S Y B SC Syllabus 1

CHOICE BASED
CREDIT SYSTEM
SYLLABUS
FOR
CHEMISTRY-UG
Goa University, Taleigao Plateau, Goa. Page 1

ANNEXURE-I: Syllabus for Semester III and
Semester IV of B.Sc. with Chemistry Programme
ANNEXURE-II: Paper Patterns for all papers

Core Courses and Skill Enhancement Courses of Semester
III and Semester IV for SEE Semester End Examinations
ANNEXURE-III: Marking Scheme, and Time

Duration for practical examinations of Semester III and
Semester IV
ANNEXURE-IV: Syllabus for two new Generic

Elective Courses as options for Semester I and Semester II
ANNEXURE-V: Paper Patterns for the new

optional Generic Elective courses of Semester I and
Semester II SEE Semester End Examinations
ANNEXURE-VI: Syllabus, Paper Patterns and

Marking Scheme for Laboratory Courses for Semester III
and Semester IV of General Industrial Chemistry Courses
of B.Sc. with Industrial Chemistry Programme
ANNEXURE-VII: New Course Codes as per

OC-66 of Goa University for all papers offered in the
subject of Chemistry from Semester I to Semester VI

ANNEXURE-I
Syllabus for
B.Sc. with Chemistry

Programme
SEMESTER-III AND SEMESTER-IV
ANNEXURE-Ia :Syllabus for Semester III Core Course (CC) of Chemistry

...................................................................................................................... (1 Course)
CHC 103
ANNEXURE-Ib: Syllabus for Semester III Skill Enhancement Course (SEC) of

Chemistry……………………………………………………………… (1Course)
CHS101/ CHS106
ANNEXURE-Ic : Syllabus for Semester IV Core Course (CC) of Chemistry

....................................................................................................................... ( 1 Course)
CHC 104
ANNEXURE-Id: Syllabus for Semester IV Skill Enhancement Course (SEC) of

Chemistry...................................................................................................... (1Course)
CHS 102 /CHS 107

ANNEXURE-Ia
Syllabus of B.Sc. CHEMISTRY
SEMESTER III
CORE COURSE: CHC103
(06 Credits: Theory-04, Practicals-02)
(PHYSICAL CHEMISTRY AND ORGANIC CHEMISTRY)
Theory: 60 Hours (04 Credits)
Section A: Physical Chemistry-2 (30 Hours; 02 credits)
1. Solutions (7 Hours)
Thermodynamics of ideal solutions: Ideal solutions and Raoult’s law, deviations from
Raoult’s law – non-ideal solutions. Vapour pressure-composition and temperature
composition curves of ideal and non-ideal solutions. Azeotropes.
Partial miscibility of liquids: Critical solution temperature, distillation and fractional
distillation.
2. Phase Equilibrium (8 Hours)

Phases, components and degrees of freedom of a system, criteria of phase equilibrium,
Phase diagrams of one-component systems (water, sulphur and CO2) and two component
systems involving eutectics, congruent and incongruent melting points (Zn-Mg, NaCl-H2O).
3. Conductance (5 Hours)
Conductivity, equivalent and molar conductivity and their variation with dilution for weak
and strong electrolytes. Kohlrausch’s law of independent migration of ions. Ionic mobility
and factors affecting ionic mobility. Transference number and its experimental determination
using moving boundary methods. Applications of conductance measurements: solubility and
solubility products of sparingly soluble salts, ionic product of water, conductometric titrations
(only acid-base).

4. Electrochemistry (10 Hours)
Reversible and irreversible cells. Concept of EMF of a cell. Measurement of EMF of a cell.
Nernst equation and its importance. Types of electrodes. Standard electrode potential.
Electrochemical series. Thermodynamics of a reversible cell, Concentration cells with
transference and without transference. Liquid junction potential and salt bridge. pH
determination using hydrogen electrode and quinhydrone electrode.
Section B: Organic Chemistry-3 (30 Hours; 02 Credits)
1. Carboxylic acids and their derivatives (6 Hours)

Carboxylic acids (aliphatic and aromatic)
Preparation: Acidic and Alkaline hydrolysis of esters.
Reactions: Hell - Volhard - Zelinsky Reaction.
Carboxylic acid derivatives (aliphatic): (upto 5 carbons)
Preparation: Acid chlorides, Anhydrides, Esters and Amides from acids and their
interconversions.
Reactions: Comparative study of nucleophilicity of acyl derivatives. Reformatsky reaction,
Perkin condensation (mechanism).
2. Amines and Diazonium Salts (6 Hours)

Amines (aliphatic and aromatic): (upto 5 carbons)
Preparation: from alkyl halides, Gabriel’s phthalimide synthesis, Hofmann bromamide
reaction (Hofmann rearrangement).
Reactions: Hofmann vs. Saytzeff elimination, Carbylamine test, Hinsberg test, with HNO2,
Schotten – Baumann reaction. Electrophilic substitution (case aniline): nitration,
bromination, sulphonation.
Diazonium salts: Preparation from aromatic amines, conversion to benzene, phenol, dyes.
3. Amino Acids and Peptides (6 Hours)

Preparation of Amino Acids: Strecker synthesis, Gabriel’s phthalimide synthesis.
Terms: Zwitterion, Isoelectric point and Electrophoresis.
Reactions of Amino acids: Ester of – COOH group, acetylation of –NH2 group, complexation

with Cu2+ ions, ninhydrin test. Synthesis of simple peptides (upto dipeptides) by N-protection
(t-butyloxycarbonyl and phthaloyl) & C-activating groups and Merrifield solid-phase
synthesis.
4. UV –Visible Spectroscopy in Organic Chemistry (8 Hours)

Introduction to spectroscopy :
UV Spectroscopy: Beer-Lambert’s law, Types of electronic transitions, λmax, Chromophores
and Auxochromes, Bathochromic and Hypsochromic shifts, Intensity of absorption.
Visible Spectroscopy: Effect of conjugation on colour. Application of Woodward - Fieser
rules for calculation of λmax for the following systems: α, β unsaturated aldehydes, ketones.
Conjugated dienes: alicyclic, homoannular and heteroannular, extended conjugated systems
(aldehydes, ketones and dienes). Distinction between cis and trans isomers.
5. Carbohydrates: (4 Hours)
Classification and General Properties, Glucose and Fructose (open chain and cyclic
structure), Determination of configuration of monosaccharides, absolute configuration of
Glucose and Fructose, Mutarotation, Osazone formation, Killiani Fischer synthesis.
Reference Books:
1. Castellan, G.W. Physical Chemistry 4th Ed. Narosa (2004).
2. Kotz, J.C., Treichel, P.M. & Townsend, J.R. General Chemistry, Cengage Learning
India Pvt. Ltd.: New Delhi (2009)
3. Undergraduate Physical Chemistry, Vol II, J.N. Gurtu, Pragati Prakashan.
4. Advanced Physical Chemistry, Gurtu and Gurtu, Pragati Prakashan
5. Mahan, B.H. University Chemistry, 3rd Ed. Narosa (1998).
6. Petrucci, R.H. General Chemistry, 5th Ed., Macmillan Publishing Co.: New York
(1985).
7. Morrison, R. T. & Boyd, R. N. Organic Chemistry, Dorling Kindersley (India) Pvt.
Ltd. (Pearson Education).
8. Finar, I. L. Organic Chemistry (Volume 1), Dorling Kindersley (India) Pvt. Ltd.
(Pearson Education).
9. Finar, I. L. Organic Chemistry (Volume 2), Dorling Kindersley (India) Pvt. Ltd.
(Pearson Education).
10. Nelson, D. L. & Cox, M. M. Lehninger’s Principles of Biochemistry 7th Ed., W. H.
Freeman.

11. Berg, J. M., Tymoczko, J.L. & Stryer, L. Biochemistry, W.H. Freeman, 2002.Kemp,
W. Organic Spectroscopy, Palgrave.
12. Pavia, D. L. et al. Introduction to Spectroscopy 5th Ed. Cengage Learning India
13. Silverstein, Bassler and Morill, Spectrometric Identification of Organic Compounds
Ed. (2015).

SEMESTER III
CHEMISTRY- LAB
CORE COURSE: CHC103
Practicals: 60 Hours (02 Credits)
Section A: Physical Chemistry-2 (30 Hours: 01 credit)
Phase Equilibria 12 Hours

a) To draw the phase diagram of the binary system - diphenyl amine and α – Naphthol
and find the eutectic temperature. (4 Hours)
b) Study the mutual solubility of phenol and water at various temperatures and hence
determine the critical solution temperature. (4 Hours)
c) Study the effect of addition of NaCl on critical solution temperature of phenol water
system and study of the effect of impurities on it. (4 Hours)
Conductance 10 Hours
a) Determination of cell constant. (2 Hours)
b) Determination of equivalent conductance, degree of dissociation and dissociation
constant of a weak acid. (4 Hours)
c) Conductometric titrations: (4 Hours)
i. Strong acid vs. strong base
ii. Weak acid vs. strong base
Potentiometry 08 Hours
Potentiometric titrations
i. Strong acid vs. strong base (Quinhydrone method) (4 Hours)
ii. Potassium dichromate vs. Ferrous Ammonium sulphate (4 Hours)
Reference books:
1. Systematic experimental physical Chemistry by S.W. Rajbhoj, Dr. T. K. Chondhekar,

Anjali Publication, Aurangabad.
2. Practical Chemistry by O.P. Pandey, D. N. Bajpai, S. Giri, S. Chand Publication

3. Khosla, B. D., Garg, V. C. & Gulati, A. Senior Practical Physical Chemistry, R.
Chand & Co.: New Delhi (2011).
Section B: Organic Chemistry - 3 (30 Hours: 1 Credit)
I) Systematic Qualitative Organic Analysis : (6x2 =12 Hours)

Analysis of Organic Compounds possessing monofunctional groups (carboxylic, aldehyde,
ketone, amide, nitro, amines) and preparation of one derivative of each group. (Analysis of
single compound and its derivative preparation)
II) Organic Preparations : (14 Hours)

Synthesis, yield, recrystallisation and Melting Point.
(i) Hippuric acid from glycine (Benzoylation-Schotten Baumann reaction) (4 Hours)
(ii) Osazone from Glucose (Nucleophilic addition) (2 Hours)
(iii) Phthalic acid to Phthalic Anhydride to Phthalimide (4 Hours)
(iv) Preparation of Azo dye (4 Hours)
III) Organic Estimations: (Any 2) (4 Hours)

(i) Estimation of glycine by formylation method (2 Hours)
(ii) Estimation of Glucose by oxidation (2 Hours)
(iii) Estimation of Acetamide by hydrolysis (2 Hours)
Reference Books:
Organic Chemistry
1. Vogel, A.I., Tatchell, A.R., Furnis, B.S., Hannaford, A.J. & Smith, P.W.G., Textbook
of Practical Organic Chemistry, Prentice-Hall, 5th edition, 1996.
2. Mann, F.G. & Saunders, B.C. Practical Organic Chemistry Orient-Longman, 1960.
3. Ahluwalia, V.K. & Aggarwal, R. Comprehensive Practical Organic Chemistry,
Universities Press.

