pipes as authorized by your local water bureau
as a grounding object

(1) Two cables are used to connect the control unit to the test unit (standard 0.6 m or optional 3 m), a
power cable (AC line) and a signal cable (signal line). The sockets for these cables are located on
the rear panels of both units.
(2) Insert the power cable and secure by fastening the lock nut. Insert the signal cable and secure
using the clips on the sides of the plugs. Connect the power cord to the back of the control unit
and to a specified voltage AC outlet rated at 1.5 KVA or more. (2)
The maximum power consumption of this instrument is 0.5 kW. When sharing an outlet with other
electric appliances, ensure that the total power consumption does not exceed the outlet capacity.

Note (2): The standard power cord comes with a three-prong plug. If the plug does not fit your
outlet, you will need to change the plug.
If the outlet is not equipped with a ground terminal, connect the cord to the outlet via the ground
adapter (triangular add-on), ensuring that the instrument is grounded using a ground cord
extension.

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 Coolant outlet

MPC-102L Only

Coolant inlet

MPC-102L Only
OUT IN

Signal cable
Power cable

Circuit

Coolant circulation hose (with insulation pipe)

10 A
Protector
Coolant circulation hose (with insulation pipe)

RS-232C
Connector

Power cord

Coolant circulation device (IN)

(To water drain) AC Outlet

MPC-102L Only
Coolant circulation device (OUT)
(To water tap)

Fig. 4: Rear view of Model MPC-102L

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4. Routine Daily Inspection

The following should be checked routinely before using the instrument:

Table 1 Checklist
Item Check that…

Appearance ・ Housing, cables, hoses, etc. are undamaged

Coolant piping ・ All coolant hoses are free of leaks and other damage
(MPC-102L Only) ・ Each connection is securely fastened
・ There are no indications of coolant leakage
・ Coolant hoses are fully insulated with the insulation pipe
Electrical ・ All power cords and cables are free of damage
connections ・ The power plug is fully inserted into the outlet
・ The grounding cable is properly connected (only applicable if
using the ground adapter)
(After turning the main power on…)
Operation ・ The display appears to be functioning correctly
・ Control panel keys respond appropriately when pressed
・ The Expected pour point has been correctly entered

! Warning: Do not attempt to repair the instrument yourself. In the

event that the instrument exhibits any abnormal behavior
whatsoever, contact Tanaka Scientific Limited or an
authorized distributor.

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5. Prior to Testing

5.1. Turning the Power on

After turning the main power switch on, the display panel should display the main screen shown in Fig.
5: . Pressing the FUNCTION key at this point will give you access to detailed settings, as shown in
Fig. 6: .

SAMPLE TEMP EXP.PP

PP 00.0
L
1.0 23.5 BATH
23.3
Test Mode Preheat (Y/N) Expected Pour/Cloud Point
Current Specimen Temperature Bath Temperature

Fig. 5: Main Display Screen

Test mode: Displays the current testing mode. Test type is shown at the top, pressure
in the middle, and detection interval (in °C) at the bottom.
Current Specimen Temperature: Displays the temperature measured by the pour point temperature
sensor. When a pour point (or a cloud point) is detected, this value will
begin flashing and remain constant until reset.
Preheat (Y/N): Indicates if the specimen is to be preheating before cooling by an arrow
( : Yes, : No).
Bath Temperature: Displays the temperature of the bath (before testing only).
Expected Pour/Cloud Point: The Expected pour point or cloud point entered prior to testing.

Proj 00%
Recv 00% PP Sensor 23.5
Prev CP CP Sensor 23.6
Prev PP -37.5 Bath 23.3
Received light intensity Previous result Current temperature

Fig. 6: Details Screen

Light Intensity: Displays the fraction of light reflected from the bottom of the specimen
cup to the cloud point sensor.
Previous Results: Shows the last measured pour and cloud points. The data is updated
each time a test is completed.
Current Temperature: Displays the current temperatures at the pour point, cloud point and bath
sensors.

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5.2. Setting the Coolant Temperature (MPC-102L Only)

! Caution: Never press the START key unless coolant is circulating

normally. Starting the unit with no coolant present may
damage the thermo-module that cools and heats the
bath.

