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    Experiment No. 12,13,14,15

    Uploaded by

    Shweta Singh
    The document describes procedures for preparing three different pharmaceutical preparations: 1) Peppermint Spirit by dissolving peppermint oil in alcohol and filtering to produce a clear liquid. It is used aromatically and in dental preparations. 2) Chloroform Spirit by mixing chloroform and alcohol in a ratio of 50:10 ml. It is used as a preservative and stored in a closed container. 3) Starch Mucilage by boiling starch in water to form a gel, then diluting to 100ml with water. It is used as an emulsifying and suspending agent and stored in a cool place.

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    © All Rights Reserved
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    Experiment No. 12,13,14,15

    Uploaded by

    Shweta Singh
    465 views4 pages
    The document describes procedures for preparing three different pharmaceutical preparations: 1) Peppermint Spirit by dissolving peppermint oil in alcohol and filtering to produce a clear liquid. It is used aromatically and in dental preparations. 2) Chloroform Spirit by mixing chloroform and alcohol in a ratio of 50:10 ml. It is used as a preservative and stored in a closed container. 3) Starch Mucilage by boiling starch in water to form a gel, then diluting to 100ml with water. It is used as an emulsifying and suspending agent and stored in a cool place.

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    EXPERIMENT NO. 12,13,14,15

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    The document describes procedures for preparing three different pharmaceutical preparations: 1) Peppermint Spirit by dissolving peppermint oil in alcohol and filtering to produce a clear liquid. It is used aromatically and in dental preparations. 2) Chloroform Spirit by mixing chloroform and alcohol in a ratio of 50:10 ml. It is used as a preservative and stored in a closed container. 3) Starch Mucilage by boiling starch in water to form a gel, then diluting to 100ml with water. It is used as an emulsifying and suspending agent and stored in a cool place.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    465 views4 pages

    Experiment No. 12,13,14,15

    Uploaded by

    Shweta Singh
    The document describes procedures for preparing three different pharmaceutical preparations: 1) Peppermint Spirit by dissolving peppermint oil in alcohol and filtering to produce a clear liquid. It is used aromatically and in dental preparations. 2) Chloroform Spirit by mixing chloroform and alcohol in a ratio of 50:10 ml. It is used as a preservative and stored in a closed container. 3) Starch Mucilage by boiling starch in water to form a gel, then diluting to 100ml with water. It is used as an emulsifying and suspending agent and stored in a cool place.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 4

    EXPERIMENT NO.

    12

    OBJECT
    To prepare and dispense Peppermint Spirit 50 ml (Ref. BPC - 1968).

    REFERENCE
    Jain N.K. Sharma S.N. "A textbook of professional pharmacy", reprint 2006, Vallabh
    Prakashan, New Delhi, p.p. 224.

    FORMULA
    Peppermint Oil - 100 ml
    Alcohol (90%) (q.s.) - 1000 ml

    THEORY
    Spirits or essence consists of alcoholic or hydroalcoholic solution of volatile substances.
    Brandy and whisky were the first spirits. Spirits generally contain a high conc. of
    alcohol. As aromatic and volatile substances are more soluble in alcohol. Spirits can
    hold a greater conc. of these materials in solution than the corresponding aromatic
    waters.

    PROCEDURE
    Firstly, dissolved the peppermint oil in alcohol and shake it the solution not cleared
    then, Shaked it with talc. And then, set it aside and filtered to clear liquid and transferred
    into dispensing bottle.

    USES
    Aromatic and in dental preparation.

    STORAGE
    Should be stored in well tight container.
    EXPERIMENT NO. 13

    OBJECT
    To prepare and disperse Chloroform spirit 10 ml I.P. 1966.

    REFERENCE
    Jain N.K. Sharma S.N. "A textbook of professional pharmacy", reprint 2006, M.K. Jain
    for Vallabh Prakashan, Pitampura, Delhi.

    FORMULA
    Chloroform - 50 ml
    Alcohol (q.s.) - 10 ml

    THEORY
    Spirit consist of alcoholic or hydro-alcoholic solution of volatile substance.

    PROCEDURE
     0.5 ml of chloroform was taken will the help of pipette.
     10 ml of alcohol (90%) was added to the solution.
     The solution was then transferred to the dispensing bottle and labelled.

    STORAGE
    Store in a well closed container.

    USES
    Used as a preservative.
    EXPERIMENT NO. 14

    OBJECT
    To prepare and dispense Starch mucilage 100 ml.

    REFERENCE
    Jain N.K. Sharma S.N. "A textbook of professional pharmacy", reprint 2006, Vallabh
    Prakashan, New Delhi, p.p. 176.

    FORMULA
    Starch - 2.5 g
    Purified Water (q.s.) - Upto 100 ml

    THEORY
    These are also employed as diluting agents for water soluble substances and are
    especially useful in stabilizing suspensions and emulsions. Acacia mucilage is an
    outstanding example which is also employed as emulsifying and suspending agents.

    PROCEDURE
    60 ml of water was boiled in 500 ml conical flask to this was added the suspension made
    (in mortar) of 2.5 g starch and 30 ml water.
    When the suspension came in gelatin form after continuous stirring which is free from
    lumps it was removed from heat and rotated under cold water stream. To maintain the
    level up to 100 ml water was added in the conical flask. Then the mucilage was
    transferred into a dispensing bottle and labelled it.

    STORAGE
    Store in a cool place and air tight container.

    DOSE
    As directed by physician.

    USES
    As emulsifying and suspending agent.
    EXPERIMENT NO.15

    OBJECT
    To prepare and submit throat paint.

    REFERENCE
    Carter S.J., "Dispensing for Pharmaceutical Students", 12th edition, reprints 2005, CBS
    Publishers, New Delhi, pp. 84 to 85.

    FORMULA
    Potassium Iodide 25g
    Iodine 12.5g
    Ethanol 40 ml
    Distilled water 25 mL
    Peppermint oil 4 mL
    Glycerine 1000 mL

    THEORY
    Throat paints are simple solutions of substances in viscous solvents such as glycerine
    and liquid paraffin. Due to their high viscosity they are used for infections of mouth and
    throat. The other name for mouth paint is Mandl’s Paint.

    PROCEDURE
    Dissolve potassium iodide in small amount of water and then dissolve iodine into it.
    Finally add peppermint oil and alcohol and make up the volume with glycerol.

    STORAGE
    Store in cool dry place away from light in dark bottles.

    USE
    For mouth and throat infections.

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