Heat Treatment

DATASHEET FOR NON-HEAT-TREATERS
THE CONTRACT HEAT TREATMENT ASSOCIATION
STRESS RELIEVING, NORMALISING AND ANNEALING

WHAT ARE THE TREATMENTS? Stress Relieving Stress relieving is applied to both ferrous and non-ferrous alloys and is intended to remove internal residual stresses generated by prior manufacturing processes such as machining, cold rolling and welding. Without it, subsequent processing may give rise to unacceptable distortion and/or the material can suffer from service problems such as stress corrosion cracking. The treatment is not intended to produce significant changes in material structures or mechanical properties, and is therefore normally restricted to relatively low temperatures. Air-hardening steels (e.g. some automotive gear steels) are often tempered (subcritically annealed) after normalising to soften the structure and/or promote machinability. Many aircraft specifications also call for this combination of treatments. Steels that are not usually normalised are those which would harden significantly during air cooling (e.g. many tool steels), or those which gain no structural benefit or produce inappropriate structures or mechanical properties (e.g. the stainless steels). Annealing The primary purpose of an annealing treatment is to reduce the hardness of a material and facilitate the progress of subsequent manufacturing operations. Annealing is commonly used after casting, forging or rolling to soften materials and minimise residual stresses, improve machinability, and increase ductility by carefully controlling the microstructure. Many steels in strip form are annealed, as are most tool steels and stainless steels. Non-ferrous alloys are also annealed. There are several process variations that qualify as annealing treatments: Full annealing is performed on steels by heating to a high temperature (typically 830-950C), then cooling slowly to ambient temperature. Non-ferrous materials are softened and refined by full annealing at temperatures appropriate for each alloy. Isothermal / cyclic annealing is performed by heating steels to the full annealing temperature, cooling to an intermediate temperature (typically 550-700C) and soaking for a long period to allow transformation to proceed slowly, followed by cooling to ambient temperature. Intercritical annealing is applied by heating steels to below the full annealing temperature (typically 723910C) according to composition. A prolonged soak is followed by cooling to ambient temperature. Subcritical annealing takes place at a temperature for steels of typically 650-720C, allowing a prolonged soak before cooling to ambient temperature. Homogenisation annealing can be applied to both ferrous and non-ferrous materials and is a prolonged high-temperature soak intended to break down segregation in the materials structure. Solution annealing is applied commonly to austenitic stainless steels, typically at 1010-1150C. With unstabilised grades, the treatment must be followed by fast cooling or quenching. It is applied as a softening process during manufacture or to optimise corrosion resistance (e.g. after welding).
Carbon steels and alloy steels can be given two forms of stress relief: (1) Treatment at typically 150-200C relieves peak stresses after hardening without significantly reducing hardness (e.g. case-hardened components, bearings, etc.): (2) Treatment at typically 600-680C (e.g. after welding, machining etc.) provides virtually complete stress relief. Non-ferrous alloys are stress relieved at a wide variety of temperatures related to alloy type and condition. Alloys that have been age-hardened are restricted to stress relieving temperatures below the ageing temperature. Austenitic stainless steels are stress relieved below 480C or above 900C, temperatures in between reducing corrosion resistance in grades that are not stabilised or low-carbon. Treatments above 900C are often full solution anneals.
Normalising Applied to some, but not all, engineering steels, normalising can soften, harden or stress relieve a material, depending on its initial state. The objective of the treatment is to counter the effects of prior processes, such as casting, forging or rolling, by refining the existing non-uniform structure into one which enhances machinability/formability or, in certain product forms, meets final mechanical property requirements. A primary purpose is to condition a steel so that, after subsequent shaping, a component responds satisfactorily to a hardening operation (e.g. aiding dimensional stability). Normalising consists of heating a suitable steel to a temperature typically in the range 830-950C (at or above the hardening temperature of hardening steels, or above the carburising temperature for carburising steels) and then cooling in air. Heating is usually carried out in air, so subsequent machining or surface finishing is required to remove scale or decarburised layers.