Start the coolant circulation device and enter a temperature (refer to the Coolant Circulation Device
Instruction Manual). Since the lower limit of the measuring range of the instrument depends on the
coolant temperature (see Table 2), ensure that you have selected the correct temperature for the
specimen you are testing.
Table 2 Coolant Circulation Device Set Temperature
Coolant circulation device set
Measuring range
temperature
0℃ ＋51℃ to -40℃

-40℃ ＋51℃ to -65℃

5.3. Specimen Preparation

Compound
Detector

O Ring

Cloud point sensor Pressure conducting tube

(Light guide)
Temperature sensor

Metallic tip

Fig. 7 Cross Section of the Detector Assembly

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(1) The specimen cup and pressure conducting tube should be removed from the detector, cleaned
with an appropriate solvent and dried prior to use. Wipe any oil from the temperature and cloud
point sensors with a tissue or a waste cloth.
(2) With the metallic tip facing away from the detector assembly, insert the pressure conducting tube
into the hole in the detector around the temperature sensor (see Fig. 7)
(3) Fill the specimen cup with specimen up to the reference mark and insert into the bath.
(4) Insert the detector assembly into the bath vertically, taking care not to knock the cloud point
sensor or pressure conducting tube against the specimen cup. The detector assembly should
then be screwed securely into place. Be careful not to twist the wires between the detector and
main unit.
(5) Finally, fix the insulation pad in place to prevent problems arising from condensation during
testing

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5.4. Test Mode Selection
The instrument contains 25 preset test modes, which are combinations of test type, pressure and
detection interval (see Fig. 8).
Selecting the correct mode can be time consuming, and so the test modes that are available to
users can be customized (refer to the attached Maintenance Manual for more information).

The MODE key is used to select from the available test modes. While holding the MODE key down,
press either the left arrow or right arrow keys to cycle backwards or forwards through the available
modes.

The following preset test modes are available:

1 PP/CP L 1.0
Test type 2 PP/CP L 2.5
PP/CP: Simultaneous cloud point and pour point testing 3 PP/CP L 3.0
4 PP/CP H 1.0
PP : Pour point testing only
5 PP/CP H 2.5
CP : Cloud point testing only 6 PP/CP H 3.0
7 PP L 1.0
8 PP L 2.5
Pressure: Air pressure used in pour point detection
9 PP L 3.0
Not applicable to test type CP. 10 PP H 1.0
In the ascending order of pressure, the options are L, H, VH and UH. 11 PP H 2.5
L : For specimens such as gas oil that loses fluidity as wax precipitates 12 PP H 3.0
13 PP/CP VH 1.0
H : For specimens such as lubricants that loses fluidity as viscosity
14 PP/CP VH 2.5
increases 15 PP/CP VH 3.0
VH: Primarily for lubricants that contains additives more than a fixed 16 PP/CP UH 1.0
17 PP/CP UH 2.5
quantity.
18 PP/CP UH 3.0
UH: Primarily for heavy fuel oils, like bunker C (No.6 fuel oil). 19 PP VH 1.0
20 PP VH 2.5
Note : If the sample shows the result that higher than you expected, 21 PP VH 3.0
22 PP UH 1.0
please try the test again with higher pressure mode.
23 PP UH 2.5
24 PP UH 3.0
Detection interval: Temperature interval (°C) used in pour point detection 25 CP

1.0: Detection at every 1.0°C from 15°C above the Expected pour point Fig. 8 Preset Test Modes
2.5: Detection at every 2.5°C from 15°C above the Expected pour point
3.0: Detection at every 3.0°C from 15°C avove the Expected pour point
Cloud point detection intervals are fixed at 0.1°C* or 1.0°C in PP/CP and
CP test types. For changing interval, refer to the Maintenance Manual.

Note : CP detection of 0.1°C is applicable from firmware ver.2.2

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5.5. Setting the Expected Pour/Cloud Point

! Caution: Ensure that an approximate pour/cloud point is entered

prior to every test run. If an appropriate estimation is not
entered or the value entered is much greater than the
actual pour/cloud point, the testing procedure may be
prolonged or produce incorrect results.

