FINAL Chemical Credit Sys14-15 To BOS

SHIVAJI UNIVERSITY, KOLHAPUR – Syllabus w.e.f.
2014 - 15
SHIVAJI UNIVERSITY, KOLHAPUR

FINAL YEAR B.TECH
Chemical Technology
Curriculum Structure
Semester – VII
Contact hours
Sr.No. Subject Credits
Code Subject Title L T P
1
CH411 Advanced Separation Techniques 04 - - 04
2
CH412 Elective –I
04 - - 04
3 Process Economics and Project
CH413
Engineering 03 - - 03
4 03 01 04
Reaction Engineering – II
CH414 -
5
CH415 Special Chemical Technologies-I 04 - - 04
6 Advanced Separation Techniques

CH411L - - 02 01
Laboratory
7 Reaction Engineering – II -
CH414L Laboratory - 02 01
8 CH416L
Plant Design and Case studies - 02 01
9 CH417L Major Project-Phase I - - 02 01
10 CH418 Report of Industrial Training - - - 01
11 HS411 Audit Course V 02 - - -
Professional Ethics
Total 20 01 08 24
Total Contact hours per week = 29
Note: Tutorials and practical shall be conducted in batches with batch strength not exceeding
15 students.
List of Subjects as Elective-I:
CH412.1 Petroleum Refinery Engineering, CH412.2 Biochemical Engineering , CH412.3 Polymer Chemistry,,
CH412.4 Introduction to Food Process Engineering , CH412.5 Surface Chemistry , CH412.6 Environmental
Science and Microbiology, CH412.7 Drugs and Pharmaceutical Technology.
Shivaji University 1
SHIVAJI UNIVERSITY, KOLHAPUR – Syllabus w.e.f. 2014 - 15
SHIVAJI UNIVERSITY, KOLHAPUR

FINAL YEAR B.TECH
Chemical Technology
Curriculum Structure
Semester – VIII
Sr. Contact Hours

No. Subject Credits
Code Subject Title L T P
1. Energy Conservation in
CH421
Chemical Industries 04 - - 04
2.
CH422 Elective-II
04 - - 04
3. CH423 Process Modeling and -
Simulation 04 - 04
4. CH424
Special Chemical Technologies-
04 - - 04
II
5. CH425 04 - - 04
Transport Phenomena
6. HS421T Industrial Safety and Hazard - 01 - 01
Management
7. CH423L Process Modeling and - - 02 01
Simulation Laboratory
8.
CH426L Major Project- Phase II - 01 03 02
9. HS422 Audit Course VI 02 - - -

Constitution of India
Total 22 02 05 24
Total Contact hours per week = 29
List of Subjects as Elective-II:
CH422.1 Petrochemical Technology, CH422.2. Industrial Biotechnology, CH422.3. Polymer Technology,

CH422.4 Food Process Technology, CH422.5 Catalysis, CH422.6 Environmental Chemistry and Biochemistry
CH422.7 Open Elective (to be chosen from any of the specialized program available on the campus)
Shivaji University, Kolhapur

Department of Technology
Final Year B. Tech (Chemical Technology) (Semester VII)
CH411 ADVANCED SEPARATION TECHNIQUES
Teaching Scheme: L: 4 hours/week Credits: 4
UNIT I Introduction to the subject (04Hours)
Review of conventional separation techniques. Concept of advanced

separation techniques. Need for advancement in separation techniques. Advantages of
separation techniques.
UNIT II (10Hours)
Separation Processes: Industrial Chemical Processes, Mechanism of
Separation by phase addition or creation. Separation by barrier, Separation by solid
agent, Separation by external field or gradient. Component Recoveries and product
purities, Separation power. Selection of feasible separation processes. Crystallization
from the melt: Introduction. Progressive freezing: component Separation by
progressive freezing, Pertinent variables in progressive freezing. Applications, Zone
melting: component separation by zone melting, pertinent variables in zone melting,
Application. Melt crystallization from the bulk: Investigations, commercial equipment
and application. Falling-film crystallization: Principles of operation, commercial
equipment and applications.
UNIT III (10Hours)

Enhanced distillation: Introduction. Azeotropism. Azeotropic distillation:
Introduction, exploitation of homogeneous azeotropes, exploitation of pressure
sensitivity, exploitation of boundary curvature, Exploitation of azeotropy and liquid
Extractive distillation: Introduction, solvent effect in extractive distillation, extractive
distillation design and optimization, solvent screening and selection extractive
distillation by salt effects. Reactive distillation: Introduction, simulation, modeling
and design feasibility, Mechanical design and implementation issues, process
applications.
UNIT IV (08Hours)
Supercritical fluid separation processes : Introduction. Physical properties
of pure supercritical fluids; thermodynamic properties and transport properties.
Process concept in super critical fluid extraction. Phase equilibria: Liquid- Fluid
equilibria, Solid- Fluid equilibria, Polymer- Fluid equilibria and the Glass Transition,
Co solvents and surfactants, phase equilibria models. Mass Transfer. Applications:
Food and Pharmaceutical applications, Temperature controlled residuum Oil super
critical extraction [ROSE], Extraction from aqueous solution, Adsorption and
desorption, Polymer de volatilization and fractionation, Drying and Aero gel

formation, Clearing, Crystallization, Reactive separations.
UNIT V (10Hours)
Membrane separation processes: Introduction. Advantages of membrane
separations, Basic equations, Basic concept, Membrane types, Economics. Electro
dialysis: Process description, examples, membranes, membrane efficiency, process
description and configuration, Energy requirements, Equipment and economics.
Reverse osmosis and Nano filtration: Processes description, examples Basic principles
of operations, RO and NF membranes, process limitations and configuration.
Economics. Ultra filtration: Process description, UF membranes, membrane
characterization, process limitations, process configurations, Energy requirements,
Design and economics. Micro filtration: process description, Examples, MF
membranes, membrane characterization, process limitations, Equipments
configurations, process Applications and Economics. Gas- Separations membranes:
Process descriptions, examples, Basic principles of operations, selectivity and
permeability, Gas- Separation membranes, membrane system design features, energy
requirements and economics. Per vaporization: Process description, definition,
operational factors, vapor feed, examples, per evaporation membranes, modules.
UNIT VI (08Hours)
Biochemical separation processes: Introduction. Initial product harvest and
concentration: centrifugation, Filtration, Selection of cell separation Unit operation,
Cell disruption, protein refolding. Initial purification: Precipitation, Extraction,
Adsorption, Membrane processes. Final Purification and product formulation,
Chromatography, Lyophilization and drying. Integration of fermentation and
downstream processing operations.
REFERENCE BOOKS:
1. Perry Robert H. and Green Don W., “Perry’s chemical Engineers Handbook” 7th
edition. McGraw Hill Publication, New York.
2. Seader J. D. and Henley Ernest J, “Separation Process Principles”, John Wiley and
Sons, Inc, New York
3. Ladisch Michael R., “Bioseparations Engineering, Principles, Practice and
Economics”, Wiley Interscience, John Wiley and Sons, Inc. Publications New York
4. Long Robert B. “Separation Process in Waste Minimization”, Marcel Dekker, Inc,
New York

CH412 ELECTIVE-I
CH412.1 PETROLEUM REFINERY ENGINEERING
UNIT I Introduction (08Hours)

Genesis, occurrence, exploration, drilling of crude oil. Composition and Evaluation of
crude oil and testing of petroleum products. Refining of petroleum – Atmospheric and
vacuum distillation.
UNIT II Refining of petroleum (08Hours)

Atmospheric and vacuum distillation. Pretreatment of crude oil and transportation.
UNIT III Cracking processes (08Hours)
Thermal cracking, Vis-breaking, Coking. Catalytic cracking (FCC), Hydro cracking,
Rebuilding processes, bitumen blowing.
UNIT IV Treatment techniques (10Hours)

Study of techniques for removal of sulphur compounds to improve performance,
Storage and stability. Product treatment processes - various solvent treatment
processes, Dewaxing, Clay treatment and Hydro fining.
UNIT V Cracking and Reforming (10Hours)

Cracking of naphtha and gas for the production of ethylene, propylene isobutylene
and butadiene. Production of acetylene from methane Catalytic Reforming of
petroleum feed stocks. Extraction of Aromatics.
UNIT VI Threats and Challenges before Petroleum Industries (08Hours)
TEXT BOOKS:
1 B.K.Bhaskara Rao, "Modern Petroleum Refining Processes", 2nd Edition. Oxford
and IBH Publishing Company, New Delhi, 1990.
REFERENCE BOOKS:
1 W.L.Nelson, “Petroleum Refinery Engineering”, 4th Edition. McGraw Hill, New
York, 1985
2. Robert. A. Meyers, “Handbook of Petroleum Refining Processes”, McGraw Hill,
1986.
3. G.D.Hobson and W.Phol, “Modern Petroleum Technology”, Applied science
Publishers, IV Edition, 1975.