This datasheet is compiled in good faith solely to assist others to evaluate the heat treatment techniques described. Users do so entirely at their own risk. Neither CHTA nor the presenter is responsible for any consequences from any such use. Datasheets shall not be used for contractual purposes neither directly nor by implication.
c Contract Heat Treatment Association 1996
WHAT ARE THE BENEFITS? Stress relieving, normalising and annealing all prepare metals and alloys for further processing or for the intended service conditions. They control the ability of materials to be machined with ease, perform without distortion in service, be formed without cracking or splitting, be subsequently hardened or carburised with minimal distortion, or to resist corrosive environments. WHAT SORT OF MATERIALS CAN BE TREATED? All commercial alloys can be annealed and stress relieved. Normalising is restricted to certain steels for the reasons indicated above. WHAT ARE THE LIMITATIONS? Stress relieving of carbon or low-alloy steel fabrications is frequently the last heat treatment applied, so it must be ensured that the mechanical properties of the materials treated will not be adversely affected. Stress relieving between machining operations can be performed on pre-treated material. The stress relieving effectiveness may have to be reduced to prevent loss of mechanical properties. Many austenitic stainless steels require fast cooling after high-temperature stress relief or solution annealing. A degree of distortion or reintroduction of residual stresses is inevitable in such cases. The size and shape of items that can be stress relieved, annealed or normalised depends on the type of equipment operated by the heat treater. For large items, check the availability of suitably-sized facilities at an early stage. WHAT PROBLEMS COULD ARISE? Most stress relieving operations are carried out in air, but protective media are also available. In air, alloys are subject to discolouration or scaling depending on the alloy and temperature used. Post-treatment cleaning may therefore be required. Normalising is usually performed in air on semifinished steel products where scaling and decarburisation pose no problems because they are removed by subsequent machining. A protective medium may sometimes be necessary; e.g. when normalising final-size products prior to localised surface hardening. Annealing processes can take place in air or in protective media such as molten salt, controlled gaseous atmospheres or vacuum. Prolonged soaks, as required by some annealing operations, necessitate
the selection of a protective medium. There is always a risk of distortion/sagging when high-temperature treatments are applied to vulnerable thin-wall vessels or large, heavy components. Your heat treater may have to use special supports or fixtures to combat this problem. HOW DO I SPECIFY? All of the following information should be included if possible. If uncertain, ask your heat treater before producing a specification: The process required: this could be stress relieve, normalise or anneal; indicate if bright treatment is necessary, or if treatment in air is satisfactory. Material type, grade, and the standard from which it is drawn, with drawing, composition and mill certificate where available. Any general standards applicable (national, international or company) that contain relevant details which must be adhered to. Existing condition; e.g. details of any prior heat treatment, such as hardening and tempering, solution treatment and ageing, intended to establish mechanical or other properties. The level of mechanical properties required. Generally a hardness range or tensile strength range can be quoted from the standard being worked to. It is not possible to meet a specific figure due to the variables outside the heat treaters control (e.g. in annealing to remove the effects of severe cold work). A maximum hardness level is often requested for normalised or annealed materials. Standards such as BS 10083-1 and BS 970 provide information for some steels. The type(s) of testing required; e.g. hardness (Vickers, Brinell), tensile etc. and any special locations for testing or the removal of samples for test pieces. Requirements for any special certificates or data to be provided by your heat treater. Other services required; e.g. straightening (with working limits), cleaning/blasting, laboratory or specialised NDT services etc. WHERE DO I GO? In order to locate heat treaters offering stress relieving, normalising or annealing services, consult the current edition of CHTAs Buyers Guide. It is advisable to involve your heat treater at an early stage.
Published by The Contract Heat Treatment Association Secretariat: c/o WHTC, Aston University, Aston Triangle, Birmingham B4 7ET, UK

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DATASHEET FOR NON-HEAT-TREATERS

THE CONTRACT HEAT TREATMENT ASSOCIATION

STRESS RELIEVING, NORMALISING AND ANNEALING

c Contract Heat Treatment Association 1996

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