In this instrument, the entry of an Expected pour/cloud point is essential. Be sure to enter an
appropriate value prior to each test. For PP/CP and PP tests, the estimate refers to the pour point,
while in CP tests, the estimate refers to the cloud point.
The Expected cloud/pour point display field in the upper right of the main screen (see Fig. 5 on page
14) consists of five individual fields for input purposes, the sign, a 2-digit integer, the decimal point,
and a single decimal place. Move the cursor (displayed as an underscore) using the left or right arrow
keys and increment or decrement the value of the selected digit using the up and down arrow keys
(the sign field alternates between blank for positive and - for negative).
The maximum value that can be set is 51.0.
When CP test with 1.0°C interval is chosen, the value of the decimal place is ignored, with only the
integer value being of significance. To avoid any confusion, it is suggested that an integral value is
entered in these situations.
If nothing at all is known about the pour or cloud points, it is better to choose a low value. Although
this will result in long measurement times, the results will be accurate.

5.6. Preheating Selection

Preheating refers to heating the specimen to 45°C once before cooling (refer to ASTM D97). As with
the Expected pour/cloud point, this setting should be reviewed prior to each test.
An arrow on the left of the Expected pour/cloud point display indicates if preheating is selected.
" " indicates preheating and " " indicates no preheating. To change this setting, move the cursor
(underscore) with the left and right arrow keys to the preheating arrow and change the setting with
the up or down key.
Preheating should be selected in the Expected pour/cloud point is higher than room temperature.

5.7. Entering Sample Names

To enable sample name input, the instrument must be configured in advance as described in the
attached Maintenance Manual.
When sample name input is enabled, the Sample Name Input Screen (Fig.9 on page 19) may be
accessed by repeatedly pressing the FUNCTION key until the screen is displayed. The order in which

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 the display cycles with each press of the FUNCTION key is:
Main Display Screen → Details Screen → Sample Name Input Screen → Main Display Screen

When specimen name input is disabled, the Sample Name Input Screen cannot be accessed by pressing
the FUNCTION key.
Be sure to enter the specimen name prior to testing. The cursor can be moved with the left and right
arrow keys, and individual characters changed using the up and down arrow keys.

Sample
AAAAAA

Sample name
Fig. 9 Sample Name Input Screen

Sample names can consist of up to six characters, with characters being one of the following 59
characters.
Each unit is initialized to AAAAAA prior to shipping.

A B C D E F G H I J K L M

N O P Q R S T U V W X Y Z

! “ # $ % & ‘ ( ) * + ,

- . / 0 1 2 3 4 5 6 7 8 9

: ; < = > ? @

After testing, the sample name is automatically stored in the data list with the test result (see
Section 7 Data Storage Function on page 27).
When a printer is connected, the sample name is printed with the test result.

This completes the test preparations.

For safety reasons, each step should be confirmed before starting a test.

- 19 -
6. Test Procedure

6.1. Starting a Test

! Warning: If the instrument makes any abnormal noises or exhibits any

abnormal behavior, stop operation immediately, turn the
power off at the mains, and contact Tanaka Scientific Limited
or an authorized distributor.

Press the START key (3). The RUN lamp will come on, the Expected pour/cloud point is displayed in
the specimen temperature field for three seconds, and testing begins (4).

Note (3)：The START key is disabled while the Details Screen or Sample Name Input Screen are
being displayed. Use the FUNCTION key to cycle through to the main screen before
pressing the START key.

Note (4)：Once testing has begun, test mode, preheating, and Expected pour/cloud point settings
cannot be changed. To change settings, press the RESET key to abort the current test.

From this point, testing proceeds automatically. An explanation of the automatic testing procedure follows.

6.2. Automatic Testing Process

6.2.1. Preheating

※ This process is skipped if preheating is not selected (" " displayed in the preheating display field).

During preheating, both the RUN and WARM lamps will light up and bath heating begins (5).
When the bath has reached the temperature set out below, the WARM lamp extinguishes and
bath cooling begins (5).