ANNEXURE-Ib
SEMESTER III
SKILL ENHANCEMENT COURSE (SEC)
(4 Credits: Theory -03, Practical-01)
----------------------------------------------------------------------------------------------------------------
SKILL ENHANCEMENT COURSE: CHS101
NATURAL RESOURCES AND ANALYSIS
I. Review of energy sources (renewable and non-renewable). Classification of fuels and

their calorific value. 2 Hours
II. Coal: Uses of coal (fuel and nonfuel) in various industries, its composition, carbonization
of coal. Coal gas, Producer gas and Water gas—composition and uses. Fractionation of coal
tar, uses of coal tar, requisites of a good metallurgical coke, coal gasification (Hydro
gasification and Catalytic gasification), coal liquefaction and solvent refining. 10 Hours
III. Petroleum and Petrochemical Industry: Composition of crude petroleum, Refining

and different types of petroleum products and their applications.
Fractional Distillation (Principle and process), Cracking (Thermal and catalytic cracking),
Reforming petroleum and non-petroleum fuels (LPG, CNG, LNG, bio-gas, fuels derived
from biomass), fuel from waste, synthetic fuels (gaseous and liquids), clean fuels.
Petrochemicals: Vinyl acetate, Propylene oxide, Isoprene, Butadiene, Toluene and its
Derivatives. 10 Hours
IV. Analysis of food products: Nutritional value of foods, idea about food processing and
food preservation and adulteration.
a) Identification of adulterants in some common food items like coffee powder, asafoetida,
chilli powder, turmeric powder, coriander powder, pulses etc.
b) Analysis of preservatives and colouring matter. 10 Hours
V. Analysis of soil: Composition of soil, Concept of pH and pH measurement,

complexometric titrations, chelation, chelating agents, use of indicators. 7 Hours
VI. Analysis of water: Definition of pure water, sources responsible for contaminating
water, water sampling methods, water purification methods. 6 Hours

SEMESTER III
CHEMISTRY- LAB

----------------------------------------------------------------------------------------------------------------
Practicals: 30 Hours (01 Credit)
Instruction: Practicals/ demonstrations
1. Determination of pH of soil samples. 3 Hours
2. Determination of pH of a water samples 3 Hours
3. Estimation of Calcium and Magnesium ions as calcium carbonate by complexometric
titration. 6 Hours
4. Determination of dissolved oxygen (DO) in a given water sample. 4 Hours
5. Determination of acidity of a water sample 4 Hours
6. Determination of alkalinity in a given water sample 4 Hours
7. Measurement of dissolved CO2. 4 Hours
8. Percentage of available chlorine in bleaching powder. 2 Hours
Reference Books for Theory and Practicals:
1. Svehla, G. Vogel’s Qualitative Inorganic Analysis, Pearson Education, 2012.

2. Mendham, J. Vogel’s Quantitative Chemical Analysis, Pearson, 2009.
3. Stocchi, E. Industrial Chemistry, Vol-I, Ellis Horwood Ltd. UK (1990).
Jain, P.C. & Jain, M. Engineering Chemistry
4. Sharma, B.K. & Gaur, H. Industrial Chemistry, Goel Publishing House, Meerut (1996).
5. Skoog, D.A. Holler F.J. & Nieman, T.A. Principles of Instrumental Analysis, Cengage
Learning India Ed.
6. Harris, D. C. Quantitative Chemical Analysis, W. H. Freeman.
7. Dean, J. A. Analytical Chemistry Notebook, McGraw Hill.
8. Day, R. A. & Underwood, A. L. Quantitative Analysis, Prentice Hall of India.

SEMESTER III
(4 Credits: Theory-03, Practical-01)
___________________________________________________________________________
PHARMACEUTICAL CHEMISTRY AND INTELLECTUAL PROPERTY RIGHTS

Pharmaceutical Chemistry : History and Introduction:

Pharmaceutical Chemistry-Historical background of Drug discovery, design and
development. Pharmacophore and Concept of structure-activity relationship. Main Classes of
drugs with examples: anti-infective agents, cardiovascular agents, central nervous system
agents, analgesics and anti-inflammatory agents, antibiotics and anti-HIV drugs. Basic
Retrosynthetic approach with reference to Ibuprofen and Dapsone. (8 Hours)
IUPAC names, Synthesis and uses of representative drugs:

Synthesis of Aspirin, paracetamol, lbuprofen, Chloramphenicol, Sulphanethoxazole,
Sulphacetamide,Trimethoprim, Acyclovir, Clotrimazole, Phenobarbital, Diazepam, Glyceryl
trinitrate, Dapsone, metronidazole, AZT- Zidovudine. (8 Hours)
Mechanism of Action of representative drugs:

Analgesic and Anti-inflammatory drugs (Ibuprofen), Antilepral agent (Dapsone),
Sulphonamides, antiamoebic (metronidazole), Central nervous depressant (Phenobarbital)
(6 Hours)
Structure Activity Relationship of representative drugs:

Analgesic and Anti-inflammatory drugs (Ibuprofen), Antilepral agent (Dapsone),
Sulphonamides (suphacetamide), antiamoebic (metronidazole), Central nervous depressant
(Phenobarbital), Antibiotic (Chloramphenicol), Antimalarial (Trimethoprim) (8 Hours)
Introduction to Intellectual Property:

Historical Perspective, Different Types of IP, Importance of protecting IP.
Copyrights: Introduction, How to obtain, Differences from Patents.

Trade Marks: Introduction, How to obtain, Different types of marks – Collective marks,
certification marks, service marks, Trade names, etc. Differences from Designs.
Patents: Historical Perspective, Basic and associated right, WIPO, PCT system, Traditional
Knowledge, Patents and Healthcare – balancing promoting innovation with public health,
Software patents and their importance for India.
Geographical Indications: Definition, rules for registration, prevention of illegal
exploitation, importance to India.
Industrial Designs: Definition, How to obtain, features, International design registration.
Importance for pharmaceutical industry.
Trade Secrets: Introduction and Historical Perspectives, Scope of Protection, Risks involved
and legal aspects of Trade Secret Protection. (10 Hours)
Different International Agreements

World Trade Organization (WTO): (i) General Agreement on Tariffs & Trade (GATT),
Trade Related Intellectual Property Rights (TRIPS) agreement (ii) General Agreement on
Trade related Services (GATS) (iii) Madrid Protocol (iv) Berne Convention (v) Budapest
Treaty. (3 Hours)
Indian Patent Act: Prior Art search for patents with an illustration. (2 Hours)

SEMESTER III
CHEMISTRY-LAB
Practicals: 30 Hours (01 Credit)
I) Preparations (Each practical for four hours)(Any four) (4x4=16 Hours)
1) Aspirin 2) Benzimidazole 3) 2,4-diphenyl Quinoxaline
4) Benzocaine 5) Sulphacetamide
II) Titrimetric Assay (Each practical for three hours) (3x2=06 Hours)
1. Assay of Aspirin 2) Assay of Ibuprofen
2. Patent filing application procedures with two exercises. (2x2=4 Hours)
3. Patent Prior Art search on pharmaceutical patent. (4 Hours)
Reference Books for Theory and Practicals:

1. G.L. Patrick: Introduction to Medicinal Chemistry, Oxford University Press, UK.
2. Hakishan, V.K. Kapoor: Medicinal and Pharmaceutical Chemistry, Vallabh
Prakashan, Pitampura, New Delhi.
3. William O. Foye, Thomas L., Lemke , David A. William: Principles of Medicinal
Chemistry, B.I. Waverly Pvt. Ltd. New Delhi.
4. Wilson, Gisvold and Doerge Textbook of Organic, Medicinal and Pharmaceutical
Chemistry.
5. Lednicer and Meischer, Organic Chemistry of Drug Synthesis. Vol. I to III. John
Wiley & Sons, 2005.
6. Medicinal Chemistry, D. Shriram, P. Yogeshwari, Pearson Education, 2007.
7. Medicinal Chemistry-Burger, John Wiley & Sons N.Y,1997.
8. Medicinal Chemistry, Chatwal, Himalaya Publishing house, 2002.
9. N.K. Acharya: Textbook on intellectual property rights, Asia Law House (2001).
10. Manjula Guru & M.B. Rao, Understanding Trips: Managing Knowledge in
Developing Countries, Sage Publications (2003).
11. P. Ganguli, Intellectual Property Rights: Unleashing the Knowledge Economy, Tata
McGraw-Hill (2001).
12. Arthur Raphael Miller, Micheal H.Davis; Intellectual Property: Patents, Trademarks
and Copyright in a Nutshell, West Group Publishers (2000).
13. Jayashree Watal, Intellectual property rights in the WTO and developing countries,
Oxford University Press, Oxford.
14. Indian Pharmacopoiea, latest edition.

ANNEXURE-Ic
Syllabus of B.Sc. CHEMISTRY
SEMESTER IV
CORE COURSE: CHC104
(6 Credits: Theory-04, Practicals-02)
(PHYSICAL CHEMISTRY AND INORGANIC CHEMISTRY)
Section A: Physical Chemistry-3 (30 Hours; 02 credits)

1. Kinetic Theory of Gases (8 Hours)
Postulates of Kinetic Theory of Gases, deviation of real gases from ideal behaviour,
compressibility factor, causes of deviation. van der Waals equation of state for real gases.
Boyle temperature (derivation not required). Critical phenomena, critical constants and
their calculation from van der Waals equation. Andrews isotherms for CO2. Maxwell
Boltzmann distribution laws of molecular velocities and molecular energies (graphic
representation – derivation not required) and their importance. Temperature dependence
of these distributions. Most probable, average and root mean square velocities (no
derivation), collision number, collision frequency, collision diameter and mean free path
of molecules.
2. Liquids (6 Hours)
Surface tension and its determination using stalagmometer. Effect of temperature on
surface tension. Viscosity of a liquid and determination of coefficient of viscosity using
Ostwald viscometer and factors affecting viscosity.
3. Solids (8 Hours)
Forms of solids, symmetry elements, unit cells, crystal systems, Bravais lattice.
Laws of crystallography - Law of constancy of interfacial angles, Law of rational indices.
Miller indices, X–Ray diffraction by crystals, Bragg’s law. Particle size determination
using powder method. Structures of NaCl, KCl and CsCl (qualitative treatment only).

4. Chemical Kinetics (8 Hours)
The concept of reaction rates. Effect of temperature, pressure and catalyst on reaction
rates. Order and molecularity of a reaction. Derivation of integrated rate equations for
zero, first and second order reactions (both for equal and unequal concentrations of
reactants). Half–life of a reaction. General methods for determination of order of a
reaction. Concept of activation energy and its calculation from Arrhenius equation.
Theories of Reaction Rates: Collision theory and Activated Complex theory of
bimolecular reactions.
Section B: Inorganic Chemistry-2 (30 hour: 02 credits)

1. Transition Elements (10 Hours)
General characteristic properties of 3d series with special reference to electronic
configuration, variable valency, colour, magnetic and catalytic properties. Ability to form
complexes and stability of various oxidation states (Latimer diagrams) for Mn, Fe and Cu.
Lanthanides: Electronic configurations, oxidation states, colour, magnetic properties,
lanthanide contraction, separation of lanthanides (ion exchange method only).
Actinides : Electronic configuration and General characteristics.
2. Coordination Chemistry (10 Hours)

IUPAC system of nomenclature. Bonding in complexes based on Valence Bond Theory
(VBT), Inner and outer orbital complexes of Cr, Fe, Co, Ni and Cu (coordination numbers 4
and 6). Different types of structural and stereo-isomerism including optical isomerism in
complexes with coordination numbers 4 and 6. Drawbacks of VBT.
3. Crystal Field Theory (10 Hours)

Crystal field splitting in octahedral complexes. Crystal field stabilization energy (CFSE),
Crystal field effects for weak and strong fields. Spectrochemical series. Crystal Field
Splitting in Tetrahedral complexes. Calculation of CFSE. Comparison of CFSE for Oh and
Td complexes. Factors affecting the magnitude of 10Dq. Merits and Demerits of Crystal
Field Theory.

