Chemical of Steel

ee Standard provided by BIS via BSB Edge Private Limited to DIFFUSION ENGINEERS LIMITE
NAGPUR(qc_t5@diffusionengineers.com) 59.95.101.71 [for non-commercial use only].
( Reaffirmed 2002 )
(Reaffirmed!2012)!
(Reaffirmed 2018)
IS t 228 ( Part 3 ) • 1987
Indjan Standard
METHODS FOR
CHEMICAL ANALYSIS OF STEELS
PART 3 DETERMINATION OF PHOSPHORUS
BY ALKALIMETRIC METHOD
( Third Revision)
Methods of Chemical Analysis of Ferrous Metals

Sectional Committee, SMDC 2
ChDirmtlll R'presentillg
DR C. S. P. ITER Bhabha Atomic Research Centre, Bombay
Ml'ffliJlrI
SHRI G. M. MPABAO Steel Authority of India Ltd (Bhilai Steel Plant),
Bhilai
Smu R. D. AGARWAL (...4ltmUll,)
8mn 8. V . BHAGWAT Khandelwal Ferro Alloy. Ltd, Nagpur
SJl:BI D. N. GUPTA (...4ltlNUJt.)
SHRI P. CHAKRA Indian Metals &. Ferro Alloys Ltd, Koraput
CH_18T &. METALLURGIST Ministry of Transport ( Department of Railway.)
A8818TAXT RESEAROH OI"I"IOER
(MET-%), RDSO, LUOKNOW
( ...4lt".,uat. )
CHIEI" CHEMIST Tata Iron &. Steel Co Ltd,jamshedpur
ASSISTANT CHlEl" CHEMIST (...4ltlNUJt,)
SHKI M. K. CHAKRAVARTY Ministry of Defence (DGI )
SaRI P. K. SEN (...4ltmUll,)
DR M. M. CHAKRABORTY Indian Iron &. Steel Co Ltd, Bumpur
SHRI M. S. CHATTERJEE ( ...4lt,rIl4l, )
SHRI C. K. DmSll1T Ordnance Factory Board (Ministry of Defence).
Calcutta
SHRI S. N. MOITBA (...4ltmUll,)
SaRI V. B. KBAKNA Directorate General of Supplie. &. DispOlaJa,
New Delhi
SHRlj. N. MUKHERJEE Steel Authority of India Ltd (Durgapur Steel
Plant ), Durgapur
( Ql1ItillU,d 011 pag' 2 )
C Copyright 1987
BUREAU OF INDIAN STANDARDS
This publication is protected under the Indiall Copyright ...4&1 (XIV of 1957) and
reproduction in whole or in part by any means except with written permission of the
publisher shall be deemed to be an infringement of copyright under the said Act.
IS : 228 ( Part 3) • 1987

( CotltitllUd fr"". "/HIg' I )
Mmallws R'/If',smling
SaBI P. NABAIN Mahindra Ugine Steel Co Ltd, Bombay
SaRI G. R. SARKA ( AI',rlUll, )
SaBI N. P. PANDA Steel Authority of India Lid (Rourkela Steel
Plant), Rourkela
SHKI B. MAHAPATRA (Alt_t,)
DB L. P. PANDBY National Metallurgical Laboratory (CSIR),
Jamahedpur
DB D. C. PBA8SAR National Physical Laboratory (CSIR).
New Delhi
5 SRI J. RAJ ( AI'",I4I, )
SSKI G. RUABAO Ferro Alloys Corporation Ltd, Shreeramnagar
SHBI K. RAMAXBI8SNAN Easen & Co, Bangalore
Da J. RA.JABAK (AI'",IG', )
SSBI A. P. SINSA Steel Authorjty of India Ltd (Bokaro Steel
Plant), Bokaro
SSBI K. ANl'lAS ( AlmlUll, )
SSBI N. V. SUBBABAYAI'PA ViJvelvaraya Iron & Steel Ltd, Bhadravati
Da P. SUBBASMANIAK Defence Metallurgical R"learch Laboratory,
Hyderabad
Ssal T. H. RAO ( AlllrtIGtI )
DR CH. VII:NKATB8WABLU Dhablll' Atomic Rel .. arch Centre, Bombay
SaBI K. RAOSAVBNDRAN. Director General, BIS ( Ex-ojJi&jo Mmaller )
Director ( Struc & Met)
S,cr,'tlry
SaRI M. L. SSARKA
Auistant Director ( Metall), BIS
Ferrous Metals Analysis Subcommittee, SMDC 2 : 3