<Expected pour/cloud point of over 35.0°C>

The bath is heated to a temperature of "Expected pour/cloud point + 13°C". When the specimen
temperature is 10°C above the Expected pour/cloud point, cooling begins.
<Expected pour/cloud point under 35.0°C>
The bath is heated to 48°C. When the specimen temperature reaches 45°C, cooling begins.

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 Note (5)：The level of cooling/heating is indicated by a red LED at the upper right of the test unit.
The led is continuously lit to indicate full output (100%), extinguished to indicate no output
(0%), and flashes to indicate any intermediate output levels. As the output level is nearly
always changing, the led is almost always flashing. If the lamp remains dark for an
extended period of time, the thermo-module connections may be faulty.

6.2.2. Light Intensity Measurement Check

※ This step is only applicable to cloud point testing modes (“CP” or “PP/CP” displayed in the test
mode field).

Immediately upon starting the test, the intensity of light incident upon the cloud point sensor is
measured and displayed in the EXP.PP field. This is done during the three seconds that the
Expected pour/cloud point is displayed in the current specimen temperature field.
After three seconds, the current specimen temperature and EXP.PP fields return to normal (6),
with the bath temperature field displaying the following information depending on test mode:
Test mode PP/CP ⇒ The cloud point temperature sensor temperature is displayed (
Fig. 10 ).
Test mode PP or CP ⇒ The field is blank.
Note (6): During testing operations, the value displayed in the EXP.PP field can be toggled between
Expected pour point and current cloud point sensor temperature by pressing either the up
or down arrow key.

SAMPLE TEMP EXP.PP

PP/CP -25.0
L
1. 0 -12.3 CP
-13.0
Cloud point temperature

Fig. 10 Cloud Point Temperature Display (Test mode PP/CP only)

If the intensity of light measured by the cloud point sensor is not in the range of 10% to 90%, the
cloud point cannot be tested and the following error messages are displayed:
Test mode PP/CP ⇒ TRBL is displayed in the cloud point temperature field, but pour point testing
continues (see Fig. 11 on page 22).
Test mode CP ⇒ The test ends, and the error message shown in Fig. 12 on page 22 is
displayed.

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 The intensity of light measured will not fall within the specified range if the sensor is faulty, the
detector is incorrectly set, or there is a problem with the specimen. If the error message continues
despite the sensor functioning correctly and being correctly setup, the specimen itself is the
problem, and cannot be tested using this instrument.

SAMPLE TEMP EXP.PP

PP/CP -25.0
L
1. 0 -12.3 CP
TRBL Trouble

Fig. 11 Cloud Point Test Failure Display (Test mode PP/CP)

TROUBLE No.01

PHOTO SYSTEM

Fig. 12 Cloud Point Test Failure Display (Test mode CP)

6.2.3. Air Leak Check

※ This step is only applicable to pour point testing modes (“PP” or “PP/CP” displayed in the test
mode field).

The pour point sensor is checked for air leaks immediately after preheating, if preheating is
enabled, or three seconds after test start otherwise.
If any leaks are found, the test is aborted and the error message shown in Fig. 13 is displayed.

TROUBLE No.09

PRESSURE LEAK

Fig. 13: Air Leak Detected

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6.2.4. Cooling
The bath is cooled at preset rates, with different rates used above and below the switching
temperature of 40°C (7) above the Expected pour point. The product is shipped to cool at a rate of
4°C/min (7) until the switching temperature is reached and at a rate of 1°C/min (7) thereafter.
Note (7): For instructions on changing bath cooling rates and switching temperature, refer to the
attached Maintenance Manual.

6.2.5. Pour Point Detection Starting Temperature

※ This step is only applicable to pour point testing modes (“PP” or “PP/CP” displayed in the test
mode field).

When the specimen temperature has reached a prescribed temperature (8), the first pour point
detection attempt begins. Detection is repeated at the detection interval chosen prior to testing,
which is shown in the test mode field.
Note (8): Pour point detection start temperature depends on the Expected pour point. If the
Expected pour point is below 30.0°C, a starting temperature of 15 above the Expected pour
point is used, otherwise a starting temperature somewhere in the range of 9°C to 14°C
above the Expected pour point is used.