Reference Books:
Physical Chemistry
1. Barrow, G.M. Physical Chemistry Tata McGraw‐Hill (2007).
2. Castellan, G.W. Physical Chemistry 4th Ed. Narosa (2004).
3. Kotz, J.C., Treichel, P.M. & Townsend, J.R. General Chemistry Cengage Learning
India Pvt. Ltd., New Delhi (2009).
4. Essentials of Physical Chemistry by A. Bahl and G.D. Tuli, S. Chand Publication,
5. Mahan, B.H. University Chemistry 3rd Ed. Narosa (1998).
6. Petrucci, R.H. General Chemistry 5th Ed. Macmillan Publishing Co.: New York
(1985).
7. Undergraduate Physical Chemistry, Vol II, J.N. Gurtu, Pragati Prakashan.
8. Advanced Physical Chemistry, Gurtu and Gurtu , Pragati Prakashan
Inorganic Chemistry
1. Cotton, F.A. & Wilkinson, G. Basic Inorganic Chemistry, Wiley.
2. Shriver, D.F. & Atkins, P.W. Inorganic Chemistry, Oxford University Press.
3. Wulfsberg, G. Inorganic Chemistry, Viva Books Pvt. Ltd.
4. Rodgers, G.E. Inorganic & Solid State Chemistry, Cengage Learning India Ltd.,2008.
5. Kotz, J.C., Treichel, P.M. & Townsend, J.R. General Chemistry Cengage Learning India
Pvt. Ltd., New Delhi (2009).
6. Mahan, B.H. University Chemistry 3rd Ed. Narosa (1998).
7. Petrucci, R.H. General Chemistry 5th Ed. Macmillan Publishing Co.: New York (1985).
8. Principles of Inorganic chemistry by B.R. Puri, S. Sharma and Kalia, Vallabh Publication.
9. Inorganic Chemistry Principles of Structure and Reactivity James E Huheey, Ellen A.
Keiter, Richard L.Keiter, Okhil K Medhi.

SEMESTER IV
CHEMISTRY- LAB
CORE COURSE: CHC104
Practicals: 60 Hours ( 02 Credits)
Section A: Physical Chemistry-3 (30 HOURS: 01 Credit)

1. Surface tension measurement (4 Hours)
Determination of the surface tension of a liquid or a dilute solution using a stalagmometer.
2. Solutions of Solids in Liquids (4 Hours)
0 0
Determine solubility curve for KCl from 25 C to 50 C.
3. Viscosity measurement (10 Hours)
a) Determination of the viscosity of a liquid or dilute solution using an Ostwald’s
viscometer.
b) Study of the variation of viscosity of an aqueous solution with concentration of solute.
4. Chemical Kinetics (12 Hours)
1. To determine the rate constant and order of reaction between KI and K2S2O8.
2. Study of saponification of ethyl acetate with sodium hydroxide at equal concentration of
ester and alkali.
3. Compare the strengths of HCl and H2SO4 by studying kinetics of hydrolysis of
methyl acetate.
Section B: Inorganic Chemistry-2 (3 HOURS : 01 Credit)

I. Semi-micro qualitative analysis: not more than four ionic species (two anions and
two cations): (4 Mixtures) (4 x 3= 12 Hours)
Cations : NH4+, Pb2+, Ag+, Bi3+, Cu2+, Cd2+, Sn2+, Fe3+, Al3+, Co2+, Cr3+, Ni2+, Mn2+, Zn2+,
Ba2+, Sr2+, Ca2+, K+.
Anions : CO32-, S2–, SO2–, SO42-, NO3–, Cl–, Br–, I–, NO2–, PO43-, F-
(Spot tests should be carried out wherever feasible)
II. GRAVIMETRIC/VOLUMETRIC (4 x 3 = 12 Hours)

1. Estimate the amount of Nickel present in a given solution as bis(dimethylglyoximato)
Nickel(II) in a given solution gravimetrically by counterpoise filter paper.

2. Estimation of (i) Mg2+ or (ii) Zn2+ by complexometric titrations using EDTA.
3. To estimate the amount of Bismuth present in the given solution of Bi(NO3)2.3H2O
by complexometric titration.
4. To estimate the amount of Nitrite present in the given NaNO2 solution by titrating
v/s Ceric ammmonium sulphate / Ceric sulphate.
III. COLORIMETRIC EXPERIMENTS (2x 3 = 06 Hours)

1. Draw calibration curve (absorbance at λmax vs. concentration) for various
concentrations of a given coloured compound (KMnO4/ CuSO4) and estimate the
concentration of the same in a given solution.
2. Determine the composition of the Fe3+-salicylic acid complex solution by Job’s
method.
Reference Books: (Physical Chemistry)

2. Khosla, B. D.; Garg, V. C. &Gulati, A. Senior Practical Physical Chemistry, R.
1. Chand & Co.: New Delhi (2011).
2. Systematic experimental physical Chemistry by S.W. Rajbhoj, Dr. T. K. Chondhekar,
Anjali Publication
3. Practical Chemistry by O.P. Pandey, D. N. Bajpai, S. Giri, S. Chand Publication
4. Senior Practical Physical Chemistry, B.D. Khosla, V.C. Garg, A. Gulati, R. Chand &
Comp , New-Delhi
Reference Books: (Inorganic Chemistry)

1. Svehla, G., Vogel’s Qualitative Inorganic Analysis, Pearson Education, 2012.

ANNEXURE - Id
SEMESTER IV
----------------------------------------------------------------------------------------------------------------
CHEMISTRY OF COSMETICS AND PERFUMES
Theory: 45 Hours (03Credits)
1. Cosmetic Formulation, principles and preparations 15 Hours

Introduction to cosmeticology. Definition of cosmetics as per EU and Indian guidelines.
Cleansing and care needs for face, eye lids, lips, hands, feet, nail, scalp, neck, body, and
underarms. Examples of marketed products. A general study including preparation and uses
of the following: Hair dye, hair spray, sunscreen lotions, face powder, lipsticks, talcum
powder, nail enamel, creams (cold, vanishing and shaving), Formulation, preparation and
packaging of cosmetics for hair - Shampoo and conditioners. Examples from marketed
products.
2. Herbal Cosmetics 15 Hours

Definition of herb, herbal medicine, herbal medicinal product, herbal drug preparation.
Classification of herbal cosmetics. Development of Ayurvedic and Herbal formulations and
their evaluation by physical methods, chemical methods and microscopical techniques.
Herbal cosmetics for skin care (lotions, vanishing cream, foundation creams, anti sunburn
preparations, face packs, lipsticks, face powders, soaps). Herbal cosmetics for hair care:
Henna and Hibiscus.
3. Perfumes and Flavors 15 Hours

Classification of perfumes. Perfume ingredients listed as allergens. Deodorants,
antiperspirants and artificial flavours. Essential oils and their importance in cosmetic
industries with reference to Eugenol, Geraniol, sandalwood oil, eucalyptus, rose oil, 2-phenyl
ethyl alcohol, Jasmone, Civetone, Muscone. Volatile Oils : General methods of obtaining
volatile oils from plants; Study of volatile oils of Mentha, Lemon peel, Orange peel, Lemon
grass, Eucalyptus, Musk, Sandal wood.

SEMESTER IV
CHEMISTRY- LAB
------------------------------------------------------------------------------------------------
Practicals: 30 HOURS (01 CREDIT)
Demonstration/Practicals (Any Ten) 3 x 10 = 30 Hours
1. Preparation of talcum powder.
2. Preparation of shampoo.
3. Preparation of enamels.
4. Preparation of hair remover.
5. Preparation of cold cream.
6. Preparation of nail polish and nail polish remover.
7. Preparation of vanishing cream.
8. Preparation of shaving cream.
9. Herbal preparations and evaluations of lotions.
10. Herbal preparations and evaluations of face packs.
11. Herbal preparations and evaluations of soaps.
12. Extraction of volatile oil from lemon peel.
13. Extraction of volatile oil from lemon grass.
14. Extraction of volatile oil from orange peel.
Reference Books:
1. E. Stocchi: Industrial Chemistry, Vol -I, Ellis Horwood Ltd. UK.
2. P.C. Jain, M. Jain: Engineering Chemistry, Dhanpat Rai & Sons, Delhi.
3. Sharma, B.K. & Gaur, H. Industrial Chemistry, Goel Publishing House, Meerut
(1996).
4. G.L. Patrick: Introduction to Medicinal Chemistry, Oxford University Press, UK. 65.
5. Hakishan, V.K. Kapoor: Medicinal and Pharmaceutical Chemistry, Vallabh
Prakashan, Pitampura, New Delhi.
6. Keith Wilson and John Walker: Practical Biochemistry.
7. Thomas M. Devlin: Textbook of Biochemistry.
8. Talwar, G.P. & Srivastava, M. Textbook of Biochemistry and Human Biology, 3rd
Ed.PHI Learning.
9. Text book of herbal cosmetics by Vimaladevi M. CBS Publishing 1st Ed. 2015.
10. The complete technology book on herbal beauty products with formulation and
processes by H. Panda, Asia pacific business press Inc. 2005.
11. Essential oils: A practical guide by John Gordon, Aetheric publishing.

