Cetie Guide No1 Eng
Cetie Guide No1 Eng
Cetie Guide No1 Eng
PRACTICAL GUIDELINE N° 1
Edition 2008
CAPPING OF STILL WINES ON A CORK MOUTH FINISH
Contributors
• Sofia Afonso CE Liège
• Jean-Marie Aracil FFSL - Fédération Française des Syndicats du Liège
• Thierry Bergeon Thierry Bergeon Embouteillage
• Jean-Marc Berthier Gai France
• Jean-Michel Blanc Saint-Gobain Emballage
• Francis Bonnel Chantovent
• Jacques Chantereau Ets André Zalkin
• Grégory Choplin Ets André Zalkin
• Michel Coulet Thierry Bergeon Embouteillage
• Alexandre Depoortere Arol
• Delphine Ducasse FFSL - Fédération Française des Syndicats du Liège
Ducasse-Buzet
• Jean-Michel Fox Nomacorc
• Felix Gonzalez Ramondin Capsules
• Jacques Granger Alcan Packaging Capsules
• Bruno Guillemat Pernod Ricard
• Mickael James Nomacorc
• Thierry Laborie Euralis Agro Vigne
• Michel Laure Arol
• Yves Lehmann Nomacorc
• Jacques Lemblé FFSL - Fédération Française des Syndicats du Liège
Bouchons Trescases
• Pascal Montier Saint-Gobain Emballage
• Jacinthe de Montecler Pernod Ricard
• Sergio Moutinho CE Liège
• Marcos Garcia Muñoz Anfevi
• Jean-Michel Riboulet Cevaqoe
• Yannick Riou Remy Kaps
• Giuseppe Sicco Saint-Gobain Vetri
• Martine Sow Novembal
• Jean-Claude Tissot O-I Europe
• Anthony Vallée Ets André Zalkin
Animator
• Patrick Bizart Oeneo-Bouchage
INTRODUCTION
This new edition is the up-dating of the French language practical guide entitled Capping
of still wines on a cork mouth finish, edited in 1996 by INE, Institut National de
l’Embouteillage ; INE has been merged in CETIE at January 1st, 2002.
Fulfilling the obligation of suppliers to inform the users, they also contribute to guarantee
the delivery on the market of safe and wholesome products as well as consumer safety.
Such characteristics are essential to secure the durability of products.
Various European involved parties have participated in the writing of this practical guide.
All drawings and pictures shown in this guideline are given as examples to facilitate the
understanding of explanations. As a consequence, they are neither a recommendation
of equipments nor representing the whole existing equipments available on the market.
FOREWORD
This guideline applies to the capping of still wines with a cork mouth finish as per CETIE
data sheet GME 50.01 which has been used as a base for the European standard EN
12726.
If application is done on another finish, the user must carry out sealing tests to ensure
that this application is technically acceptable.
Still wines are defined as having a level of carbonation below 1.2 grams per litre of
liquid, and for which the over-pressure due to carbon dioxide is below one bar in sealed
containers when kept at a temperature of 20°C.
For wines with a level of carbonation above 1.2 grams per litre of liquid (but below 2 000
mg), suitable stoppers must be used (diameter above 24 mm for natural cork, to be
defined for other types of stoppers).
SUMMARY
INTRODUCTION
FOREWORD
1. PRESENTATION OF THE STUDY page 5
2. LIMITS OF THE STUDY page 6
3. CAPPING page 7
31. Presentation
32. Functions
33. Sealing
34. Suitability of stopper length / control height of the finish
35. Brief physical principles
351. Definitions
352. Pressure developed within bottles
353. Hydraulic pressure
5. STOPPERS page 20
51. Functions
52. The various categories of stoppers
53. Natural & Technical cork stoppers
531. Drawings
5311. Natural corkwood stoppers
5312. Technical cork stoppers
532. Inspection conditions
533. Characteristics
54. Synthetic stoppers
541. Drawing
542. Characteristics
55. Storage conditions
Standard units
Reference standards
The standards or documents referred to do not quote any dates of publication. Everyone
involved should check the validity of these documents.
Equipment used for inspection (gauges, standard measures, pressure gauges, etc.)
must be calibrated regularly. Recommended frequency is 12 months maximum for
equipment used in normal conditions versus their design. This time period must be
decreased in case of more intensive use or more delicate equipment.