If the pour point is detected in the first detection attempt, the test ends with the error message
shown in Fig. 15. In this case, a higher value of Expected pour point should be entered and the
test retried.

TROUBLE No.08

PP OVER > -10

Fig. 14: First Attempt for Pour Point Detection

Example error message that is displayed when the Expected pour point is set to -25.0 but the pour
point is detected on the first attempt at a temperature of -10.0°C.

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6.2.6. Cloud Point Detection

※ This step is only applicable to cloud point testing modes (“CP” or “PP/CP” displayed in the test
mode field).

The cloud point is detected when the intensity of light measured at the bottom of the specimen cup
drops due to clouding. Cloud point detection occurs at 0.1oC interval or integer values of
temperature as the temperature drops. When 1.0oC interval is selected, the reported cloud point is
the next lower integer. For example, MPC reports cloud point -13.2oC in 0.1oC interval, and then
-14.0oC in 1.0oC interval.
After cloud point detection, will be as follows:
Test mode PP/CP ⇒ The result flashes in the cloud point temperature field (see Fig. 15) (9) while
pour point detection continues.
Test mode CP ⇒ The result flashes in the current specimen temperature field (see Fig. 16) (9).
The RUN lamp is extinguished and a buzzer sounds intermittently for 8 seconds.

SAMPLE TEMP EXP.PP

PP/CP -25.0
L
1.0 -19.3 CP
-19.0
Decreasing Flashing

Fig. 15: Cloud Point Detection (Test mode CP/PP)

CLOUD POINT EXP.CP

CP -15.0

-19.0 FAST
Flashing
Appears when a CP is detected
in fast cooling sequence.

Fig. 16: Cloud Point Detection (Test mode CP)

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6.2.7. Pour Point Detection

※ This step is only applicable to pour point testing modes (“PP” or “PP/CP” displayed in the test
mode field).

When specimen flow is found to have stopped (see Section 2 on page8), the pour point
temperature flashes in the current specimen temperature field (see Figure 17 and see Figure 18)
(9). The RUN lamp is extinguished and a buzzer sounds intermittently for 8 seconds.

SAMPLE TEMP EXP.PP

PP/CP -25.0
L
1. 0 -25.0 CP
-19.0
Flashing Flashing

Fig. 17: Pour Point Detection (Test mode PP/CP)

SAMPLE TEMP EXP.PP

PP -25.0
L
1. 0 -25.0
Flashing

Fig. 18: Pour Point Detection (Test mode PP)

Note (9): Measured cloud points and pour points are displayed until either the RESET or START
key is pressed. Upon pressing either the RESET or START keys, the results are cleared
from the display, which returns to normal, and are stored in the last test results fields,
which can be seen in the details screen.

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6.2.8. Data Printouts

※ This step is only applicable if an optional printer is connected.

After pour/cloud point detection, the Expected pour/cloud point and measured point are
automatically printed. To print detailed experimental information, such as such as specimen
temperature and pressurization times during testing, press the START key once after the
summary data has printed (10).
Note, however, that data cannot be printed after the RESET key has been pressed.

Note (10): The instrument can be modified to automatically print detailed experimental data after
every test run. For details, refer to the Maintenance Manual.

6.2.9. Bath Heating

After pour/cloud point detection, bath heating begins to return the specimen to room
temperature (WARM lamp lights) (11)The bath is heated quickly to a temperature of 20°C (12)and
held at that temperature for 3 minutes (12). To stop the heating process, press the RESET key.
Note that this will also clear the test results from the display. After the specified time of 3 minutes,
the WARM lamp is extinguished, heating stops and a buzzer sounds intermittently for 8 seconds.
To begin heating after heating has finished or been aborted, press the WARM key.

Note (11)：If the bath temperature is over 20°C when testing completes, the WARM lamp turns on,
but no heating is performed. This continues for 3 minutes.

Note (12)：Both the temperature and duration of heating can be modified. For details, refer to the
Maintenance Manual.

