UNIT 4

CONCRETE TESTING WITH MIX DESIGN

Tests of cement, Fine aggregate, Coarse aggregate and Quality control at batching plant and
Quality control at site - Water - Fresh concrete testing - Hardened concrete testing - Durability
testing - Maturity of concrete - Modulus of rupture - Modulus of elasticity - Permeability - Test
on permeability - RCPT - Half cell - Construction and measurement determination of pH of
concrete - Phenolphthalein test - Non-destructive testing of concrete. Concept of proportioning
concrete mixes - mix design - IS code method - ACI method - Testing, evaluation and control of
concrete quality.

TESTS OF CEMENT

i. Field Tests on Cement

Field tests on cements are carried to know the quality of cement supplied at site. It gives
some idea about cement quality based on color, touch and feel and other tests.
The following are the field tests on cement
(a) The color of the cement should be uniform. It should be grey color with a light greenish
shade.
(b) The cement should be free from any hard lumps. Such lumps are formed by the absorption of
moisture from the atmosphere. Any bag of cement containing such lumps should be rejected.
(c) The cement should feel smooth when touched or rubbed in between fingers. If it is felt rough,
it indicates adulteration with sand.
(d) If hand is inserted in a bag of cement or heap of cement, it should feel cool and not warm.
(e) If a small quantity of cement is thrown in a bucket of water, the particles should float for
some time before it sinks.
(f) A thick paste of cement with water is made on a piece of glass plate and it is kept under water
for 24 hours. It should set and not crack.
(g) A block of cement 25 mm ×25 mm and 200 mm long is prepared and it is immersed for 7
days in water. It is then placed on supports 15cm apart and it is loaded with a weight of about 34
kg. The block should not show signs of failure.
 (h) The briquettes of a lean mortar (1:6) are made. The size of briquette may be about 75 mm
×25 mm ×12 mm. They are immersed in water for a period of 3 days after drying. If the cement
is of sound quality, the briquettes will not be broken easily.
ii. Laboratory Tests on Cement
1. Fineness test
a. Sieve test
b. Air permeability test
2. Standard consistency test
3. Setting time test
4. Soundness test
1. FINENESS TEST
a) Sieve test - The principle of this is to determine the proportion of cement whose grain
size is larger than specified mesh size. The apparatus used are 90µm IS Sieve, Balance capable
of weighing 10g to the nearest 10mg, a nylon or pure bristle brush preferably with 25 to 40mm,
bristle for cleaning the sieve.

Procedure to determine fineness of cement

 Weigh approximately 10g of cement to the nearest 0.01g and place it on the sieve.
Agitate the sieve by swirling, planetary and linear movements, until no more fine
material passes through it.
  Weigh the residue and express its mass as a percentage R1,of the quantity first placed on
the sieve to the nearest 0.1 percent.
 Gently brush all the fine material off the base of the sieve.
 Repeat the whole procedure using a fresh 10g sample to obtain R2. Then calculate R as
the mean of R1 and R2 as a percentage, expressed to the nearest 0.1 percent.
 When the results differ by more than 1 percent absolute, carry out a third sieving and
calculate the mean of the three values.
Reporting of Results
Report the value of R, to the nearest 0.1 percent, as the residue on the 90µm sieve.
b) Air permeability test - Blaine‘s air permeability apparatus consists essentially of a means
of drawing a definite quantity of air through a prepared bed of cement of definite porosity. The
fineness is expressed as a total surface area in square centimeters per gram. The apparatus used
are Blaine air permeability apparatus, balance and timer.

Procedure to determine fineness of cement

The procedure consists of 4 steps
 Determination of the density of cement - To determine the density or specific gravity of
cement

 Determination of the bed volume

 Apply a very thin film of light mineral oil to the cell interior. Place the perforated disc on
the ledge in cell. Place two new filter paper discs on the perforated disc.
 Fill the cell with mercury. Level the mercury to the top of the cell with a glass plate.
 Remove the mercury from cell and it, M1.
 Remove the top filter paper from the permeability cell and compress a trial quantity of
2.80 g of cement into the space above filter paper to the gauge line in the cell. Place the
other filter paper above the cement bed.
 Fill the remaining space in the cell above the filter paper with mercury. Level the
mercury to the top of the cell with a glass plate and remove mercury from the cell and
weigh it, M2.
 Calculate the volume occupied by the cement bed in the cell from the following equation.
V = (M1-M2)/D,
Where, D = Density of mercury (13.54 g/cm3)
 Average at least two volume determinations that agree to within ±0.005cm3 and record
this value.
 Determination of apparatus constant
 Take an amount (W) of standard cement so as to give the cement bed of porosity
e=0.500.
W = (1-e) ρ*V or W = 0.500ρV
 Place the perforated disc on the ledge at the bottom of the cell and place on it a new filter
paper disc. Place the weighed quantity of standard cement, W, in the cell taking care to
avoid loss.
 Tap the cell to level the cement. Place a second new filter paper disc on the leveled
cement.
 Compress the cement with the plunger until the plunger collar is in contact with the top of
the cell. Slowly withdraw the plunger a short distance, rotate 900, repress the cement bed,
and then slowly withdraw.
  Attach the permeability cell to the manometer tube with an air tight connection and
slowly evacuate the air in the manometer U-tube until the liquid reaches the top mark,
then tightly close the valve.
 Start the timer when the bottom of the meniscus reaches next to the top mark and stop the
timer when the bottom of the meniscus reaches the bottom mark. Record the time t and
temperature of test.
 Repeat the whole procedure on two further samples of the same reference cement.
Calculate the average time of the three determinations. Then calculate the apparatus
constant using the formula given below.

Where,
K=Apparatus constant
S0=Specific surface of reference cement
ρ0=Density of reference cement
t0=Mean of three measured times
η0=Air viscosity at the mean of the three temperatures.
 Determination of fineness
 Repeat the steps (1 to 6) as done in determination of apparatus constant, but this time
using the cement whose fineness is to be calculated.
 Calculate fineness of cement using following formula.

Where,
S = Specific surface area
K = Apparatus constant
ρ = Density of cement
t = Time
2. STANDARD CONSISTENCY TEST
The basic aim is to find out the water content required to produce a cement paste of
standard consistency as specified by the IS: 4031 (Part 4) – 1988. The principle is that standard
consistency of cement is that consistency at which the Vicat plunger penetrates to a point 5-7mm
from the bottom of Vicat mould.
Apparatus – Vicat apparatus conforming to IS: 5513 – 1976, Balance, whose permissible
variation at a load of 1000g should be +1.0g, Gauging trowel conforming to IS: 10086 – 1982.

Procedure to determine consistency of cement

 Weigh approximately 400g of cement and mix it with a weighed quantity of water. The
time of gauging should be between 3 to 5 minutes.
 Fill the Vicat mould with paste and level it with a trowel.
 Lower the plunger gently till it touches the cement surface.
 Release the plunger allowing it to sink into the paste.
 Note the reading on the gauge.
 Repeat the above procedure taking fresh samples of cement and different quantities of
water until the reading on the gauge is 5 to 7mm.
Reporting of Results - Express the amount of water as a percentage of the weight of dry cement
to the first place of decimal.

3. SETTING TIME TEST - Initial and Final Setting Time

To calculate the initial and final setting time as per IS: 4031 (Part 5) – 1988. To do so we
need Vicat apparatus conforming to IS: 5513 – 1976, Balance, whose permissible variation at a
load of 1000g should be +1.0g, Gauging trowel conforming to IS: 10086 – 1982.
Procedure to determine initial and final setting time of cement
 Prepare a cement paste by gauging the cement with 0.85 times the water required to give
a paste of standard consistency.
  Start a stop-watch, the moment water is added to the cement.
 Fill the Vicat mould completely with the cement paste gauged as above, the mould
resting on a non-porous plate and smooth off the surface of the paste making it level with
the top of the mould. The cement block thus prepared in the mould is the test block.
Initial Setting Time
 Place the test block under the rod bearing the needle.
 Lower the needle gently in order to make contact with the surface of the cement paste and
release quickly, allowing it to penetrate the test block.
 Repeat the procedure till the needle fails to pierce the test block to a point 5.0 ± 0.5mm
measured from the bottom of the mould.
 The time period elapsing between the time, water is added to the cement and the time, the
needle fails to pierce the test block by 5.0 ± 0.5mm measured from the bottom of the
mould, is the initial setting time.
Final Setting Time
 Replace the above needle by the one with an annular attachment.
 The cement should be considered as finally set when, upon applying the needle gently to
the surface of the test block, the needle makes an impression therein, while the
attachment fails to do so.
 The period elapsing between the time, water is added to the cement and the time, the
needle makes an impression on the surface of the test block, while the attachment fails to
do so, is the final setting time.

4. SOUNDNESS TEST - Soundness of cement is determined by Le-Chatelier method as per

IS: 4031 (Part 3) – 1988. The apparatus for conducting the Le-Chatelier test should conform to
IS: 5514 – 1969, Balance, whose permissible variation at a load of 1000g should be +1.0g and
Water bath.
Procedure to determine soundness of cement
 Place the mould on a glass sheet and fill it with the cement paste formed by gauging
cement with 0.78 times the water required to give a paste of standard consistency.
 Cover the mould with another piece of glass sheet, place a small weight on this covering
glass sheet and immediately submerge the whole assembly in water at a temperature of
27 ± 2oC and keep it there for 24hrs.
 Measure the distance separating the indicator points to the nearest 0.5mm (say d1).
 Submerge the mould again in water at the temperature prescribed above. Bring the water
to boiling point in 25 to 30 minutes and keep it boiling for 3hrs.
 Remove the mould from the water, allow it to cool and measure the distance between the
indicator points (say d2)
 (d2–d1) represents the expansion of cement.

