Applied Sciences: Artificial Intelligence-Based Model For The Prediction of Dynamic Modulus of Stone Mastic Asphalt
Applied Sciences: Artificial Intelligence-Based Model For The Prediction of Dynamic Modulus of Stone Mastic Asphalt
Applied Sciences: Artificial Intelligence-Based Model For The Prediction of Dynamic Modulus of Stone Mastic Asphalt
sciences
Article
Artificial Intelligence-Based Model for the Prediction
of Dynamic Modulus of Stone Mastic Asphalt
Thanh-Hai Le 1 , Hoang-Long Nguyen 1, *, Binh Thai Pham 1 , May Huu Nguyen 1 ,
Cao-Thang Pham 2 , Ngoc-Lan Nguyen 3 , Tien-Thinh Le 4, * and Hai-Bang Ly 1, *
1 University of Transport Technology, Hanoi 100000, Vietnam; hailt@utt.edu.vn (T.-H.L.);
binhpt@utt.edu.vn (B.T.P.); maynh@utt.edu.vn (M.H.N.)
2 Le Quy Don Technical University, Hanoi 100000, Vietnam; caothang.cdsb@gmail.com
3 University of Transport and Communications, Hanoi 100000, Vietnam; nguyenngoclan@utc.edu.vn
4 Institute of Research and Development, Duy Tan University, Da Nang 550000, Vietnam
* Correspondence: longnh@utt.edu.vn (H.-L.N.); letienthinh@duytan.edu.vn (T.-T.L.);
banglh@utt.edu.vn (H.-B.L.)
Received: 1 July 2020; Accepted: 26 July 2020; Published: 29 July 2020
Abstract: Stone Mastic Asphalt (SMA) is a tough, stable, rut-resistant mixture that takes advantage
of the stone-to-stone contact to provide strength and durability for the material. Besides, the warm
mix asphalt (WMA) technology allows reducing emissions and energy consumption by reducing
the production temperature by 30–50 ◦ C, compared to conventional hot mix asphalt technology
(HMA). The dynamic modulus |E*| has been acknowledged as a vital material property in the
mechanistic-empirical design and analysis and further reflects the strains and displacements of such
layered pavement structures. The objective of this study is twofold, aiming at favoring the potential
use of SMA with WMA technique. To this aim, first, laboratory tests were conducted to compare the
performance of SMA and HMA through the dynamic modulus. Second, an advanced hybrid artificial
intelligence technique to accurately predict the dynamic modulus of asphalt mixtures was developed.
This hybrid model (ANN-TLBO) was based on an Artificial Neural Network (ANN) algorithm and
Teaching Learning Based Optimization (TLBO) technique. A database containing the as-obtained
experimental tests (96 data) was used for the development and assessment of the ANN-TLBO model.
The experimental results showed that SMA mixtures exhibited higher values of the dynamic modulus
|E*| than HMA, and the WMA technology increased the dynamic modulus values compared with
the hot technology. Furthermore, the proposed hybrid algorithm could successfully predict the
dynamic modulus with remarkable values of R2 of 0.989 and 0.985 for the training and testing datasets,
respectively. Lastly, the effects of temperature and frequency on the dynamic modulus were evaluated
and discussed.
Keywords: stone mastic asphalt; warm mix asphalt; hot mix asphalt; dynamic modulus; artificial
neural network; teaching–learning-based optimization
1. Introduction
In recent decades, the manufacture and application of asphalt mixture have been significantly
increasing because of excellent adhesion to mineral aggregates and viscoelastic properties [1,2]. In order
to address economic and environmental objectives, a number of asphalt mixtures were proposed,
including dense-graded asphalt concrete, stone mastic asphalt (SMA), rubberized asphalt, crumb rubber
asphalt concrete, and asphalt concrete incorporated [3–5]. Additionally, from a practical viewpoint,
mixing techniques were also considered as an important stage for an asphalt mixture, gaining its
targeted performances [3,4,6,7]. Among these, dense-graded asphalt and stone mastic asphalt (SMA)
mixtures applying the hot (HMA) and warm (WMA) mixing techniques are two typical applications of
asphalt mixtures that received more attention from researchers [4,8–10].
Historically, hot mix asphalt (HMA) has been the most popular paving material for
roadways [11–15]. The mechanism of this technology is based on high temperatures during mixing
and compaction stages to ensure the workability and achieve the desired in-place density of the
asphalt mixture. However, HMA mixtures disclosure some notable defects, such as high energy
consumption, significant greenhouse gas emissions, hazardous fume, and unpleasant odors [12].