COtlVltl4l'
DB C. S. P. IYER Bhabha Atomic Research Centre, Bombay
MerMlTS
SSRI S. BASKARAN Bharat Heavy Electricall Ltd, Hyderabad
SSRI MATA SAR.4.N ( AI,,,tIG" I)
Ssal B. RASA (AI',rtIGl, II )
SaBI U. P. B08E Steel Authority of India Lid ( Bhilai Steel Plant),
Bhilai
SSln E. M. VEBOaESE ( A/'"M" )
ClllBl" CaEMIsT Tata Iron & Steel Co Ltd,Jamshedpur
A8SISTANT CSIEI" CS.MIST (AI"mG" )
Da M. M. CSAXKABORTY Indian Iron & Steel Co Ltd, Burnpur
SaRI L. N. DAB (Al'ImG', )
SlJRl H. K. Du Steel Authority of India Ltd (Rourkela Steel
Plant), Rourkela
SaRI K. BIBHNOl ( Alt"tlaf, )
SSBI A. K. GUPTA National Physical Laboratory (CSIR ).
New Delhi
( COII'itlUld 011 IJI',' 11 )
2
IS : 228 ( Part 3 ) • 1987
Indian Standard
METHODS FOR
CHEMICAL ANALYSIS OF STEELS
PART 3 DETERMINATION OF PHOSPHORUS
BY ALKALI METRIC METHOD
( Third Revision)
o. FOR E W 0 R 0
0.1 This Indian Standard (Part 3 ) (Third Revision) was adopted by
the Indian Standards Institution on 16 January 1987, after the draft
finalized by the Methods of Chemical Analysis of Ferrous Metals
Sectional Committee had been approved by the Structural and Metals
Division Council.
0.2 IS : 228, which was issued as a tentative standard in 1952 and
revised in 1959, covered the chemical analysis of pig iron, cast iron and
plain carbon and low alloy steels. For the convenience it was decided
to publish a comprehensive series on chemical analysis of steels
including high alloy steels. Accordingly, revision of IS: 228 was
taken up again and new series on methods of chemical analysis of steels
including high alloy steels was published in various parts as IS : 228
( Parts 1 to 13) (see Appendix A ) covering separate method of analysis
for each constituent in steels. However, IS: 228-1959· version has
been retained for the analysis of pig iron and cast iron till a separate
standard for analysis of pig iron and cast iron is published.
0.2.1 This revision of IS : 228 (Part 3 )-1972t· has been undertaken
on the basis of experience gained during the implementation of the
standard by the manufacturers and testing laberatories.
0.3 In this revision method for determination of phosphorus in
following alloy steels has been incorporated:
a) Stainless steel, high chromium, nickel chromium and similar
alloy steels without tungsten or vanadium,
·Meth~d. of chemical analysil of pig iron, Calt iron and plaiD carbon and low al10y
ateel. ('.lIlSed).
tMethods for chemical analYIP of steel.: Part 3 Determination of phosphol'Ul by
alkalimetric method (s,c~ ,t/Ii.r;'" ).
3
IS : 228 ( Part 3 ) • 1987

b) Steel containing high silicon, titanium or zirconium,
c) Chromium vanadium steels or other steels containing
vanadium but no tungsten,
d) High speed steels or other steels containing tungsten with or
without vanadium,
e) Austenitic manganese steels, and
f) Steels containing arsenic up to 0·1 percent.
0.4 In reporting the result of a test or analysis made in accordance

with this standard, if the final value, observed or calculated, is to be
rounded off, it shall be done in accordance with IS : 2-1960·.
1. SCOPE
1.1 This standard (Part 3) covers method for determination of
phosphorus content of plain carbon steel and alJoy steels by alkali-
metric method.
2. SAMPLING
2.1 The samples shall be drawn and prepared as prescribed in the
relevant Indian Standard.
3. Q.UALITY OF REAGENTS
3.1 Unless specified otherwise, analytical grade reagents and distilled
water (see IS : 1070-1977t) shall be employed in the test.
4. OUTLINE OF THE METHOD