This completes the automatic testing process.

To perform another test, return to Part 5.3: Specimen Preparation on page 15.
To finish using the instrument, simply turn off the main switch.

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7. Data Storage Functionality

This instrument has the capacity to automatically store the results of the last 50 tests.
To access the results history, press and release the RESET key while holding down the MODE key.
The Test History Screen shown in Fig. 19 is displayed.
The most recent test results are always shown as data No.1, with data id numbers in increments of
one. Data recorded more than 50 test runs ago is discarded. Result sets can be scrolled through by
pressing the up and down arrow keys.

No.1 DATE:03/02/13 11:15

Latest data Sample: UVWXYZ
MODE:PP/CP , L,1.0
PP:-28.0 CP:-10.0

No.30 DATE:02/12/12 16:24

Oldest data Sample: AAAAAA
MODE:PP ,UH,3.0
PP:- 6.0 CP:

Fig. 19 Test History Screen

If the optional clock card is not installed, the date and time fields will all show 01/01/01 01:01.
The specimen name field always shows a value, even when specimen name input is disabled. (In this
case AAAAAA will typically be displayed as it is the default value).
If the optional printer is connected, pressing the FUNCTION key will print the entire test history.

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8. Maintenance and Post-sales Servicing

8.1. Periodic Maintenance

This instrument is fully inspected and calibrated prior to shipping, and should require no readjustment
immediately upon delivery.
To ensure high performance and maximum safety, however, the instrument needs to be maintained
and adjusted periodically. For more details on maintenance and recalibration techniques, refer to the
attached Maintenance Manual.

8.2. Consumables and Accessories

! Caution: Use only Tanaka Scientific Limited genuine

consumables, parts and accessories or such parts as
recommended by Tanaka Scientific Limited.

For orders and inquiries about consumables, parts and accessories for this instrument, contact
Tanaka Scientific Limited or an authorized distributor. Contact details are provided with the product
warranty at the end of this manual.
When placing an order, be sure to quote the product model "MPC-102A" or “MPC-102L”.
The most commonly used consumables and accessories are listed in Table 3

Table 3: Consumables and Accessories for Model MPC-102A/102L

・ Compound detector
・ Specimen Cup with Reflex Seal
・ Reflex Seal
・ Pressure Conducting Tube
・ O-Ring G-35 (cooling bath flange)
・ O-Ring P-8 (to secure pressure conducting
tube)

For details on replacing consumables, refer to the Maintenance Manual.

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8.3. Troubleshooting

! Warning: Do not make any modifications or alterations to the

instrument without the approval of Tanaka Scientific
Limited.

! Warning: Do not attempt to repair the instrument yourself. In the

event that the instrument exhibits any abnormal
behavior whatsoever, contact Tanaka Scientific Limited
or an authorized distributor.

! Warning: Only Tanaka Scientific Limited service personnel or

authorized representatives are to repair or maintain the
instrument.

Should the instrument become faulty, contact Tanaka Scientific Limited or an authorized distributor.
Contact details are provided with the product warranty at the end of this manual.
Provide as much information as possible about the problem.
Equipment failures will be resolved in one of three ways:

1. Tanaka Scientific Limited will send a replacement part to the local distributor or directly to the
customer. The user or local distributor executes replacements and inspections.
2. The customer will need to send part or all of the faulty equipment to Tanaka Scientific Limited for
repairs.
In some metropolitan areas, our sales staff may pickup the equipment from the customer.

To troubleshoot simple problems, refer to the attached Maintenance Manual.

8.4. Period of Warranty

This instrument will be guaranteed for a period of one year from the date of delivery.
For details, see the Product Warranty at the end of this manual.

8.5. Period of Availability of Maintenance Tools

The tools and parts necessary for maintenance of this instrument are guaranteed to be held by
Tanaka Scientific Limited for a period of five years from the date of delivery of the instrument.

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9. Post-delivery Notes

9.1. Long Periods of Dormancy

When the instrument is not used for a long period of time, unplug the power cord from the
outlet.
It is recommended that the instrument is covered when in storage to reduce the impact of dust
and moisture.