In addition, the high-temperature requirement and relatively longer cooling periods somehow limit its
applicability, especially for high volume roadways built with heat-sensitive polymer modified mixes.
Adapting with the need to reduce resource consumption and environmental emissions, Warm Mix
Asphalt (WMA) has gradually been acknowledged as a promising technology in the pavement structure.
This technique includes several notable advantages in the environmental aspect as well as enhances the
characteristics of asphalt binders and mixtures [4,9,12,16,17]. This technology can significantly reduce
the temperature of asphalt mixtures for the mixing and compacting processes by lowering the viscosity
and casing foaming in the asphalt binders. The energy required to produce WMA decreases emissions
and odors from plants and hence creates a better working condition at the plant and the paving
site [18,19]. In this technique, emissions and energy consumption can be significantly reduced due to its
necessary mix temperature lower 30–50 ◦ C compared to conventional HMA [11,16]. These features lead
to numerous benefits in several respects of WMA productions, such as environmental (reduced factory
emissions), cost-effective, production, and paving process (increased workability and compaction
performance) [4,16,17,20,21]. So far, it is quite acceptable to state that WMA is a potential solution that
can balance environmental and performance objectives [3].
Indeed, the changes in features of asphalt mixtures (HMA or SMA) in cases of HMA or WMA
techniques can be reflected through several characteristics, including chemical, physic-mechanical
properties, and durability [3,14,16,17,21]. Among these characteristics, dynamic modulus, |E*|, has not
only been increasingly acknowledged as a vital material property in mechanistic-empirical design
and analysis [22] but has further reflected the pavement structures (e.g., strain and displacement)
caused by loading rate and temperature [23,24]. It is a primary property determined in the superpave
simple performance method protocol that supplements the design of volumetric. Besides, the dynamic
modulus |E*| plays a vital role as an essential linear viscoelastic characteristic that can be employed
in asphalt mixtures and pavements models [25]. In other words, the dynamic modulus |E*| can be
employed as a useful index to evaluate the effectiveness of the mixing technologies.
Various approaches have been, therefore, proposed for predicting the dynamic modulus |E*|
utilizing regression analysis based on laboratory measurements [7,22,26–28], modification of existing
predictive equation in AASHTOWare [29], or Artificial Intelligence (AI) methods [25,30–33]. The most
commonly used comprehensive and scientific approach, in terms of laboratory measurements,
is related to a mechanistic approach, namely Mechanistic-Empirical Pavement Design Guide (MEPDG).
This approach recommended the determination of the dynamic modulus at three levels [34]. However,
the experimental part might not always be possible due to the lack of facilities or equipment. Besides,
several models have been presented to overcome these difficulties, especially those proposed in
the works of Witczak 1999 [35], Witczak 2006 [22], Hirsch [36], and Al-Khateeb [37]. Even though
these models have been roughly validated, the effectiveness is still being questioned, owing to the
variation of predicted results for different asphalt mixtures [22,38–44]. In addition, several studies have
found that these models sometimes seem to overemphasize the effect of temperature, other mixture
properties, or overpredict the dynamic modulus, for instance, in the works of Obulareddy [38],
Birgisson et al. [24], Tran and Hall [40], and Kim et al. [42]. In several extreme conditions, i.e., high or
low temperature, the Witczak 2006 and the Al-Khateeb models have also been found to overpredict the
dynamic modulus [31,45–47]. On the contrary, the Hirsch model has been found to underpredict the
dynamic modulus, as reported in the works of Bari and Witczak [22], Obulareddy [38], Kim et al. [42],
Appl. Sci. 2020, 10, 5242 3 of 22
and Ceylan et al. [47]. These results showed that the prediction models of the expected dynamic
modulus |E*| still need further clarification and investigation.
Considering the modern approach, Ceylan et al. [30] presented and compared a series of Artificial
Neural Network (ANN) models with some existing models to predict the dynamic modulus |E*| of
HMA. The ANN models indicated a notable accuracy compared with the conventional regression
models and can be applied to the mechanistic-empirical pavement design guide. Far et al. [31] attempted
to develop novel models to predict the dynamic modulus |E*| of HMA mixtures in the case of long-term
pavement performance. The data consisted of measured moduli from many geographical places
around the United States. The obtained results indicated that the predicted dynamic modulus |E*|
utilizing ANN and measured dynamic modulus |E*| values were well matched. Sakhaeifar et al. [25]
also proposed a fundamental modeling framework to predict dynamic modulus |E*| of HMA using
viscoelastic principles combined with the physical and mechanical characteristics of the mixture.