4.1 Phosphorus is converted to orthophosphoric acid and precipitated
as ammonium phosphomolybdate. The precipitate is dissolved in
known excess of standard sodium hydroxide solution and the excess
is titrated against standard nitric acid solution.
4.2 Reagents
4.2.1 Dilute Nitric Acid-I: 1, 1 : 3, 1 : 5 and 2: 98 (v/v).
4.2.2 Potassium Permanganate Solution - Dissolve 2 g of potassium
permanganate in 100 ml of water .
• Rulel for rounding off numerical valu",. ("visld).

tSpecification for water for general laboratory ule (second revisioll ).
4
IS : 228 ( Part 3 ) • 1987

4.2.3 Sodium Nitrite Solucion - 5 percent (m/v).
4.2.4 Conctntiated Ammonium l-!ydroxide ---- Relative density 0·90.
4.2.5 Concentrated Nitric Acid - Rela tive density 1'42 (conforming to
IS: 264-j976·).
4.2.6 Ammonium Molybdate Solution - Add solution A (see 4.2.6.1)
slowly and with constant stirring to solution B ( see 4.2.6.2 ) kept cool in
a cold waterbath. Add 10 m! of ammonium phosphate solution
( 1 gil) and keep the solution at least for 24 hours. Filter the solution
through What man filter paper No. 040 before use.
4.2.6.1 Solui':on A - ulssolve JUU g of mOJYDOIC acid (l\ti003, 0,)
percent ), or 118 g of ammonium molybdate in a mixture of 145 ml of
ammonium hydroxide (rd = 0'90) and 270 ml of water. Cool the
solution.
4.2.6.2 Solution B - Add 490 ml of concentrated nitric acid
to 1 150 ml of wa ter and cool.
•. 2.7 Potassium Nitrate Solution- 1 percent (m/v).
4.2.8 Phenolphthalein Solution - 1 percent. Dissolve 1 g of powder
phenolphthalein in 100 ml of rectified spirit or methyl alcohol.
4.2.9 Sodium Hydroxide Solution - 0'1 N, dissolve 4'5 g of sodium
hydroxide in one litre of freshly boiled and cooled distilled water, and
standardize against standard nitric acid (4.2.10).
4.2.10 Standard Nitric Acid Solution - 0'1 N, dilute 7 ml of concentrated
nitric acid to one litre with freshly boiled distilled water. Standardize
against sodium carbonate previously ignited at 350°C and cooled,
4.2.11 Lilute Hydrochloric Acid - 1 : 1 (v/v) and 2 percent (v/v),
4.2.12 Hydrofluoric Acid - 40 percent.
4.2.13 Perchloric Acid - 70 percent.
4.2.14 Sodium Carbonate - 5 percent (m/v).
4.2.15 Ferrous Sulphate Solution - Dissolve 100 g of ferrous sulphate
crystals ( FeSO" 7H zO ) in one litre of dilute sulphuric acid ( 5 : 95 ).
4.2.16 Dilute Ammonium Hydroxide - 1 : 1, 1 : 20 (v/v).
4.2.17 Sulphurous Acid - Saturate water with sulphur dioxide gas.
-Specification for nitric acid ( stcond rtvlSion ).
5
IS : 228 ( Part 3 ) • 1987
4.2.18 Concentrated Hydrochloric Acid - Relative density 1·16 ( conform-
ing to IS: 265-1976.). I
4.2.19 Dilute Hydrobromic Acid - 1 : 4 (vlv).
5. PROCEDURE FOR PLAIN CARBON STEEL AND LOW

ALLOY STEEL WITHOUT VANADIUM
5.1 Transfer 2 g of the sample in a 250-ml conical flask. Add 30 ml of
dilute nitric acid (l : 1) till the vigorous reaction subsides. Keep the
flask at low heat till it dissolves.
5.2 Add 5 to 10 ml of potassium permanganate solution and boil for

few minutes. If manganese dioxide does not precipitate add further
permanganate solution till a precipitate of manganese dioxide appears
and boil for few minutes. Add sodium nitrite solution dropwise till
the brown precipitate is dissolved. Boil to expel oxides of nitrogen.
5.3 Add ammonium hydroxide till brown precipitate of ferric

hydroxide appears. Dissolve the precipitate adding dilute nitric
acid (l : I) dropwise and add 2 to 3 ml of concentrated nitric acid.
NOTE - Quantity of nitric acid added at this stage will depend upon the actual
volume of the solutioD. The analyst will ensure that the acidity of the solution
before precipitation of phosphomoiybdate complex is maintained at 5-10 perlent.
5.4 Warm the solution to about 60-80°C and add 50 ml of ammonium