9.2. Lost Instruction Manuals

This manual and the Maintenance Manual are part of the instrument. Should you lose either
manual, contact Tanaka Scientific Limited or an authorized distributor for a new copy.
For safety, keep a copy of the address and telephone number of Tanaka Scientific Limited or
an authorized distributor.

9.3. Transfer
When transferring this instrument to a third party, be sure to contact Tanaka Scientific Limited
if the voltage or frequency of the power supply needs to be changed.
Be sure to transfer the instrument with this manual and the Maintenance Manual.

9.4. Disposal
This instrument does not contain any hazardous materials, and can be disposed of as ordinary
industrial waste.

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10. Specifications
Related Specifications: Pour point test standards: ASTM D 6749, D97, ISO 3016
Cloud point test standards: ASTM D 2500, ISO 3015
Type: Bench Top, Air cooled (MPC-102A) or Liquid cooled (MPC-102L), Single position
Testing Limitations: MPC-102A 51°C to -30°C (at room temperature: 20°C)
PC-102L 51°C to -65°C (when -35°C coolant is circulated using the optional
Coolant Circulation Device TCU-40)
51°C to -40°C (with tap water)
Built-In Testing Modes: 25 built-in modes
Preheating System: Built-in preheating function for heating the bath to either 45°C or "10°C above the
Expected pour/cloud point", whichever is higher, before cooling
Program Control System: Sequence control by microcomputer
Display Type: Fluorescent display (VFD module). Temperature display: Units of 0.1°C
Temperature Sensor: Platinum resistance sensor, 100Ω/0°C (Pt100)
Detector Unit: Compound detector (Temperature sensor, pour point sensor, and cloud point
sensor assembled in a resin detector housing)
Temperature Sensor: Platinum resistance thermometer sensor consisting of two stainless sheath
elements 100Ω/0°C (PT100)
Pour Point Sensor: Detection Method: Changes in the specimen surface by applying fine pressure
via a pressure conducting tube detected by a pressure switch (micro pressure
sensor) (Patented)
Air Pressure System: A pressurizing syringe and solenoid valve
Testing Intervals: Every 1°C, 2.5°C, or 3°C (Selection by mode)
Cloud point sensor: Detection Method: Detects light reflected from a reflector located on the bottom
of the specimen cup
Photoelectric detector: Consists of a LED, phototransistor, and light-receiving
amplifier
Testing Interval: Every 1°C or 0.1°C (selectable)
Testing Container: Flat-bottom borosilicate-1 (∅21×45L) specimen cup with a reference mark for
4-ml specimen
Reflection seal attach to the bottom for cloud point detection
Temperature Control Unit: Structure: Aluminum block cooled with Peltier cooler
Cooling rate: Separate setting from 1 to 5 °C/min (in increments of 1 °C/min) for
temperatures above and below a switching temperature(13). Depending on
temperature range and radiation efficiency, actual cooling rates may be lower
than selected. The instrument is shipped with cooling rates of 4 °C /min above
the switching temperature and 1°C /min below.
Note(13)：The cooling rate switching temperature can be changed relative to the Expected

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 pour/cloud point. At shipping, the switching temperature is set to 40°C above the
Expected pour/cloud point.
Safety and self-diagnosis systems:
1. If the temperature on the hot side of the Peltier cooler exceeds 60°C,
a warning buzzer sounds and the power supply is automatically cut to
prevent fire hazards.
2. The following error conditions are automatically detected, and
displayed on the main screen, accompanied by an intermittent buzzer:
・ Temperature sensor line cuts are detected.
・ The intensity of light detected by the cloud point detection sensor is
incorrect.
・ The internal battery that maintains internal memory settings is
getting flat. (Tested at power-on only)
3. Computer runaway (Buzzer sounding only)
・ Some kind of circuit failure is detected.
Data Outputs: Supporting LAS RS-232C × 1ch (standard)
Remarks: One additional channel available as an option (program
alteration necessary).
Power Supply: 100/120 or 220/240 VAC (Factory setted) 50/60 Hz 0.5 kW
Dimensions and Weights: Control unit: W230×D455×H110 mm Approx. 6.0 kg
Test unit: W230×D480×H275 mm Approx. 18.0 kg
Minimum Footprint: W300×D550 mm
Standard Accessories:
Specimen Cup with Reflex Seal ································································································· 5 pcs
Insulator Pad ······························································································································ 1 pc
Spare Pressure Conducting Tube ······························································································ 1 pc
AC Power Cord ························································································································· 1 pc
Connection cable (power) 0.6m ································································································· 1 pc
Connection cable (signal) 0.6m·································································································· 1 pc
Instruction manual ······················································································································ 1 copy
Maintenance manual ·················································································································· 1 copy
<Above common to MPC-102A and MPC-102L>