TEST ON AGGREGATE
1. Test for determination of Flakiness Index and Elongation Index
2. Test for organic impurities in fine aggregate
3. Test for determination of clay, fine silt and fine dust
4. Test for determination of specific gravity
5. Test for Bulk density and Voids
6. Test for aggregate Crushing value
7. Test for aggregate Impact value
8. Test for aggregate Abrasion value
Test for determination of Flakiness Index and Elongation Index
The Flakiness index of aggregates is the percentage by weight of particles whose least
dimension (thickness) is less than three- fifths (0.6times) of their mean dimension. This test is
not applicable to sizes smaller than 6.3mm.
The Elongation index of an aggregate is the percentage by weight of particles whose
greatest dimension (length) is greater than nine-fifths (1.8times) their mean dimension. This test
is not applicable for sizes smaller than 6.3mm.
The particle shape of aggregates is determined by the percentages of flaky and elongated
particles contained in it. For base course and construction of bituminous and cement concrete
types, the presence of flaky and elongated particles are considered undesirable as these cause
inherent weakness with possibilities of breaking down under heavy loads. Thus, evaluation of
shape of the particles, particularly with reference to flakiness and elongation is necessary.
The apparatus for the shape tests consists of the following:
i. A standard thickness gauge
ii. A standard length gauge
iii. IS sieves of sizes 63, 50 40, 31.5, 25, 20, 16, 12.5,10 and 6.3mm
iv. A balance of capacity 5kg, readable and accurate up to 1 gm

Thickness Gauge (Flakiness)

 Length gauge (Elongation)
Procedure
 Sieve the sample through the IS sieves (as specified in the table).
 Take a minimum of 200 pieces of each fraction to be tested and weigh them.
 In order to separate the flaky materials, gauge each fraction for thickness on a thickness
gauge. The width of the slot used should be of the dimensions specified in column (4) of
the table for the appropriate size of the material.
 Weigh the flaky material passing the gauge to an accuracy of at least 0.1 per cent of the
test
 In order to separate the elongated materials, gauge each fraction for length on a length
gauge. The width of the slot used should be of the dimensions specified in column (6) of
the table for the appropriate size of the material.
 Weigh the elongated material retained on the gauge to an accuracy of at least 0.1 per cent
of the test sample.
 Flakiness Index = (X1+ X2+…..) / (W1 + W2 + ….) X 100
Elongation Index = (Y1 + Y2 + …) / (W1 + W2 + ….) X 100
Recommended value - The shape tests give only a rough idea of the relative shapes of aggregates.
Flaky and elongated particles should be avoided in pavement construction, particularly in surface
course. If such particles are present in appreciable proportions, the strength of pavement layer
would be adversely affected due to possibility of breaking under loads. Workability is reduced
for cement concrete. IRC recommendations for maximum limits of flakiness index are as given.
Test for Organic Impurities in Fine Aggregate - The aggregate must be checked for organic
impurities such as decayed vegetations, humus, and coal dust, etc. Color test is a reliable
indicator of the presence of harmful organic matter in aggregates except in areas where there are
deposits of lignite.
Procedure
 Fill a 350 ml clear glass medicine bottle upto 75 ml mark with a 3% solution of caustic
soda or sodium hydroxide. A 3% solution of caustic soda is made by dissolving 3 gm of
sodium hydroxide (which can be purchased from any local laboratory chemicals shop) in
100 ml of clean water (preferably distilled water). The solution should be kept in glass
bottle tightly closed with a rubber stopper. Handling sodium hydroxide with moist hands
may result in serious burns. Care should be taken not to spill the solution for it is highly
injurious to clothing, leather and other materials.
 The representative sands sample is next added gradually until the volume measured by
the sandy layer is 125 ml. The volume is then made up to 200 ml by the addition of more
of the solution. The bottle is then corked and shaken vigorously and allowed to stand for
24 hours.
 At the end o f this period, the color of the liquid will indicate whether the sand contains a
dangerous amount of matter or not. A colorless liquid indicates clean sand free from
organic matter. A straw-colored solution indicates some organic matter but not enough to
be seriously objectionable. Darker color means that the sand contains injurious, amounts
and should not be used unless it is washed and a retest then shows that it is satisfactory.
Test for determination of clay, fine silt and fine dust
This is a gravimetric method for determining the clay, fine silt and fine dust, which
includes particles up to 20 micron as per IS 2386- II (1963). Differences in the nature and density
of materials or in the temperature at the time of testing may vary the separation point.
The apparatus shall consist of the following:
 A watertight screw-topped glass jar of dimensions similar to a 1-kg fruit preserving jar.
 A device for rotating the jar about its long axis, with this axis horizontal, at a speed of
80±20 rev/min.
 A sedimentation pipette of the Andreason type of approximately 25 ml capacity and of
the general form indicated in Figure. This consists mainly of a pipette fitted at the top
 with a two-way tap and held rigidly in a clamp which can be raised or lowered as
required, and which is fitted with a scale from which the changes in height of the pipette
can be read.
 The volume of the pipette A, including the connecting bore of the tap B, is determined by
filling with distilled water; by reversing the tap, the water is run out into a bottle, weighed
and the volume calculated.
 A 1000 ml measuring cylinder.
 A scale or balance of capacity not less than 10 kg, readable and accurate to 1 gm.
 A scale or balance of capacity not less than 250 g, readable and accurate to 0·001 gm.
 A well-ventilated oven, thermostatically controlled, to maintain a temperature of 100 to
110°c.
Chemicals - A solution containing 8 g of sodium oxalate per liter of distilled water shall be
taken. For use, this stock solution is diluted with distilled water to one tenth (that is 100 ml
diluted with distilled water to one liter).
Test Sample - The sample for test shall be prepared from the main sample taking particular care
that the test sample contains a correct proportion of the finer material. The amount of sample
taken for test shall be in accordance with table below.

All-in aggregates shall be separated into fine and coarse fractions by sieving on a 4·75-mm IS
Sieve and the two samples so obtained shall be tested separately.
Method for Fine Aggregate - Approximately 300 g of the sample in the air-dry condition, passing
the 4·75·mm IS Sieve, shall be weighed and placed in the screw-topped glass jar, together with
300 ml of the diluted sodium oxalate solution. The rubber washer and cap shall be fixed, care
being taken to ensure water tightness. The jar shall then be rotated about its long axis, with this
axis horizontal, at a speed of 80±20 rev/min for a period of 15 minutes. At the end of 15 minutes,
the suspension shall be poured into the 1000 ml measuring cylinder and the residue washed by
gentle swirling and decantation of successive 150 ml portions of sodium oxalate solution, the
washings being added to the cylinder until the volume is made up to 1000 ml. The common
procedure is given in determination paragraph.
Method for Coarse Aggregate - The weighed sample shall be placed in a suitable container,
covered with a measured volume of sodium oxalate solution (0.8 g per liter), agitated vigorously
to remove all adherent fine material and the liquid suspension transferred to the 1000 ml
measuring cylinder. This process shall be repeated as necessary until all clayey material has been
transferred to the cylinder. The volume shall be made up to 1000 ml with sodium oxalate
solution. The common procedure is given in determination paragraph.

Determination - The suspension in the measuring cylinder shall be thoroughly mixed by

inversion and the tube and contents immediately placed in position under the pipette. The pipette
A shall then be gently lowered until the tip touches the surface of the liquid, and then lowered a
further 10 cm into the liquid. Three minutes after placing the tube in position, the pipette A and
the bore of tap B shall be filled by opening Band applying gentle suction at C. A small surplus
may be drawn up into the bulb between tap B and tube C, but this shall be allowed to run away
and any solid matter shall be washed out with distilled water from E. The pipette shall then be
removed from the measuring cylinder and its contents run into a weighed container, any adherent
solids being washed into the container by distilled water from E through the tap B. The contents
of the container shall be dried at 100 to 110°C to constant weight, cooled and weighed.
Calculations - The proportion of fine silt and clay or fine dust shall then be calculated from the
following formula:

Where,
W1 = weight in g of the original sample,
W2 = weight in g of the dried residue,
V = volume in ml of the pipette, and
0·8 = weight in g of sodium oxalate in one litre of the diluted solution.
Reporting of Results - The clay, fine silt and fine dust content shall be reported to the nearest 0·1
percent.

Test for aggregate Crushing value - This test helps to determine the aggregate crushing value of
coarse aggregates as per IS: 2386 (Part IV) – 1963. The apparatus used is cylindrical measure
and plunger, Compression testing machine, IS Sieves of sizes – 12.5mm, 10mm and 2.36mm
Procedure to determine Aggregate Crushing Value
 The aggregates passing through 12.5mm and retained on 10mm IS Sieve are oven-dried
at a temperature of 100 to 110oC for 3 to 4hrs.
 The cylinder of the apparatus is filled in 3 layers, each layer tamped with 25 strokes of a
tamping rod.
 The weight of aggregates is measured (Weight ‗A‘).
 The surface of the aggregates is then leveled and the plunger inserted. The apparatus is
then placed in the compression testing machine and loaded at a uniform rate so as to
achieve 40t load in 10 minutes. After this, the load is released.
 The sample is then sieved through a 2.36mm IS Sieve and the fraction passing through
the sieve is weighed (Weight ‗B‘).
 Two tests should be conducted.
Aggregate crushing value = (B/A) x 100%.