molybdate solution, stopper the flask, shake vigorously for a few
minutes and allow to stand for half an hour.
5.5 Filter the precipitate through a filter paper pulp pad by suction.
Wash the flask, precipitate and filter pad twice with 5 ml portions of
dilute nitric acid (2 ; 98) and five times with 5 ml portions of potassium
nitrate. Continue washing of the precipitate and filter pad with
potassium nitrate solution until the washings are acid free (10 ml
portion of the washings in presence of phenolphthalein should turn
pink on adding one drop of 0·1 N sodium hydroxide solution).
5.6 Transfer the pulp along with the precipitate to the flask. Add
about 25 ml of water, few drops of phenolphthalein and a known
volume of sodium hydroxide solution (which should be 1-2 ml in excess)
and shake to dissolve the precipitate. Dilute to about 100 ml and
titrate with standard Qitric acid solution to the disappearance of pink
colour.
·Specification for hydrochloric acid ( stCImd revision).
6
IS: 228 (Part 3 ) - 1987
6. PROCEDURE FOR ALLOY STEELS

6.1 Stainless Steel, High ChrolDiulD, Nickel ChrOlDiUID and
SilDilar Alloy Steel Without Tungsten or VanadiulD - Transfer
2 g of the sample in a 400-ml beaker. Add 50 ml of a I : I mixture
of concentrated hydrochloric acid and nitric acid and a few drops
of hydrofluoric acid. Place the beaker at low heat until the reaction
subsides and then add IS ml of perchloric acid. Evaporate to copious
fumes and fume for a few minutes. Coo), take up with 40 ml of water
and 10 ml {f concentrated niLric acid, boil for few minutes, filter
through paper pulp and wash with hot dilute nitric acid (I: 5).
Collect the filtrate in SOO-ml conical flask and proceed as in 5.2 to 5.6.
6.2 Steel Containing High Silicon, TitanidID or ZirconiUID

6.2.1 Follow the procedure given in 6.1 up to filtration and proceed as
follows.
6.2.2 Collect the filtrate in a sOO-ml conical flask and preserve it.
Take the precipitate and pulp ( as in 6.1) in a platinum crucible and
ignite, fume with 1 ml hydrofluoric acid and a few drops of
concentrated nitric acid at low temperature. Fuse the residue with
sodium carbonate. Dissolve the melt in water, filter through paper
pulp and wash with sodium carbonate solution. Acidify the filtrate
with concentrated nitric acid and add to the main filtrate. Proceed
further as in 5.2 to 5.6.
6.3 ChrolDiulD VanadiulD Steels or Other Steels Containing

VanadiulD But No Tungsten
6.3.1 Proceed as in 6.1 when the solution is ready for the
precipitation of phosphomolybdate complex.
6.3.2 Cuol the solution to 1O-20°C, add 5 ml of ferrous sulphate
solution and 2 to 3 drops of sulphurous acid, and shake to mix well.
Add 50 ml of ammonium molybdate solution, stopper the flask, shake
vigorously for a few minutes and allow to stand overnight. Proceed
6.4 High Speed Steels or Other Steels Containing Tungsten

with or Without VanadiulD
6.4.1 Transfer 2 g of the sample to a 400-ml beaker. Decompose the
sample in 60 ml of dilute nitric acid (1 : 3) and a few drops of
hydrofluoric acid, if required. Add 20 ml concentrated hydrochloric
acid, 60 ml concentrated nitric acid and few drops of hydrofluoric
acid and evaporate to dryness . Digest with 20 ml of concentrated
7
IS : 228 ( Part 3 ) - 1987
hydrochloric acid, dilute to 50 ml with water and boil. Filter through