The glass finish specified in CETIE data sheet GME 50.01 and in European standard EN
12726, has been approved by :
- the European glass manufacturers
- the Confédération Européenne du Liège (European Cork Federation)
- the cap manufacturers
- the CETIE members as well as numerous professionals
This finish has been designed to be used with a stopper at 44mm length maximum.
For bigger lengths, see paragraph 34 page 10 : “Fitting between stopper length and
finish height”.
If all specifications described in this document are met, the internal equilibrium pressure
(over-pressure) within the bottle can reach 1 bar maximum.
Depending on the different parameters taken for this study, the value must be, 1 hour
after capping, between 12 and 40 daN with a cork stopper and between 10 and 45 daN
with a synthetic stopper.
Its value and the way of its measurement can be specified in a “cahier des charges”.
3. CAPPING
31. PRESENTATION
32. FUNCTIONS
The materials used must bring no change to the original characteristics of the wine and
must be in conformity with any applicable legislation :
• materials and articles intended to come into contact with foodstuffs
• packaging and packaging waste
33. SEALING
To fulfil the sealing function, the wine must not be able to pour between the glass and
the stopper at the point situated at 45 mm from the top of the finish.
The suitable diameter at this place has been calculated in relation with the percentage of
the cork dimensional recovery during the first minutes after capping.
It is necessary to leave enough time to the stopper to exert on the glass an adequate
force.
As a consequence it is necessary to wait at minimum 3 minutes before to put bottles in a
horizontal position.
In this way the stopper will not be stained by the wine on its roule.
Very often a stained stopper witnesses that one or several conditions described in this
document have not been met :
- non suitability of dimensions
- too high pressure during and after capping
- bottles put too early in a horizontal position
- etc.
The sealing defect which can result means a risk for the integrity of the wine quality.
The inspection dimension d.2, situated at the height H from the top of the finish, has
been calculated to ensure the sealing in relation with the percentage of the cork
dimensional recovery.
351. Definitions
• Absolute pressure
Value of the pressure within an enclosed space, assuming a zero pressure. For
example: atmospheric pressure = 1.013 bar.
• Equilibrium pressure
Value of the pressure obtained within a container for a specific product, volume
and homogeneous temperature at thermodynamic equilibrium, i.e. at the end of
an infinite period of time.
In practice, to obtain a close approximation of the equilibrium pressure rapidly, the
container is shaken until the temperatures and pressures stabilise.
Formal calculations and temperature-pressure curves generally give the
equilibrium pressure.
• Homogeneous temperature
The changes in temperature in a medium are not instantaneous, it depends upon
the environment. Thermal exchanges between two bodies are not immediate,
they depend upon state (gaseous, liquid, solid) and the environment in which they
are to be found.
The bottler should bear this point in mind when bottling, but also during transport and
storage when the capping may be subject to unforeseen constraints or particularly
thermal factors.
The factors having a significant impact on the pressure developed within the bottle are :
• the head space (stopper in place) = free space
• the alcoholic content of the product
• the sugar content of the product
• the composition of the gases in the head space
• the temperature (homogeneous) of the product
• Head space
The percentage of head space at 20° C must be sufficient to allow the expansion of the
wine if the temperature rises, without the pressure into the bottle be above 1 bar.
The table below gives, as examples, for 75 cl bottles and depending on their filling level,
the percentages of head space after capping with stoppers of different lengths, in normal
conditions of application.
It can be seen that, in all situations, the percentage of head space is around 1% at the
maximum, i.e. low.
* usages to ban
Graph in page 15 has been established with the curves of distilled water with addition of
(in volume) :
10 % ethanol for the lower curve (B)
16 % ethanol for the higher curve (A)
The impact of sugar content is low for the wines concerned by this guideline.
Indeed, almost all wines are showing an expansion curve situated between the two
curves A and B in the graph page 15.
9 Ambient air which contains around 20% of oxygen (soluble) and 80% of nitrogen,
practically insoluble.
9 Carbon dioxyde
Ambient air is replaced by CO2.
Warning:
The added volume of CO2 will partly dissolve more or less quickly depending on
the actual dissolved CO2 rate in the wine.
9 Vacuum (relative)
Ambient air is removed before sealing.
This is the preferred solution, but its application is efficient only with suitable
equipment, correctly adjusted and maintained. Application must be associated
with checks of vacuum values in the bottle after sealing.