The proposed dynamic modulus models were verified as reliable and appropriate for a wide scope of
temperatures and recommended in the AASHTO TP62-03 test protocol. Despite that, the application of
a machine learning approach to SMA mixtures is still limited, and further elaboration of the dynamic
modulus in function of the temperature and frequency is required.
On the basis of sustainable development and environmental standpoints, the current study,
therefore, aims at favoring the potential use of SMA with warm technology from two different angles.
From an experimental point of view, dynamic modulus tests were performed to highlight the beneficial
aspect of SMA using warm technology compared with the hot technology, as well as conventional
dense-graded asphalt concretes. From a simulation angle, a novel machine learning algorithm was
developed to accurately predict the desired mechanical property of the asphalt mixtures, and thus to
facilitate the use in the design process or the construction and operation stages. To this aim, a total of
576 experimental tests on dynamic modulus were carried out to construct a database of 96 instances
by taking the average values per 6. In parallel, the ANN-TLBO machine learning algorithm was
developed, consisting of one well-known machine learning model (ANN) and an effective optimization
algorithm, namely Teaching-Learning Based Optimization (TLBO). The performance of the proposed
ANN-TLBO model was evaluated by three common statistical criteria, including root mean square
error (RMSE), mean absolute error (MAE), and coefficient of determination (R2 ).
The present paper is structured as follows: (i) an overview of the state of the art of the problem is
presented in the first section; (ii) the significance of the study is given in Section 2; (iii) the experimental
procedure is provided in the next section, including the materials, design, mixing, and testing of
the asphalt mixtures; (iv) a brief overview of the machine learning algorithms is given in Section 4;
and (v) the experimental and simulation results are presented in Section 5. Several conclusions and
perspectives are finally given in the last section of the paper.
modulus of the four mentioned asphalt mixtures; (iv) the dependency of the dynamic modulus on
diverse input variables was proposed thanks to the developed ML algorithm.
3. Experimental
Table 1. Physical properties of coarse and fine aggregates and mineral filler.
Table 2. Physical properties of Polymer Modified Bitumen (PMB) III and PMB III with Sasobit.
(a) (b)
100 100
Lower limit Upper limit
80 80
Passing (%)
Passing (%)
20 20
0 0
0.075 0.75 7.5 0.075 0.75 7.5
Sieve size (mm) Sieve size (mm)
Figure 1. Mixture gradation aggregate (a) Stone Mastic Asphalt (SMA) samples, (b) hot mix asphalt
Figure 1. Mixture gradation aggregate (a) Stone Mastic Asphalt (SMA) samples, (b) hot mix asphalt
(HMA) samples.
(HMA) samples.
Regarding the determination of the dynamic modulus |E*|, laboratory tests in accordance with
AASHTORegarding the determination
TP 62 [52] were conducted. of The
the dynamic
short-termmodulus
aging of|E*|, laboratory
asphalt concrete tests in accordance
was firstly conducted,with
AASHTO
followed by TPthe62 AASHTO
[52] were conducted.
R30 standard. TheThe
short-term aging
compaction of asphalt
process concrete
was next was firstly
performed on a conducted,
rotating
followed by the AASHTO R30 standard. The compaction process was next performed
compactor in order to achieve air void content of 7 ± 0.5%. The specimen, flattened at both ends, on a had
rotating
a
compactor in order to achieve air void content
height of 100 mm and a diameter of 100 mm (Figure 2). of 7 ± 0.5%. The specimen, flattened at both ends, had
a height of 100 mm
All samples and
were a diameter
placed of 100 mmchamber
in a thermostatic (Figure 2).
to maintain a constant temperature. The test
was conducted on a CRT NU-14 device (Figure 3). The experimental tests on the dynamic modulus
|E*| used six frequency values, i.e., 0.1 Hz, 0.5 Hz, 1 Hz, 5 Hz, 10 Hz, and 25 Hz and four temperature
values, i.e., 10 ◦ C, 25 ◦ C, 45 ◦ C, 60 ◦ C.
Appl. Sci.