SEMESTER IV
----------------------------------------------------------------------------------------------------
ADVANCES IN ENERGY TECHNOLOGY
Theory: 45 HOURS (03 Credits)
1. INTRODUCTION 5 Hours
1.1 Man and Energy
1.2 Chemical Energy System, Electrochemical energy system.
1.3 Resources and energy: Natural resources- energy environment triangle, energy
problem, World energy resources, Energy conversion, Energy conversion
processes.
1.4 Future Energy Resources.
2. CHEMICAL ENERGY SOURCES 16 Hours

2.1 Petroleum: Origin, nature of sources of material for crude oil, composition of
petroleum, refining of petroleum, products derived from petroleum.
2.2 Natural gas: Occurrence, natural gas liquid.
2.3 Coal: Origin, constitution of coal, coal gasification, and indirect liquification,
purification of synthesis gas. Coal combustion, chemical obtained from coal.
2.4 Nuclear Fission: Power from nuclear fission, heavy water reactor (HWRs) fast
breeder reactors (FBRs)
2.5 Nuclear Fusion: Cold fusion
3. ELECTROCHEMICAL ENERGY SYSTEM: 12 Hours

3.1 Introduction, fundamentals of batteries, choice of materials, classification of
batteries, sizes of batteries.
3.2 Some common batteries: Button cells, Portable equipment batteries, SLI batteries,
Vehicle traction batteries, Stationary batteries, Battery characteristic power
density.
3.3 Primary batteries: Combination of materials for a primary battery, alkaline MnO2
batteries performance and advantages, secondary batteries.
3.4 Types and classification, sealed storage batteries, metal hydride electrode.
4. FUEL CELLS: 07 Hours

4.1 Introduction, Classification, Choice of electrolyte. Electrodes and requirement of
Electrocatalysis.
4.2 Use of Carbon in fuel cells, fuel cells using carbon nanomaterials
4.3 Biochemical fuel cells, classification ,mechanism and applications

5. SOLAR ENERGY: 05 Hours
5.1 Photochemical and photogalvanic conversion.
5.2 Hydrogen energy: Merits of hydrogen fuel cell, Hydrogen economy concept,
Photo assisted electrolysis of water.
5.3 Miscellaneous Sources: Tidal Energy, Geothermal Energy
References:
1. R. Narayan and B. Viswanathan, Chemical and Electrochemical Energy Systems,

University Press, 1998.
2. C. Vincent and B. Scrosati, Modern Batteries, An introduction to Electrochemical
Power Sources, Arnold, 1997.
3. M. Sharon and M. Sharon, Nano Forms of Carbon and its Application, Monad Nano
Tech , Mumbai, 2007.
4. R. Probstein and R. Hicks, Synthetic Fuels, Mc Graw Hill, 1985.
5. International Journal of Hydrogen Energy 16, 35-45 (1991)
6. S. Manahan, Fundamentals of Environmental Chemistry, Lewis Publication, New
York, 1993.
7. S. P. Sukhatme, Solar Energy Principles of Thermal Collection and Storage , Tata
McGraw Hill, 2006.

SEMESTER IV
CHEMISTRY-LAB
SKILL ENHANCEMENT COURSE : CHS107
----------------------------------------------------------------------------------------------------------------
Practicals: 30 HOURS ( 01 Credit)
A. Electrochemical Energy
1. Construct a Daniel cell and determine the voltage of the cell at varying concentration. (4 Hours)
2. Determination of electrochemical equivalent of copper (4 Hours)
B. Supports for Electro-catalyst
1. Preparation of Carbon ( from Coconut shell) and determination of surface area using
volumetric method. (4 Hours)
2. Verification of Fruendlich adsorption isotherm of Coconut shell Carbon. (4 Hours)
C. Photochemical Energy
1. Extraction of photosynthetic pigments from different parts of the plants and its identification
from absorption wavelength (2 samples to be studied) (4 Hours)
2. Kinetics of photochemical reactions between iodine and oxalate using visible light
(Colorimetrically) (4 Hours)
D. Sources of Chemical Energy
1. Determination of moisture content in the sample of coal/ charcoal. (2 Hours)
2. Determination of sulphur and ash content in the sample of Coal/Charcoal. (4 Hours)
References:
1. O. P. Virmani and A.K. Narula, Applied Chemistry theory and Practice, New Age,
International Publishers, IInd Edition.
2. Robert Bruce Thompson, Illustrated Guide to Home Chemistry Experiments O’Reilly
Media. Inc.
3. S. W. Rajbhoj and Dr. T. K. Chondhekar, Systemetic Experimental Physical Chemistry,
Anjali Publication Aurangabad.

ANNEXURE II
Pattern of Question papers
for
Semester End Examination (SEE)
and
Scheme of marking
ANNEXURE- IIa : Pattern for Semester III and Semester IV Core Course (CC)
SEE Question Papers of B.Sc. With Chemistry Programme
Semester III CHC103 …………. for 4 credits
Semester IV CHC104 ………….. for 4 credits
ANNEXURE -IIb: Pattern for Semester III and Semester IV
Skill Enhancement Course (SEC)
Semester III CHS101………….. for 3 credits
OR
CHS106………….. for 3 credits
Semester IV CHS102…………... for 3 credits
OR
CHS107…………... for 3 credits

ANNEXURE - IIa
SEMESTER III
CORE COURSE: CHC103
(Credits: Theory-04, Practicals-02)
Time Duration: 2 Hours Total Marks: 80
Section A: Physical Chemistry-2 Marks: 40

Q.1.Answer any five of the following: (2x5=10 marks)
i) Solutions.
ii) Phase Equilibria.
iii) Conductance.
iv) Electrochemistry.
v) Solutions.
vi) Phase Equilibria.
vii) Electrochemistry.
Q.2.A. i) Solutions. 4 marks
ii) Phase Equilibria. 3 marks
OR
Q.2.A. iii) Solutions . 4 marks
iv) Phase Equilibria. 3 marks
Q.2.B. i) Electrochemistry. 4 marks
ii) Electrochemistry 4 marks
Q.3.A.i) Conductance. 4 marks
ii) Electrochemistry. 3 marks
OR
Q.3.A. iii) Conductance. 4 marks
iv) Electrochemistry. 3 marks
Q.3.B. i) PhaseEquilibria 4 marks
ii)Solutions 4 marks

Section B: Organic Chemistry-3 Marks: 40
Q.4. Answer any five questions of the following.: (2 x 5=10 marks)
i) Carboxylic Acids and derivatives.
ii) Amines and Diazonium salts
iii) Amino acids ,Peptides and Proteins
iv) Carbohydrates
v) Amines and Diazonium salts
vi) UV –Visible Spectroscopy in Organic Chemistry
vii) Carbohydrates
Q.5.A. i) UV –Visible Spectroscopy in Organic Chemistry 4 marks
ii) Carboxylic acids and derivatives 3 marks
OR
iii) Carbohydrates 4 marks
iv) Amino acids,Peptides and Proteins 3 marks
Q.5.B. i) UV-Visible Spectroscopy in Organic Chemistry 4 marks
ii) Carboxylic acids and derivatives 4 marks
Q.6.A. i) Amino acids ,Peptides and Proteins 4 marks
ii) UV-Visible Spectroscopy in Organic Chemistry 3 marks
OR
iii) Amines and diazonium salts 4 marks
iv) Amino acids ,Peptides and Proteins 3 marks
Q.6.B. i) Amines and Diazonium salts 4 marks
ii) UV-Visible Spectroscopy in Organic Chemistry 4 Marks

SEMESTER IV
CORE COURSE: CHC104
Time Duration : 2 Hours Total Marks: 80
Section A: Physical Chemistry-3 Marks: 40

Q.1.Answer any five of the following: (2x5=10 marks)
i) Kinetic Theory of Gases.

ii) Liquids.
iii) Solids.
iv) Chemical Kinetics.
v) Kinetic Theory of Gases Solutions.
vi) Solids.
vii) Chemical Kinetics.
Q.2.A. i) Kinetic Theory of Gases. 4 marks

ii) Liquids. 3 marks
OR
Q.2.A. iii) Kinetic Theory of Gases . 4 marks
iv) Liquids . 3 marks
Q.2.B. i) Chemical Kinetics. 4 marks
ii) Solids. 4 marks
Q.3.A.i) Chemical Kinetics. 4 marks
ii) Solids. 3 marks
OR
Q.3.A. iii) Chemical Kinetics. 4 marks
iv) Solids. 3 marks
Q.3.B. i) Kinetic Theory of Gases 4 marks
ii) Liquids 4 marks

SECTION B : Inorganic Chemistry-2 Marks : 40
Q.1. Answer any five from the following (2x5 = 10 marks)
i) Transition Elements
ii) Transition Elements
iii Transition Elements
iv) Coordination Chemistry
v) Coordination Chemistry
vi) Crystal Field Theory
vii) Crystal Field Theory
Q.2. A. Answer the following
i) Transition Elements 4 marks
ii) Coordination Chemistry 3 marks
OR
Q.2. A. iii) Transition Elements 4 marks
iv) Coordination Chemistry 3 marks
Q.2.B. i) Crystal Field Theory 4 marks
ii) Coordination Chemistry 4 Marks
Q.3. A. Answer the following
i) Crystal Field Theory 4 marks
ii) Transition Elements 3 marks
OR
Q.3. A. iii) Crystal Field Theory 4 marks
iv) Transition Elements 3 marks
Q.3.B i) Coordination Chemistry 4 marks
ii) Crystal Field Theory 4 marks

ANNEXURE – IIb
SEMESTER III
(4Credits: Theory-03, Practicals-01)
----------------------------------------------------------------------------------------------------
Q.1. Answer any ten the following: (2x10= 20 marks)
i) Review of energy sources

ii) Review of energy sources
iii) Coal
iv) Coal
v) Coal
vi) Petroleum and petroleum industry
vii) Petroleum and petroleum industry
viii) Petroleum and petroleum industry
ix) Analysis of food products
x) Analysis of food products
xi) Analysis of soil
xii) Analysis of soil
xiii) Analysis of water
xiv) Analysis of water
Q.2 A. i) Coal 3 marks

ii) Petroleum and petroleum industry 2 marks
OR
Q.2 A. iii) Petroleum and petroleum industry 3 marks
iv) Coal 2 marks
Q.2 B. i) Coal 3 marks
ii) Petroleum and petroleum industry 2 marks
Q.3 A. i) Analysis of food products 3 marks

ii) Analysis of water 2 marks
OR
Q.3 A. iii) Analysis of food products 3 marks

iv) Analysis of soil 2 marks
Q.3 B. i) Analysis of soil 3 marks
Q.4 A. i) Analysis of water 3 marks
ii) Analysis of soil 2 marks
OR
iii) Analysis of water 3 marks
iv) Petroleum and petroleum industry 2 marks
Q.5 A. i) Analysis of food products 3 marks
OR
Q.5 A. iii) Coal 3 marks
iv) Petroleum and petroleum industry 2 marks
ii) Analysis of food products 2 marks

SEMESTER III
Time Duration: 2 Hours Total Marks:

60
Q.1. Answer any ten of the following. (2x10=20 marks)
i) Pharmaceutical Chemistry: History and Introduction

ii) IUPAC names, Synthesis and uses of representative drugs
iii) Mechanism of Action of representative drugs
iv) Structure Activity Relationship of representative drugs
v) Introduction to Intellectual Property
vi) Different International Agreements
vii) Introduction to Intellectual Property
viii) Pharmaceutical Chemistry: History and Introduction
ix) IUPAC names, Synthesis and uses of representative drugs
x) Mechanism of Action of representative drugs
xi) Structure Activity Relationship of representative drugs
xii) Pharmaceutical Chemistry: History and Introduction.
xiii) Introduction to Intellectual Property.
xiv) IUPAC names, Synthesis and uses of representative drugs
Q2. A) i) IUPAC names, Synthesis and uses of representative drugs 3 marks
ii) Introduction to Intellectual Property 2 marks
OR
A) iii) Structure Activity Relationship of representative drugs 3 marks
iv) Mechanism of Action of representative drugs 2 marks
B) i) Introduction to Intellectual Property 3 marks
ii) Pharmaceutical Chemistry: History and Introduction 2 marks
Q3. A) i) IUPAC names, Synthesis and uses of representative drugs 3 marks

ii) Introduction to Intellectual Property 2 marks
OR
A) iii) Structure Activity Relationship of representative drugs. 3 marks
iv) Pharmaceutical Chemistry: History and Introduction. 2 marks
B) i) Mechanism of Action of representative drugs. 3 marks
ii) Indian Patent Act. 2 marks
Q4. A) i) Introduction to Intellectual Property 3 marks
ii) Indian Patent Act. 2marks
OR
A) iii) Pharmaceutical Chemistry: History and Introduction. 3 marks
iv) Different International Agreements 2 marks
B) i) Structure Activity Relationship of representative drugs. 3marks
ii) IUPAC names, Synthesis and uses of representative drugs 2 marks
Q5. A) i) Mechanism of Action of representative drugs 3 marks
ii) Introduction to Intellectual Property 2marks
OR
A) iii) Pharmaceutical Chemistry: History and Introduction. 3 marks
iv) IUPAC names, Synthesis and uses of representative drugs 2 marks
B) i) Structure Activity Relationship of representative drugs. 3marks
ii) Different International Agreements 2 marks