CH412 ELECTIVE-I
CH412.2 BIOCHEMICAL ENGINEERING
UNIT I Introduction (08Hours)

Principles of microbiology, structure of cells, microbes, bacteria, fungi, algae,
chemicals of life - lipids, sugars and polysaccharides, amino acids, proteins,
nucleotides, RNA and DNA, hierarchy of cellular organization, Principles of genetic
Engineering, Recombinant DNA technology, mutation.
UNIT II Kinetics of enzyme catalyzed reactions (10Hours)

The enzyme substrate complex and enzyme action, simple enzyme kinetics
with one and two substrates, determination of elementary step rate constants. Isolation
and utilization of Enzymes -production of crude enzyme extracts, enzyme
purification, applications of hydrolytic enzymes, other enzyme applications, Enzyme
production – intercellular and extra cellular enzymes.
UNIT III Metabolic pathways and energetics of the cell (10Hours)

Concept of energy coupling, ATP and NAD, Photosynthesis, Carbon
metabolism, EMP pathway, Tricabocyclic cycle and electron transport chain, aerobic
and anaerobic metabolic pathways, transport across cell membranes, Synthesis and
regulation of biomolecules.
UNIT IV Typical growth characteristics of microbial cells (10Hours)

Factors affecting growth, Batch and Continuous cell growth , nutrient media,
enrichment culture, culture production and preservation, Immobilization Technology
– Techniques of immobilization, Characteristics and applications, Reactors for
immobilized enzyme systems
UNIT V AND VI Introduction to bio reactors and Future Trends (14Hours)

Types of bio reactors, Continuously Stirred aerated tank bioreactors,
Determination of volumetric mass transfer rate of oxygen from air bubbles and effect
of mechanical mixing and aeration on oxygen transfer rate, heat transfer and power
consumption, Fermentation-methods and applications, downstream processing and
product recovery in bio processes
TEXT BOOKS:
1. M.L.Shuler and F.Kargi, “Bioprocess Engineering: Basic concepts”, 1st Edition,

Prentice Hall, New Jersey, 1992
2. Mukesh Doble, Sathyanarayana N, “Biochemical Engineering”, Gummai, Prentice
Hall, 2007.
REFERENCE BOOKS:
1. Trevan, Boffey, Goulding and Stanbury, “Biotechnology”, Tata McGraw Hill
Publishing Co., NewDelhi, 1987
2. S.Aaiba, “Biochemical Engineering”, Academic Press, 1965.
3. D.G. Rao, “Introduction to Biochemical Engineering”, Tata McGraw Hill, 2005.
4. J.E.Bailey and D.F.Ollis, “Biochemical Engineering Fundamentals”, McGraw
Hill, 1986.

CH412 ELECTIVE-I
CH412.3 POLYMER CHEMISTRY
UNIT I Scope of Polymer Chemistry (08Hours)

Definition of monomers, homopolymers and copolymers, Chemistry of important
monomers, Thermosets, Thermoplastic, Elastomers (f) Tg, Tm, and solution
properties of polymers
UNIT II Condensation polymerization (10Hours)

Mechanism, kinetic and molecular weight build up , Bulk, Solution, Emulsion and
suspension polymerization, comparison of condensation and addition polymerization
UNIT III Addition polymerization (10Hours)

Type of addition polymerization, Radical, cationic and anionic polymerization,
Mechanism and kinetics of polymerization, Copolymerization, Stereo-Regular
polymerization, Block and Graft polymerization
UNIT IV Characterization of molecular weight polymers (10Hours)

End-Group analysis method, Viscosity of measurement method, G.P.C. Techniques
for measurement
UNIT V AND VI Application of polymers present and future (12Hours)

Fiber forming synthetic polymer, Properties of fiber forming synthetic polymer , future
trends in plastic fibre and elastomers
TEXT BOOKS:
1. F.W. Billmeyer, “Text Book of Polymer science”
2. M.S. Bhatnagar, “Text Book of polymer”
3. Gawaskar, Vishwanathan, Sreedhar and Jaydev, “Polymer science”
4. B.K. Sharma, “Polymer chemistry”,

CH412 ELECTIVE-I
CH412.4 INTRODUCTION TO FOOD PROCESS ENGINEERING
UNIT I Food chemistry (08Hours)

Lipids, proteins, carbohydrates, composition of foods nutrition. Food Microbiology:
Introduction growth factors, degradation and spoilage of foods epidemiology of food
borne diseases, food infections.
Food Biotechnology: Fermentation and enzymatic processes.
Aseptic Techniques: Food handling, food sterilization sterilization of food
processing equipments.
UNIT II Transport Phenomena in food processing (10Hours)

Non Newtonian flow heat transfer simultaneous heat and momentum transfer thermal
time distribution mixing Unit operations in food systems, evaporation.
UNIT III Preservation techniques (10Hours)

Study of different preservation techniques like: Thermal, Dehydration, microwave
irradiation cold fermentation and by chemicals.
UNIT IV Packaging and storage (10Hours)

Principles, shelf life, canning, modified atmosphere packaging, refrigeration.
UNIT V Post Harvesting Techniques (07Hours)

Grain drying and storage fruit and vegetable processing seafood and meat processing
UNIT VI Supercritical extraction (07Hours)

Study of basic concepts of supercritical fluid extraction. Flavours, spices and essence
extraction using SFE technique.
REFERENCE BOOKS:
1. R. Paul Singh and Demis R. Heldman, Introduction to Food Engineering, 2nd ed,
Academic Press, 1993.
2. Ernest L. Watson and John C Harper, Elements of Food Engineering, 2nd ed. Von
Nostrand Reinhold Co., 1987.
3. R. Macral, R. K. Robinson, and M. J. Sadler, Encyclopedia of Food Science, Food
Technology and Nutrition, Vol. 8, Academic Press 1993.
CH412 ELECTIVE-I
CH412.5 SURFACE CHEMISTRY
UNIT I
Adsorption and Surface Phenomenon (12Hours)
Physisorption and chemisorption,
adsorption isotherms, Langmuir and B. E. T .equation and significance in surface area
determination, surface films, states of insoluble films, L. B. films and their
application, adsorption from solution, adsorption types, surface excess concentration,
Gibb's adsorption equation: derivation, significance and experimental verification
UNIT II
Micelle (12Hours)
Surface activity, surface active agents and their classification, micellisation, critical
micelle concentration (cmc) thermodynamics of micellisation , factors affecting cmc,
methods of determination of cmc, reverse micelle, solublisation of water insoluble
organic substances, use of surfactants in oil recovery.
UNIT III
Emulsion (12Hours)
Types of emulsion, theories of emulsion and emulsion stability, identification
of emulsion types, inversion emulsion, micro emulsion: theory and application.
UNIT IV
Liquid gas and liquid interfaces (12Hours)
Surface tension, capillary action, methods of determination of surface tension, surface
tension across curved surfaces, vapour pressure of droplet (Kelvin equation), surface
spreading, spreading coefficient, cohesion and adhesion energy, contact angle,
constant angle hysteresis, wetting and detergency.
REFFERNCE BOOKS
1. Physical chemistry of surfaces: A. W. Adamson.
2. Theory of adsorption and catalysis by Alfred Clark ,
3. Chemisorption by B. M. W. Trapnell and H.O. Hayward.
4. Introduction to colloide and surface chemistry by D. J. Shaw.
5. Surface chemistry by J. J. Bikermann
6. Adsorption and Catalysis by Solids by D. K. Chakrabarty, Wiley Eastern Ltd.,1991.

