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Make up 500 mL of aqueous solution containing 20 g sodium thiosulphate. 2 M hydrochloric acid is
also needed. Bt. Mat Taib for their keen and endless guidance, encouragement, critics and. The tubes
collect any gas given off and the properties of the gas should be tested. Discard any disposable tare
containers or weighing paper in the nearest wastebasket. To test what is in the cooler inner cone hold
a splint of wood in the flame so that it passes through the inner cone. Bundle Chemistry Required
Practicals (without triple) This bundle contains the revision mats for the required practicals that now
involved in the new AQA specification for 2018 (without triple). Different soils have different types
of porosity and permeability. Without a subpoena, voluntary compliance on the part of your Internet
Service Provider, or additional records from a third party, information stored or retrieved for this
purpose alone cannot usually be used to identify you. Water will spray into the flask from the jet. (e)
Carbon dioxide Many reactions can be used to produce carbon dioxide gas. These nails are in
contact with air, water and salt. As you approach the endpoint, you may need to add a partial drop of
titrant. Note whether the blue colour restored and if any heat is given back. The products will be
gaseous, or metals which are deposited on the negative electrode. Note any loss in mass. (c) Effect of
heat on copper sulphate crystals Crush blue copper sulphate crystals and put them into a dry test-
tube to a depth of 4 cm. See also Free Kiswahili Notes, Exams, Schemes of Work, Lesson Plans:
Form 1 to 4 (c) Hydrogen chloride Put rock salt, sodium chloride, into a 100 mL filtering flask. You
can preserve large crystals by painting with a clear varnish. (ii) You can also support the seed crystal
at the end of a glass tube. The smallest should give the carbon dioxide in the shortest time. Read the
temperature, heat to boiling and read the temperature again. 7(a). Solubility in water Test different
salts taken to show that each has a different solubility in water. The solution should be delivered
quickly until a couple of mL from the endpoint. Note any change in the reading if the thermometer
touches the bottom of the test-tube. Put one drop of lemon juice on to the spot then note any change
of colour. Needed by the majority of living organisms for respiration Is produced by green plants as
a by-product of photosynthesis. 8.SULPHUR DIOXIDE GAS Physical Properties Colour Colourless
Odour Pungent odour Density compared to air (heavier or lighter) Heavier than air Chemical
Properties Solubility in water Soluble. Concentrated hydrochloric acid is used in the manufacture of
many chemicals. 2.CARBON DIOXIDE Physical Properties Colour Colourless Odour Odourless
Density compared to air (heavier or lighter) Heavier than air Chemical Properties Solubility in water
Fairly soluble in water. Be careful! Sodium sinks in the kerosene and float in the water. The
coefficient or permeability (k) also known as hydraulic conductivity, is a. This is an approximate
dimension of a single molecule of the oil. IRJET- Soil Water Retention Curve of an Unsaturated
Sand Under Square Footing. This experiment investigates the progress of this reaction. When the
glass tubing cools, drop seed crystals on its end until one catches in the smaller hole. Krishna Reddy,
Engineering Properties of Soils Based on.
Attempt to work out the questions from the first principles and not use the formula method, which
has its own limitations. Then pull the screening wire with the lead further into the stopper so that the
lead electrode is firmly held in the stopper. Tube 4: Half cover 2 nails with water containing a little
common salt dissolved in it. It reacts with water to form a weak acid called carbonic acid. It is
important that when candidates record reading they include the appropriate number of decimal
places. The permeability coefficient can be determined in the laboratory using falling. This is the
stability indicator light, indicating that the weight is stable. To test whether unburned carbon gives
the yellow colour to the flame, sprinkle powdered charcoal into the flame to see if this gives the same
effect. (iii) Open the air hole again. The calorimeters shown here can determine the heat of a solution
reaction at constant (atmospheric) pressure. Show replies stephenkemp193 4 years ago Thank you for
your review, your students do not need to do all the activities that are on the sheets. The specific
catalysts are not usually available in school laboratories. V: discharge velocity, which is the quantity
of water flowing I unit time. Solutions with a pH value of 7 are neither acidic nor basic, they are
neutral. Stir the inflammable liquid gently with the thermometer and read the thermometer when the
inflammable liquid boils. (ii) Use a very small test-tube or seal one end of a piece of glass tubing, 8
cm length and 3 cm external diameter. Put 50 mL of water in the flask and add 2 mL of hydrogen
peroxide solution. An investigation into the resistance of a wire - A GRADE GCSE chemistry gcse