SEMESTER IV
(4 Credits : Theory -03, Practical-01)
----------------------------------------------------------------------------------------------------------------
Time Duration : 2 Hours Total Marks : 60
Q.1) Answer any ten the following: (2 x10 =20 marks)

i) Cosmetic Formulation, principles and preparations.
ii) Cosmetic Formulation, principles and preparations.
iii) Cosmetic Formulation, principles and preparations.
iv) Cosmetic Formulation, principles and preparations.
v) Herbal Cosmetics.
vi) Herbal Cosmetics.
vii) Herbal Cosmetics.
viii) Herbal Cosmetics.
ix) Perfumes and flavors.
x) Perfumes and flavors.
xi) Perfumes and flavors.
xii) Perfumes and flavors.
xiii) Herbal Cosmetics
xiv) Perfumes and Flavors
Q. 2) A) i) Cosmetics formulation, principles and preparations. 3 marks

ii) Cosmetics formulation, principles and preparations. 2 marks
OR
iii) Cosmetics formulation, principles and preparations. 3 marks
iv) Cosmetics formulation, principles and preparations. 2 marks
2 B) i) Herbal cosmetics. 5 marks
Q.3) A) i) Herbal Cosmetics. 3 marks

ii) Herbal Cosmetics. 2 marks
OR

iii) Herbal Cosmetics. 3 marks
iv) Herbal Cosmetics. 2 marks
Q.3) B) i) Perfumes and flavors. 5 marks
Q.4) A) i) Perfumes and flavors. 3marks

ii) Perfumes and flavors 2marks
OR
iii) Perfumes and flavors. 3 marks
iv) Perfumes and flavors. 2 marks
Q. 4) B) i) Cosmetics formulation, principles and preparations. 5 marks
Q. 5) A) i) Cosmetics formulation, principles and preparations. 3 marks

ii) Herbal Cosmetics. 2 marks
OR
iii) Perfumes and flavors. 3 marks
iv) Cosmetics formulation, principles and preparations. 2 marks
Q.5) B) i) Herbal Cosmetics / Perfumes and flavors. 5 marks

SEMESTER III
(4 Credits: Theory -03, Practical-01)
------------------------------------------------------------------------------------------------
Time Duration : 2 Hours Total marks: 60

Q. 1. Answer any ten of the following: (2x10 = 20 marks)
i) Introduction
ii) Chemical energies sources
iii) Electrochemical energy system
iv) Fuel cells
v) Solar energy
vi) Chemical energies sources
vii) Electrochemical energy system
viii) Fuel cells
ix) Solar energy
x) Chemical energies sources
xi) Electrochemical energy system
xii) Fuel cells
xiii) Solar energy
xiv) Introduction
Q2. A) i) Chemical energies sources 3marks

ii) Electrochemical energy system 2 marks
OR
iii) Chemical energies sources 3 marks
iv) Electrochemical energy system 2 marks
Q2. B) i) Solar Energy 3 marks

ii) Fuel Cells 2 marks
Q3. A) i) Chemical energies sources 3 marks

ii)Solar Energy 2 marks
OR

iv)Solar Energy 2 marks
Q3. B) i) Electrochemical energy system 3 marks
ii) Introduction 2 marks
Q4. A) i) Electrochemical energy system 3 marks

ii)Solar Energy 2 marks
OR
iii) Electrochemical energy system 3 marks
iv)Solar Energy 2 marks
Q4 B) i) Chemical energies sources 3 marks

Q5. A)i) Chemical energies sources 3 marks

OR
iv) Fuel Cells 2 marks
Q5. B) i) Electrochemical energy system 3 marks

ii) Solar Energy 2 marks

ANNEXURE III
Laboratory Exercises, Marks distribution and

duration of time for Practical Examinations
ANNEXURE- IIIa : For Semester III and Semester IV Core Course (CC)-LAB
of B.Sc. with Chemistry Programme. ........1 paper per Semester
……….2 credits
ANNEXURE- IIIb: For Semester III and Semester IV Skill Enhancement Course
(SEC) - LAB of B.Sc. with Chemistry Programme............... 1 paper per Semester
......1 credit

ANNEXURE -IIIa
SEMESTER III
CORE COURSE: CHC103
Time duration: 6 Hours ( 02 Credits) Total Marks: 50
Section A: Physical Chemistry

Time duration: 3 Hours( 01 Credit) Marks : 25
Experiment: (Any one experiment may be given)………………………….15 marks
Marks allotted to the experiment
(Systematic work-2 marks, Observation- 6 marks, Calculation and graphs- 7 marks)
Journal: ……………………………………………………….. 5 marks
Oral :………………………………………………………… 5 marks
Section B: Organic Chemistry

Time duration: 3 Hours (01 Credit) Marks: 25
Experiment: Organic spotting to be given for the examination. ………………..15 marks
(Preliminary tests- 2 marks, chemical type – 2 marks, detection of elements- 2 marks,
functional group tests- 2marks, m.p./b.p- 2 marks, Systematic work-3 marks, result-2 marks)
Journal:……………………………………………………………………………5 marks
Oral:……………………………………………………………………………… 5 marks
---------------------------------------------------------------------------------------------------------------
NOTE: For Journal marks Examiner(s) shall take into account the regularity of the candidate
in attending the Laboratory course, completeness of the exercises, presentation and style of
writing the journal.
For Oral examination, Examiner(s) shall assess the knowledge of the candidate in the course
as well as the experiment(s) performed by the candidate.

SEMESTER IV
CORE COURSE: CHC104
Time Duration: 6 Hours (02 Credits) Total Marks :50
Section A: Physical Chemistry
Time duration: 3 Hours (01 Credit) Marks : 25
Experiment (Any one experiment may be given)……………………………15marks
Marks allotted to the experiment
(Systematic work-2 marks, Observation: 6 marks, Calculation and graphs: 7 marks)
Journal:……………………………………………………………………… 5 marks
Oral:………………………………………………………………………… 5 marks
Section B : Inorganic Chemistry

Time Duration: 3 Hours (01 Credit) Marks: 25
Any one experiment from the following to be given

Semi-Micro Analysis: One Salt containing one cation and one anion .......................15 marks
Probable Radicals : 3 Marks

Anion : 4 Marks
Cation : 5 Marks
Systematic work : 3 marks
OR
Volumetric Analysis ................................................................................................. 15 marks
Result : 10 marks
Systematic work : 3 marks
Calculations : 2 marks
Oral : .............................................................................................................5 marks
Journal : .............................................................................................................5marks
NOTE : For Journal marks, Examiner(s) shall take into account the regularity of the
candidate in attending the Laboratory course, completeness of the exercises, presentation and
style of writing the journal.
as well as the experiment(s) performed by the candidate

ANNEXURE - IIIb
SEMESTER III
COURSE: CHS101
--------------------------------------------------------------------------------------------
Time Duration: 3 Hours ( 01 Credit) Total Marks :25
Experiment (Any one experiment may be given)………………………15 marks

Break up : Preliminary test/ arrangements 02 marks
Experimental reading 08 marks
Systematic presentation 02 marks
Results 03 marks
Oral : ………………………………………………..5 marks
Journal :……………………………………………..5 marks
-----------------------------------------------------------------------------------------------------------

SEMESTER III
COURSE: CHS106
Time Duration:3 Hours( 01 Credit) Total Marks: 25

Experiment: One experiment on Preparation or Assay of drug ……………….. 10 marks
For preparation (Systematic work 2marks , product quality 3marks , % yield-3 marks, m.p -2marks)
For Assay (Systematic work 2marks, readings 3marks , Calculation-3 marks, result -2marks)
Patent filing application exercise: …………………………………………………..5 marks
Journal :………………………………………………………………………………. 5 marks
Oral:………………………………………………………………………………… 5 marks
----------------------------------------------------------------------------------------------------------------

SEMESTER IV
COURSE : CHS102
Time Duration: 3 Hours (01 Credit) Marks : 25

1) Experiment No 1: Any one experiment from Preparations/Extraction can be given
for examination. ……………………………………….15 marks
2) Preparations : (Product-5 marks, Systematic work-2 marks, Quality-3 marks,

Calculations-3 marks, Results-2 marks)
2) Extraction : (Product-5 marks, Systematic work-2 marks, Quality-3 marks,
Boiling points-3 marks, Results-2 marks)
3) Journal: …………………………………………………………… 5 marks
4) Oral : ……………………………………………………………. 5 marks
----------------------------------------------------------------------------------------------------------------

SEMESTER IV
COURSE : CHS107
--------------------------------------------------------------------------------------------------------------------------------------
Time Duration : 3 Hours( 01 Credit) Total marks: 25
Any one experiment could be performed
Experiment :…………………………………………………………….. 15 marks
Experimental Work: 8 marks, observation= 3 marks, calculations = 4 marks
Journal :………………………………………………………………. 5 marks
Oral :………………………………………………………………. 5 marks
----------------------------------------------------------------------------------------------------------------

ANNEXURE IV
ANNEXURE-IVa: Syllabus for Semester I Generic Elective (GE) of

Chemistry............ ………………………………………………………….(1 Course)
CHG103
ANNEXURE-IVb: Syllabus for Semester II Generic Elective (GE) of

Chemistry........................................................................................................ (1 Course)
CHG104

ANNEXURE-IVa
SEMESTER I
GENERIC ELECTIVE:CHG103
(Credits: 04)
BASIC CHEMISTRY AND INDIAN SCIENTISTS
------------------------------------------------------------------------------------------------
Theory: (04 Credits) 60 Hours
1. Importance of science in life. (4 Hours)
Towards scientific approach, involvement of science in daily life, Different branches
of science : significance and applications.
( Viz: chemistry, physics, biology, microbiology, medical science etc.)
2. Indian Scientists : Who have made great contributions to science and cemented the
way for others to walk on. (9 Hours)
1) Anandibai Joshi – Physician (1865 - 1887).

2) Janaki Ammal – Botanist (1897 - 1984).
3) Kamala Sohonie – Bio-chemist (1912 – 1998).
4) Anna Mani – Physicist and meteorologist (1918- 2001).
5) Asmita Chatterjee – Chemist and Author (1917 – 2006).
6) Rajeshwari Chatterjee – Scientist and Academic (1922-2010).
7) Darshan Ranganathan – Org. Chemist (1941 – 2001).
8) Prof. C. V. Raman – Physcist and Nobel laureate (1888-1970).
9) Dr. Jagdish Chandra Bose – Physicist (1858-1937).
10) Dr. A.P. J. Abdul Kalam – Missile Man of India (1931-2015)
3. Basic Organic Chemistry. (9 Hours)
Different branches of chemistry, introduction to organic chemistry, classification of Organic

compounds and example of each. Importance of organic chemistry in day to day life;
toothpastes, soaps, shampoos, cosmetics, drugs, dyes and paints.