When temperature is moving, internal pressure within the bottle is moving in the same
way.
Roughly in the sealed bottle, the curve pressure in relation with temperature is always
showing the same shape.
It can be seen that between temperatures T°1 and T°2 we are facing a situation of
leakers (hatched area).
Indicative curve showing the approximate temperatures to which the wine will contact
the stopper and will apply a hydraulic pressure.
In all cases, this pressure will result either in a move up of the stopper, or in a leak
(and/or both situations at the same time).
Curve A : curve of expansion of distilled water with an addition of 16 % ethanol (in volume)
Curve B : curve of expansion of distilled water with an addition of 10 % ethanol (in volume)
Taking in consideration the average head space between the stopper and the most used
filling levels (55 and 63 mm), it can be seen at which temperature the wine will come in
contact with the stopper.
stopper length = 49 mm
filling level at 20 °C = 55 mm
⇒ contact at temperature between 29°C et 31°C
In the case of hot filling, it can be seen which are the filling levels and the stopper
lengths to be used, depending on temperature.
Warning : All parameters have been taken at their average value. If the situation is very
close of curve A, it is strongly recommended to draw the actual expansion
curve of the product.
NOTE : In the hatched quarter circle (at the bottom of the left side of the graph) are the
capping told « à la giclée » as well as the use of a stopper of 53 mm length with
a filling level at 55 mm. It can be easily understand why the working group bans
the use of these two practices.
D.1 27 ± 0,5
D.2 29 ± 0.5
D.3 29.5 ± 0,5 preferable difference : D.3 - D.4 = 2 mm
(to maintain the capsule on the neck)
D.4 27.5 maxi
Internal profile :
All mean diameters measured on the 45
mm length must be greater than the
actual mean diameter d 1.
Provisional exception for light weight
bottles :
At 25 mm max height, the measured
mean diameters can be lower (0.5 max)
than the actual mean Ø d 1.
Through bore 17.5 min through the neck for use of a filling tube with a Ø 16 mm max
5. STOPPERS
51. FUNCTIONS
• Sealing to liquids.
• Carrying information.
• Natural corkwood stoppers are made entirely from cork, wrought to size and
punched from the bark of a cork oak. They can be sealed (colmated) as part of an
additional treatment consisting of filling the pores (lenticels) with cork dust and
glue. Stoppers which have undergone this filling operation are normally
designated as “colmated natural cork stoppers”.
531. Drawings
H ± 0.7
Note:
It is recommended not to
use a chamfer as this
reduces the sealing surface
between cork and glass. Ø 24 ± 0.5
* these heights are intended for use with adapted neck finishes and bottles.
It is reminded that a glass finish adhering to standard EN 12726 has been designed
for use with a cork stopper having a length of 44 mm and a diameter of 24 mm.
H Ø
Agglomerated cork stopper 38 to 44 mm 22.5 to 23.5 mm
Treated agglomerated cork stopper 38 to 49 mm 22.5 to 24.5 mm
1+1 stopper 40 to 44 mm 23 to 24 mm
533. Characteristics
Characteristics
Bulk density Moisture Degree of Extraction force Liquid tightness Dust level
content dimensional
Types of stoppers recovery after
compression in daN in bars
Stopper length (relative pressure) in mg / stopper
in kg/m3 in % in %
38 mm 44 mm
Natural cork and
0.9 to 1.2 1.5 to 2.0
colmated natural Non Applicable 6.0 ± 2.0 90 minimum 12 to 35 15 to 40
according to range according to range
cork stoppers
Agglomerated cork
stoppers for still 290 ± 40 6.0 ± 2.0 90 minimum 12 to 35 15 to 40 0.9 2.0
wine
1+1 stoppers 270 ± 40 6.0 ± 2.0 90 minimum 12 to 35 15 to 40 1.2 2.0
Treated
0.9 to 1.2 1.5 to 2.0
agglomerated cork 260 ± 40 6.0 ± 2.0 90 minimum 12 to 35 15 to 40
according to type according to type
stoppers
541. Drawing
H ± 0.3
Ø* ± 0.3
542. Characteristics
See data sheet CETIE EC 3-01 “Good practices for the use of synthetic stoppers”.
The storage time should be specified by the supplier because it depends on the surface
treatment and type of packaging used.
Stoppers should be left in their original packaging and good storage conditions should
be applied:
- Stoppers should be stored above ground.