Appl.2020, 10, 5242
Sci. 2020, 10, x 6 of 246 of 22
(a)
(b)
All samples were placed in a thermostatic chamber to maintain a constant temperature. The test
was conducted on a CRT NU-14 device (Figure 3). The experimental tests on the dynamic modulus
|E*| used six frequency values, i.e., 0.1 Hz, 0.5 Hz, 1 Hz, 5 Hz, 10 Hz, and 25 Hz and four temperature
values, i.e., 10 °C, 25 °C, 45 °C, 60 °C.
(a) (b)
Figure 3. The
TheSMA
SMAsamples preparation
samples and
preparation testing:
and (a) Gyratory
testing: Compactor
(a) Gyratory machine,
Compactor (b) CRT
machine, NU-
(b) CRT
14 machine.
NU-14 machine.
3.3. Instrumentation
The samples were mixed by an asphalt mixer with 30-L capacity manufactured by Daiwakenko
(Tokyo–Japan). The samples were compacted by Gyratory Compactor 4140 manufactured by Troxler
(TROXLER, Durham, NC, USA). All samples were placed in a thermostatic chamber to maintain a
constant testing temperature. The test was conducted on a CRT NU-14 device (Cooper, London, UK).
Appl. Sci. 2020, 10, 5242 7 of 22
3.3. Instrumentation
The samples were mixed by an asphalt mixer with 30-L capacity manufactured by Daiwakenko
(Tokyo–Japan). The samples were compacted by Gyratory Compactor 4140 manufactured by Troxler
(TROXLER, Durham, NC, USA). All samples were placed in a thermostatic chamber to maintain a
constant testing temperature. The test was conducted on a CRT NU-14 device (Cooper, London, UK).
4. Methods Used
Table 4. Statistical analysis and summary of the input and output variables used in this study.
k
1X
MAE = |xcai − xmei | (3)
k
i=1
where, xmei and xme indicate the measured value of the specimen ith and the measured mean value,
respectively; xcai and xca indicate the output value of the specimen ith and the average value of output
predicted from the modeling, respectively; k means the sum of samples.
(a) SMA - W
7000
T=10°C T=25°C
5000
T=45°C T=60°C
4000
3000
2000
1000
6000
5000
T=45°C T=60°C
4000
3000
2000
1000
0
0 2 4 6 8 10 12 14 16 18 20 22 24 26
Frequency (Hz)
(c) HMA - W
7000
T=10°C T=25°C
Dynamic Modulus |E*|
6000
5000
T=45°C T=60°C
4000
3000
2000
1000
0
0 2 4 6 8 10 12 14 16 18 20 22 24 26
Frequency (Hz)
(d) HMA - H
7000
T=10°C T=25°C
Dynamic Modulus |E*|
6000
5000
T=45°C T=60°C
4000
3000
2000
1000
0
0 2 4 6 8 10 12 14 16 18 20 22 24 26
Frequency (Hz)
Figure 4. Experimental
Figure 4. Experimentalresults
resultsof
of dynamic
dynamic modulus |E*| in
modulus|E*| functionofofthe
in function thefrequency,
frequency,
inin
thethe case
case of of
(a) SMA-W; (b) SMA-H; (c) HMA-W; and (d) HMA-H.
(a) SMA-W; (b) SMA-H; (c) HMA-W; and (d) HMA-H.
Appl. Sci. 2020, 10, x 11 of 24
Appl. Sci. 2020, 10, 5242 10 of 22
Figure 5. Cont.
Appl. Sci. 2020, 10, x 12 of 24
Appl. Sci. 2020, 10, 5242 11 of 22
Figure 5. Experimental results of dynamic modulus |E*| in function of the test temperature for different
Figure 5. Experimental results of dynamic modulus |E*| in function of the test temperature for
frequencies: (a) 0.1 Hz; (b) 0.5 Hz; (c) 1 Hz; (d) 5 Hz; (e) 10 Hz; (f) 25 Hz.
different frequencies: (a) 0.1 Hz; (b) 0.5 Hz; (c) 1 Hz; (d) 5 Hz; (e) 10 Hz; (f) 25 Hz.
It could be concluded that, compared to the HMA, the SMA showed superior performance in
terms of the dynamic modulus |E*|. Besides, the warm technology exhibited higher dynamic
modulus |E*| than using the hot technology. Considering SMA and the mixtures using the warm
technique, similar observations were also reported in the literature [12]. Indeed, Al-Qadi et al.