4. Hydrogen and Water: (8 Hours)
Hydrogen: chemistry of hydrogen, the hydrogen economy.
Water: water cycle, domestic and industrial water supplies. Water as a solvent, chemical
and physical test of water. Hard and Soft water.
5. Oxygen and Sulphur: (8 Hours)

Air as a resource, properties of oxygen, fire triangle, combustion and respiration.
Sources of sulphur: Volcanic regions, oil, gas and minerals. Allotropes of sulphur,
oxides of sulphur, use of sulphuric acid.
6. Carbon and Nitrogen: (10 Hours)

Carbon in air, carbon cycle, removal of carbon dioxide, production of carbon dioxide,
oxides of carbon, carbon monoxide, applications of carbon.
Nitrogen cycle, properties of nitrogen, manufacture of ammonia and nitric acid,
Uses of ammonia.
7. Halogens and Noble gases: (6 Hours)

Halogens: Similarities and applications.
Noble gases; Properties and Uses.
8. Chemistry & Industry : (6 Hours)

Minerals and ores: General Awareness
Chemical plants: Cost, Environmental impact and recycling.
References:
1) Chemistry by Richard Harwood ,Cambridge University press.published 1998
2) First lady doctor of India. The Telegraph . Retrieved 2016-05-01.
3) Lilavati’s Daughter’s by Indian Academy of Sciences (Bangalore) 2008.
4) Organic Chemistry. Morrison , Boyd, Bhattacharjee . Seventh Edition. Pearson.
5) Wings of fire: An Autobiography by A. P. J. Abdul Kalam. Orient blackswan.
6) Jagdish Chandra Bose by Sanjay Goyal.
7) Prof. C. V. Raman: A biography by Uma Parameswaran. Ed.2011, Penguin.

ANNEXURE - IVb
SEMESTER II
GENERIC ELECTIVE: CHG104
(Credits: 04)
CHEMISTRY IN DAILY LIFE
-----------------------------------------------------------------------------------------------
Theory: (04 Credits) 60 Hours
1. Different techniques in Chemistry (5 Hours)
Introduction: Discoveries of different techniques and their applications, viz. purification
techniques: distillation, recrystallization, chromatography. X-ray and radioactivity.
2. Organic Chemistry in medical sciences. (6 Hours)

Introduction to Pharmaceutical chemistry, Classification of Drugs, names and uses of the
following drugs with one example each: Antibiotics, Analgesics, Antihistamines,
Anticonvulsant, Hypnotics and Sedatives.
3. Medicinal plants. (5 Hours)

Introduction: Importance of plant kingdom in general and medicinal plants in particular. Viz.
Tulsi, Aloevera, Turmeric, Vinca rosea, Cinchona, Datura etc.
Compounds obtained from them, their uses and applications.
4. Cellulose and starch. (4 Hours)

Cellulose: General properties.
Various compounds obtained from Starch: General properties. Isolation method.
Different types and uses.
5. Acids, Bases, Salts (10 Hours)

Introduction- acids, alkalies and salts, litmus, pH scale, Ionic nature of acids and alkalies,
importance of water, the chemical reaction of acids and bases- acid reactions in everyday
life, alkalies and bases, characteristic reactions of acids, Salts and their preparations: The
importance of salts, their solubility, water of crystallisation, preparation of soluble salts.
6. Corrosion: (5 Hours)
Definition, types, reactions, EMF series, method for prevention of metal corrosion,
environmental modifications, metal selection and surface conditions, Cathodic protection.
Corrosion Inhibitors, Coating and Plating. Applications.
7. Nanomaterials: (5 Hours)
Overview of nanostructures, nanomaterials and nanotechnology.
Classification: 1, 2, and 3 dimensional nanomaterials, nanomaterials in nature,
examples: Nanotubes, fullerenes, nanowires, applications of nanostrucutres,
8. Macro and micro nutrients in Health Sciences: (10 Hours)
Macronutrients: Carbohydrates, Fats and Proteins w.r.t. Classification, Functions,

Health and Diseases, Food Sources, Deficiencies and Excess.
Micronutrients
Vitamins : Introduction and Classification with respect to Fat soluble Vitamins :Vitamin A,
Vitamin D, Vitamin E, Vitamin K.
Water soluble Vitamins : Thiamine, Riboflavin, Niacin, Pantothenic acid, Vitamin B6,
Biotin, Folate, Cyanocobalamin, Ascorbic Acid.
9. Environmental Pollution (10 Hours)

Air Pollution: Definition of pollutant, pollution. Different sectors of atmosphere, Green house
effect, Green House effect, Global warming, ozone layer depletion.
Different types of pollutant. Photochemical smog. Effect of CO on human system.
Control Measures.
Water Pollution Sources, Effects, different types of water pollutants,
Entry into the food chain. Harmful effects, Control measures.
References:
1. Chemistry, Richard Harwood, Cambridge University Press, 1st ed., (Topic 1)
2. College Inorganic Chemistry for T.Y. B. Sc. Laxmi Devi, Patel, Dhume, Turakia, Dixit,
18th revised edition, Himalaya Publishing House.(Topic 2)
3. Food Science, Nutrition and Safety, Sukhneet Suri and Anita Malhotra, Pearsons.
4. B. K. Sharma. Instrumental Methods of Chemical Analysis: Goel Publishing House,
Meerut
5. B. S. Baliga and A. Zaveri, College Analytical Chemistry, 15th edition,Himalaya
Publishing House, 2004.
6. Goth’s medical pharmacology, by W. G. Clark, D. C Brater, A. R. Johnson . Galgotia
Publications.
7. Medicinal Chemistry by A. Kar. Wiley Eastern Limited , New Delhi.
8. Sharma O. P. Economic botany. Tata McGraw Hill publishing Com.Ltd.
9. Sambamurthy A.V.S.S & Subramanyam N.S. 1989. A text book of Economic Botany.
Wiley Eastern Limited, New Delhi.
10. An Introduction to Medical Botany & pharma cognosy by N. C. Kumar. Emkay
publications , Delhi.
11. Study Material for Vocational Subject by Dr. B. G. Mhatre, Dr .V. S. Narkar, and Prof. R.
K. Pathak.
12. Pharmaceutical Chemistry Organic Volume II, by G. R. Chatwal, Himalaya Publishing
House.

ANNEXURE V
Pattern of Question papers
for
Semester End Examination (SEE)
and
Scheme of marking
ANNEXURE- Va : Paper Pattern for Semester I Generic Elective (GE)
SEE Question paper of B.Sc. With Chemistry programme
Semester I CHG103 ………………………………………. for 4 credits
ANNEXURE – Vb : Paper Pattern for Semester II Generic Elective (GE)
SEE Question paper of B.Sc. With Chemistry programme
Semester II CHG104 ………………………………………. for 4 credits

ANNEXURE - Va
SEMESTER I
BASIC CHEMISTRY AND INDIAN SCIENTISTS
(4 Credits: Theory 04)
---------------------------------------------------------------------------------------
Time Duration : 2 Hours Marks: 80
Q.1) Answer any ten of the following: (2 x10 =20 marks)
i) Importance of Science in life.
ii) Indian Scientists.
iii) Indian Scientists.
iv) Basic Organic Chemistry.
v)Basic Organic Chemistry.
iv) Hydrogen and Water
vii) Oxygen and Sulphur
viii)Oxygen and Sulphur
ix) Carbon and Nitrogen
x) Carbon and Nitrogen
xi) Halogens and Nobel Gases.
xii) Chemistry and Industry.
xiii) Indian Scientists
xiv) Hydrogen and Water
Q. 2) A) i) Indian Scientists. 4 marks

ii) Importance of Science in life. 3 marks
OR
iii) Indian Scientists. 4 marks
iv) Importance of Science in life. 3 marks
2 B) i)Basic Organic Chemistry 4 marks

ii)Basic Organic Chemistry 4 marks
Q.3) A) i) Hydrogen and Water 4 marks

ii) Basic Organic Chemistry 3 marks
OR
iii) Basic Organic Chemistry 4 marks
iv) Oxygen and Sulphur 3 marks
Q.3) B)i) Oxygen and Sulphur 4 marks
ii) Oxygen and Sulphur 4 marks
Q.4) A) i) Carbon and Nitrogen 4 marks

ii) Hydrogen and water 3 marks
OR
iii) Carbon and Nitrogen 4 marks
iv) Indian scientists 3 marks
Q. 4) B)i) Carbon and Nitrogen 4 marks
ii) Carbon and Nitrogen 4 marks
Q. 5) A) i) Hydrogen and water 4 marks

ii) Halogens and Nobel Gases 3 marks
OR
iii) Halogens and Nobel Gases 4 marks
iv) Chemistry and Industry 3 marks
Q.5) B) i)Halogens and Nobel Gases / Chemistry and Industry 4 marks
ii) Halogens and Nobel Gases / Chemistry and Industry 4 marks

ANNEXURE - Vb
SEMESTER II
CHEMISTRY IN DAILY LIFE
(4 Credits: Theory 04)
Time Duration: 2 Hours Marks : 80

Q.1 Answer any ten of the following: (2x10=20 Marks)
i) Different techniques in chemistry.
ii) Organic chemistry in medical sciences.
iii) Medicinal Plants
iv) Cellulose and Starch
v) Acids,bases,salts.
vi) Acids,bases and salts
vii) Corrosion
viii) Nanomaterials
ix) Macro and Micro nutrients in health sciences
x) Macro and Micro nutrients in health sciences
xi) Environmental Pollution
xii)Environmental Pollution
xiii) Organic Chemistry in medical sciences
xiv) Acids, Bases, Salts/Macro and micro nutrients in health sciences.
Q2. A) i) ) Different techniques in chemistry 4 marks

ii)Organic Chemistry in medical sciences 3 marks
OR
iii)Medicinal Plants 4 marks
iv)Different techniques in Chemistry 3 marks

B) i) Cellulose and starch 4 marks
ii) Acids, bases and salts 4 marks
Q3. A) i) Acids, bases and salts 4 marks

ii) Organic Chemistry in medical sciences 3 marks
OR
iii) Acids ,bases and salts 4 marks
iv) Organic Chemistry in medical sciences 3 marks
B) i) Corrosion 4 marks
ii) Nanomaterials 4 marks
Q4. A) i) Environmental Pollution 4 marks

ii) Medicinal Plants 3 marks
OR
iii) Environmental Pollution 4 marks
iv) Cellulose and starch 3 marks
B) i) Environmental Pollution 4 marks
ii) a) Acids, bases and salts 2 marks
b) Macro and micro nutrients in health sciences 2 marks
Q5. A)i) Macro and micro nutrients in health sciences 4 marks
ii) Corrosion 3 marks
OR
iii) Macro and micro nutrients in health sciences 4 marks
iv) Environmental pollution 3 marks
B) i) Macro and micro nutrients in health sciences 4 marks
ii) Nanomaterial 4 marks