Test for Aggregate Impact value - This test is done to determine the aggregate impact value of
coarse aggregates as per IS: 2386 (Part IV) – 1963. The apparatus used for determining
aggregate impact value of coarse aggregates is Impact testing machine conforming to IS: 2386
(Part IV)- 1963,IS Sieves of sizes – 12.5mm, 10mm and 2.36mm, A cylindrical metal measure of
75mm dia. and 50mm depth, A tamping rod of 10mm circular cross section and 230mm length,
rounded at one end and Oven.
Preparation of Sample
i. The test sample should conform to the following grading:
a. Passing through 12.5mm IS Sieve – 100%
b. Retention on 10mm IS Sieve – 100%
ii. The sample should be oven-dried for 4hrs. at a temperature of 100 to 110oC and cooled.
iii. The measure should be about one-third full with the prepared aggregates and tamped with
25 strokes of the tamping rod.
A further similar quantity of aggregates should be added and a further tamping of 25
strokes given. The measure should finally be filled to overflow, tamped 25 times and the surplus
aggregates struck off, using a tamping rod as a straight edge. The net weight of the aggregates in
the measure should be determined to the nearest gram (Weight ‗A‘).
Procedure to determine Aggregate Impact Value
i) The cup of the impact testing machine should be fixed firmly in position on the base
of the machine and the whole of the test sample placed in it and compacted by 25
strokes of the tamping rod.
ii) The hammer should be raised to 380mm above the upper surface of the aggregates in
the cup and allowed to fall freely onto the aggregates. The test sample should be
 subjected to a total of 15 such blows, each being delivered at an interval of not less
than one second.
Reporting of Results
i. The sample should be removed and sieved through a 2.36mm IS Sieve. The fraction
passing through should be weighed (Weight ‗B‘). The fraction retained on the sieve
should also be weighed (Weight ‗C‘) and if the total weight (B+C) is less than the initial
weight (A) by more than one gram, the result should be discarded and a fresh test done.
ii. The ratio of the weight of the fines formed to the total sample weight should be expressed
as a percentage.
Aggregate impact value = (B/A) x 100%
iii. Two such tests should be carried out and the mean of the results should be reported.

Test for aggregate Abrasion value - This test helps to determine the abrasion value of coarse
aggregates as per IS: 2386 (Part IV) – 1963.
The apparatus used in this test are Los Angles abrasion testing machine, IS Sieve of size –
1.7mm, Abrasive charge – 12 Nos. of cast iron or steel spheres approximately 48 mm diameter
and each weighing between 390 and 445g ensuring that the total weight of charge is 5000 +25g
and Oven.
Sample Preparation - The test sample should consist of clean aggregates which has been dried in
an oven at 105 to 110oC to a substantially constant weight and should conform to one of the
grading shown in the table below:

Procedure to determine Aggregate Abrasion Value

The test sample and the abrasive charge should be placed in the Los Angles abrasion
testing machine and the machine rotated at a speed of 20 to 33 revolutions per minute for 1000
revolutions. At the completion of the test, the material should be discharged and sieved through
1.70mm IS Sieve.

Reporting of Results

 The material coarser than 1.70mm IS Sieve should be washed dried in an oven at a
temperature of 100 to 110oC to a constant weight and weighed (Weight ‗B‘).
 The proportion of loss between weight ‗A‘ and weight ‗B‘ of the test sample should be
expressed as a percentage of the original weight of the test sample. This value should be
reported as,
 Aggregate abrasion value = (A-B)/B x 100%.

Test for Determination of Specific Gravity - The specific gravity of a substance is the ratio of
the unit weight of the substance to the unit weight of water. A representative aggregate sample in
SSD (Saturated surface dry) condition is obtained by quartering and the following weights are
used in the tests for the various sizes of aggregates.

Less than 4.75 mm - 500 to 700 gm

4.75 mm to 10 mm - 1000 to 1500 gm
10 mm to 20 mm - 1500 to 2000 gm
20 mm to 40 mm - more than 2000 gm
Procedure
 Take a suitable size jar, the top open side of which have flange, so that a glass plate may
be put on it.
 The jar should be filled with clean water up to the flange and slide on it the glass plate. If
there is any air bubble, which can be seen from top of glass plate, then the jar top should
be filled with more water. There should not be any air bubble. Take the weight of jar
fully filled with water and upon it glass plate (weight A).
 About half empty the jar fill it with known weight of SSD aggregate sample weight (B).
As mentioned at b, fill the jar up to the top and putt glass plate on it. There should not be
any air bubble. Take its weigh (weight C).
Specific gravity on SSD basis = B/ [B-(C-A)]

Test for Bulk density and Voids - Bulk density is the weight of a unit volume of aggregate,
usually stated in kg per liter on room dry basis in estimating quantities of materials and in mix
computation, when batching is done on a volumetric basis.
Concrete material proportion by weight can be converted to proportions by volume, by dividing
with the bulk density of the materials available for use at site. The bulk density of cement may be
taken 1.44 kg/lit.
For determination of bulk density the container size shall be as given below:

Nominal Inside Thickness of

Size of Inside dia
capacity height metal (min)
particle (mm)
(litres) (mm) (mm)

4.75 mm and
3 150 170 3.15
under

Over 4.75
mm to 40 15 250 300 4.00
mm

Over 40 mm 30 350 310 5.00

Procedure
 About 100 kg of aggregate sample should be dried in the room.
 Take the weight in kg of empty container + glass plate (Weight A).
 The container is to be filled with loose sand or loose aggregate i.e. sand or aggregate
should be dropped in the container from about 5 cm heights from top of container. Take
the weight of container filled with sand or aggregate + glass plate (Weight B).
 Empty the container filled it with clean water up to the top ridge putt glass plate. There
shall not be any air bubble. Take is weight (Weight C). All weight should be taken in kg.
Loose bulk density in kg/lit on the basis
Off room dry sand or aggregate = [B-A]/[C-A]
And voids percentage = [(Specific gravity – bulk density)/ Specific gravity] x100

WATER - Water is the key ingredient, which when mixed with cement, forms a paste that binds
the aggregate together. The water causes the hardening of concrete through a process called
hydration. Hydration is a chemical reaction in which the major compounds in cement form
chemical bonds with water molecules and become hydrates or hydration products. Details of the
hydration process are explored in the next section. The water needs to be pure in order to prevent
side reactions from occurring which may weaken the concrete or otherwise interfere with the
hydration process. The role of water is important because the water to cement ratio is the most
critical factor in the production of "perfect" concrete. Too much water reduces concrete strength,
while too little will make the concrete unworkable. Concrete needs to be workable so that it may
be consolidated and shaped into different forms (i.e. walls, domes, etc.). Because concrete must
be both strong and workable, a careful balance of the cement to water ratio is required when
making concrete.
Function of Water in Concrete
The water serves the following purpose:
1. To wet the surface of aggregates to develop adhesion because the cement pastes adheres
quickly and satisfactory to the wet surface of the aggregates than to a dry surface.
 2. To prepare a plastic mixture of the various ingredients and to impart workability to
concrete to facilitate placing in the desired position and
3. Water is also needed for the hydration of the cementing materials to set and harden
during the period of curing.

Quality control at batching plant

Quality Control of RMC can be divided into three convenient areas like forward control,
immediate control and retrospective control.
Forward control basically deals with procedures of quality control to be followed before the
production process.
This covers
 Materials storage,
 Monitoring of quality of materials,
 Modification of mix design,
 Plant maintenance,
 Calibration of equipment and
 Plant and transit mixer condition.
Immediate control is concerned with instant action to control the quality of concrete during
production or that of deliveries closely following production.
This covers
 Weighing – correct reading of batch data and accurate weighing,
 Visual observation and testing of concrete during production and delivery (assessment of
uniformity, cohesion, workability, adjustment of water content) and
 Making corresponding adjustments at the plant automatically or manually to batched
quantities to allow for observed, measured or reported changes in materials or concrete
qualities.
Retrospective control primarily deals with the quality control procedures after production.
This covers
 Sampling of concrete, testing and monitoring of results,
 Weighbridge checks of laden and unladen vehicle weights,
 Stock control of materials and
  Diagnosis and correction of identified faults.
Quality control at site
 Study duties responsibilities, Tender specification, standards, codes of practice and work
instruction.
 Evolve effective acceptance/rejection procedures for construction materials in
coordination with the project purchase department.
 Do proper sampling and testing of steel, cement, concrete, aggregates, water, etc., and
verify test results in view of standards and work specifications prior to their use in
construction. Also control quality of electrodes to their use in welding.
 Set procedures to control quality at the points of storage for raw materials, mixing and
placing of concrete.
 Follow the prescribed curing and deshuttering schedules.
 Observe procedures to control quality of welded joints of structural steel members.
 Evolve a system to check quality of workmanship in all construction activities.
 Keep all revised Indian Standards and codes of practice available in QC laboratory and
have them handy during discussion with client/consultant.
 Maintain sequence of construction required under any activity.
 Discuss QA/QC issues as a separate agenda during site review meetings with staff.
 Observe regular schedule for maintenance, repairs and calibration of plants and
equipments.
 Keep spare parts/materials for laboratory equipments weigh batchers, batching plant, etc.,
always keep spare vibrators ready at site.
 Carry work instruction cards in pocket while supervising/inspecting works.
 Regularly maintain the formats prescribed under ISO 9002 Quality assurance system
 Practice sound housekeeping methods to achieve saving, safety and quality.

FRESH CONCRETE TESTING

 Slump test
 Compacting factor test
 Vee Bee test and
 Flow table test
  Kelly ball test
Slump Test

This test is performed to check the consistency of freshly made concrete. The slump test
is done to make sure a concrete mix is workable. The measured slump must be within a set
range, or tolerance, from the target slump.
Tools and apparatus used for slump test (equipment):
 Standard slump cone (100 mm top diameter x 200 mm bottom diameter x 300 mm
high)
 Small scoop - Bullet-nosed rod (600 mm long x 16 mm diameter)
 Rule - Slump plate (500 mm x 500 mm)
Procedure of slump test for concrete
1. Clean the cone. Dampen with water and place on the slump plate. The slump plate should
be clean, firm, level and non-absorbent. Collect a sample of concrete to perform the slum
test.
2. Stand firmly on the foot pieces and fill 1/3 the volume of the cone with the sample.
Compact the concrete by 'rodding' 25 times. Rodding means to push a steel rod in and out
of the concrete to compact it into the cylinder, or slump cone. Always rod in a definite
pattern, working from outside into the middle.
3. Now fill to 2/3 and again rod 25 times, just into the top of the first layer.
4. Fill to overflowing, rodding again this time just into the top of the second layer. Top up
the cone till it overflows.
5. Level off the surface with the steel rod using a rolling action. Clean any concrete from
around the base and top of the cone, push down on the handles and step off the foot
pieces.
6. Carefully lift the cone straight up making sure not to move the sample.
7. Turn the cone upside down and place the rod across the up-turned cone.
8. Take several measurements and report the average distance to the top of the sample. If
the sample fails by being outside the tolerance (ie the slump is too high or too low),
another must be taken. If this also fails the remainder of the batch should be rejected.
 Slump Cone test and apparatus

Compacting factor test

Compacting factor of fresh concrete is done to determine the workability of fresh

concrete by compacting factor test as per IS: 1199 – 1959. The apparatus used is Compacting
factor apparatus.