CH412 ELECTIVE-I
CH412.6 ENVIRONMENTAL SCIENCE AND MICROBIOLOGY

UNIT I
Environmental segments (12Hours)
Lithosphere, Hydrosphere, Biosphere, Composition of Atmosphere,
Troposphere, Stratosphere, Mesosphere. Thermosphere, Chemical species and
particulars in atmosphere, ions radicals particles Reactions in atmosphere.
UNIT II
Principle of Ecology (12Hours)
Definition of Ecology and environment, kind of ecology, environmental and
eco-factors, climate factor, medium factor, biotic factor, Ecosystem and its
components, Nutrient cycle in ecosystem, carbon nitrogen, sulphur and phosphorous
cycle (brief details)
UNIT III
Water chemistry (12Hours)
Hydraulic cycle, specification of water, physical and chemical properties of
water, chemistry of pollution due to detergents, pesticides, polymers trace organic
metals, petroleum and radioactive components.
UNIT IV
Environmental Microbiology (12Hours)
Basic principle of microbial transformation of organic matter. Biodegradation
acclimatization of waster and microbial inhibition. Species of algae and their
significance in water engineering. Eutrophication. Water borne diseases and their
control. Role of microorganism in water and waste water engineering, Role of
microorganism in air pollution control (Bio filters and bio scrubbers)
TEXT BOOKS:
1. A. K. Datta, “Introduction to Environmental Science & Engineering”, Oxford &
IBH,New Delhi
2. Subramaniam, “Text book of Environmental Science”, Narosa
REFERENCE BOOKS:
1. Purohit & Purohit, “Text book of Microbiology”, Agro Publication
2. Subramaniam & Sambamurty, “Ecology”, Narosa
3. Davis & Cornwell, “Introduction to Environmental Science & Environmental
Engineering”, Mcgraw Hill Inst.
4. Botkin Keller, “Environmental Science”, Wiley & Son, New York

CH412 ELECTIVE-I
CH412.7 DRUGS AND PHARMACEUTICAL TECHNOLOGY
UNIT- I
Development of drugs and pharmaceutical industry (10Hours)
Organic therapeutic agents uses and economics. Drug metabolism physio chemical
principles – radio activitypharma kinetics –action of drugs of human bodies.
UNIT- II
Chemical conversion processes (10Hours)
Alkylation – carboxylation – condensation and cyclisation –dehydration,
Esterification (alcohoysis) halogenation – oxidation sulforation – complex chemical
conversion – fermentation.
UNIT-III (10Hours)
Compressed tablets
Wet granulation – dry granulation – direct compression – tablet presses formulation –
coating – pills – capsules sustained action dosage forms – parenter solutions –oral
liquids – injections – cirtmerts – standard of
hygienes and good manufacturing practice.
UNIT- IV
Vitamins (10Hours)
Cold remedies – laxatives – analgesic – non steroical contraceptives – external
antiseptics – antacids and others.
UNIT- V
Antibiotics (10Hours)
Biologicals – harmones – vitamins – preservations – analytical methods or test for
various drugs and pharmaceuticals packing – packing techniques – quality control.
Text Books:
1. E.A. Rawlines Bertleys,”Text books of pharmaceuticals” III Edition, billlieere
Tincall, London, 1977.
Reference Books:
1. S.H. Yalkorsky and J. Swarbrick, “Drug and pharmaceutical Science” Volume I,
II, III, IV, V, VI, and VII Marcel Dekar Inc. New York 1975.
2. Remingtons,” Pharmaceutical Science”, Mack Publishing Co, 1975.

CH413 PROCESS ECONOMICS AND PROJECT ENGINEERING

UNIT I (07Hours)
Introduction: Scales of Production, Selection of Plant Capacity, Plant
Location. Availability of Raw Materials, Energy Gestation Period. Expansion,
Diversification and Obsolescence. Scope for Standardization in Design and
Production .Economics of Research and Development .Indian Chemical Industry,
Current Status and Trends.
UNIT II (07Hours)
Cost Estimation: Factors Affecting Investment and Production Cost .Capital
Investment, Fixed Investment and Working Capital .Estimating Equipment Cost by 6
/10 Factor Rule Method of Estimating Capital Investment .Different Costs Involved in
Total Product Cost .Computer Atomization in Costing.
UNIT III (07Hours)

Interest and Investment Cost: Simple and Compound Interest, Nominal and
Effective Rates of Interest, Continuous Interest, Ordinary Annuity, Perpetuities and
Capital Costs Taxes and Insurances: Types of Taxes and Tax Returns. Types of
Insurance and Legal Responsibility.
UNIT IV (07Hours)
Depreciation: Types of Depreciation, Service Life, Salvage Value, Present
Value. Methods of Determining Depreciation, Single Unit and Group Depreciation
.Causes of Obsolescence and Inadequacy.
UNIT V (08Hours)
Profitability, Alternative Investment and Replacement: Mathematical
Methods of Profitability Evaluation, Cash Flow Diagram. Break Even Analyses,
Balance Sheet, Pricing Issue Method and Income Statement.
UNIT VI (09Hours)
Project conception, Planning, Engineering and Management: Project
conception and definition, Selection of plant capacity, Causes for time and cost over
runs of a Project, Process Optimization, and Selection of Alternative Processes
Equipment
Project engineering: Management and Organization, Project Planning, Scheduling and
Controlling, Use of BAR chart, CPM and PERT Techniques, General site
considerations, Plant Location and Site Selection, Site Layout, Plant Layout, Battery
Limits and Off Site Facilities.
REFERENCE BOOKS:
1. Peter M.S. Timmerhaus K.D., Plant Design and Economics for Chemical
Engineers.
McGraw Hill.
2. Vilbrandt F.C. and C.E. Dryden, Chemical Plant Design. McGraw Hill
3. T.R. Banga and S.C.Sharma, Industrial Organization & Engineering Economics,
Khanna Publications, New Delhi.
4. O.P.Khanna Industrial Engineering & Management, Dhanpat Rai Publications Pvt.
Ltd. New Delhi.
5. Dewett & Varma, Elementary Economic Theory: S Chand & Company Ltd New
Delhi

CH414 REACTION ENGINEERING - II

T: 1 hour/week
UNIT I (04Hours)
Review of Reaction Engineering Basics
UNIT II (07Hours)
Temperature effects in homogeneous reactions: Equilibrium Conversion,
Optimum temperature progression, Adiabatic and non adiabatic operations, Rate,
Temperature and conversion profiles for exothermic and endothermic reactions,
Stable operating condition in reactors.
UNIT III (09Hours)

Non-Ideal flow : Residence time distribution in vessels: E, F and C curve and
their relationship for closed vessels, conversion in reactors having non ideal flow;
models for non-ideal flow: Dispersion model, Tank in Series model, Multi parameter
model.
UNIT IV (09Hours)
Fluid-solid catalyzed reactions : Introduction, Rate equation, Film resistance
controlling, surface flow controlling , Pure diffusion controlling, Heat effects during
reaction, Experimental methods for finding rates, Product distribution in multiple
reactions, Various types of catalytic reactors : Fixed bed reactor- construction,
operation and design, Isothermal operation, Adiabatic operation, Fluidized bed
reactor, Slurry reactor, Trickle bed reactor.
UNIT V (09Hours)
Reactor stability and scale up: Choice of reactor, Factors affecting choice of
reactor, Optimum yield and conversion, Selectivity and reactivity.
UNIT VI (07Hours)
Modeling of reactors and numerical problems based on the reactor design
REFERENCES:
1. Octave Levenspeil, “Chemical Reaction Engineering”, 2nd Edition, John Wiley,
London.
2. S. M. Walas, “Reaction Kinetics for Chemical Engineers”, McGraw Hill, New
York
3. J. M. Smith, “Chemical Engineering Kinetics”, McGraw Hill, New York.
4. J. Rajaram and J. C. Kuriacose, “Kinetics and Mechanics of Chemical
Transformation”, McMillan India Ltd., 1993.

CH415 SPECIAL CHEMICAL TECHNOLOGIES-I
UNIT I Wood and Wood Chemical industry: (06 Hours)

Composite wood, plywood etc.; Manufacture of oleoresin, turpentine, methanol,
rosin, and tall oil; Ethanol production; Essential oils, perfumes, flavours and cosmetics.
UNIT II Leather industry (06 Hours)
Leather industry: Skin and hides; Tanning processes; Leather making; Embossing;
Leather chemicals.
UNIT III Introduction to Biotechnology: (13 Hours)

Basic concepts in biotechnology and historical development, Biotechnology
an interdisciplinary pursuit – public perception of biotechnology –Biotechnology and
developing world – Ethics of biotechnology – future , scope and applications of
biotechnology.
UNIT IV Fermentation industries: (09 Hours)

Introduction to fermentation industry. Absolute Alcohol, Beer, wines & liquors,
vinegar, citric acid and lactic acid.
UNIT V Agrochemical Industries: (09 Hours)
Insecticides, pesticides, Herbicides, plant growth, Nutrients and regulators, compound
Fertilizers, Bio fertilizers, complex fertilizers, and various grades of N.P.K. fertilizer.
UNIT VI Surface Coating technology: (13 Hours)
Classification of paints, water soluble paints and their manufacturing processes;
Natural and Synthetic resins; solvents and plasticizers. Definition and classification of
varnish; Oleoresinious and spirit varnishes;Manufacture of different types of varnishes.
Ceramic coating; Electroplating; Galvanizing; Tinning, Polymer coating; Protective and
decorative coatings. Powder coating.
TEXT BOOK:
1. George T. Austin, “Shreve's Chemical Process Industries”, 5th edition. McGraw Hill Book
Company, 1985.
REFERENCE BOOKS:
1. S.D. Shukla, G.N. Pandey. “A Text book of Chemical Technology”, 3rd Edition.
2. C.E. Dryden, “Outlines of Chemical Technology”, Affiliated East-West Press, 1973.

3. D. Venkteshwaralu, “Chemical Technology”, I & III manuals of Chemical Technology
Chemical Engineering. Ed. Dev. III Madras, 1977.
4. Faith, “Industrial Chemicals”
5. Rogers, “Industrial Chemistry.