ANNEXURE VI
Syllabus for B.Sc. Industrial Chemistry Programme
And
Paper Patterns and Marking Scheme for( SEE ) Examination and Time
Duration and Marking Scheme for Laboratory Courses
ANNEXURE VIa
Semester III Core Course of Industrial
Chemistry………(1 course) CHC153 (4+2) credits
ANNEXURE VIb Semester IV Core Course of Industrial

Chemistry…….(1 course) CHC154 (4+2) credits
ANNEXURE VIc Pattern of Semester III SEE Question paper of B.Sc

Industrial Chemistry CHC153……..for 4 credits
ANNEXURE VId Pattern of Semester IV SEE Question paper of B.Sc

Industrial Chemistry CHC154……..for 4 credits
ANNEXURE VIe Laboratory exercises, marks distribution and duration

of time for practical examination for Semester III of B.Sc. Industrial Chemistry
CHC153 ……for 2 credits
ANNEXURE VIf Laboratory exercises, marks distribution and duration

of time for practical examination for Semester IV of B.Sc. Industrial Chemistry
CHC154 ……for 2 credits

ANNEXURE VIa
B.Sc. WITH INDUSTRIAL CHEMISTRY
CHOICE BASED CREDIT SYSTEM
SEMESTER- III
CORE COURSE CHC153
GENERAL INDUSTRIAL CHEMISTRY
--------------------------------------------------------------------------------------------------------
Theory: 60 Hours(04 Credits)
Section A: Material Science (30 Hours:02 Credits)
I) Mechanical properties of materials and change with respect to temperature.
(3Hours)
II) Polymeric materials: Industrial Polymers – their constitution, chemical and

physical properties. Industrial applications (5 Hours)
III) Metals and alloys – important metals and alloys: iron, copper, nickel, and their
alloys - Mechanical and chemical properties and their application. (8 Hours)
IV) Cement – Composition, Manufacturing processes (Dry and Wet), Types of

cement, setting and hardening of cement. (4 Hours)
V) Ceramics – Introduction , Types ( Conventional) , Manufacturing processes,

Applications, Refractories (5 Hours )
VI) Glass –Manufacture (Tank and Pot Furnaces) , Distinction between Tank And
Pot Furnaces, physical and chemical properties, types of glasses, composition
and applications. (5 Hours)

Section B : Chemical Unit processes (30 Hours: 02 Credits)
VII) Nitration: Introduction – Nitrating agents. Kinetics and mechanism of nitration

Processes such as nitration of (i) Paraffinic Hydrocarbons (ii) Benzene to
nitrobenzene and m- dinitrobenzene (iii) Chlorobenzene to o – and p –
nitrochlorobenzene (iv) Acetanilide to p- nitroacetanilide. (9 Hours)
VIII) Halogenation : Reagents for halogenation. Halogenation of aromatics – side

chain and nuclear halogenations. Commercial manufacture – Chlorobenzenes,
monochloroacetic acid, Chloromethanes and dichlorofluromethane chloral.
(7 Hours)
IX) Sulphonation : Introduction – Sulphonating agents, chemical and physical
factors in sulphonation, Kinetics and mechanism of sulphonation reaction.
Commercial sulphonation of benzene, naphthalene, alkyl benzene, Batch vs
continuous sulphonation. (7 Hours)
X) Hydrolysis - Introduction, hydrolyzing agents, mechanism of ester hydrolysis

(Acid and Alkaline) (2 Hours)
XI) Temperature measuring instruments:

Principle, construction and working of following measuring instruments
Temperature glass thermometers, bimetallic thermometer, vapor filled
thermometer resistance thermometer radiation pyrometers. (5 Hours)

SEMESTER III
GENERAL INDUSTRIAL CHEMISTRY - LAB
CORE COURSE: CHC153
Practicals: 60 Hours (02 Credits)
Instruction: There will be two practicals each of three hours duration from Section A
and Section B respectively for the examination.
SECTION A (30 Hours: 01 Credit)

1. Measurement of dissolved CO2. (3 Hours)
2. Estimation of Aluminum gravimetrically from Bauxite Ore (3Hours)
3. Analysis of Brass (Volumetrically) (4Hours)
4. Estimation of chromium colorimetry or spectrophotometry (4Hours)
5. Estimation of Iron (Volumetrically) (2 experiments) (4Hours)
6. Rate of Corrosion with respect to Al and Fe plates (6Hours)
7. Dissociation constant of acetic acid – conductometry (4Hours)
8. Percentage of available chlorine in bleaching powder. (2Hours)
SECTION B (30 Hours: 01 Credit)

1. Analysis of oils and fats (iodine value, saponification value, acid value).
(4Hours)
2. Nitration - i)Nitration of acetanilide (4Hours)
ii)Nitration of nitrobenzene (4Hours)
3. Halogenation i) Preparation of p-bromoacetanilide (4Hours)

ii) Preparationof 2, 4, 6- tribromophenol (3Hours)
4. Hydrolysis i) Hydrolysis of benzamide (4Hours)
ii) Hydrolysis of ethylbenzoate (4Hours)

5. Preparation of methyl orange. (3Hours)

Note: In addition to the above laboratory exercises, each student as a part of teaching
curriculum, shall be required to visit at least two industrial units, one in each semester
and submit individual report
Reference Books for Theory:

1. Lee, J.D. Concise Inorganic Chemistry ELBS, 1991.
2. Cotton, F.A., Wilkinson, G. & Gaus, P.L. Basic Inorganic Chemistry, 3rd ed., Wiley.
3. UGC course material as prescribed by UGC
4. Finar, I.L. Organic Chemistry (Vol. I & II), E.L.B.S.
5. Morrison, R.T. & Boyd, R.N. Organic Chemistry, Pearson, 2010.
6. Bahl, A. & Bahl, B.S. Advanced Organic Chemistry, S. Chand, 2010.
Reference Books for Practicals

3. S.W. Rajbhoj and T. K. Chondhekar, Systematic Experimental Physical Chemistry , Anjali
Publication ,Second Edition 2000.
4. Sunita Rattan , Experiments in Applied Chemistry, S.K. Kataria & Sons ,Second edition
,2008
5. Khosla, B. D.; Garg, V. C. & Gulati, A. Senior Practical Physical Chemistry, R.
6. UGC practical manual for experimental analysis.
___________________

ANNEXURE - VIb
SEMESTER- IV
CORE COURSE CHC154
---------------------------------------------------------------------------------------------------------------
Theory: (60 Hours :04 Credits)
Section A: Material Science (30 Hours: 02 Credits)

I) Segments of environment
Air, Oxygen, nitrogen cycle, water, Biosphere, Flora and Fauna, Energy, Soil (5Hours)
II) Types of Pollution:

(i) Various pollutants
(ii) Air Pollution – Green House Effect.
(iii) Water pollution – Organic /Inorganic pollutants Sewage analysis
(iv) Pesticide pollution
(v) Radiation pollution,
(vi) Noise pollution (5Hours)
III) Effluent treatment

Waste water treatment methods,
Physical: i) Sedimentation,(Clarification), Filtration etc.
Chemical: i) Disinfection: Chlorination, UV-radiation, Ozonation
ii) Coagulation iii) adsorption iv) Oxidation
Biological: i) Aerobic treatment and its mechanism
ii) Anaerobic treatment and its mechanism (5Hours)
IV) Bag filters, electrostatic precipitators, mist eliminators, wet scrubbers (6Hours)
Absorbers
V) Solid Waste Management (4Hours)
VI) Industrial safety with respect to Chemical hazards (3Hours)

VI) Pollutants and their statutory limits. Pollution evaluation methods (2Hours)
Section B : Chemical Unit processes and instrumentation (30 Hours: 02 Credits)

VII) Alkylation : Introduction ; types of alkylation , Alkylating agents, Thermodynamics
and mechanism of alkylation reactions. Manufacture of alkyl benzenes (for
detergents), ethyl benzene. (3Hours)
VIII) Esterification: Introduction, Hydrodynamics and Kinetics of esterification

reactions, Esterification by organic acids, by addition of unsaturated compounds,
esterification of carboxyl acid derivatives , commercial manufacture of ethyl
acetate, cellulose acetate. (3Hours)
IX) Amination:
a. By reduction: Introduction, Methods of reduction – metal and acid catalytic,
electrolytic, metal and alkali sulfites, metal hydrides, sodium metal, concentrated
caustic oxidation, reduction, Commercial manufacture of aniline , m – nitoaniline
b. By aminolysis : Introduction, ammoniating agents, factors affecting aminolysis,
manufacture of monomethylaniline (6 Hours)
X) Hydrogenation : Introduction – Kinetics and thermodynamics of hydrogenation

reactions, catalysts for hydrogenation reactions, Hydrogenation of vegetable oil,
Manufacture of methanol from carbon monoxide and hydrogen, hydrogenation of
acids and esters to alcohol, catalytic reforming. (6Hours)
XI) Oxidation: Introduction – Types of oxidation reactions, oxidizing agents, Liquid

phase oxidation, vapor phase oxidation. Commercial manufacture of benzoic acid,
maleic anhydride, phthalic anhydride, acrolein , acetaldehyde and acetic acid.
(6Hours)
XII) Pressure measuring instruments – Manometers , barometers, bourdon pressure

gauge : bellow type, diaphragm type pressure gauges, Macleod gauges, Pirani
gauges, etc.
Liquids level measuring instrument: direct – indirect liquid level measurement,
Float type liquid level gauge, ultrasonic level gauges; viscosity measurement (6Hours)

SEMESTER- IV
GENERAL INDUSTRIAL CHEMISTRY – LAB
CORE COURSE: CHC154
Practicals: 60 Hours (02 credits)
Instruction: There will be two practicals each of three hours duration from Section A
and Section B respectively for the examination.
SECTION A (30 Hours: 01 Credit)

One experiment each on following in a given water sample. (3×10 =30Hours)
1. Determination of solids content.
2. Determination of Hardness.
3. Determination of acidity.
4. Determination of Alkalinity.
5. Determination of dissolved oxygen
6. Determination of BOD.
7. Determination of COD.
8. Determination of mixture of halide potentiometrically.
9. Estimation of Available Oxygen in Hydrogen Peroxide.
10. Determination of alkali in water samples and soaps.
SECTION B (30 Hours: 01 Credit)

1. Esterification : benzocaine (4Hours)
2. Oxidation; p-nitrobenzoic acid,,benzyl,anthraquinone.(2experiments)
(2×4 = 8Hours)
3. Reduction: p- aminobenzoic acid, m-nitroaniline. (3Hours)
4. Preparation of o – chlorobenzoic acid (3Hours)
5. Preparation of o –benzoyl benzoic acid (4Hours)
6. Estimation of glucose in food samples. (4Hours)
7. Preparation of soap. (4Hours)

Note: In addition to the above laboratory exercises, each student as a part of teaching
curriculum, shall be required to visit at least two industrial units, one in each semester
and submit individual report.
Reference Books for Theory

1. Lee, J.D. Concise Inorganic Chemistry ELBS, 1991.
2. Cotton, F.A., Wilkinson, G. & Gaus, P.L. Basic Inorganic Chemistry, 3rd ed., Wiley.
3. UGC course material as prescribed by UGC
4. Finar, I.L. Organic Chemistry (Vol. I & II), E.L.B.S.
5. Morrison, R.T. & Boyd, R.N. Organic Chemistry, Pearson, 2010.
6. Bahl, A. & Bahl, B.S. Advanced Organic Chemistry, S. Chand, 2010.
Reference Books for Practicals