Procedure
 The sample of concrete is placed in the upper hopper up to the brim.
  The trap-door is opened so that the concrete falls into the lower hopper.
The trap-door of the lower hopper is opened and the concrete is allowed to fall into the
cylinder.
 The excess concrete remaining above the top level of the cylinder is then cut off with the
help of plane blades
 The concrete in the cylinder is weighed. This is known as weight of partially compacted
concrete.
 The cylinder is filled with a fresh sample of concrete and vibrated to obtain full
compaction. The concrete in the cylinder is weighed again. This weight is known as the
weight of fully compacted concrete.

Compacting factor = (Weight of partially compacted concrete)/(Weight of fully compacted

concrete) = (W1-W2 / W2-W)

Note - The test is sufficiently sensitive to enable difference in work ability arising from the initial
process in the hydration of cement to be measured. Each test, there for should be carried out at a
constant time interval after the mixing is completed, if strictly comparable results are to be
obtained. Convenient time for releasing the concrete from the upper hopper has been found to be
two minutes after the completion of mixing.
 Compaction factor apparatus

Vee Bee test

To determine the workability of fresh concrete by using a Vee-Bee consistometer as per IS: 1199
– 1959. The apparatus used is Vee-Bee consistometer.

Procedure
 A conventional slump test is performed, placing the slump cone inside the cylindrical part
of the consistometer.
 The glass disc attached to the swivel arm is turned and placed on the top of the concrete
in the pot.
 The electrical vibrator is switched on and a stop-watch is started, simultaneously.
Vibration is continued till the conical shape of the concrete disappears and the concrete
assumes a cylindrical shape.
 When the concrete fully assumes a cylindrical shape, the stop-watch is switched off
immediately. The time is noted.
 The consistency of the concrete should be expressed in VB-degrees, which is equal to the
time in seconds recorded above.

Vee Bee test apparatus

Flow table test

To determine the workability of fresh concrete by using a Flow table test as per IS: 5512 – 1983.
The apparatus used is Flow table apparatus.

Procedure
 The 700 mm square flow table is hinged to a rigid base, proved with a stop that allows
the far end to be raised by 40 mm.
 A cone, similar to that used for slump testing but truncated, is filled with concrete in two
layers.
 Each layer is tamped 10 times with a special wooden bar and the concrete of the upper
layer finished off level with the top of the cone. Any excess is cleaned off the outside of
the cone.
 The cone is then raised allowing the concrete to flow out and spread out a little on the
flow table.
 The table top is then raised until it meets the stop and allowed to drop freely 15 times.
 This causes the concrete to spread further, in a roughly circular shape.
 The flow diameter is the average of the maximum diameter of the pool of concrete and
the diameter at right angles.

As well as getting an accurate measurement of the workability of the concrete, the flow test
gives an indication of the cohesion. A mix that is prone to segregation will produce a non-
circular pool of concrete. Cement paste may be seen separating from the aggregate. If the
mix is prone to bleeding, a ring of clear water may form after a few minutes.
Flow table test apparatus

Kelly ball test

The simple and inexpensive test can be quickly performed on in-place concrete and the
results can be correlated to slump. This method is used to determine the penetration of a
hemispherical metal weight into freshly mixed concrete, which is related to the workability
of the concrete.
The apparatus consists of a cylinder with one end having a hemispherical shape and the other end
fit with a graduated handle. The weight assembly is lowered through a frame into the concrete
and the penetration measured. The test apparatus consists of a 6 inch diameter, 30 pound ball
attached to a stem, as shown in Figure. The stem, which is graduated in ¼ inch increments, slides
through a frame that rests on the fresh concrete. To perform the test, the concrete to be tested is
stuck off level. The ball is released and the depth of penetration is measured to the nearest ¼
inch. At least three measurements must be made for each sample.

The Kelly ball test provides an indication of yield stress, as the test essentially measures
whether the stress applied by the weight of the ball is greater than the yield stress of the concrete.
For a given concrete mixture, the results of the Kelly ball test can be correlated to slump.

Advantages
 The test is faster than the slump test and can be preformed on in-place concrete to obtain
a direct result quickly
 It has been claimed that the Kelly ball test provides more accurate results than the slump
test.
Disadvantages
 Like the slump test, the Kelly ball test is a static test.
 The test must be performed on a level concrete surface.
 The test is no longer widely used.
 Large aggregate can influence the results
HARDENED CONCRETE TESTING

1. Compressive strength test on concrete

Out of many test applied to the concrete, this is the utmost important which gives an idea
about all the characteristics of concrete. By this single test one judge that whether Concreting has
been done properly or not.
For cube test two types of specimens either cubes of 15 cm X 15 cm X 15 cm or 10cm X
10 cm x 10 cm depending upon the size of aggregate are used. For most of the works cubical
moulds of size 15 cm x 15cm x 15 cm are commonly used. This concrete is poured in the mould
and tempered properly so as not to have any voids. After 24 hours these moulds are removed and
test specimens are put in water for curing. The top surface of these specimen should be made
even and smooth. This is done by putting cement paste and spreading smoothly on whole area of
specimen.
 These specimens are tested by compression testing machine after 7 days curing or 28
days curing. Load should be applied gradually at the rate of 140 kg/cm2 per minute till the
Specimens fails. Load at the failure divided by area of specimen gives the compressive strength
of concrete.
The apparatus in this test is a Compression testing machine The proportion and material for
making these test specimens are from the same concrete used in the field. The specimen used for
testing is 6 cubes of 15 cm size Mix. M15 or above. The mixing can be done manually.
Hand mixing
 Mix the cement and fine aggregate on a water tight none-absorbent platform until the
mixture is thoroughly blended and is of uniform color
 Add the coarse aggregate and mix with cement and fine aggregate until the coarse
aggregate is uniformly distributed throughout the batch
 Add water and mix it until the concrete appears to be homogeneous and of the desired
consistency
Sampling
 Clean the mounds and apply oil
 Fill the concrete in the molds in layers approximately 5cm thick
 Compact each layer with not less than 35strokes per layer using a tamping rod (steel bar
16mm diameter and 60cm long, bullet pointed at lower end)
 Level the top surface and smoothen it with a trowel
Curing
The test specimens are stored in moist air for 24hours and after this period the specimens are
marked and removed from the molds and kept submerged in clear fresh water until taken out
prior to test. The water for curing should be tested every 7days and the temperature of water
must be at 27±2oC.
Procedure
i. Remove the specimen from water after specified curing time and wipe out excess water
from the surface.
ii. Take the dimension of the specimen to the nearest 0.2m
iii. Clean the bearing surface of the testing machine
 iv. Place the specimen in the machine in such a manner that the load shall be applied to the
opposite sides of the cube cast.
v. Align the specimen centrally on the base plate of the machine.
vi. Rotate the movable portion gently by hand so that it touches the top surface of the
specimen.
vii. Apply the load gradually without shock and continuously at the rate of 140kg/cm2/minute
till the specimen fails
viii. Record the maximum load and note any unusual features in the type of failure.

Note
Minimum three specimens should be tested at each selected age. If strength of any specimen
varies by more than 15 per cent of average strength, results of such specimen should be rejected.
Average of there specimens gives the crushing strength of concrete. The strength requirements of
concrete.
Calculations
Size of the cube =15cm x15cm x15cm
Area of the specimen (calculated from the mean size of the specimen )=225cm2
Characteristic compressive strength(f ck)at 7 days =
Expected maximum load =fck * area * f.s
Range to be selected is …………………..
Similar calculation should be done for 28 day compressive strength
Maximum load applied =……….tones = ………….N
Compressive strength = (Load in N/ Area in mm2)=…………N/mm2
=………….N/mm2

Report
a) Identification mark
b) Date of test
c) Age of specimen
d) Curing conditions, including date of manufacture of specimen
f) Appearance of fractured faces of concrete and the type of fracture if they are unusual
Result
Average compressive strength of the concrete cube = ………….N/ mm2 (at 7 days)
Average compressive strength of the concrete cube =………. N/mm2 (at 28 days)

Percentage strength of concrete at various ages

The strength of concrete increases with age. Table shows the strength of concrete at different
ages in comparison with the strength at 28 days after casting.

Age Strength per cent

1 day 16%
3 days 40%
7 days 65%
14 days 90%
28 days 99%

Compressive strength of different grades of concrete at 7 and 28 days

Grade of Minimum compressive Specified characteristic compressive

Concrete strength N/mm2 at 7 days strength (N/mm2) at 28 days
M15 10 15
M20 13.5 20
M25 17 25
M30 20 30
M35 23.5 35
M40 27 40
M45 30 45
TENSILE STRENGTH TEST ON CONCRETE

The tensile strength of concrete is one of the basic and important properties. Splitting
tensile strength test on concrete cylinder is a method to determine the tensile strength of
concrete. The concrete is very weak in tension due to its brittle nature and is not expected to
resist the direct tension. The concrete develops cracks when subjected to tensile forces. Thus, it
is necessary to determine the tensile strength of concrete to determine the load at which the
concrete members may crack. The main aim is to determine the splitting tensile of concrete.
Equipment for Splitting Tensile Test of Concrete - Compression testing machine, two packing
strips of plywood 30 cm long and 12mm wide.