coursework rates reaction concentration Physics Coursework. Copper metal deposits and the blue
colour gradually disappear as the magnesium displaces the copper ion. Read the temperature, heat to
boiling and read the temperature again. 7(a). Solubility in water Test different salts taken to show that
each has a different solubility in water. Repeat the experiment with a smaller concentration of
thiosulphate. The sulphur dioxide produced can be collected in gas jars covered with cardboard discs,
which have central holes for the delivery tube. (e) REDUCTION OF POTASSIUM
PERMANGANATE WITH SULFUR DIOXIDE (i) Add 10 mL of 0.1M solution of potassium
permanganate and 10 mL 3M solution of dilute sulphuric acid to 200 mL of water containing sulphur
dioxide. I will include a sheet explaining the grading more fully in those resources that have grades
included. If the volume of the pipette is larger than the volume of the pipette bulb, you may need to
remove the bulb from the pipette and squeeze it and replace it on the pipette a second time, to fill the
pipette volume completely. IRJET- Soil Water Retention Curve of an Unsaturated Sand Under
Square Footing. Pure hydrogen burns with a quiet “pop” sound. (ii) Alternatively, add sulphuric acid
from a syringe. Bundle ALL Physics Chemistry and Biology Required Practical Revision The
questions are 9-1 graded exam style questions. Bt. Mat Taib for their keen and endless guidance,
encouragement, critics and. You can also fill a burette using a disposable transfer pipette. For
example if temperature readings between 21 0 C and 28 0 C are plotted, there is no need to begin the
axes at zero. First heat the porous pot strongly and then gently warm the cotton wool to produce
ethanol vapour. Test the third test-tube of gas by holding a lighted taper or splint over the mouth as
soon as you take out the stopper.
ENERGY FROM CHEMICAL REACTIONS The following group of reactions involve ions in
aqueous solution. Finally, the paper should be rinsed into the beaker, to remove all traces of the
solid. Hide replies Empty reply does not make any sense for the end user Submit reply Cancel Report
this resource to let us know if it violates our terms and conditions. In this experiment, the data
collected were recorded in the table as. Put 50 mL of water in the flask and add 2 mL of hydrogen
peroxide solution. As you approach the endpoint, you may need to add a partial drop of titrant. Put a
cardboard cover over the top to prevent diffusion of the gas. The colour changes or the identity of
any gases evolved may provide evidence as to the identity of the unknown. Show replies cal-w11 2
years ago Thank you very much. Your TA can show you how to deliver a partial drop of solution,
when near the endpoint. (b) Volumetric (measuring) Flasks Erlenmeyer flasks and beakers are used
for mixing, transporting, and reacting, but not for accurate measurements. Wait until a clear
boundary appears between the two liquids and then run off the denser layer into a beaker below.
11(b). HEATING AND BURNING DIFFERENT SUBSTANCES Substances that gain mass when
heated. Some useful questions but don't think the risk assessments are that relevant. These nails are
in contact with air and water and form the control experiment. Please comment if you find this
useful. ?8.00 Review 3 Select overall rating (no rating) Your rating is required to reflect your
happiness. Madam Hajah Kamilah Bt Salleh, our Chemistry teacher Madam. Noorzaila. The water
levels inside and outside the tube should be the same and the level should be marked on the tube.
Candidates should indicate at what stage a change occurs, writing any deductions alongside the
observations on which they are based. It reacts with water to form a weak acid called carbonic acid.
Put a capillary tube, sealed at one end, into the inflammable liquid with the sealed end up and the
open end down in the inflammable liquid. Something that burns in air will burn five times more
ferociously in pure oxygen gas. The list is not intended to be exhaustive: in particular, items (such as
Bunsen burners, tripods) that are commonly regarded as standard equipment in a chemical laboratory
are not included in this list. Heat a 3 mm bore piece of glass tubing in a flame until the end softens
sufficiently to squeeze with pliers to make a smaller hole. Take 40 mL of thiosulphate solution and
add 10 mL of distilled water. If cork is used, this must be made leak proof by covering the whole of
the bottom surface round the electrodes and the glass edge with Faraday’s wax or a similar soft wax.
Make up 500 mL of aqueous solution containing 20 g sodium thiosulphate. 2 M hydrochloric acid is
also needed. You can preserve large crystals by painting with a clear varnish. (ii) You can also support
the seed crystal at the end of a glass tube. Using a pair of tongs or tweezers, dip a piece of cotton
wool into concentrated hydrochloric acid and another piece into concentrated ammonium hydroxide.
Solutions with a pH value of 7 are neither acidic nor basic, they are neutral. Do check the level
indicator bubble before weighing. Each required practical contains a 2 page questions sheet and
matching answer sheet for students.