3. S.W. Rajbhoj and T. K. Chondhekar, Systematic Experimental Physical Chemistry,
Anjali Publication, Second Edition 2000.
4. Sunita Rattan, Experiments in Applied Chemistry, S.K. Kataria & Sons ,Second edition
,2008
5. Khosla, B. D.; Garg, V. C. & Gulati, A. Senior Practical Physical Chemistry, R.
6. UGC practical manual for experimental analysis

ANNEXURE - VIc
SEMESTER- III
CORE COURSE: CHC153
-------------------------------------------------------------------------------------------
Note : All questions are compulsory
Section A: Material Science (40 marks)

Q.1. Answer ANY FIVE from the following ( 2 x 5 = 10 Marks)
i) Mechanical properties
ii) Polymeric materials
iii) Metals and alloys
iv) Cement
v) Ceramics
vi) Glass
vii) Metals and alloys
Q.2 A) i) Mechanical properties 4 Marks

ii) Metal and alloys 3 Marks
OR
Q.2 A) iii) Polymeric materials 4 Marks
iv) Cement 3 Marks
Q.2 B) i) Metals and alloys 4 Marks
ii) Ceramics 4 Marks
Q.3 A) i) Ceramics 4 Marks
ii) Glass 3 Marks
OR

Q.3 A) iii) Glass 4 Marks
iv) Cements 3 Marks
Q.3 B) i) Metals and alloys 4 Marks

ii) Polymeric material 4 Marks
Section B : Chemical Unit processes (40 Marks)

i) Nitration
ii) Halogenation
iii) Sulphonation
iv) Hydrolysis
v) Temperature measuring instruments
vi) Nitration
vii) Halogenation
Q.5. A) i) Nitration 4 Marks

ii) Halogenation 3 Marks
OR
Q.5. A.) iii) Sulphonation 4 Marks
iv) Halogenation. 3 Marks
Q.5.B) i) Sulphonation 4 Marks

ii) Temperature measuring instruments 4 Marks
Q.6.A) i) Nitration 4 Marks

ii) Hydrolysis 3 Marks
OR
Q6. A)i) Halogenation 4 Marks
ii) Sulphonation 3 Marks
Q.6.B. i) Nitration 4 Marks
ii) Temperature measuring instruments 4 Marks

ANNEXURE - VId
SEMESTER- IV
CORE COURSE: CHC154

--------------------------------------------------------------------------------------------
Section A: Material Science (40 marks)
i) Segments of environment
ii) Types of pollution
iii) Effluent analysis
iv) Bag filters
v) Solid waste management
vi) Industrial safety
vii) Pollutants and statutory limits
Q.2.A.i) Segments of environment 4 marks

ii) Types of pollution 3 Marks
OR
Q.2.A.iii) Segments of environment 4 Marks
iv) Pollutants and statutory limits 3 marks
Q. 2.B. i) Bag filters 4 Marks
ii) Industrial safety 4 Marks
Q. 3.A. i) Effluent analysis 4 marks

ii) Solid waste management 3 marks

OR
Q. 3.A. iii) Bag filters 4 Marks
iv) Solid waste management 3 marks
Q. 3.B. i) Types of pollution 4 Marks
ii) Effluent analysis 4 marks
Section B : Chemical Unit processes and instrumentation (40 Marks)

i) Alkylation
ii) Esterification
iii) Amination
iv) Hydrogenation
v) Oxidation
vi) Pressure measuring instruments
vii) Amination
Q.5. A i) Alkylation 4 Marks

ii) Hydrogenation 3 Marks
OR
Q.5. A iii) Pressure measuring instruments 4 Marks
iv) Hydrogenation 3 Marks
Q.5. B i) Oxidation 4 Marks
ii) Esterification 4 Marks
Q.6. A. ii) Amination 4 Marks

iii) Oxidation 3 Marks
OR
Q.6.A. iii) Hydrogenation 4 Marks
iv) Oxidation 3 Marks
Q.6. A. i) Amination 4 Marks
ii) Pressure measuring instruments 4 Marks

ANNEXURE VIe
SEMESTER III
CORE COURSE: CHC153
GENERAL INDUSTRIAL CHEMISTRY-LAB
Time Duration:6 Hours Total Marks:50
SECTION A ( 3 Hours)
Each Practical of three hours duration. (25 marks)
Experiment:…………………………………………………… 15 marks
Results 03 marks
Oral (Viva) …………………………………………..05 marks
Journal………………………………………………..05 marks
SECTION B ( 3 Hours)
Experiment:………………………………………………… 15 marks
Results 03 marks
Oral (Viva) ……………………………………………..03 marks
Journal ………………………………………………...02 marks
On- Job –Training……………………………………..05 marks

ANNEXURE - VIf
SEMESTER IV
CORE COURSE: CHC154
GENERAL INDUSTRIAL CHEMISTRY- LAB
------------------------------------------------------------------------------------------------
(Marking Scheme)
SECTION A (03 Hours)
Experiment:…………………………………………………. 15 marks
Results 03 marks
Oral (Viva)……………………………………………… 05 marks
Journal………………………………………………………... 05 marks
SECTION B (3 Hours)
Experiment:……………………………………………………..… 15 marks
Results 03 marks
Oral (Viva)……………………………………………… 03 marks
Journal ……………………………………………….. 02 marks
On- Job –Training……………………………………. 05 marks
ANNEXURE VII
Course Codes of Chemistry - UG
Course codes in the subject of CHEMISTRY under CBCS as per OC-66 for
Bachelor of Science Programme & Bachelor of Science (Honours) Programme
Class & Semester Initial code New code as per OC-66 Credits
FYBSc SEM I DSC 2A CHC101 6 Credits
GE 1 CHG 101/CHG103 4 Credits
FYBSc SEM II DSC 2B CHC102 6 Credits
GE 2 CHG 102/CHG104 4 Credits
SYBSc SEM III DSC 2C CHC103 6 Credits
SEC 1 CHS 101/CHS106 4 Credits
SYBSc SEM IV DSC 2D CHC104 6 Credits
SEC 2 CHS 102/CHS107 4 Credits
TYBSc ( Semester V & VI) for Bachelor of Science ( Honours programme)
DSC 5 CHC105 6 Credits

PHYSICAL CHEMISTRY
INORGANIC CHEMISTRY
TYBSc ORGANIC CHEMISTRY
SEM V DSE 1 CHD101 4 Credits
DSE 2 CHD102/CHD 105 4 Credits

PHYSICAL CHEMISTRY
TYBSc INORGANIC CHEMISTRY
SEM VI DSC 10 CHC110 6 Credits
ORGANIC CHEMISTRY
DSE 3 CHD103/CHD106 4 Credits
DSE 4 (DSP) CHP 101 4 Credits
TYBSc ( Semester V & VI) for Bachelor of Science programme
SEC 3 CHS103 4 credits

TYBSc SEM V SEC 4 CHS104 4 credits
DSE 2A CHD101 4 credits
TYBSc SEM VI SEC 5 CHS105 4 credits
DSE 2B(DSP) CHP101 or CHD 104/CHD107 4 credits
CHG103 New Alternative GE 1 for Semester I

CHG104 New Alternative GE 2 for Semester II

CHD101 Same paper for Semester V of the two programmes i.e. DSE 1 & DSE 2A
CHD105 Alternative for CHD 102
COURSE CODES FOR B.Sc WITH INDUSTRIAL CHEMISTRY
SEM I CHC151( Industrial Chemistry)

SEM II CHC152( Industrial Chemistry)
SEM III CHC153( Industrial Chemistry)
SEM IV CHC154( Industrial Chemistry)
------------------------------------------------------------------------------------------------------------

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CHOICE BASED

Goa University, Taleigao Plateau, Goa. Page 1

ANNEXURE-II: Paper Patterns for all papers

ANNEXURE-III: Marking Scheme, and Time

ANNEXURE-IV: Syllabus for two new Generic

ANNEXURE-V: Paper Patterns for the new

ANNEXURE-VI: Syllabus, Paper Patterns and

ANNEXURE-VII: New Course Codes as per

Goa University, Taleigao Plateau, Goa. Page 2

B.Sc. with Chemistry

ANNEXURE-Ia :Syllabus for Semester III Core Course (CC) of Chemistry

ANNEXURE-Ib: Syllabus for Semester III Skill Enhancement Course (SEC) of

ANNEXURE-Ic : Syllabus for Semester IV Core Course (CC) of Chemistry

ANNEXURE-Id: Syllabus for Semester IV Skill Enhancement Course (SEC) of

CHS 102 /CHS 107

Goa University, Taleigao Plateau, Goa. Page 3

Syllabus of B.Sc. CHEMISTRY

Section A: Physical Chemistry-2 (30 Hours; 02 credits)

2. Phase Equilibrium (8 Hours)

Goa University, Taleigao Plateau, Goa. Page 4

Section B: Organic Chemistry-3 (30 Hours; 02 Credits)

1. Carboxylic acids and their derivatives (6 Hours)

2. Amines and Diazonium Salts (6 Hours)

3. Amino Acids and Peptides (6 Hours)

Goa University, Taleigao Plateau, Goa. Page 5

4. UV –Visible Spectroscopy in Organic Chemistry (8 Hours)

Goa University, Taleigao Plateau, Goa. Page 6

Goa University, Taleigao Plateau, Goa. Page 7

Section A: Physical Chemistry-2 (30 Hours: 01 credit)

Phase Equilibria 12 Hours

1. Systematic experimental physical Chemistry by S.W. Rajbhoj, Dr. T. K. Chondhekar,

Goa University, Taleigao Plateau, Goa. Page 8

Section B: Organic Chemistry - 3 (30 Hours: 1 Credit)

I) Systematic Qualitative Organic Analysis : (6x2 =12 Hours)

II) Organic Preparations : (14 Hours)

III) Organic Estimations: (Any 2) (4 Hours)

Goa University, Taleigao Plateau, Goa. Page 9

SKILL ENHANCEMENT COURSE (SEC)

(4 Credits: Theory -03, Practical-01)

SKILL ENHANCEMENT COURSE: CHS101

NATURAL RESOURCES AND ANALYSIS

Theory: 45 Hours (03 Credits)

I. Review of energy sources (renewable and non-renewable). Classification of fuels and

III. Petroleum and Petrochemical Industry: Composition of crude petroleum, Refining

V. Analysis of soil: Composition of soil, Concept of pH and pH measurement,

Goa University, Taleigao Plateau, Goa. Page 10

SKILL ENHANCEMENT COURSE: CHS101

NATURAL RESOURCES AND ANALYSIS

Instruction: Practicals/ demonstrations

1. Determination of pH of soil samples. 3 Hours

2. Determination of pH of a water samples 3 Hours

3. Estimation of Calcium and Magnesium ions as calcium carbonate by complexometric

5. Determination of acidity of a water sample 4 Hours

6. Determination of alkalinity in a given water sample 4 Hours

7. Measurement of dissolved CO2. 4 Hours

8. Percentage of available chlorine in bleaching powder. 2 Hours

Reference Books for Theory and Practicals:

1. Svehla, G. Vogel’s Qualitative Inorganic Analysis, Pearson Education, 2012.

Goa University, Taleigao Plateau, Goa. Page 11