a paper pulp as far as possible by decantation, keeping back the
precipitate of tungstic acid in the beaker. Wash twice with hot dilute
hydrochloric acid (2 percent). Collect the filtrate in a 500-ml conical
flask and evaporate to a small volume. Add 30 ml concentrated
nitric :lcid, and evaporate to syrupy liquid. Add 5 ml concentrated
nitric acid, dilute to about 25 ml and boil for a few minutes.
6.4.2 To recover phosphorus from the precipitate of tungstic acid,
dissolve the precipitate in the beaker with minimum quantity of dilute
ammonium hydroxide (1 : 1) and pour it through the filter pad
collecting the solution in a beaker, wash the beaker and the filter pad
with dilute ammonium hydroxide (1 : 1) until all of the tungstic acid
has been dissolved and collected. Add a few ml of the main filtrate
(end of 6.4.1 ) to this solution and slightly acidify with dilute nitric
acid (1 : 1). Add dilute ammonium hydroxide (1 : 1) in slight excess
and heat to flocculation. Filter through Whatman filter paper No. 42
and wash with dilute amm'onium hydroxide (1 : 20). Dissolve the
precipitate in minimum hot dilute nitric acid (1 : 5) and add to the
main filtrate ( see 6.4.1 ).
6.4.3 Treat the filtrate as in 5.2 and 5.3. If the sample contains
vanadium, proceed further as in 6.3.2. In the absence of vanadium,
complete the determination as in 5.4 to 5.6.
6.5 Austenitic Manganese Steels - Decompose 2 g of the sample

in a 400-ml beaker in 40 ml of dilute nitric acid (1 : 3). Add 15 ml
of perchloric acid and evaporate just to white fumes. Add hydrofluoric
acid drop by drop until all the hydrated silica is dissolved and a few
drops in excess. Heat so that perchIoric acid refluxes on the sides of
the beaker for about 25 minutes. Cool, add about 40 ml of water and
10 ml concentrated nitric acid and boil for few minutes. Proceed
6.6 Steels Containing High Arsenic Up to 0'1 Percent
6.6.1 Decompose 2 g of the sample in 400-ml beaker in 40 ml of

dilute nitric acid (l : 3), Add 20 mi of perchloric acid and fume to
expeU nitric acid, Cool, add about 80 ml of dilute hydrobromic acid
and evaporate to copious fumes. Cool, add about 40 ml of water
apd 10 ml nitric acid. Proceed further as in 5.2 to 5.6.
7. BLANK DETERMINATION
7.1 Make a blank determination following the same procedure and

using the same quantity of all reagents.
8
IS : 228 ( Part 3 ) • 1987
8. CALCULATION
8.1 Calculate phosphorus, percent, as:
Phosphorus (percent) = (B - ~) X C X 100
where
A = millilitres of standard nitric acid solution required in the
sample in the titration of the excess sodium hydroxide
( see 5.6),
B = millilitres of standard nitric acid solution required in the
blank determination (see 1.1 ),
C = phosphorus eq uivalent of 1 ml standard nitric acid
solution, and
D = quantity of sample in g.
8.2 Reproducibility - ± 0'0015 tJercent.
APPENDIX A
( Clause 0.2 )
IS : 228 Methods for chemical analysis of steels:
(Part I )-1972 Determination of carbon by volumetric method
( for carbon "> 0·1 percent) ( second revision)
( Part 2 )-1972 Determination of manganese in plain carbon and
low alloy steels by arsenite method ( second revision)
(Part 3 )-1972 Determination of phosphorus by alkalimetric
method (second revision)
( Part 4 )-1974 Determination of carbon by gravimetric method
( for carbon ;;;. 0·1 percent) (second revision)
( Part 5 )-1974 Determination of nickel by dimethylglyoxime
(gravimetric) method (for nickel> 0·5 percent) (second
revision)
(Part 6 )-1974 Determination of chromium by persulphate
oxidation method (for chromium;> 0·5 percent) ($econd
revision)
9
IS: 228 (Part 3) -1987