Appl. Sci. 2020, 10, 5242 12 of 22
It could be concluded that, compared to the HMA, the SMA showed superior performance in
terms of the dynamic modulus |E*|. Besides, the warm technology exhibited higher dynamic modulus
|E*| than using the hot technology. Considering SMA and the mixtures using the warm technique,
similar observations were also reported in the literature [12]. Indeed, Al-Qadi et al. showed that the
SMA-W exhibited significant improvement compared with SMA-H. Moreover, the authors showed
that, in terms of additives, Sasobit disclosed the highest performance compared with the control mix,
Evotherm, and foamed asphalt. Besides, the curing time was proved to be another critical factor
affecting the dynamic modulus. Several curing times using Sasobit were tested in the work, and the
results showed that 1-day curing time was optimal. In this study, taking advantage of such a result,
the curing time was directly chosen as one day. The analysis of the effect of curing time might be
the objective of further research, as different natures of aggregates, filler, or bitumen might have a
certain influence on the dynamic modulus. Besides, another study confirmed the addition of additives
enhanced the dynamic modulus compared with the control asphalt mixtures, for instance, in the
work of Goh and You [80]. Last but not least, the success in decreasing the mixing and compacting
temperatures was proven in the literature but only for recycled aggregates [12,48]; this study showed a
similarly successful result of the dynamic modulus of asphalt mixture in using conventional aggregates.
Figure 6. Optimization
Figure 6. Optimizationofofweight
weight parameters
parameters ofofANN
ANN models
models using
using the TLBO
the TLBO algorithm:
algorithm: (a) R2 ,
(a) R2, (b)
(b) RMSE,
RMSE,and
and(c)
(c) MAE.
MAE.
for the training and testing datasets, respectively. These results showed a very good prediction
performance of the two proposed models. However, using an optimization, the ANN-TLBO was
Appl. Sci. 2020, 10, 5242 14 of 22
found to be the superior predictor compared with the single ANN.
Figure 7. Regression graphs using individual ANN model: (a) training and (b) testing parts; ANN-TLBO
Figure 7. Regression graphs using individual ANN model: (a) training and (b) testing parts; ANN-
model: (c) training and (d) testing parts.
TLBO model: (c) training and (d) testing parts.
The summary of the prediction performance of ANN and ANN-TLBO is presented in Table 6.
TheThe
summary
values of of
R2,the prediction
RMSE, and MAEperformance
were calculatedofbased
ANN on and ANN-TLBO
the formulations is presented
given in Table 6.
in the previous
2
The values of R , RMSE, and MAE were calculated based on the formulations given in the previous
section, whereas ErrorMean was the mean values of errors and ErrorStD was the standard deviation of
errors. The “Slope” represented the slope between the ideal regression line (discontinuous lines in
Figure 7) and the linear fit, given by the models (continuous lines in Figure 7). The two additional
error criteria also confirmed that ANN-TLBO is superior to ANN in predicting the dynamic modulus
|E*|. For illustration purposes, the values of the dynamic modulus |E*| in function of sample index
using individual ANN and ANN-TLBO models are plotted in Figure 8 for the training and testing
datasets. It is clearly seen that the predicted values were in excellent agreement with the experimental
dynamic modulus |E*| values.
Figure 7) and the linear fit, given by the models (continuous lines in Figure 7). The two additional
error criteria also confirmed that ANN-TLBO is superior to ANN in predicting the dynamic modulus
|E*|. For illustration purposes, the values of the dynamic modulus |E*| in function of sample index
using individual ANN and ANN-TLBO models are plotted in Figure 8 for the training and testing
datasets. It is clearly seen that the predicted values were in excellent agreement with the experimental
Appl. Sci. 2020, 10, 5242
dynamic modulus |E*| values. 15 of 22
Dynamic
Figure 8.Figure modulus
8. Dynamic in function
modulus ofofsample
in function index,using
sample index, using individual
individual ANNANNmodelmodel for (a) training
for (a) training
part and part
(b) testing part, using
and (b) testing ANN-TLBO
part, using ANN-TLBOmodelmodel for (c)training
for (c) training part
part andand (d) testing
(d) testing part. part.
Overall, the prediction capability of ANN-TLBO was quantified based on various performance
indicators. The proposed hybrid model showed high prediction capability and outperformed
individual ANN, clearly demonstrating the efficiency of using TLBO as an optimization tool.