CH411L ADVANCED SEPARATION TECHNIQUES Laboratory
Teaching Scheme: P: 2hours/week Credit: 1
LABORATORY PRACTICALS:
1. Study of membrane separation operations:
1.1 Microfiltration 1.2 Ultrafiltration
1.3 Nanofiltration 1.4 Reverse osmosis
1.5 Pervaporation 1.6. Gas permeation
2. Demonstration Experiments:
2.1 Chromatography experiments
2.2 Ion Exchange.
3. Conceptual Experiments:
3.1 Pressure swing Adsorption
3.2 Supercritical Fluid extraction
3.3 Electrostatic precipitator.
Note: Any 8 experiments to be performed from the above list.

CH414L REACTION ENGINEERING - II Laboratory
LABORATORY PRACTICALS:
1. Study of Adiabatic continuous stirred tank reactor
2. Study of RTD in packed bed
3. Study of RTD studies in continuous stirred tank reactor
4. Study of non-catalytic homogeneous reaction in an isothermal tubular flow
reactor
5. Study of non-catalytic homogeneous reaction in a batch reactor
6. Study of non-catalytic homogeneous reaction in continuous stirred tank
reactor
7. Study of non-catalytic homogeneous reaction in plug flow reactor

Final Year B. Tech (Chemical Technology) (Semester VIII)
CH 416L PLANT DESIGN AND CASE STUDIES

(Laboratory work: Design and Drawing to be taken adhering to the below
mentioned theory topics unitized in 5 numbers)
Teaching Scheme: P: 2 hours/week Credits: 1
UNIT I (02Hours)
Introduction: The role of Chemical Engineer in Chemical Plant Design.
Chemical Engineering Design, need for Plant Design.
UNIT II (06Hours)
Plant location and layout: Start-up and shut-down; Cost estimation, capital
investment, and profitability; Construction of P&I diagram.
UNIT III (04Hours)

Principles of scale-up : Principles of scale-up for fluid mechanical, heat
transfer, mass transfer equipment and homogeneous and heterogeneous chemical
reactors; Selection and specifications of process equipment and utilities
UNIT IV (06Hours)
Heat exchange networks: Mass exchange network; Distillation sequencing;
Reaction-separation system; Heat integration of reactors, distillation columns,
evaporators.
UNIT V (08Hours)
Process Auxiliaries : Introduction, Piping, Explanation of CODES, Selection
of Piping, Pipe strength, Wall thickness, Nominal Pipe Size (NPS), Criteria for
Selection of Materials, Pipe sizing by ID, Choosing the final pipe size, Process steam
piping, piping layout, piping insulation, methods of providing flexibility for piping.
REFERENCE BOOKS:
1. Rudd, D.F. and Watson, C.C., “Strategy of Process Engineering”, John Wiley &
Sons, Inc.
2. Smith, R., “Chemical Process Design”, McGraw-Hill Co. Inc.
3. Sieder, W.D., Seader, J.D. and Lewin, D.R., “Product & Process Design
Principles”, John Wiley & Sons, Inc.
4. Douglas J.M., “Conceptual Design of Chemical Processes”, McGraw-Hill, Inc.
5. Peters, M.S. and Timmerhaus, K.D., “Plant Design and Economics for Chemical
Engineers”, McGraw-Hill, Inc.

CH417L MAJOR PROJECT (Phase I)
Teaching Scheme: P: 2 hour/week Credits: 01
The project topic will consists of either some investigation work or design
problem or experimental set up of some development work or prototype equipment or
dissertation related to field of chemical engineering.
Project will be undertaken in the beginning of the seventh term in consultation

with concerned guide and must be completed in eighth term. The project proposal
must be submitted in the beginning of the seventh term by every student or a group of
students (not more than five students in a group).
The students shall submit the report to the corresponding guide, present their
work in due time based on following points,
• Introduction.
• Literature survey.
• Physical/chemical properties etc.
• Experimental setup and procedure.
• Extent of project completed.
Presentation can be performed with OHP slides / LCD.
The progress of the project shall be evaluated by a committee of internal

teachers which shall include concerned guide also and shall award the term work
marks. The oral examination of the project shall be conducted by concerned guide.

CH418 REPORT OF INDUSTRIAL TRAINING
Credit: 1
The industrial training after semester VI will cover the study of a reputed
chemical industry from standpoint of chemical engineering principles. The report of
the training is required to be submitted by the students. The evaluation of this
particular activity is included in this Semester (VII).

Audit Course V
HS411 PROFESSIONAL ETHICS
Teaching Scheme: L: 2 hours/week No Credits

The course auditor will conduct an examination of 50 marks so as to evaluate
the students and these marks will be converted to grade as per standard guidelines.
UNIT I (04 Hours)

Engineering Ethics – Moral Issues, Ethical theories and their uses
UNIT II (04 Hours)

Engineering as Experimentation – Code of Ethics
UNIT III (04 Hours)
Engineer’s Responsibility for Safety
UNIT IV (04 Hours)
Responsibilities in Rights
UNIT V (04 Hours)
Global issues of engineering ethics

UNIT VI (08 Hours)
Introduction to Entrepreneurship awareness and Development: Functions -why
men become economic innovators-Various Assistance Programmes for Small Scale
and large Scale Industries through agencies, like IDBI, IFC, ICICI, NSIC, SFC,
SIDCO and DIC.
REFERENCE BOOKS:
1. Charles D.Fleddermann, “Engineering Ethics”, Prentice Hall, New Mexico, 1999.
2. Seth, M. L., “Principles of Economics”, Lakshmi Narain Agarwal, Agra.
3. Agarwal, A. N., “Indian Economy”, Vikas Publishing House Pvt. Ltd., New Delhi.
4. Datta R. and Sundharam, “Indian Economy”, K. P. M., S. Chand & Co. Ltd., New
Delhi

CH421 ENERGY CONSERVATION IN CHEMICAL INDUSTRIES
Teaching Scheme: L: 4 hours/week Credits:4
UNIT I Energy Outlook (08Hours)

Introduction, Scope of the Problem. Thermodynamic Efficiencies. The
Fundamental Strategy. The Second Law of Thermodynamics Revisited: Difference
between Laws, Definitions Available Energy. Availability, and Energy, Available
Energy and Fuel. Characterizing Energy Use: Understanding Energy use, Missing
Data. An illustrative Onsite Audit, An illustrative Steam Power Balance
UNIT II Optimum performance of Existing Facilities (10Hours)
Principle I Minimize Waste ,Combustion Principles, Illustrative Problems —
Combustion Efficiency, Steam Trap Principles, Principle 2 Manage Energy Use
Effectively, Facilities Improvement - An Overall Site Approach, Utilizing the Energy
Audit, Overall Site Interactions, Cogeneration, Total Site Cogeneration Potential, II
illustrative Problem: Maximum Potential Fuel Utilization, The Linear Programming
Approach Methodology of Thermodynamic Analysis: General Considerations,
Introduction, Sign Conventions, Detailed Procedures, Illustrative Examples.
UNIT III Detailed Thermodynamic Analysis of Common Unit Operations
(10Hours)
Introduction, Heat Exchange, Expansion – Pressure Letdown Mixing,
Distillation — A Combination of Simple Processes Combustion Air Preheating. Use
of thermodynamic Analysis to Improve Energy Efficiency: Introduction, Overall
Strategy, Reducing available Energy (Work) Losses, Accepting 1nevitahle”
Inefficiencies, Optimization through Lost Work Analysis. Research Guidance and
Economics: Capital— Cost Relationships, Background Information, The Entire Plant
Energy System Is Pertinent, Investment Optimization, Defining the limits of Current
Technology, Fundamental Process Improvements
UNIT IV Systematic Design Methods (08Hours)
Introduction, Process Synthesis, Applications to Cogeneration Systems,
Thermo economics, Systematic Option station. Guidelines and Recommendations for
improving process conditions: Introduction, Chemical Reactions, Separations, Heat
Transfer, Process Machinery, System Interactions and Economics, A Check list of
Energy Conservation Items, Shortcomings of Guidelines
UNIT V Energy Conservation Measures (07Hours)
Introduction, Management Systems for Energy Conservation, Energy Audits
and Energy Monitoring, Combined heat and power generation: introduction,
Technology of CHP Systems, Balancing Heat and Power Loads, Economic Incentives
for Further CHP systems, Technical Potential for Further CHP systems. Good
Housekeeping (Minor) Conservation Measures
UNIT VI Heat and Power Recovery (07Hours)

Introduction, Heat Transfer Equipment, Exchanger Networks. Heat Recovery
from Waste Fuels, Heat Exchanger Fouling, Fleet Pumps. Power recovery: Power
recovery from pressure reduction of process fluids. Power recovery from low grade
waste heat
TEXT BOOKS:
1. Murphy W.R. and McKay G., “Energy Management (BH)”,
2. Hinrich & Klein Bach, “Energy: its use and the environment”,
3. Boyle, “Renewable Energy: Power for a sustainable future”
4.Rao S. & Parulekar B.B., “Energy technology”, Khhanna publisher
5. Capenart & Turner, “Guide to energy management”, 6 ed. Kennedy Fairmont press