Sampling of Concrete Cylinders - The cylinder mould shall is of metal 3mm thick. Each mould is
capable of being opened longitudinally to facilitate the removal of the specimen and is provided
with a means of keeping it closed while in use. The mean internal diameter of the mould is 15 cm
± 0.2 mm and the height is 30 +/- 0.1 cm. Each mould is provided with a metal base plate mould
and base plate should be coated with a thin film of mould oil before use, in order to prevent
adhesion of concrete.
Tamping Bar - The tamping bar is a steel bar of 16 mm diameter, 60 cm long and bullet pointed
at the lower end.
Compacting of Concrete - The test specimen should be made as soon as practicable after the
concrete is filled into the mould in layers approximately 5 cm deep. Each layer is compacted
either by hand or by vibration.
Compacting by Hand - When compacting by hand, the standard tamping bar is used and the
stroke of the bar should be distributed in a uniform manner. The number of strokes for each layer
should not less than 30. The stroke should penetrate in to the underlying layer and the bottom
layer should be rodded throughout its depth. After top layer has been compacted .The surface of
the concrete should be finished level with the top of the mould using a trowel and covered with a
glass or metal plate to prevent evaporation.
Curing of Specimen - The test specimen should be stored in a place at a temperature of 27° ±2°C
for 24±0.5 hrs from the time addition of water to the dry ingredients. After this period the
specimen should be marked and removed from the moulds and immediately submerged in clean
fresh water or saturated lime solution and kept there until taken out just prior to the test. The
water or solution in which the specimen s are kept should be renewed every seven days and
should be maintained at a temperature of 27° ± 2°c.Concrete cylinder 15 cm diameter &30cm
long.
Note
Cast 6 cylinders (3 for split test &3 for compression test)

Procedure of Splitting Tensile Test

i. Take the wet specimen from water after 7 days of curing
ii. Wipe out water from the surface of specimen
 iii. Draw diametrical lines on the two ends of the specimen to ensure that they are on the
same axial place.
iv. Note the weight and dimension of the specimen.
v. Set the compression testing machine for the required range.
vi. Keep are plywood strip on the lower plate and place the specimen.
vii. Align the specimen so that the lines marked on the ends are vertical and centered over the
bottom plate.
viii. Place the other plywood strip above the specimen.
ix. Bring down the upper plate to touch the plywood strip.
x. Apply the load continuously without shock at a rate of approximately 14-
21kg/cm2/minute (Which corresponds to a total load of 9900kg/minute to
14850kg/minute)
xi. Note down the breaking load(P)
Calculations
Range Calculation
As per IS456, split tensile strength of concrete = 0.7 Fck
The splitting tensile strength is calculated using the formula
Tsp = 2P/ pi DL
Where P = applied load
D = diameter of the specimen
L = length of the specimen
Therefore P = Tsp* pi DL/2
Expected load = P * f*s
Range to be selected is…………..
Split tensile strength
T = 2P/ pi DL
Report
(I) Date of test
(II) Identification mark and size of the specimen
(III) Age of test specimen and date of test
(IV) Curing history as detailed earlier
(V) Weight of specimen in kg
(VI) Type of fracture face, if they are unusual.
Result
Splitting tensile strength of given concrete =……………….N/mm²

FLEXURAL STRENGTH TEST

Objective

To determine the Flexural Strength of Concrete, which comes into play when a road slab with
inadequate sub-grade support is subjected to wheel loads and / or there are volume changes due
to temperature / shrinking.

Reference standards

IS: 516-1959 – Methods of tests for strength of concrete

Equipment & apparatus

 Beam mould of size 15 x 15x 70 cm (when size of aggregate is less than 38 mm) or of
size 10 x 10 x 50 cm (when size of aggregate is less than 19 mm)

 Tamping bar (40 cm long, weighing 2 kg and tamping section having size of 25 mm x
25 mm)
 Flexural test machine– The bed of the testing machine shall be provided with two steel
rollers, 38 mm in diameter, on which the specimen is to be supported, and these rollers
shall be so mounted that the distance from centre to centre is 60 cm for 15.0 cm
specimens or 40 cm for 10.0 cm specimens. The load shall be applied through two
 similar rollers mounted at the third points of the supporting span that is, spaced at 20 or
13.3 cm centre to centre. The load shall be divided equally between the two loading
rollers, and all rollers shall be mounted in such a manner that the load is applied axially
and without subjecting the specimen to any torsion stresses or restraints.

Procedure

i. Prepare the test specimen by filling the concrete into the mould in 3 layers of
approximately equal thickness. Tamp each layer 35 times using the tamping bar as
specified above. Tamping should be distributed uniformly over the entire crossection of
the beam mould and throughout the depth of each layer.
ii. Clean the bearing surfaces of the supporting and loading rollers, and remove any loose
sand or other material from the surfaces of the specimen where they are to make contact
with the rollers.
iii. Circular rollers manufactured out of steel having cross section with diameter 38 mm will
be used for providing support and loading points to the specimens. The length of the
rollers shall be at least 10 mm more than the width of the test specimen. A total of four
rollers shall be used, three out of which shall be capable of rotating along their own
axes. The distance between the outer rollers (i.e. span) shall be 3d and the distance
between the inner rollers shall be d. The inner rollers shall be equally spaced between
the outer rollers, such that the entire system is systematic.
 iv. The specimen stored in water shall be tested immediately on removal from water; whilst
they are still wet. The test specimen shall be placed in the machine correctly centered
with the longitudinal axis of the specimen at right angles to the rollers. For molded
specimens, the mould filling direction shall be normal to the direction of loading.
v. The load shall be applied at a rate of loading of 400 kg/min for the 15.0 cm specimens
and at a rate of 180 kg/min for the 10.0 cm specimens.

Calculation
The Flexural Strength or modulus of rupture (fb) is given by
fb = pl/bd2 (when a > 20.0cm for 15.0cm specimen or > 13.0cm for 10cm specimen)
or
fb = 3pa/bd2 (when a < 20.0cm but > 17.0 for 15.0cm specimen or < 13.3 cm but > 11.0cm for
10.0cm specimen.)
Where,
a = the distance between the line of fracture and the nearer support, measured on the center line
of the tensile side of the specimen
b = width of specimen (cm)
d = failure point depth (cm)
l = supported length (cm)
p = max. Load (kg)
Reports
The Flexural strength of the concrete is reported to two significant figures.

Safety & precautions:

 Use hand gloves while, safety shoes at the time of test.

 After test switch off the machine.
 Keep all the exposed metal parts greased.
 Keep the guide rods firmly fixed to the base & top plate.
 Equipment should be cleaned thoroughly before testing & after testing.

MODULUS OF RUPTURE
Flexural strength, also known as modulus of rupture, bend strength, or fracture strength a
mechanical parameter for brittle material, is defined as a material's ability to resist deformation
under load.

MATURITY OF CONCRETE
Concrete maturity indicates how far curing has progressed. Maturity is the relationship
between concrete temperature, time, and strength gain. It is represented by an index value that
can be measured in real time in the field.
The maturity method, often simply referred to as ―maturity,‖ is a way of evaluating
new concrete‘s in-place strength by relating time and temperature measurements to actual
strength values.
To expedite schedules, increase safety, and improve construction methods, construction
teams want to know the strength of their concrete at the job site in real time. Since maturity is
related to concrete strength, the maturity method is a way to accomplish this without solely
relying on standard test specimens and laboratory testing.
Maturity is calculated by tracking changes in fresh concrete temperature over time. Since
each concrete mix has its own strength-maturity relationship, we can use maturity to estimate the
strength of that mix at any moment after placement. When we know the maturity of a certain
concrete, we can use that concrete‘s specific strength-maturity relationship to make a reliable
estimate of its strength.

Basic Steps

1. Track internal temperatures during curing

2. Use the tracked internal temperature history to calculate maturity
3. Use the strength-maturity relationship to estimate strength
MODULUS OF ELASTICITY
The modulus of elasticity or ―Young‘s Modulus‖ is defined as the slope of the stress-
strain curve within the proportional limit of a material. For a concrete material, the secant
modulus is defined as the slope of the straight line drawn from the origin of axes to the stress-
strain curve at some percentage of the ultimate strength. This is the value most commonly used
in structural design.
Since no portion of the stress-strain curve is a straight line, the usual method of determining the
Young‘s Modulus is to measure the tangent modulus, which is defined as the slope of the tangent
to the stress-strain curve at some percentage of the ultimate strength of the concrete as
determined by compression tests.
From the figure it‘s seen that the secant modulus is almost same to the tangent modulus obtained
at some lower percentage of the ultimate strength.

Significance of elastic modulus of concrete:

The elastic modulus of concrete is a very important mechanical parameter reflecting the ability
of the concrete to deform elastically. For example, in prestressed concrete structures, elastic
shortening of prestressed concrete is one of the main factors contributing to prestress loss.

In addition, in order to make full use of the compressive strength potential, the structures using
high-strength concrete tend to be slimmer and require a higher elastic modulus so as to maintain
its stiffness. Therefore, knowledge of the modulus of high-strength concrete is very important in
avoiding excessive deformation, providing satisfactory serviceability and achieving the most
cost-effective designs.

PERMEABILITY
Permeability in concrete has direct relationship with the durability of the concrete. The
lesser the permeability, the more durable the concrete will be. Permeability will make the
concrete vulnerable to external media attack. These media include water, chemicals, sulfates, and
etc. These external media, once capable of penetrating into concrete it will deteriorate the life
span of that particular concrete structure. For example, water can cause corrosion to steel
reinforcement bar in concrete. The permeability also reduces the resistance of concrete towards
freeze-thaw action. Therefore, permeability is a very important characteristic of that need to be
achieved in any application.

The permeability occurs in hardened concrete in two scenarios; firstly from the trapped
air pockets from incomplete compaction, and secondly from the empty space due to loss of
mixing water by evaporation. In both situations the air space is not good for concrete durability.
It is therefore very important to make that any concrete placed in the formworks gets proper and
adequate compaction. Some contractors might add water to the properly design concrete mix in
order to make it more workable at site. This practice shall not be allowed at all for any reason.
With so much development in concrete technology, now it is possible to do concreting without
the need to compact it (or at least with minimum compaction). This type of concrete is known as
self compacting concrete, which as it name sounds is capable of compacting on its own. It
creates a very highly compacted and dense concrete; thus resulting in low permeability.