(Part 7 )-1974 Determination of molybdenum by rx-benzoinoxime
method (for molybdenum > I percent) (second revision)
( Part 8 )-1975 Determination of silicon by the gravimetric method
( for silicon;;' 0'1 percent) ( second revision)
(Part 9 )-1975 Determination of sulphur in plain carbon steels by
evolution method (second revision)
(Part 10 )-1976 Determination of molybdenum by thiocyanate
( photometric) method ( for molybdenum up to 1 percent)
in low and high alloy steels ( second revision)
(Part 11 )-1976 Determination of silicon by photometric method in .
carbon steels and low alloy steels (for silicon 0'01 to
0'05 percent) (second revision)
(Part 12 )-1976 Determination of manganese by period ate
( photometrie) method in low and high alloy steels (for
manganese up to 2 percent) (second revi.sion)
(Part 13 )-1982 Determination of arsenic
10
IS : 228 ( Part 3) . 1987
( Cora/illu,d f'lIm ~,e 2)
MImb"s RepreSlll/illl
S}[RIJ. MUXBERJEE Steel Authority of India Ltd (Durgapur Steel
Plant ), Durgapur
SlIRI P. K. BANERJEE (Allemale )
SBRI P. NARAIN Mahindra Ugine Steel Co Ltd, Bombay
SaRI G. R. SARMA (Allerltale)
SHRI R. S. NATH Sleel Authority of India Ltd (Bokaro Steel
Plant), Bokaro
SURI N . GUNJJAPPA (Alterll4le)
DR L. P. PANuEY National Metallurgical Laboratory (CSIR),
Jamshedpur
SHRI G. RAMDA!I Visvelvaraya Iron & Steel Ltd, Bhadravati
SURI R. D. VANDRIWALLA Italab Pvc Ltd, Bombay
SURI J. C. DEY ( Alternale)
II
BUREAU OF INDIAN STANDARDS
Headquarters:
Manak Bhavan, 9 Bahadur Shah Zafar Marg, NEW DELHI 110002
Telephones: 323 0131, 323 3375, 323 9402
Fax 91 11 3234062, 91 113239399, 91113239382
Telegrams : Manaksanstha
(Common to all Offices)
Central Laboratory: Telephone
Plot No. 2019, Site IV, Sahibabad Industrial Area, SAHIBABAD 201010 8-77 00 32
Regional OMees:
Central : Manak Bhavan, 9 Bahadur Shah Zafar Marg, NEW DELHI 110~2 3237617
"Eastern: 1/14 CIT Scheme VII M, V.I.P. Road, Maniktola, CALCUTTA 700054 3378662
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tWestern : Manakalaya, E9 Behind Marol Telephone Exchange, Andheri (East), 832 92 95
MUMBAI 400093
Branch OMces:
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NIT Building, Second Floor, Gokulpat Market, NAG PUR 440010 5251 71
Institution of Engineers ( India ) Building, 1332 Shivaji Nagar, PUNE 411005 323635
"Sales Office is at 5 Chowringhee Approach, P. O. Princep Street,

CALCUTTA 700072 271085
tSales Office is at Novelty Chambers, Grant Road, MUMBAI 400007 309 65 28
*Sales Office is at 'F' Block, Unity Building, Narashimaraja Square, 222 39 71
BANGALORE 560002
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ee Standard provided by BIS via BSB Edge Private Limited to DIFFUSION ENGINEERS LIMITE

NAGPUR(qc_t5@diffusionengineers.com) 59.95.101.71 [for non-commercial use only].

Methods of Chemical Analysis of Ferrous Metals

IS : 228 ( Part 3) • 1987

Ferrous Metals Analysis Subcommittee, SMDC 2 : 3

IS : 228 ( Part 3 ) • 1987

IS : 228 ( Part 3 ) • 1987

0.4 In reporting the result of a test or analysis made in accordance

4. OUTLINE OF THE METHOD

• Rulel for rounding off numerical valu",. ("visld).

IS : 228 ( Part 3 ) • 1987

-Specification for nitric acid ( stcond rtvlSion ).

4.2.19 Dilute Hydrobromic Acid - 1 : 4 (vlv).

5. PROCEDURE FOR PLAIN CARBON STEEL AND LOW

5.2 Add 5 to 10 ml of potassium permanganate solution and boil for

5.3 Add ammonium hydroxide till brown precipitate of ferric

5.4 Warm the solution to about 60-80°C and add 50 ml of ammonium

·Specification for hydrochloric acid ( stCImd revision).

6. PROCEDURE FOR ALLOY STEELS

6.2 Steel Containing High Silicon, TitanidID or ZirconiUID

6.3 ChrolDiulD VanadiulD Steels or Other Steels Containing

6.4 High Speed Steels or Other Steels Containing Tungsten

hydrochloric acid, dilute to 50 ml with water and boil. Filter through

6.5 Austenitic Manganese Steels - Decompose 2 g of the sample

6.6 Steels Containing High Arsenic Up to 0'1 Percent

6.6.1 Decompose 2 g of the sample in 400-ml beaker in 40 ml of

7.1 Make a blank determination following the same procedure and

IS : 228 ( Part 3 ) • 1987

Phosphorus (percent) = (B - ~) X C X 100

8.2 Reproducibility - ± 0'0015 tJercent.

IS: 228 (Part 3) -1987

"Sales Office is at 5 Chowringhee Approach, P. O. Princep Street,

Printed at New India Printing Press, Khurja, India

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