CH422 ELECTIVE-II
CH422.1 PETROCHEMICAL TECHNOLOGY
UNIT I (08Hours)
General Introduction - History, economics and future of petrochemicals, energy
crisis and petrochemical industry, sources and classification of petrochemicals.
UNIT II (10Hours)
First generation petrochemicals - alkanes - C1, C2, C3, C4 petrochemicals,
alkenes -C2,C3,C4 petrochemicals, alkynes - C2,C3,C4 petrochemicals, B-T-X
aromatics, diene based petrochemicals.
UNIT III (10Hours)

Second generation petrochemicals - synthesis gas, methanol, formaldehyde
chloromethanes, ethanol, acetaldehyde, acetic acid, acetic anhydride, isopropyl
alcohol, ethylene oxide, propylene oxide, acetone, vinyl chloride, phenol, aniline and
styrene.
UNIT IV (10Hours)
Third generation petrochemicals - plastics, rubbers and fibres, olefinic polymers,
polyethylene, polypropylene, polyisobutylene, diene polymers - polybutadiene,
neoprene, polyisoprene, SBR, synthetic fibres.
UNIT V (10Hours)
Miscellaneous petrochemicals - petroleum proteins, synthetic detergents, resin and
rubber chemicals, explosives - TNT and RDX.
UNIT VI (04Hours)
Threats and challenges before the petrochemical industry
TEXT BOOKS:
1.S.Maiti, “Introduction to petrochemicals”, Oxford and IBH publishing Co., 1992.
REFERENCE BOOKS:
1. H.Steines, Pergamon, “Introduction to petrochemical Industry”, 1961.
2. G.D.Hobson and W.Pohl, “Modern Petroleum Technology”, Applied Science
Publishers, IV Edition, 1975.
3. Richard frank Goldstein and A. Lawrence Waddams, “The Petroleum Chemical
Industry”, E&FN Spon Ltd., 1967.
4. G.T.Austin, “Shreve’s Chemical Process Industries”, McGraw Hill, V Edition,
1986.

CH422 ELECTIVE-II
CH422.2 INDUSTRIAL BIOTECHNOLOGY
UNIT I (10Hours)
Introduction: Basic concepts in biotechnology and historical development,
Biotechnology an interdisciplinary pursuit – public perception of biotechnology –
Biotechnology and developing world – Ethics of biotechnology – future and scope of
biotechnology.
UNIT II (10Hours)
General requirements of Fermentation Process: An overview of aerobic and
anaerobic fermentation processes and their application in industry; basic design and
construction of fermentor and its auxiliaries, sensors and monitoring instruments,
media design and sterilization for fermentation processes.
UNIT III (10Hours)
Solid and liquid substrate fermentation: cheese production – single cell protein
(SCP) – mushroom production – soya sauce production – leaching of metals – vitamin
C and vitamin B12 production – sewage treatment – biogas production – ethanol from
molasses.
UNIT IV (10Hours)
Genetics and biotechnology: The role of genes within cells, elucidation of the
genetic code, genetic elements that control gene expression, methods of creating
recombinantDNA molecules, safety guidelines of recombinantDNA research, plasmid
and phage vectors.
UNIT V (10Hours)
Food and Medicine biotechnology: Biotechnology in relation to the food industry,

types of micro-organisms brewing and alcoholic brewerages – wine production –beer
production. Antibiotics – penicillin production, vaccines and monoclonal antibodies,
human insulin production.
UNIT VI (04Hours)
Future scope of Biotechnology
TEXT BOOK:
1. John E.Smith, “Biotechnology”, 3rd edition, Cambridge University Press.
REFERENCE BOOKS:
1. Atkinson.B and Mavituna.F, “Biochemical Engineering and Biotechnology

Handbook”, McGraw HillMillan, 1993.
2. J.E.Bailey and D.F.Ollis, “Biochemical Engineering Fundamentals”, McGraw Hill,

1986.

CH422 ELECTIVE-II
CH422.3 POLYMER TECHNOLOGY

UNIT I (12Hours)
Introduction: definitions: polymer& macro molecule, monomer,
functionality, average functionality, co-polymer, polymer Blend, plastic and resin.
Classification of polymers: based on source, structure, applications, thermal behavior,
and mode of polymerization. Concept of average molecular weight of polymers,
molecular weight distribution, poly disparity index. Determination of average
molecular weights: End group analysis, osmometry, light scattering techniques,
viscometer, and Gel permeation chromatography.
UNIT II (04Hours)
Natural polymers: brief study of i) Natural rubber ii) shellac iii) rosin
iv) cellulose v) proteins.
UNIT III (06Hours)
Mechanism and kinetics: Addition or chain polymerization a) Free
radical addition polymerization b) Ionic addition polymerizations c) Coordination
polymerization. d) Coordination or step growth or condensation polymerization.
UNIT IV (10Hours)
Methods of polymerization: mass or Bulk polymerization process,
solution polymerization process, suspension polymerization process and emulsion
polymerization method comparison of merits and demerits of these methods.
Properties of polymers: crystalline and amorphous status, melting and glass transition
temperatures and their determination, effect of polymer structure on mechanical,
physical, chemical and thermal properties.
UNIT V (10Hours)
Degradation of polymers, Role of the following additives in the
polymers: i) Fillers and reinforcing fillers ii) Plasticizers iii) Lubricants iv)
Antioxidants and UV stabilizers v) Blowing agents vi) Coupling agents vii) Flame
retardants viii) Inhibitors
Brief description of manufacture, properties and uses: i) Polyethylene
(HDPE&LDPE), ii) Poly propylene iii) Polyvinylchloride iv) Polystyrene v) Polytetra
fluoroethylene vi) Polymethyl methacrylate vii) Polyvinyl acetate & Polyvinyl
alcohol
UNIT VI (10Hours)
Brief description of manufacture, properties and uses: i) Polyesters
(Polyethylene terephalate polycarbonate and unsaturated polyesters) ii) Nylon (Nylon
66) iii) Phenol- Formaldehyde resins iv) Epoxy resins v) Polyurethane vi) Silicones
Compounding of polymer resins, brief description: i) Compression and
transfer moulding ii) Injection moulding iii) Extrusion iv) Blow moulding v)
Calendaring vi) Laminating and pultrusion
TEXT BOOKS:
1. J.A. Brydson, Newnes-Butterwarths “Plastic materials”, (London) 1989.
2. Bill Meyer, F.W.Jr., “Text book of polymer science”, (3rd edition.) John
Wiely&sons 1984
REFERENCE BOOKS:
1. J.H. Brison and C.C. Gosselin, “Introduction to plastics”, Newnes, London 1968.
2. C.C.Winding and G.D.Hiatt, “Polymeric Materials”, McGraw Hill Book Co. 1961
3. Gowarikar, “Polymer Science”

CH422 ELECTIVE-II
CH422.4 FOOD PROCESS TECHNOLOGY
UNIT I (06Hours)
An overview: General aspects of food industry; world food needs and Indian
situation.
UNIT II (10Hours)
Food constituents, quality and derivative factors: Constituents of food; quality and
nutritive aspects; food additives; standards; deteriorative factors and their control
UNIT III
General engineering aspects and processing methods (10Hours)
Preliminary processing methods; conversion and preservation operations.
UNIT IV (10Hours)
Food preservation methods : Preservation by heat and cold; dehydration;
concentration; drying irradiation; microwave heating; sterilization and pasteurization;
fermentation and pickling; packing methods.
UNIT V
Production and utilization of food products (10Hours)
Cereal grains; pulses; vegetables; fruits; spices; fats and oils; bakery; confectionery
and chocolate products; soft and alcoholic beverages; dairy products; meat; poultry
and fish products.
UNIT VI (04Hours)
Threats and challenges before the Food Processing Industry
REFERENCE BOOKS:
1. Heid, J.L; Joslyn, M.A., " Fundamentals of Food Processing Operation ", The AVI
Publishing Co., Westport, 1967.
2. Potter, N.N.; " Food Science ", The AVI Publishings Co., Westport, 1963.
3. Heldman D.R.; " Food Process Engineering ", The AVI Publishing Co., Westport,
1975.
4. Charm, S.E.; " The Fundamentals of Food Engineering ", The AVI Publishing Co.,
Westport, 1963
5. R. Macral, R. K. Robinson, and M. J. Sadler, Encyclopedia of Food Science, Food
Technology and Nutrition, Vol. 8, Academic Press 1993.