Since loss of mixing water is one of the reasons for higher permeability, simply adding
water to concrete will create more air space after evaporation. Therefore, for any concrete to be
watertight, the water-cement ratio shall be as low as possible. According to American Concrete
Institute, for concrete exposed to fresh water the maximum water-cement shall not exceed 0.48,
while this value shall be less than 0.44 if the concrete will be exposed to seawater.

Besides improper compaction and loss of mixing water, there are few other factors that
affect the permeability in concrete. As the age of the concrete increases, the permeability will
reduce. This is because concrete is material that will continue to hydrate over a long period of
time as long as there is a presence of un-hydrated lime. So with the presence of water, the
hydration products will fill the empty spaces in the matrix. Another factor that improves the
permeability is the fineness of cement. Finer cement particles will hydrate much faster; thus
creating the impermeable concrete faster.

Significance
 Permeability of concrete plays an important role in durability because it controls the rate
of entry of moisture that may contain aggressive chemicals and the movement of water
during heating or freezing. Higher the permeability lesser will be the durability
  Permeability of concrete is of interest also in relation to the water-tightness of liquid-
retaining structures. Higher the permeability lesser will be the water-tightness

Test of permeability on concrete

1. Sorptivity Test
ASTM C1585 measures the sorptivity of a concrete specimen that has been conditioned
at a constant relative humidity and then allowed to equilibrate to a presumed stable internal
relative humidity. The specimens are 4-in. (100-mm) diameter, 2-in. (50-mm) long cylinders.
Prior to testing, the specimens are stored in a chamber at a temperature of 122°F (50°C) and a
relative humidity of 80% for 3 days. The target relative humidity of 80% was chosen since this is
a common value observed for in-service bridge decks. The specimens are then sealed in
individual containers and stored in the laboratory at 73°F (23°C) for 2 weeks to allow the
internal relative humidity of the specimens to come to equilibrium. The sides of the specimens
are then sealed with tape and the ends of the specimens opposite the absorbing surface are
covered to impede evaporation from this surface during the test. The specimens are then
weighed, and the absorbing surfaces are exposed to water, either by immersion into a reservoir or
by ponding. At increasing time intervals, the specimens are removed from exposure to water, the
surfaces blotted to remove excess surface water, and the specimens reweighed. Frequent
measurements are made during the first 6 hours of testing, followed by daily measurements for at
least 8 days. The change in mass over time is used to calculate the sorptivity. Typically, the rate
over the first 6 hours is higher than the rate over the succeeding days. These are expressed as
initial and secondary rates, respectively.
2. Chloride Diffusion Coefficient
The chloride diffusion coefficient of concrete can be determined using ASTM C1556.
Test specimens with a minimum dimension of 3 in. (75 mm) across the finished surface and a
minimum length of 3 in. (75 mm) are used. Prior to final preparation for testing, specimens
should be in a state of saturation to minimize the influence of transport mechanisms other than
concentration driven diffusion. The specimens are then allowed to surface dry and the sides and
one end of the specimens sealed. The specimens are then immersed in lime-saturated water for 6
days to complete re-saturation. The specimens are removed from the lime water, rinsed free of
lime and immersed in salt solution. The standard solution is 15% by mass sodium chloride
(NaCl), but other concentrations can be used. Specimens remain immersed in the salt solution for
a minimum of 35 days, with longer periods necessary for high performance concretes with low
permeability. Following exposure to the salt solution, the specimens are rinsed and allowed to
dry for 1 day under laboratory conditions. If the sampling for chloride analysis is delayed more
than 48 hours, the specimens should be sealed in a plastic bag and stored in the laboratory. If
longer than 7 days, the bagged specimens should be frozen until sampling to prevent continued
migration of chloride ions. Samples for chloride analysis are obtained by profile grinding in
incremental depths of 0.04 to 0.08 in. (1 to 2 mm) parallel to the exposed surface. A sample of
the concrete is also obtained prior to the salt exposure to provide its background chloride content.
The samples are analyzed for total acid-soluble chloride content using either AASHTO T
260(3) or ASTM C1152.(4) The results of the chloride analysis tests are used to calculate the
apparent chloride diffusion coefficient by fitting an equation to the data using non-linear
regression analysis.
RCPT
Rapid Chloride Permeability (RCP) test is another method used to figure out concrete
durability; however, is loaded with limitations. The RCP test is the standard test method for
electrical indication of concrete‘s ability to resist chloride ion penetration.
The concrete cylindrical specimens - 50 mm thick are first prepared by coating the dry
side surface with a special sealer and then vacuum conditioning it for 22 hrs as per the ASTM
Codal procedure. The saturated specimens are then mounted in the Plexiglass cells, the sealant
applied and the reservoirs filled with NaCl & NaOH solutions respectively. The cell terminals
are then connected to the Power supply unit through cables provided – one for each channel and
the test started.
The passing current magnitude depends on the ions passing through the pores of the
concrete specimen (including chloride ions), which in turn depend on the permeability of
concrete.
Advantages
 Is relatively quick—can be used for quality control
 Has simple and convenient setup and procedures
 Provides results that are easy to interpret
 Correlates well with 90-day chloride ponding test
Disadvantages
 May not represent the true permeability (or potential permeability) for concrete that
contains supplementary cementitious materials or chemical admixtures
 May allow measurements before a steady state is achieved
 Can cause physical and chemical changes in the specimen, resulting in unrealistic values
 May not be suitable for concretes that contain conducting materials (such as steel or
carbon fibers)
 Has low inherent repeatability and reproducibility

HALF CELL
 What is the Half Cell Potential Test?
In the presence of oxygen and humidity in the concrete, corrosion of the steel bars begins.
A symptom of the corrosion of steel in concrete is the development of macro cells, which is the
co-existence of passive and corroding areas on the same reinforcement bar. The current flow in
the steel is accompanied by an electrical field which is measured at the concrete surface,
identifying the location of the most corroded areas at the most negative values.
This is the basis of the half cell potential testing applied to the routine inspection of reinforced
steel concrete structures. When surface measurements are taken, they are obviously measured
away from the reinforcement due to the concrete cover. The potentials measured are therefore
affected by the potential ohmic drop in the concrete. Several factors have a significant effect on
the potentials measured

 Concrete Cover Depth

 Concrete Resistivity
 High Resistive Surface Layers
 Polarization Effects

 How do we do Half Cell Potential Testing?

To measure half cell potentials, an electrical connection is made to the
steel reinforcement in the concrete member to assess. This is connected to a high impedance
digital multi meter, backed up with a data-logging device. The other connection to the milli-
voltmeter is taken to a copper half cell, which has a porous connection at one end which can be
touched to the concrete surface. This will then register the corrosion potential of the steel
reinforcement nearest to the point of contact. We measure the results on a regular grid and by
plotting results as a contour map areas of corroding steel may readily be seen. We never use this
technique in isolation, but as part of a combined measurement of the chloride content of the
concrete and its variation with depth and also the cover to the steel and the depth of carbonation.
PHENOLPHTHALEIN TEST
Carbonation of concrete is associated with the corrosion of steel reinforcement and with
shrinkage. However, it also increases both the compressive and tensile strength of concrete, so
not all of its effects on concrete are bad.
Carbonation is the result of the dissolution of CO2 in the concrete pore fluid and this
reacts with calcium from calcium hydroxide and calcium silicate hydrate to form calcite
(CaCO3). Aragonite may form in hot conditions.
Within a few hours, or a day or two at most, the surface of fresh concrete will have
reacted with CO2 from the air. Gradually, the process penetrates deeper into the concrete at a rate
proportional to the square root of time. After a year or so it may typically have reached a depth
of perhaps 1 mm for dense concrete of low permeability made with a low water/cement ratio, or
up to 5 mm or more for more porous and permeable concrete made using a high water/cement
ratio.
Testing for carbonation
The affected depth from the concrete surface can be readily shown by the use of
phenolphthalein indicator solution. This is available from chemical suppliers. Phenolphthalein is
a white or pale yellow crystalline material. For use as an indicator it is dissolved in a suitable
solvent such as isopropyl alcohol (isopropanol) in a 1% solution.

The phenolphthalein indicator solution is applied to a fresh fracture surface of concrete. If

the indicator turns purple, the pH is above 8.6. Where the solution remains colorless, the pH of
the concrete is below 8.6, suggesting carbonation. A fully-carbonated paste has a pH of about
8.4. The phenolphthalein indicator solution is applied to a fresh fracture surface of concrete. If
the indicator turns purple, the pH is above 8.6. Where the solution remains colorless, the pH of
the concrete is below 8.6, suggesting carbonation. A fully-carbonated paste has a pH of about
8.4.
In practice, a pH of 8.6 may only give a faintly discernible slightly pink color. A strong,
immediate, color change to purple suggests a pH that is rather higher, perhaps pH 9 or 10.
 Normal concrete pore solution is saturated with calcium hydroxide and also contains
sodium and potassium hydroxide; the pH is typically 13-14. Concrete with a pore solution of pH
10-12 is less alkaline than sound concrete but would still produce a strong color change with
phenolphthalein indicator. It therefore follows that the indicator test is likely to underestimate the
depth to which carbonation has occurred.
In confirmation of this, microscopy - either optical microscopy using thin-sections, or
scanning electron microscopy using polished sections - shows carbonation effects at greater
depths than indicated by phenolphthalein indicator. Nevertheless, this test is very useful as a
means of making an initial assessment - it is quick, easy and widely used.
The indicator has not changed color near the top and bottom surfaces, suggesting that
these near-surface regions are carbonated to a depth of at least 4 mm from the top surface and 6
mm from the lower surface. Where the indicator has turned purple - the center of the slab - the
pH of the concrete pore fluid remains high (above 8.6, probably nearer 10). Whether the cement
paste here is completely uncarbonated is unclear, despite the strong purple indicator color; a
more complete assessment would require microscopic examination. Indicator was not applied to
the concrete at the right of this image and so the concrete here retains its original color.
The carbonation depth is approximately proportional to the square root of time. For example, if
the carbonation depth is 1mm in a one-year-old concrete, it will be about 3mm after 9 years,
5mm after 25 years and 10mm after 100 years.
NON-DESTRUCTIVE TESTING OF CONCRETE
Non destructive test is a method of testing existing concrete structures to assess the
strength and durability of concrete structure. In the non destructive method of testing, without
loading the specimen to failure (i.e. without destructing the concrete) strength of concrete can be
measured. Now days this method has become a part of quality control process. This method of
testing also helps us to investigate crack depth, micro cracks and deterioration of concrete.
Non destructive testing of concrete is a very simple method of testing but it requires
skilled and experienced persons having some special knowledge to interpret and analyze test
results. Various non-destructive methods of testing concrete have been developed to analyze
properties of hardened concrete, which are given below.
1. Surface Hardness Test - These are of indentation type, include the Williams testing pistol
and impact hammers, and are used only for estimation of concrete strength.