- Stoppers should be stored in a clean, dry, odour-free and ventilated room.
- Stoppers should be stored at temperatures kept between 15 and 25°C (59 and
77°F) and sharp variations in temperature should be avoided.
- Stoppers should be stored in an environment with a relative humidity of between 40
and 65%.
- Stoppers must be kept away from all chemicals, pesticides, fungicides,
agrochemicals, chlorine-based sanitary products and treated wooden structures
(most especially those treated with halophenols).
Storage for 48 hours at a mean temperature of 20°C (68°F) before bottling enables the
stoppers to attain the optimal conditions for their use.
6. CONDITIONS OF APPLICATION
61. FOREWORD
Beyond the quality of components, the success of the sealing operation depends also on
general conditions in which this operation is carried out and particularly of the following
factors:
Any adjustment to equipment can only be done by specially trained technicians. Dates of
adjustments as well as setting values must be documented and recorded.
Note: The conditions for application of synthetic stoppers are similar to those for corks.
See document CETIE EC 3-01 "Good practices for the use of synthetic stoppers".
Schematic diagram
• Compression
- Position the pushing pin inside the jaws at the point of maximum tightness
(approximately at ¾ of its stroke).
It is very important to check, for each run, the cleanliness and degree of wear of:
- the jaws
- the slides
- the pivot rollers
- the whole of the system (screw, springs…)
as well as the lubrication of the system (with food-grade lubricants).
NOTE
In the event of heating of compression jaws:
- frequently check the cleanliness of the jaws,
- double the frequency of lubrication.
The jaws are very important wear parts which affect the quality of the sealing operation.
Their working life depends on the material of the jaws, the stoppers used, and the
maintenance of the system.
Order of working life : 1 million bottles minimum.
In particular, the condition of the surfaces should be monitored. Look for a good fitting
join at the edges, without "parrot mouth", the absence of nicks on the edges of the jaws
and absence of grooves in the ellipse of the jaws. Ensure also lack of clearance in the
roller of the moving slide (this should be changed at the same time as the jaws), and the
flatness of the slides without streaking or excessive wear.
Schematic diagram
• Check:
- the diameter
- the positioning
height, centring, jamming, parallelism with respect to the surface of the
stopper
• Specifications
+ 0.5
- Ø 14 mm
-0
- Vertical positioning.
• Check:
- the fitting of the internal profile with the finish and the bottle
Schematic diagram
In the same way as the jaws, the mouthpieces and centring devices are also very
important wear parts which affect the quality of the operation.
They must be removed and cleaned once a day and after each incident.
For the mouthpiece, monitor the conical way (17 mm at the highest point, 16 mm at the
exit). Check the roundness to ensure no oval shaping or angular geometry. Ensure the
absence of signs of wear in the form of "file marks" at the intersection of the four jaws.
Take care that the angle of the centring taper is adjusted to provide good guidance for
the neck of the bottle, without any signs of lateral wear or chips.
• Check:
- The star grip device which must allow correct centring of the bottle under the
jaws. If necessary adjust the guides.
- The height of the heads which must be correctly adjusted with respect to the
bottle platform to allow:
- correct presentation under the head,
- good implementation of the compensation.
The surface must be flat and clean so as to ensure both the slipping and the vertical
positioning of the bottle.
• Check:
- that the support surface of the platform is parallel with the base of the pushing
pin
The smallest bottle (minimum height) must not be able to be turned by hand
once it is located between the mouthpiece and the bottle platform.
NOTE:
- Minimum output:
Out-put below which the pushing speed is likely to cause the “crushing” of the
stopper during its penetration into the neck of the bottle.
- But beware, on certain single-head machines, the displacement of the bottle too
rapidly and/or too abruptly into the guiding star grip can cause the wine to rise up the
walls of the neck, just at the time when the bottle has halted for capping. If such a
rising occurs, check the machine and/or reduce the speed.
The presence of a liquid (water or wine) between the stopper and the interior of the
glass finish forms an incompressible capillary film which can cause:
- the start of seepage and the formation of a passageway through which the wine
can leak out.
in this case, you should cause the process to get yet worse by maintaining the
cork in a permanently softened state.
In any event, higher quality corking will be achieved when residual moisture between the
glass and the stopper is at a minimum.