CH422 ELECTIVE-II
CH422.5 CATALYSIS
UNIT I (08Hours)
Review of chemical kinetics, homogeneous catalysis, acid base catalysis
UNIT II
Enzymatic reaction kinetics and design for enzymatic reaction. (08Hours)
UNIT III (08Hours)
Heterogeneous catalysis: reaction rates and selectivity, Fixed bed and fluidized bed
catalytic reactors.
UNIT IV (10Hours)
Catalyst deactivation with separable kinetics, Reactor Design with and without
catalyst deactivation, temperature – time trajectories, effect of deactivation on
selectivity, determination of order of deactivation by integral and differential
methods.
UNIT V (08Hours)
Role of diffusion in catalysis.
UNIT VI
Selection, preparation, and evaluation of catalysts. (08Hours)
REFERENCE BOOKS:
1.H. S. Fogler., “Elements of Chemical Reaction Engineering”, PHI, 3 rd Ed. (2002).
2.O. Levenspiel, “Chemical Reaction Engineering”, John Wiley, 3 rd Ed. (1999).
3.J. M. Thomas and W. J. Thomas, “Introduction of the Principles of Heterogeneous
Catalysis”, Academic Press, (1967).
4.C. N. Satterfield and T.K. Sherwood, “The Role of Diffusion in Catalysis”, Addison
Wesley, (1963).
5.P. H. Emmett (Ed.), “Catalysis”, Reinhold, (1954.)

CH422 ELECTIVE-II
CH422.6 ENVIRONMENTAL CHEMISTRY AND BIOCHEMISTRY
UNIT I
Biochemistry (10Hours)
Structure of Cell, Structure and function of biologically important compounds such as

carbohydrates protein, Lipids enzymes and Amino acids, Nucleic acids.
UNIT II (08Hours)
Environmental Chemistry Basics
UNIT III (08Hours)

Noise Pollution: Introduction, The describe scale, effects of noise – physiological and
psychological effects, Measurement of noise levels, Noise control in industrial
establishments.
UNIT IV (10Hours)
Environmental Toxicology: Classification of toxic materials, toxicity testing, toxic
effects of hydrocarbons, alcohols, aldehydes, ketones, amines.
UNIT V (10Hours)
Environmental Toxicology and control: toxic effects and control of metal pollutants
like Hg, Col, Pb, V, Cr, Co, etc. Disease measurement and control of occupational
diseases.
UNIT VI (06Hours)
Future of Environmental sciences
TEXT BOOKS:
1. S. M. Khopkar, “Environmental Pollution Monitoring & Control”, New Age
2. T. G. Spiro, W. M. Stigliani, “Chemistry of Environment”, PHI
REFERNECE BOOKS:
1. A. K. Das, “Textbook on Medical Aspects of Bioinorganic Chemistry”, CBS
2. Nelson Cox and Lehninger, “Biochemistry”
3. M. Ather & S. B. Vohra, “Heavy Metal & Environment”, New Age
4. S. S. Dara, “Environmental Chemistry » latest edition

CH422 ELECTIVE-II
CH422.7 OPEN ELECTIVE
The interested students have to choose the open elective from any of the
specialized program available on the campus. The students have to contact the
concerned subject teacher and attend the classes in the respective subject which will
be taught by the concerned teacher.

CH423 PROCESS MODELING AND SIMULATION

Unit-I (06Hours)
Mathematical models for chemical engineering systems, fundamentals, introduction to
fundamental laws
Unit -II (10Hours)

Examples of mathematical models of chemical engineering systems, constant volume
CSTRS, two heated tanks, gas phase pressurized CSTR, non-isothermal CSTR.
Examples of single component vaporizer, batch reactor, reactor with mass transfer,
ideal binary distillation column, batch distillation with holdup.
Unit –III (10Hours)
Iterative methods, bisection, false position, Newton –Raphson, successive
approximation methods, comparison of iterative methods, solution of linear
simultaneous algebraic equations, Computation of Eigen values and Eigen vectors,
Gauss elimination method, Gauss-Jordan and Gauss-Seidel’s method.
Unit –IV (10Hours)
Numerical integration by Trapezoidal and Simpson’s rules, numerical solution of
differential equations, Euler method, Runge-Kutta fourth order method. Interpolation,
Lagrange interpolation, forward difference, backward difference and central
difference interpolation methods, least square approximation of functions, linear
regression, and polynomial regression.
Unit –V (10Hours)
Study of different simulation software, Computer simulation, examples,
gravity flow tank, three CSTRs in series, binary distillation column, batch reactor
Unit –VI (06Hours)
Simulation of Non-isothermal CSTR, VLE dew point, bubble point calculations,
countercurrent heat exchanger
TEXTBOOKS:
1. W. L. Luyben, Process modeling simulation and control for chemical engineers
McGraw Hill, 2nd Ed.
2. S.K. Gupta, Numerical methods in engineering, Tata McGraw Hill.
REFERENCE BOOKS:
1. B. S. Grewal, Engineering Mathematics
2. K.Balu and K.Padmanabhan, Modeling and analysis of Chemical Engineering
processes, International private limited, 2007

CH424 SPECIAL CHEMICAL TECHNOLOGIES-II
UNIT I Green Technology: (14 Hours)
Green Chemistry: An Overview Introduction, underlying philosophy and focus, Twelve

principles of green chemistry, Ecological Threats & Green Chemistry, The Greenhouse
Effect, Climate Change, photochemical smog, Pragmatic Green, Chemistry Challenges, Old
Technology vis-à-vis Green Technology : Suitable examples, to understand comparative
advantage of Green Technology over Old one, Renewable, resources, Process intensification ,
Carbon credits .Green Chemistry & Nonconventional Fuels, Green chemistry in batteries,
production and recycling, Fuel cell and electric vehicles, Solar energy and hydrogen
production,biodiesel, bio-hydrogen, Green Chemistry & Sustainable development,
Esterification: transesterification, autogeneous pressure of methanol, transesterification under
supercritical conditions Optimisation: catalyst concentration, methanol to oil ratio, reaction
temperature, reaction time.
UNIT II Sugar Technology: (12 Hours)
Sugar Industry in India: Chemical and physical properties of sucrose and reducing sugars.
Sources for sucrose. Formation of sucrose plants. Non-sugar compounds of sugarcane.
Inorganic constituents of sugar cane juices and sugars analytical methods used in sugar
industry. Purification: Chemical technology of the purification process. Fundamental
reactions and physical chemistry aspects of clarification, liming, sulphitation and carbonation
process. Filtration of sugar juice. Evaporation: Evaporation of sugar juice. Heat transfer in
evaporations. Evaporation equipment and auxiliaries. Evaporation: Methods of obtaining
steam, and quality of steam. Steam economy. Chemistry of the evaporation process.
Crystallography: Solubility of sucrose. Nucleation in super saturated solutions – kinetics and
growth of crystallization. Chemistry of crystallization. Crystallography: Control methods and
equipment in sugar crystallization, technology of sugar crystallization. Evaporation and
circulation in vacuum pans. Centrifugation: Theory of the centrifugal process, centrifugal
operation. Centrifugation: Engineering principles of sugar centrifugals and the centrifugal
equipment and auxiliaries. Production of final molasses and molasses’s utilization. Grading of
sugar.
UNIT III Textile wet processing technology (Textile Chemistry): (14 Hours)
Brief introduction to textile industry. Study of various steps involved in the chemical
processing of textiles (pretreatments and after treatments like dyeing, printing and finishing.)
Chemistry and processes for desizing, scouring, bleaching and mercerization. Study of
applications of reactive, vat and other classes of dyestuff on various textiles. Study of all the
above treatments in chemical processing of textiles from stand point of unit operations of
chemical engineering.
UNIT IV Nanotechnology: (14 Hours)
Introduction to Nanotechnology, Nanotechnology-Definition, Classification and Applications,

Processes for producing ultrafine powders-mechanical grinding, wet chemical synthesis of
nanomaterials. Gas phase synthesis of nano materials, gas condensation processes, chemical
vapour condensation, laser ablation. Special nanomaterials, characterization and Applications
for Carbon nanotubes, nano composites, nano fluids-An overview over preparation,
properties, applications. Nanoelectronics: Introduction – micro, nano fabrication: Optical
lithography, Electron beam lithography, Atomic lithography, Molecular beam epitaxy,
MEMS, NEMS –A
TEXT BOOKS:
1.Principles of Sugar Technology - Honing P. Vol. I to III, Elsevier Publishing Company,
1953.
2.Jenkinos.G.H Elsevier, 1966. Introduction to Cane Sugar Technology .
3.Paul T. Anastaj; “Green Chemistry – Theory and Practice”
4.Albert S. Matlack; “Introduction to Green Chemistry”
5. George T. Austin, “Shreve's Chemical Process Industries”, 5th edition. McGraw Hill Book
Company, 1985.
REFERENCE BOOKS:
1. Handbook of Cane Sugar Technology - Mathur R.B.L 2nd Edition, Oxford and I.B.H.
Publishing Co., 1997.
2. Jink. R.W. and Pan Cost H.M, Handbook of Sugars, Avi Publishing Co., 1974.
3.Anastas, P.; Zimmerman, J. “Design through the Twelve Principles of Green Engineering,”
Environmental Science and Technology, 37, 94A – 101A, 2003.
4.Tyron. L. Vigo, Textile Processing and properties, 1994 Elsevier.
5. S. Kawabek, Objective Parameters of fabric, 1999, Textile Machinery Society Kyoto.
6. J.Dutta & H.Hofman, “Nano materials”,
7.. Guozhong cao, “Nano structures & Nano materials”, Imperial college press.
8. N.P.Mahalik., “Micro manufacturing and Nano Technology”
9. Mark Ratner & Denier Ratner, “Nano Technology”, Prentice Hall
10. A S Edelstein& R C Cammarata, “Nano materials”, Institute of physics publishing,
Bristol and Philadelphia.