2. Rebound Hammer Test - Rebound hammer test (Schmidt Hammer) is used to provide a
convenient and rapid indication of the compressive strength of concrete. It consists of a
spring controlled mass that slides on a plunger within a tubular housing. The operation of
rebound hammer is shown in the figure below. When the plunger of rebound hammer is
pressed against the surface of concrete, a spring controlled mass with a constant energy is
made to hit concrete surface to rebound back. The extent of rebound, which is a measure of
surface hardness, is measured on a graduated scale. This measured value is designated as
Rebound Number (rebound index). A concrete with low strength and low stiffness will
absorb more energy to yield in a lower rebound value.
The rebound hammer test method is used for the following purposes:
(a) To find out the likely compressive strength of concrete with the help of suitable co-relations
between rebound index and compressive strength.
(b) To assess the uniformity of concrete.
(c) To assess the quality of concrete in relation to standard requirements.
(d) To assess the quality of one element of concrete in relation to another.
Principle of Rebound Hammer Test
Rebound hammer test method is based on the principle that the rebound of an elastic
mass depends on the hardness of the concrete surface against which the mass strikes. The
operation of the rebound hammer is shown in figure above. When the plunger of rebound
hammer is pressed against the concrete surface, the spring controlled mass in the hammer
rebounds. The amount of rebound of the mass depends on the hardness of concrete surface. Thus,
the hardness of concrete and rebound hammer reading can be correlated with compressive
strength of concrete. The rebound value is read off along a graduated scale and is
designated as the rebound number or rebound index. The compressive strength can be read
directly from the graph provided on the body of the hammer.
Procedure of Rebound Hammer Test
Procedure for rebound hammer test on concrete structure starts with calibration of the
rebound hammer. For this, the rebound hammer is tested against the test anvil made of steel
having Brinell hardness number of about 5000 N/mm2. After the rebound hammer is tested for
accuracy on the test anvil, the rebound hammer is held at right angles to the surface of the
concrete structure for taking the readings. The test thus can be conducted horizontally on vertical
surface and vertically upwards or downwards on horizontal surfaces as shown in figure below:

Rebound Hammer Positions for Testing Concrete Structure

If the rebound hammer is held at intermediate angle, the rebound number will be different for the
same concrete.
The following points should be observed during testing:
 The concrete surface should be smooth, clean and dry.
 Ant loose particles should be rubbed off from the concrete surface with a grinding wheel
or stone, before hammer testing.
 Rebound hammer test should not be conducted on rough surfaces as a result of
incomplete compaction, loss of grout, spalled or tooled concrete surface.
 The point of impact of rebound hammer on concrete surface should be at least 20mm
away from edge or shape discontinuity.
Six readings of rebound number are taken at each point of testing and an average of value of the
readings is taken as rebound index for the corresponding point of observation on concrete
surface.
3. Penetration test

The Windsor probe is generally considered to be the best means of testing penetration.
Equipment consists of a powder-actuated gun or driver, hardened alloy probes, loaded cartridges,
a depth gauge for measuring penetration of probes and other related equipment. A probe,
diameter 0.25 in. (6.5 mm) and length 3.125 in. (8.0 cm), is driven into the concrete by means of
a precision powder charge. Depth of penetration provides an indication of the compressive
strength of the concrete. Although calibration charts are provided by the manufacturer, the
instrument should be calibrated for type of concrete and type and size of aggregate used.
Limitations and Advantages
The probe test produces quite variable results and should not be expected to give accurate
values of concrete strength. It has, however, the potential for providing a quick means of
checking quality and maturity of in situ concrete. It also provides a means of assessing strength
development with curing. The test is essentially non-destructive, since concrete and structural
members can be tested in situ, with only minor patching of holes on exposed faces.

4. Pullout Techniques
A pull-out test measures, with a special ram, the force required to pull from the concrete a
specially shaped steel rod whose enlarged end has been cast into the concrete to a depth of 3 in.
(7.6 cm). The concrete is simultaneously in tension and in shear, but the force required to pull the
concrete out can be related to its compressive strength. The pull-out technique can thus measure
quantitatively the in-situ strength of concrete when proper correlations have been made. It has
been found, over a wide range of strengths, that pull-out strengths have a coefficient of variation
comparable to that of compressive strength.
Limitations and Advantages
Although pullout tests do not measure the interior strength of mass concrete, they do give
information on the maturity and development of strength of a representative part of it. Such tests
have the advantage of measuring quantitatively the strength of concrete in place. Their main
disadvantage is that they have to be planned in advance and pull-out assemblies set into the
formwork before the concrete is placed. The pull-out, of course, creates some minor damage.
The test can be non-destructive, however, if a minimum pull-out force is applied that stops short
of failure but makes certain that a minimum strength has been reached. This is information of
distinct value in determining when forms can be removed safely.

5. Dynamic or Vibration Tests

At present the ultrasonic pulse velocity method is the only one of this type that shows
potential for testing concrete strength in situ. It measures the time of travel of an ultrasonic pulse
passing through the concrete. The fundamental design features of all commercially available
units are very similar, consisting of a pulse generator and a pulse receiver. Pulses are generated
by shock-exciting piezoelectric crystals, with similar crystals used in the receiver.

Piezoelectric crystals Ultrasonic pulse velocity tester

The time taken for the pulse to pass through the concrete is measured by electronic
measuring circuits. Pulse velocity tests can be carried out on both laboratory-sized specimens
and completed concrete structures, but some factors affect measurement:

1. There must be smooth contact with the surface under test; a coupling medium such as
a thin film of oil is mandatory.
2. It is desirable for path-lengths to be at least 12 in. (30 cm) in order to avoid any errors
introduced by heterogeneity.
3. It must be recognized that there is an increase in pulse velocity at below-freezing
temperature owing to freezing of water; from 5 to 30°C (41 – 86°F) pulse velocities
are not temperature dependent.
 4. The presence of reinforcing steel in concrete has an appreciable effect on pulse
velocity. It is therefore desirable and often mandatory to choose pulse paths that avoid
the influence of reinforcing steel or to make corrections if steel is in the pulse path.

Applications and Limitations

The pulse velocity method is an ideal tool for establishing whether concrete is uniform.
It can be used on both existing structures and those under construction. Usually, if large
differences in pulse velocity are found within a structure for no apparent reason, there is strong
reason to presume that defective or deteriorated concrete is present. High pulse velocity readings
are generally indicative of good quality concrete. A general relation between concrete quality
and pulse velocity is given in Table.

General Conditions Pulse Velocity ft/sec

Excellent Above 15,000
Good 12,000-15,000
Questionable 10,000-12,000
Poor 7,000-10,000
Very Poor below 7,000

Fairly good correlation can be obtained between cube compressive strength and pulse
velocity. These relations enable the strength of structural concrete to be predicted within ±20 per
cent, provided the types of aggregate and mix proportions are constant. The pulse velocity
method has been used to study the effects on concrete of freeze-thaw action, sulphate attack, and
acidic waters. Generally, the degree of damage is related to a reduction in pulse velocity. Cracks
can also be detected. Great care should be exercised, however, in using pulse velocity
measurements for these purposes since it is often difficult to interpret results. Sometimes the
pulse does not travel through the damaged portion of the concrete.

The pulse velocity method can also be used to estimate the rate of hardening and strength
development of concrete in the early stages to determine when to remove formwork. Holes have
to be cut in the formwork so that transducers can be in direct contact with the concrete surface.
As concrete ages, the rate of increase of pulse velocity slows down much more rapidly than the
rate of development of strength, so that beyond the strength of 2,000 to 3,000 psi (13.6 to 20.4
MPa) accuracy in determining strength is less than ±20%. Accuracy depends on careful
calibration and use of the same concrete mix proportions and aggregate in the test samples used
for calibration as in the structure.
In summary, ultrasonic pulse velocity tests have a great potential for concrete control,
particularly for establishing uniformity and detecting cracks or defects. Its use for predicting
strength is much more limited, owing to the large number of variables affecting the relation
between strength and pulse velocity.

5. Radioactive Methods
Radioactive methods of testing concrete can be used to detect the location of
reinforcement, measure density and perhaps establish whether honeycombing has occurred in
structural concrete units.
Gamma radiography is increasingly accepted in England and Europe. The equipment is
quite simple and running costs are small, although the initial price can be high. Concrete up to 18
in. (45 cm) thick can be examined without difficulty.
 Radioactive Methods

CONCEPT OF PROPORTIONING CONCRETE MIXES

Introduction
The process of selecting suitable ingredients of concrete and determining their relative
amounts with the objective of producing a concrete of the required, strength, durability, and
workability as economically as possible, is termed the concrete mix design. The proportioning of
ingredient of concrete is governed by the required performance of concrete in 2 states, namely
the plastic and the hardened states. If the plastic concrete is not workable, it cannot be properly
placed and compacted. The property of workability, therefore, becomes of vital importance.
The compressive strength of hardened concrete which is generally considered to be an
index of its other properties, depends upon many factors, e.g. quality and quantity of cement,
water and aggregates; batching and mixing; placing, compaction and curing. The cost of concrete
is made up of the cost of materials, plant and labor. The variations in the cost of materials arise
from the fact that the cement is several times costly than the aggregate, thus the aim is to produce
as lean a mix as possible. From technical point of view the rich mixes may lead to high shrinkage
and cracking in the structural concrete, and to evolution of high heat of hydration in mass
concrete which may cause cracking.
The actual cost of concrete is related to the cost of materials required for producing a
minimum mean strength called characteristic strength that is specified by the designer of the
structure. This depends on the quality control measures, but there is no doubt that the quality
control adds to the cost of concrete. The extent of quality control is often an economic
compromise, and depends on the size and type of job. The cost of labour depends on the
workability of mix, e.g., a concrete mix of inadequate workability may result in a high cost of
labour to obtain a degree of compaction with available equipment.