GENERAL NOTES FOR QUALITATIVE AND QUANTITIVE ANALYSIS Indicators An
indicator is a substance used in titrations, which has one colour in the presence of an excess of one
reagent and a different colour in the presence of an excess of the other. It covers Working
Scientifically (2.1, 2.2, 2.3, 2.4, 2.6 and 2.7). Marketing Marketing The technical storage or access is
required to create user profiles to send advertising, or to track the user on a website or across several
websites for similar marketing purposes. In this experiment the concentration of sodium thiosulphate
is made variable, whilst the concentration of acid is kept constant. After the solid is completely
dissolved, very carefully fill the flask to the 500 mL mark. Ismail B. Mahad for their sincere help and
cooperation in carrying out our. IDENTIFICATION OF PURE SUBSTANCES Melting points, mp,
of naphthalene (i) Put a very small amount of naphthalene in a capillary tube sealed at one end. The
formula for the crystals is Na 2 S 2 O 3.10H 2 O. On heating, these crystals dissolve in some of their
water of crystallization. Fix steel wool into a loop in the lower end of the Nichrome wire. Adjust the
layer of kerosene to be shallow enough to allow the top of the sodium to protrude above the surface.
Do not use metals in powder form because the reaction may be too vigorous and even cause an
explosion. You can watch the reaction through a hand lens held at the side, but never at the top. The
change in temperature is determined by measuring the initial temperature, T 1, of the reactants, and
the maximum temperature, T 2, of the contents of the calorimeter during the exothermic reaction.
Used in light bulbs and thermometers because it is not reactive. Tiwari, Soil Mechanics Laboratory,
California State University. To do this, put a glass tube into the beaker of water so that it touches the
bottom, then to drop the crystal down the tube. If you have any ideas on how to improve the
grading, please email me (my email is included in the purchase). Use the thermometer to stir the
water but do not let water enter the capillary tube. We wish to express here, our sincere appreciation
and thanks to all. Boil this fat in water and the oil will separate on the surface. Before titrating,
condition the burette with titrant solution and check that the burette is flowing freely. Add some
clear saturated solution and weigh again, w2. It is composed of an open cylinder of glass
approximately 8 cm high and 2.5 cm in diameter. A small bottle of similar size with the bottom cut
off would do just as well. We wish to express here, our sincere appreciation and thanks to all. We
must assume that the specific heat of this moderately weak solution is the same as that of water. (d)
HEAT OF A COPPER DISPLACEMENT REACTION (i) Put 25 mL 0.2 M copper sulphate
solution in a 100 mL polythene fitted with a 1-hole stopper and thermometer. Then add distilled
water a drop at a time until the bottom of the meniscus lines up exactly with the mark on the neck of
the flask. This prevents combustion since carbon dioxide does not support it and the presence of
carbon dioxide stops oxygen reaching the combustible material. 3.CHLORINE GAS Physical
Properties Colour Greenish-yellow Odour Pungent odour Poisonous Density compared to air
(heavier or lighter) Heavier than air Chemical Properties Solubility in water Soluble in water.
Concentrated hydrochloric acid is used in the manufacture of many chemicals. 2.CARBON
DIOXIDE Physical Properties Colour Colourless Odour Odourless Density compared to air (heavier
or lighter) Heavier than air Chemical Properties Solubility in water Fairly soluble in water. This rise of
temperature in not affected by the volume of 0.2 M copper sulphate used for the experiment. For
example using 1cm to represent 3 units might spread the readings better than using 1 cm to represent
4 units but the scale may be difficult to read.
The magnesium ribbon darkens just before it begins to melt. It is then dipped into salt powder and
introduced into a colourless Bunsen burner flame. Take 40 mL of thiosulphate solution and add 10
mL of distilled water. The test should show that the amount of sugar is increasing. Bundle ALL
Physics Chemistry and Biology Required Practical Revision The questions are 9-1 graded exam style
questions. Clean 25 cm of magnesium ribbon and cut into 1 cm pieces. After a minute, check for
solution on the tip to see if your burette is leaking. Ask your TA to demonstrate these techniques for
you, in the lab. Conductivity measurement.pptx Hyd. Conductivity measurement.pptx Consistency
limits and its determination Consistency limits and its determination Atterberg limit test Atterberg
limit test INDEX PROPERTIES OF SOIL INDEX PROPERTIES OF SOIL IRJET- Soil Water
Retention Curve of an Unsaturated Sand Under Square Footing. Read the temperature, heat to
boiling and read the temperature again. 7(a). Solubility in water Test different salts taken to show that
each has a different solubility in water. Note any loss in mass. (c) Effect of heat on copper sulphate
crystals Crush blue copper sulphate crystals and put them into a dry test-tube to a depth of 4 cm.