Overall, the prediction capability of ANN-TLBO was quantified based on various performance
indicators. The proposed hybrid model showed high prediction capability and outperformed individual
ANN, clearly demonstrating the efficiency of using TLBO as an optimization tool.
Figure 9. Sensitivity index of frequency and temperature for four combinations of SMA, HMA, H,
Figure 9.
and W.
and W.
As
As indicated
indicatedininmany
many studies
studies[82–85], exploring
[82–85], exploringthe the
relative importance
relative of inputs
importance mightmight
of inputs offer better
offer
in-depth knowledge
better in-depth of the output,
knowledge which which
of the output, could directly assist engineers
could directly duringduring
assist engineers the preparation phase.
the preparation
Considering the testing
phase. Considering thetemperature and frequency,
testing temperature experimental
and frequency, investigations
experimental have been conducted
investigations have been
in several works [12,80]. However, a direct linear interpolation of the as-obtained
conducted in several works [12,80]. However, a direct linear interpolation of the as-obtained results or missing
results
information on the rangeonofthe
or missing information input
rangevalues could
of input lead to
values inexact
could leadobservations. In this work,
to inexact observations. Inan attempt
this work,
was made from an experimental point of view, to cover a broad range
an attempt was made from an experimental point of view, to cover a broad range of testing of testing temperature and
frequency
temperature withandsufficiently
frequencygrid withpoints. The dependency
sufficiently grid points.ofThethe dependency
dynamic modulus of theon inputs was
dynamic then
modulus
analyzed
on inputswith
was the developed
then analyzedML withalgorithm. For each
the developed MLmixture,
algorithm. a fitFor
equation was proposed
each mixture, to highlight
a fit equation was
the dependency of the selected variable to dynamic modulus |E*|. With
proposed to highlight the dependency of the selected variable to dynamic modulus |E*|. Withreasonable accuracy, a linear
equation
reasonable was finally adopted
accuracy, a lineartoequation
fit the frequency versus
was finally the dynamic
adopted to fit themodulus.
frequencyOn versus
the contrary, a cubic
the dynamic
equation was chosen to relate the temperature with the dynamic modulus. Summarized
modulus. On the contrary, a cubic equation was chosen to relate the temperature with the dynamic information on
the sensitivity analysis of the effect of temperature and frequency is presented
modulus. Summarized information on the sensitivity analysis of the effect of temperature and in Table 7, including the
appropriate
frequency isfit, equationinform,
presented Tableand correlationthe
7, including effect. The proposed
appropriate equations
fit, equation could
form, andfacilitate
correlationthe effect.
usage
of asphalt mixtures in selecting the desired dynamic modulus in function of
The proposed equations could facilitate the usage of asphalt mixtures in selecting the desired the testing temperature
and frequency.
dynamic modulus in function of the testing temperature and frequency.
Appropriate Correlation
Mixture Technology Variable Equation Form
Fit Effect
HMA Hot Frequency Linear y = 134.2x − 15 Positive
Appl. Sci. 2020, 10, 5242 17 of 22
Author Contributions: Conceptualization, T.-H.L., H.-L.N., H.-B.L., and C. -T.P.; data curation, T.-H.L., M.H.N.,
and N.-L.N.; formal analysis, T.-H.L., H.-L.N., and C.-T.P.; methodology, H.-L.N., H.-B.L., B.T.P. and T.-T.L.; project
administration, H.-L.N. and H.-B.L.; supervision, H.-L.N., H.-B.L., B.T.P., and T.-T.L.; validation, H.-L.N., C.-T.P.,
and H.-B.L.; visualization, T.-H.L., H.-B.L. and T.-T.L.; writing—original draft, all authors.; writing—review &
editing, H.-L.N., H.-B.L., and B.T.P. All authors have read and agreed to the published version of the manuscript.