Coolant circulation hose ∅10×∅14 2m [with insulation pipe] ···················································· 2 pcs

Hose Clamps ······························································································································ 4 pcs
Dripping plate ····························································································································· 1 pc
<Above for MPC-102L only>

- 32 -
Optional Accessories:
・ Extension cables (power and signal) 3m
⇒ For use when the control unit and test unit are located separately

・ Printer Model BS2-80TS made by Sanei Electric (connected to the

RS-232C output port)
⇒ Prints pour/cloud point test results and Expected pour/cloud points
Paper Size: 80 mm wide, ∅38 mm, 15 m long (Paper Roll)
One roll can store 250 tests
(No details printed in PP/CP mode)
Power Supply: AC Adapter Input: 100-120or 220-240 VAC,
50/60 Hz, 20 W max
Output: DC 6V, 1500 mA
Dimensions and Weight: 134(W) x 60(H) x 180(D)mm/ approx. 450g
Included Parts: Connection cable……….1 m
Paper Roll………………. 1 roll

・ Clock board (Mounted on the main board in the control unit)

⇒ Necessary for printing test dates and times when the printer is
connected

・Coolant circulation device for MPC-102L (Recommended by Tanaka Scientific Limited)

Model : TCU-40 Ultra-low temperature bath circulator made by Tanaka Scientific Limited.
Bath Capacity: Approx. 8.0L
Power Supply: 120 or 220-240 VAC 50/60 Hz 500W
Dimensions and Weight: 320(W) x 590(D) x 725(H) mm Approx. 60.0 kg

・Water pressure regulator with pressure gauge: Necessary when a tap water line is connected
instead of coolant circulation device(s).
*Pressure regulator: Pressure regulator valve with a lock
*Pressure gauge: 0-400kPa. (Normally set at 50kPa.)

- 33 -
 Product Warranty

1. This product has passed a quality assurance inspection to the standards of Tanaka Scientific
Limited.
2. This product will be warranted for a period of one year from the date of delivery.
To avoid later confusion, be sure to enter the date of delivery in warranty ticket below.
3. If any faults occur due to normal use within the warranty, the product will be repaired free of
charge.
4. Be sure to notify Tanaka Scientific Limited when repairs being requested are covered under the
warranty.
5. The following faults or damage are not covered by the warranty:
・ Any fault or damage arising from failure to adhere to all warnings and precaution as described
in the instruction manual
・ Any fault or damage arising from misuse or carelessness
・ Any fault or damage arising from repairs or alterations unauthorized by Tanaka Scientific
Limited
・ Any fault or damage arising from falls or accidents during transportation after the initial
delivery
・ Any fault or damage arising from external causes, such as fire, act of God (earthquake, storm,
or flood), environmental contamination, or power supply variations
6. All other repairs, consumables and accessories are chargeable.

Product Name Mini-Pour/Cloud Point Tester

Control unit (MPC-102-C) No.

Model Name MPC-102 Serial No. Test unit (MPC-102L-T or MPC-102A-T)
No.
Warranty
One year from the date of delivery:
Period

Manufactured and sold by: Tanaka Scientific Limited

Contact: 7-10-3, Ayase, Adachi-ku, Tokyo 120-0005
T E L：+81-3-3620-1711
F A X：+81-3-3620-1713
E - m a i l：sales@tanaka-sci.com
Distributor:

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