Pressure affects the boiling point Put water in a sidearm test-tube or in a round-bottom flask with a
2-hole stopper. Heat of fusion and vaporization 10(a) Separate by sublimation Separate iodine from
a mixture of crystals of iodine and sodium chloride. This is the stability indicator light, indicating
that the weight is stable. Sometimes crystals will grow from several points simultaneously to make
boundaries where they meet. The irregular shape of the sodium changes to a sphere. Geological
evidence of extensive N-fixation by volcanic lightning during very. Heat the fat in an iron saucepan
or dish and, when it is molten, slowly add the sodium hydroxide solution with continuous stirring.
Move your eye to the level of the mark on the neck of the flask and line it up so that the circle
around the neck looks like a line, not an ellipse. The axes must be clearly labelled with the quantity
being plotted e.g. mass and its units e.g. kilograms The points plotted may be joined with a straight
line or a smooth curve. The Vaseline will melt and form an airtight layer, solidifying as the water-
cools. A significant proportion of marks for quantitative exercise will be awarded for accuracy. On
the other hand, when the water containing the ions becomes colder, it is the ions which have gained
the energy and the water has lost an equivalent amount. (a) REACTIONS THAT GIVE OUT HEAT
ENERGY Be careful. Use a wash bottle to rinse the tip of the burette and the sides of the flask.
They are for general-purpose use, but not for quantitative analysis. Air mixing with the gas helps it to
burn more rapidly and efficiently. The rinsing should be transferred to the second vessel along with
the rest of the mixture or solution. The electrodes can be labelled positive and negative. Hold the
apparatus in a beaker of water and heat gently with a Bunsen burner flame. The sand will remain on
the filter paper and may be dried and collected.
You will see the indicator change colour when the titrant hits the solution in the flask, but the colour
change disappears upon stirring. As nearly as possible at the same time, put the ammonia cotton wool
at one end of the tube and the acid cotton wool at the other. Sugar does not react with iodine, but
sugar will reduce copper (II) in Fehling’s solution to red copper (I) oxide, and this is also a sensitive
test. Collect any gas formed and test for hydrogen with the glowing splint test. (d) Ammonia (i) Put
a mixture of calcium hydroxide and ammonium chloride into a test-tube to a depth of 4 cm. In this
method, there is no chemical used in pursuing this experiment. Your burette should be conditioned
and filled with titrant solution. Show the values that can be averaged to obtain an acceptable value
for use in calculations (only those values within 0.2 cm 3 should be averaged). Be sure your eye is at
the level of meniscus, not above or below. The electrodes can be labelled positive and negative. This
prevents combustion since carbon dioxide does not support it and the presence of carbon dioxide
stops oxygen reaching the combustible material. 3.CHLORINE GAS Physical Properties Colour
Greenish-yellow Odour Pungent odour Poisonous Density compared to air (heavier or lighter)
Heavier than air Chemical Properties Solubility in water Soluble in water. The specific catalysts are
not usually available in school laboratories. Then add distilled water a drop at a time until the bottom
of the meniscus lines up exactly with the mark on the neck of the flask. Another accurate method is
to stand a conical flask containing the marble chips and acid on a balance and record the loss in mass
every half minute. At 5-minute intervals, remove 2 or 3 drops by means of a dropper and put them
on a clean white tile, taking care to keep them from running into each other. Use a rubber band to
attach the capillary tube, sealed end down, to a thermometer. Calculate the boiling point as the
average of the two readings. May it be right then, I said, as I rose, deeming it useless to. This booklet
has been produced to help students preparing for and taking practical Examinations. The hydrogen
bubbles will rise into the air, showing the low density of hydrogen gas. (b) Oxygen (i) Prepare
oxygen safely by decomposition of hydrogen peroxide solution. Inorganic Chemistry: Transition
Elements (Chemical properties of first row i. The method of separation used is basic filtration
method. The acid is contained in a thistle funnel and a tap controls the flow on to sodium sulphite in
a suitable flask. An air flow over the solution surface given by a fan will also hasten crystal growth.
Finally, the paper should be rinsed into the beaker, to remove all traces of the solid. The lead
bromide is melted in a 100 mL hard glass beaker, or in a crucible. Put one drop of lemon juice on to
the spot then note any change of colour. Doing a Titration Begin by preparing your burette, as
described on the burette page. This is usually done by running out the acid to a point one unit away
from the trial, the going drop-by-drop until an accurate end point is obtained. F actors affecting
coursework for phd biochemistry the Speed-Rates of chemistry gcse coursework rates reaction
concentration incorporate definition essay Chemical Reactions. The experiment is repeated for each
of the other conical flask, to try to obtain the end point accurately.