CH425 TRANSPORT PHENOMENA

UNIT I (10Hours)
Equations of Change: Differential equations of continuity and motion.
Representation using tensor notation. Navier-Stokes equations. Meaning and examples of
constitutive equations. Application of N-E equation to flow in specific geometries such as
laminar flow through pipe, Tangential annular flow, Radial flow between parallel disks /
concentric spheres / concentric cylinders, Falling film. Models of Non-Newtonian flow.
Non-Newtonian laminar flow through pipe. Flow of two adjacent immiscible fluids
through pipe. Solution of at least three of the above stated or analogous cases using shell
balance approach. Comparison of approaches.
UNIT II (08Hours)
Boundary Layer Theory and Turbulence : Prandtl’s equations. Steady flow
laminar boundary layer on a flat plate parallel to the flow. Blasius solution. Boundary
layer thickness. Displacement thickness. Momentum thickness. Boundary layer drag.
Turbulence. Importance in heat and mass transfer applications. Decay and production of
turbulence. Kinetic energy of turbulence. Scale of turbulence. Reynolds’s stresses. Eddy
viscosity.
UNIT III (08Hours)
Mixing: Types of mixing problems usually encountered in process industries.
Mixing in stirred tanks. Power number-Reynolds number correlation. Power input and
mixing time calculations. Zwietering correlation for suspension of solid particles.
Agitation equipment. Standard turbine design. Scale up of agitator design. Motionless
mixers.
UNIT IV (08Hours)
Unsteady State Heat Transfer: Calculation of heating and cooling time for
agitated liquid batch in coil-in-tank or jacketed vessel and also in a vessel with external
heat exchanger.
UNIT V (08Hours)
Analogies between Heat, Momentum and Mass Transfer: Extension of Blasius
solution for the laminar boundary layer on a flat plate to include (a) convective heat
transfer and (b) convective mass transfer problems for the same geometry and laminar
flow. Mass, energy and momentum transfer analogies.
UNIT VI (08Hours)
Computational Fluid Dynamics and Two Phase Flow: Introduction to the
process of discretization and use of grids. Solution of unsteady state one dimensional
laminar flow equation using CFD approach. Extension to analogous problems in heat and
mass transfer. Issue of numerical stability. Two phase flow in horizontal and vertical
pipes. Different flow regimes. Pressure drop and void fraction calculations.
REFERENCE BOOKS:
1. Noel de Nevers, “Fluid Mechanics for Chemical Engineers”, Third Edition;

McGraw Hill, 2005.
2. Geankoplis C. J, “Transport Processes and Separation Process Principles”,
Fourth Edition; Prentice Hall India, 2003.
3. Bird R. W. Stewart and E. Lightfoot, “Transport Phenomena”, Second
Edition; John Wiley and Sons Inc., 2002.
4. Kern D. Q., “Process Heat Transfer”, McGraw Hill, 1965.
HS421T INDUSTRIAL SAFETY AND HAZARD MANAGEMENT
Teaching Scheme: T: 1 hours/week Credits: 1
During the tutorial, the subject in charge is required to impart the subject
knowledge to the students. Also it is expected to encourage discussion in the class. It
is desired to give the assignments to the students, ask them to prepare charts related to
industrial safety so that they will also self study the subject content and they will be
asked to deliver seminar on a topic relevant to the subject.
UNIT I (03Hours)
Introduction: Types of Ecosystems, Factors responsible for the distribution on
Hydrologic cycles, Nutrient cycles (carbon, nitrogen, phosphorous, sulfur).
UNIT II (02Hours)
Introduction to ISO standards: ISO standards (ISO 14001) with reference to
chemical industry.
UNIT III (02Hours)
Industrial hygiene and safety aspects related to toxicity, noise, radiation:

identification, Evaluation, Control
UNIT IV (06Hours)
Fires and Explosions: Flammability Characteristics of liquids & vapors, minimum
oxygen concentration (MOC), Ignition Energy, Ignition sources, Explosions:
Detonation & Deflagration, combined explosions, BLEVE, Blast Damage due to
overpressure. Hazard identification: Various Techniques, HAZOP.
UNIT V (05Hours)
Consequence analysis: Flow of liquid/vapors through hole, flashing liquid, Pool
evaporation. Design to prevent fire & explosions: Inerting, controlling static
electricity, explosion proof equipments & instruments, ventilation, sprinkler systems.
UNIT VI (06Hours)
Hazards / Risk Assessment: Event trees, fault trees, reliability, probability,

Emergency planning: Elements of emergency planning, on-site/ off-site emergency,
plans. Case studies: Bhopal Tragedy, Flixborough Disaster, Mexico Disaster
REFERENCES BOOKS:
1. “Chemical Process Safety Fundamentals with Applications”, Daniel A Crowl,
Joseph
F.Lovvar, Prentice Hall Inc, U.S.A
2. “Safety in Process Plant Design”, Wells, G.L. Godwin, London (1980)
3. “Loss Prevention in Process Industries”, Lees, F.P. Butterworth, Oxford
4. “Environmental Protection”, Chanlett, E.T. McGraw Hill
5. “Strategy of Pollution Control”, Berthouex, P.M., and Rudd, D.F. Wiley (1977)
6. “Safety for Chemical Engineers”, A.I.Ch.E. Publications (1976-77).

CH423L PROCESS MODELING AND SIMULATION Laboratory

SIMULATION LABORATORY
The following experiments have to be conducted using C/C++/Simulink using
MATLAB
1. Gravity Flow tank.
2. Three CSTR’s in series – open loop
3. Three CSTR’s in series – Closed loop
4. Non isothermal CSTR
5. Binary Distillation column
6. Batch Reactor isothermal; Batch reactor non isothermal – closed loop
7. Isothermal batch reactor – open loop
8. Heat Exchanger
9. Interacting System- two tank liquid level
10. Non interacting system-two tank liquid level
11. Plug flow reactor
12. Bubble point calculations
13. Dew point calculations
Major requirements are Personnel Computer and MATLAB Software

CH426L MAJOR PROJECT (PHASE II)
Teaching Scheme: P: 03 hours/week Credits: 2

T: 01 hours/week
The students are required to carry out one of the following projects.
1. Process based Project: Manufacture of product.

2. Equipment based Project: Detailed design and fabrication of the equipment for a
given capacity.
3. Experimental based Project: Experimental investigation of basic or applied research
problem.
4. Industrial Problems: Any problem or project directly related to existing plants for
modification of process or equipment or regarding pollution control and energy
conservation under the guidance of a staff member and /or staff members and submit
a typed report in duplicate.
The Project Work consists of collection of literature, study of the various

processes selection of the process, computation of material and energy balances,
process design of important equipments, detailed design of one of the main
equipment, plant location and layout, cost Estimation, economic analysis, details of
experimental set up, analysis of data, pollution control, safety, marketing, conclusions
and recommendations, bibliography, etc., as applicable to the individual problem.
The object of the project is to make use of the knowledge gained by the student at
various stages of the degree course. This helps to judge the level of proficiency,
originality and capacity for application of the knowledge attained by the student at the
end of the course.
Each group should consist of maximum 5 students. For term-work (Internal)

of 100 marks, the assessment should be by conducting frequent written tests, seminars
during the year and an oral examination at the end of the year conducted by all the
staff members of the department. The Head of the Department should see that the
assessment procedure should be the same for all the students of the class.
For external 100 marks, the project work shall be assessed by an oral examination by
at least two examiners, one internal and one must by external at the end of the year.
The object of the VIVA VOCE examination (Internal and External Orals) is to
determine whether the objectives of the project work have been met by the student as
well as to assess the originality and initiative of the student as demonstrated in the
project work.
Shivaji Shivaji University, Kolhapur
Audit Course V
HS 422 CONSTITUTION OF INDIA
Teaching Scheme: P: 2hrs/week No Credits
UNIT I (05 Hours)