7. CAPSULES (OVERCAPS)
71. FUNCTIONS
• To be easily removed
either through a tear strip
or by cutting with a suitable tool
• Allow customization of the capping due to the printing possibilities of the capsule
We characterize :
NOTA
The head may be perforated to ease the fitting (evacuation of air overpressure or
airbed).
73. DIMENSIONS
L : height = 60 mm
variable on request from 35 to 70 mm (by step of 5 mm)
α : half conicity = 1°
SEAM
L : height = 60 mm
variable on request from 35 to 70 mm (by step of 5 mm)
I : deep of head = 5 mm
SEAM
L : height = 55 mm
variable on request from 35 to 70 mm (by step of 5 mm)
α : half conicity = 1°
I : deep of head = 5 mm
Rotary feeder
Most of feeding equipments allow to dislodge and to fit the different types of
capsules for wine. However the setting must be done in accordance with the type
of capsule : material, weight, length…
A. Loading
The “sticks” of capsules are put in magazines :
- with fixed platforms, simple or multiple
- with mobile platforms
- transfers : horizontal belt
: by weight
B. Dislodgement of capsules
- mechanic : with clamps
- pneumatic : with jets
: with suction pads
- mechanic and pneumatic combined
: mechanical dislodgement (with clamps or needles)
: pneumatic ejection
The pushing must not cause any offset of the bottom of the skirt, whatever the
type of capsule.
743. Prefolding
Pouch
made of rubber
Bottle finish
This operation consists to apply closely the capsule on the bottle neck. Vertical
pleats are carried out before crimping to compensate the excess of material.
Precautions
The quality of the chosen equipment must allow to avoid :
- inks and varnishes peel off at pleats
- the folding back of the bottom of the skirt
- the moving up of the capsule
744. Crimping
Principle
The bottle, with its capsule correctly drive on, is introduced in a centring device.
The capsule head comes into contact with an ejector (or plunger) having three
functions :
b) allow to the first rollers a progressive work on the external radius of the bottle
finish
Remarks
The first rollers preform the capping operation, the other ones finish it.
The capsule length must allow the rollers to move below the skirt bottom without
to come into contact with the bottle shoulders.
The load on rollers is adjusted with rubber rings in relation with their composition,
number, position, or with springs.
Precautions
To obtain a correct geometrical result, the glass bottle finish must be correctly
centred during the full time of the crimping operation.
• the speed for the moving up of the bottle pad or for the moving down of the
crimping head must be in relation with the rotation speed of the head.
NOTA
Other specifications imply contact and dialogue with the equipment manufacturer
to obtain a correct quality of the wished crimping.
A reduced conicity allows obtaining a better crimping result but may lead to
distribution troubles.
745. Shrinkage
“Tunnel” system
Shrinkage is obtained by infrared or pulsed air heating on the sides of the capsule
skirt which retract on the bottle neck.
It can be carried out only on capsules made with a shrinkable material having
been submitted to a mono oriented stretching.
Principles
• by tunnel (continuously)
System with electrical resistances positioned lengthways with the belt axis, with
or without blowing device :
- output > 1,000 bottles/hour
- length to adapt to the bottle speed
- the capsule must be drive on and maintain on the finish
- the bottle must be centred in the tunnel
- the tunnel must retract up during belt stops
An air blowing system gives a better hot air distribution and more homogeneous
shrinkage.
Precautions
Too much heating of the capsule head must be avoided in all situations, mainly
with tax stamp.
Bottle rotation during its way through the tunnel limits the non straight positions of
the skirt bottom.
Most of bottles used for the filling of still wines are “Measuring containers” at a
determined filling level (55, 63 mm and others), in accordance with the European
directive 75-107 EEC.
Dependent on the type of bottle (Bordeaux, Burgundy, others...) and the wine
temperature at filling, it is necessary to adjust the filling level :
- lower in the case of a wine temperature below 20 °C
- higher in the case of a wine temperature above 20 °C
In addition to regulatory aspect as well as over costs involved, the over filling practice
leads to a pressure increase when the temperature moves up resulting in higher risks of
leakers.
Because of the numerous profiles of bottle shoulders, it is not possible to give in this
guide the filling gauges for each type of bottle.
Refer to our Guideline for bottling quality n° 9 « Contrôle des volumes de remplissage
des préemballages en bouteille verre : guide de bonnes pratiques ». Document available
in French language only.