Funding: This research received no external funding
Conflicts of Interest: The authors declare no conflict of interest
Appendix A
ID Mix Tech. Fr. (Hz) T◦ (◦ C) E* (MPa) ID Mix Tech. Fr. (Hz) T◦ (◦ C) E* (MPa)
1 SMA Warm 0.1 10 3221.06 49 HMA Warm 0.1 10 2822.85
2 SMA Warm 0.1 25 1479.78 50 HMA Warm 0.1 25 1470.61
Appl. Sci. 2020, 10, 5242 18 of 22
ID Mix Tech. Fr. (Hz) T◦ (◦ C) E* (MPa) ID Mix Tech. Fr. (Hz) T◦ (◦ C) E* (MPa)
3 SMA Warm 0.1 45 655.06 51 HMA Warm 0.1 45 581.08
4 SMA Warm 0.1 60 340.66 52 HMA Warm 0.1 60 316.70
5 SMA Warm 0.5 10 3702.71 53 HMA Warm 0.5 10 3340.80
6 SMA Warm 0.5 25 1825.52 54 HMA Warm 0.5 25 1766.28
7 SMA Warm 0.5 45 818.73 55 HMA Warm 0.5 45 748.68
8 SMA Warm 0.5 60 426.55 56 HMA Warm 0.5 60 375.46
9 SMA Warm 1 10 3945.63 57 HMA Warm 1 10 3434.68
10 SMA Warm 1 25 1973.47 58 HMA Warm 1 25 1897.39
11 SMA Warm 1 45 906.37 59 HMA Warm 1 45 829.06
12 SMA Warm 1 60 475.75 60 HMA Warm 1 60 409.06
13 SMA Warm 5 10 4160.71 61 HMA Warm 5 10 3434.08
14 SMA Warm 5 25 2390.24 62 HMA Warm 5 25 2106.09
15 SMA Warm 5 45 1147.24 63 HMA Warm 5 45 994.26
16 SMA Warm 5 60 560.64 64 HMA Warm 5 60 452.40
17 SMA Warm 10 10 4318.67 65 HMA Warm 10 10 3608.55
18 SMA Warm 10 25 2454.36 66 HMA Warm 10 25 2135.47
19 SMA Warm 10 45 1362.23 67 HMA Warm 10 45 1116.60
20 SMA Warm 10 60 598.55 68 HMA Warm 10 60 473.85
21 SMA Warm 25 10 4762.26 69 HMA Warm 25 10 3913.48
22 SMA Warm 25 25 2643.28 70 HMA Warm 25 25 2306.67
23 SMA Warm 25 45 1755.81 71 HMA Warm 25 45 1503.70
24 SMA Warm 25 60 843.93 72 HMA Warm 25 60 690.96
25 SMA Hot 0.1 10 2927.48 73 HMA Hot 0.1 10 2376.47
26 SMA Hot 0.1 25 1205.92 74 HMA Hot 0.1 25 1188.64
27 SMA Hot 0.1 45 661.20 75 HMA Hot 0.1 45 450.33
28 SMA Hot 0.1 60 303.96 76 HMA Hot 0.1 60 277.44
29 SMA Hot 0.5 10 3345.46 77 HMA Hot 0.5 10 2752.67
30 SMA Hot 0.5 25 1572.55 78 HMA Hot 0.5 25 1406.66
31 SMA Hot 0.5 45 815.87 79 HMA Hot 0.5 45 563.33
32 SMA Hot 0.5 60 361.72 80 HMA Hot 0.5 60 335.48
33 SMA Hot 1 10 3560.48 81 HMA Hot 1 10 2723.29
34 SMA Hot 1 25 1750.65 82 HMA Hot 1 25 1516.44
35 SMA Hot 1 45 901.81 83 HMA Hot 1 45 613.94
36 SMA Hot 1 60 395.62 84 HMA Hot 1 60 372.16
37 SMA Hot 5 10 3880.80 85 HMA Hot 5 10 2970.33
38 SMA Hot 5 25 2250.72 86 HMA Hot 5 25 1688.84
39 SMA Hot 5 45 1131.55 87 HMA Hot 5 45 720.14
40 SMA Hot 5 60 426.95 88 HMA Hot 5 60 424.85
41 SMA Hot 10 10 4021.36 89 HMA Hot 10 10 3013.44
42 SMA Hot 10 25 2400.21 90 HMA Hot 10 25 1733.71
43 SMA Hot 10 45 1351.68 91 HMA Hot 10 45 796.31
44 SMA Hot 10 60 448.87 92 HMA Hot 10 60 444.47
45 SMA Hot 25 10 4434.93 93 HMA Hot 25 10 3424.61
46 SMA Hot 25 25 2639.12 94 HMA Hot 25 25 1857.80
47 SMA Hot 25 45 1794.94 95 HMA Hot 25 45 1106.78
48 SMA Hot 25 60 636.84 96 HMA Hot 25 60 629.32
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