Preamble to the constitution of India. Fundamental rights under Part – III –
details of Exercise of rights, Limitations & Important cases.
UNIT II (05Hours)
Relevance of Directive principles of State Policy under Part – IV.
Fundamental duties & their significance.
UNIT III (05 Hours)

Union Executive – President, Prime Minister, Parliament & the Supreme
Court of India.
UNIT IV (04 Hours)

State executive – Governors, Chief Minister, State Legislator and High Courts.
UNIT V (05 Hours)

Constitutional Provisions for Scheduled Castes & Tribes, Women & Children
& Backward classes. Emergency Provisions.
UNIT VI (04 Hours)

Electoral process, Amendment procedure, 42nd, 44th, 74th, 76th, 86th and
91st Constitutional amendments.
Text Book:
1. Durga Das Basu: “Introduction to the Constitution of India”(Students Edn.)
Prentice – Hall EEE, 19th/20th Edn., 2001.
2. R.C.Agarwal, “Indian Political System”, (1997) S.Chand and Company, New
Delhi.
Maciver and Page, “Society: An Introduction Analysis”, Mac Milan India
Ltd., New Delhi.
3. K.L.Sharma, “Social Stratification in India: Issues and Themes”,(1997),
Jawaharlal Nehru University, New Delhi.
Reference Book:
1. An Introduction to Constitution of India” by M.V.Pylee, Vikas Publishing,
2002.
Sharma, Brij Kishore, “Introduction to the Constitution of India:, Prentice Hall
of India, New Delhi.
2. U.R.Gahai, “(1998) Indian Political System “, New Academic Publishing
House, Jalaendhar.
3. R.N. Sharma, “Indian Social Problems “, Media Promoters and Publishers Pvt.
Ltd.
4. Yogendra Singh, “(1997) Social Stratification and Charge in India “, Manohar,
New Delhi.
Equivalence of Final Year B.Tech (Chemical Technology) Semester VII and VIII
The above detailed syllabus is a revised version of the Final Year.BTech

(Chemical Technology) course being conducted by the Shivaji University at the
Technology Department of the University. This syllabus is to be implemented from
June 2014. (Academic year 2014-15)
The Equivalence for the subjects of Chemical Technology at Final Year B

Tech Semester VII and VIII pre-revised course under the faculty of Engineering and
Technology is as follows.
Final Year.B Tech Semester VII (Chemical Technology)
Sr.No Final Year. BTech(Chemical) Final Year.BTech(Chemical) Remark

Semester VII Semester VII
Pre-revised syllabus Revised syllabus
1. No change. Only it is converted to
Advanced Separation Techniques Advanced Separation credits
Techniques
2. Special Chemical Technologies-I Special Chemical Minor changes (avoiding repetition
Technologies-I of chapters and adding
‘biotechnology introduction’ as
one more chapter) in the subject
content have been made
3. -------------------------------------- Reaction Engineering – II Introduced by split up of Chemical
Reaction Engineering subject from
semester VI into two parts
credits and one subject is added in
Elective –I Elective –I
the list and it is converted to
credits
Process Modeling and Simulation ------------------------- credits. And Shifted to VIII
Semester
6. Process Economics and Project Shifted from VIII Sem
------------------------------------
Engineering
Transport Phenomena -------------------
credits. Shifted to VIII Semester
Major Project(Phase I ) Major Project(Phase I )
credits
9. No change. Only it is included as
Audit Course V. Evaluation to be
Professional Ethics Professional Ethics
done at the institute level. It has no
credits.
10. Report of Industrial Training Report of Industrial Training No change. Only it is converted to
credits
The examination pattern is changed from percent marks into credit system and the
contents in all the subjects have been unitized into mostly 6 numbers.
The students from the pre-revised syllabus need not complete the course work of any
newly added subject.
Audit course is added which is not a part of credits. It is evaluated by AWARD of

grade which is based on conversion of marks obtained out of 50. (Obtaining passing
grade is essential)
Final Year.B Tech Semester VIII (Chemical Technology)
Sr.No. Final Year. BTech(Chemical) Final Year.BTech(Chemical) Remark

Semester VIII Semester VIII
Pre-revised syllabus Revised syllabus
1. Energy Conservation in Chemical Energy Conservation in No change. Only it is converted to

Industries Chemical Industries credits
2. Elective-II Elective-II No change. Only it is converted to
credits
3. The subject contents are merged
Nanotechnology ----------------------------
into SCT-II
4. Process Economics and Project No change. Only it is converted to
-----------------------------
Engineering credits and it is shifted to Sem VII
5. Process Modeling and Shifted from Sem VII
---------------------------------
Simulation
6. Has been little modified with a
Special Chemical space for a chapter on
Special Chemical Technologies-II
Technologies-II nanotechnology. And it is
converted to credits.
7. Only shifted from Sem VII to Sem
---------------------------- Transport Phenomena
VIII and converted to credits.
8. Industrial Safety and Hazard Industrial Safety and Hazard No change. Only it is converted to
Management Management credits

Plant Design and Case studies Plant Design and Case studies credits

Major Project(Phase II)
Major Project(Phase II) credits
11. Introduction to Constitution of Introduced Constitution of India

---------------------------------- subject as the Audit Course-VI
India
The examination pattern is changed from percent marks into credit system and the
contents in all the subjects have been unitized into mostly 6 numbers. (Chapters)
The students from the pre-revised syllabus need not complete the course work of any
newly added subject i.e. Introduction to Constitution of India.
Audit course is added which is not a part of credits. It is evaluated by

AWARD of grade which is based on conversion of marks obtained out of 50.
(Obtaining passing grade is essential)

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SHIVAJI UNIVERSITY, KOLHAPUR – Syllabus w.e.f.

SHIVAJI UNIVERSITY, KOLHAPUR

6 Advanced Separation Techniques

Total Contact hours per week = 29

List of Subjects as Elective-I:

SHIVAJI UNIVERSITY, KOLHAPUR

Sr. Contact Hours

9. HS422 Audit Course VI 02 - - -

List of Subjects as Elective-II:

CH422.1 Petrochemical Technology, CH422.2. Industrial Biotechnology, CH422.3. Polymer Technology,

Shivaji University, Kolhapur

CH411 ADVANCED SEPARATION TECHNIQUES

Teaching Scheme: L: 4 hours/week Credits: 4

UNIT I Introduction to the subject (04Hours)

Review of conventional separation techniques. Concept of advanced

UNIT III (10Hours)

desorption, Polymer de volatilization and fractionation, Drying and Aero gel

Shivaji University, Kolhapur

CH412.1 PETROLEUM REFINERY ENGINEERING

Teaching Scheme: L: 4 hours/week Credits: 4

UNIT I Introduction (08Hours)

UNIT II Refining of petroleum (08Hours)

UNIT IV Treatment techniques (10Hours)

UNIT V Cracking and Reforming (10Hours)

UNIT VI Threats and Challenges before Petroleum Industries (08Hours)

Shivaji University, Kolhapur

CH412.2 BIOCHEMICAL ENGINEERING

Teaching Scheme: L: 4 hours/week Credits: 4

UNIT I Introduction (08Hours)

UNIT II Kinetics of enzyme catalyzed reactions (10Hours)

UNIT III Metabolic pathways and energetics of the cell (10Hours)

UNIT IV Typical growth characteristics of microbial cells (10Hours)

UNIT V AND VI Introduction to bio reactors and Future Trends (14Hours)

1. M.L.Shuler and F.Kargi, “Bioprocess Engineering: Basic concepts”, 1st Edition,

Shivaji University, Kolhapur

CH412.3 POLYMER CHEMISTRY

Teaching Scheme: L: 4 hours/week Credits: 4

UNIT I Scope of Polymer Chemistry (08Hours)

UNIT II Condensation polymerization (10Hours)

UNIT III Addition polymerization (10Hours)

UNIT IV Characterization of molecular weight polymers (10Hours)

UNIT V AND VI Application of polymers present and future (12Hours)

Shivaji University, Kolhapur

CH412.4 INTRODUCTION TO FOOD PROCESS ENGINEERING

Teaching Scheme: L: 4 hours/week Credits: 4

UNIT I Food chemistry (08Hours)

UNIT II Transport Phenomena in food processing (10Hours)

UNIT III Preservation techniques (10Hours)

UNIT IV Packaging and storage (10Hours)

UNIT V Post Harvesting Techniques (07Hours)

UNIT VI Supercritical extraction (07Hours)

Shivaji University, Kolhapur

CH412.5 SURFACE CHEMISTRY

Teaching Scheme: L: 4 hours/week Credits: 4

Shivaji University, Kolhapur

CH412.6 ENVIRONMENTAL SCIENCE AND MICROBIOLOGY

Shivaji University, Kolhapur

CH412.7 DRUGS AND PHARMACEUTICAL TECHNOLOGY

Teaching Scheme: L: 4 hours/week Credits: 4