Requirements of concrete mix design

 The requirements which form the basis of selection and proportioning of mix ingredients
are The minimum compressive strength required from structural consideration
 The adequate workability necessary for full compaction with the compacting equipment
available.
 Maximum water-cement ratio and/or maximum cement content to give adequate
durability for the particular site conditions
 Maximum cement content to avoid shrinkage cracking due to temperature cycle in mass
concrete.
Types of Mixes
1. Nominal Mixes
In the past the specifications for concrete prescribed the proportions of cement,
fine and coarse aggregates. These mixes of fixed cement-aggregate ratio which ensures
adequate strength are termed nominal mixes. These offer simplicity and under normal
circumstances, have a margin of strength above that specified. However, due to the
variability of mix ingredients the nominal concrete for a given workability varies widely
in strength.
 2. Standard mixes
The nominal mixes of fixed cement-aggregate ratio (by volume) vary widely in
strength and may result in under- or over-rich mixes. For this reason, the minimum
compressive strength has been included in many specifications. These mixes are termed
standard mixes.
IS 456-2000 has designated the concrete mixes into a number of grades as M10,
M15, M20, M25, M30, M35 and M40. In this designation the letter M refers to the mix
and the number to the specified 28 day cube strength of mix in N/mm2. The mixes of
grades M10, M15, M20 and M25 correspond approximately to the mix proportions
(1:3:6), (1:2:4), (1:1.5:3) and (1:1:2) respectively.
3. Designed Mixes
In these mixes the performance of the concrete is specified by the designer but the
mix proportions are determined by the producer of concrete, except that the minimum
cement content can be laid down. This is most rational approach to the selection of mix
proportions with specific materials in mind possessing more or less unique
characteristics. The approach results in the production of concrete with the appropriate
properties most economically. However, the designed mix does not serve as a guide since
this does not guarantee the correct mix proportions for the prescribed performance.
For the concrete with undemanding performance nominal or standard mixes
(prescribed in the codes by quantities of dry ingredients per cubic meter and by slump)
may be used only for very small jobs, when the 28-day strength of concrete does not
exceed 30 N/mm2. No control testing is necessary reliance being placed on the masses of
the ingredients.

Factors affecting the choice of mix proportions

The various factors affecting the mix design are:

1. Compressive strength
It is one of the most important properties of concrete and influences many other
describable properties of the hardened concrete. The mean compressive strength required
at a specific age, usually 28 days, determines the nominal water-cement ratio of the mix.
The other factor affecting the strength of concrete at a given age and cured at a prescribed
temperature is the degree of compaction. According to Abraham‘s law the strength of
fully compacted concrete is inversely proportional to the water-cement ratio.
2. Workability
The degree of workability required depends on three factors. These are the size of
the section to be concreted, the amount of reinforcement, and the method of compaction
to be used. For the narrow and complicated section with numerous corners or inaccessible
parts, the concrete must have a high workability so that full compaction can be achieved
with a reasonable amount of effort. This also applies to the embedded steel sections. The
desired workability depends on the compacting equipment available at the site.
3. Durability
The durability of concrete is its resistance to the aggressive environmental
conditions. High strength concrete is generally more durable than low strength concrete.
In the situations when the high strength is not necessary but the conditions of exposure
are such that high durability is vital, the durability requirement will determine the water-
cement ratio to be used.
4. Maximum nominal size of aggregate
In general, larger the maximum size of aggregate, smaller is the cement
requirement for a particular water-cement ratio, because the workability of concrete
increases with increase in maximum size of the aggregate. However, the compressive
strength tends to increase with the decrease in size of aggregate.
IS 456:2000 and IS 1343:1980 recommend that the nominal size of the aggregate
should be as large as possible.
5. Grading and type of aggregate
The grading of aggregate influences the mix proportions for a specified
workability and water-cement ratio. Coarser the grading leaner will be mix which can be
used. Very lean mix is not desirable since it does not contain enough finer material to
make the concrete cohesive.
The type of aggregate influences strongly the aggregate-cement ratio for the
desired workability and stipulated water cement ratio. An important feature of a
 satisfactory aggregate is the uniformity of the grading which can be achieved by mixing
different size fractions.
6. Quality Control
The degree of control can be estimated statistically by the variations in test
results. The variation in strength results from the variations in the properties of the mix
ingredients and lack of control of accuracy in batching, mixing, placing, curing and
testing. The lower the difference between the mean and minimum strengths of the mix
lower will be the cement-content required. The factor controlling this difference is termed
as quality control.

METHODS OF MIX DESIGN

Cement Concrete Mix Design means, determination of the proportion of the concrete ingredients
i.e. Cement, Water, Fine aggregate, Coarse aggregate which would produce concrete possessing
specified properties such as Workability, Strength and Durability with maximum overall
economy. There are various methods followed for Mix Design. In this chapter, the discussion
will be on two methods as follows;
 I.S. Method
 A.C.I. Method

INDIAN STANDARD METHOD OF MIX DESIGN OF CONCRETE

The Indian Standard (First Revision) was adopted by the Bureau of Indian Standards
(BIS), after the draft finalized by the Cement and Concrete Sectional Committee had been
approved by the Civil Engineering Division Council.
This standard was first published in 1982. In this first revision, the following major
modifications have been made:
 The title of the standard has been modified as 'Concrete mix proportioning - Guidelines'
from the earlier title 'Recommended guidelines for concrete mix design'.
 The applicability of the standard has been specified for ordinary and standard concrete
grades only.
 Various requirements have been modified in line with the requirements of IS 456: 2000
'Plain and reinforced concrete - Code of practice (fourth revision).
  The requirements for selection of water-cement ratio, water content and estimation of
coarse aggregate content and fine aggregate content have been reviewed and accordingly
modified. Similarly, other requirements such as trial mixes, illustrative examples, etc,
have also been reviewed and modified.
 A new illustrative example of concrete mix proportioning using fly ash as one of the
ingredients has been added.
 Considering that the air content in normal (non -air entrained) concrete is not of much
significance in mix proportioning procedure and is also not a part of IS 456: 2000, the
consideration of air content has been deleted.
The following points should be remembered before proportioning a concrete mix a per IS-10262-
2009.

 This method of concrete mix proportioning is applicable only for ordinary and standard
concrete grades.
 The air content in concrete is considered as nil.
 The proportioning is carried out to achieve specified characteristic compressive strength
at specified age, workability of fresh concrete and durability requirements.

This method of concrete mix design consist of following 11 steps

1. Design specification
2. Testing of materials
3. Calculating target strength for mix proportioning
4. Selecting water/cement ratio
5. Calculating water content
6. Calculating cement content
7. Finding out volume proportions for Coarse aggregate & fine aggregate
8. Mix calculations
9. Trial mixing
10. Workability measurement (using slump cone method)
11. Repeating step 9 & 10 until all requirements is fulfilled.
STEP 1 - DESIGN SPECIFICATIONS
This is the step where we gather all the required information for designing a concrete mix
from the client. The data required for mix proportioning is as follows.

 Grade designation (whether M10, M15, M20 etc)

 Type of cement to be used
 Maximum nominal size of aggregates
 Minimum & maximum cement content
 Maximum water-cement ratio
 Workability
 Exposure conditions (As per IS-456-Table-4)
 Maximum temperature of concrete at the time of placing
 Method of transporting & placing
 Early age strength requirement (if any)
 Type of aggregate (angular, sub angular, rounded etc)
 Type of admixture to be used (if any)

STEP 2 - TESTING OF MATERIALS

The table given below shows the list of most necessary tests to be done on cement, coarse
aggregate, fine aggregate and admixture. After doing the test, store the test data for further
calculation.

Concrete
Tests to be done
Ingredients

Cement Specific gravity — — —

Coarse Water Free surface

Specific gravity Sieve analysis
aggregate absorption moisture
 Water Free surface
Fine aggregate Specific gravity Sieve analysis
absorption moisture

Admixture
Specific gravity — — —
(if any)

STEP 3 - TARGET STRENGTH CALCULATION

Calculate the target compressive strength of concrete using the formula given below.

f’ck= fck + 1.65s

Where,
f’ck= Target compressive strength at 28 days in N/mm2.
fck = Characteristic compressive strength at 28 days in N/mm2 (same as grade of concrete, see
table
below)
s = Standard deviation
The value of standard deviation, given in the table below, can be taken for initial calculation.

Sl. Grade of Characteristic Assumed standard deviation

No. Concrete compressive strength (N/mm2)
(N/mm2)
1 M10 10 3.5
2 M15 15
3 M20 20 4.0
4 M25 25
5 M30 30 6.0
6 M35 35
7 M40 40
8 M45 45
9 M50 50
10 M55 55
STEP 4 - SELECTION OF WATER-CEMENT RATIO
For preliminary calculation, water cement ratio as given is IS-456-Table 5 (also given
below) for different environmental exposure condition, may be used.
Note - Use Table-1 for finding out water-cement ratio of Plain Concrete and use Table-2 for
finding out water-cement ratio of Reinforced Concrete.
Table -1
Sl.No. Environmental Plain Concrete
Exposure Condition
Minimum Cement Maximum Free Minimum
Content (kg/m3) Water-Cement Grade of
Ratio Concrete
1 Mild 220 0.60 —
2 Moderate 240 0.60 M15
3 Severe 250 0.50 M20
4 Very Severe 260 0.45 M20
5 Extreme 280 0.40 M25
Table -2

Reinforced Concrete

Environmental Maximum
Sl.No. Exposure Minimum Free Minimum
Condition Cement Content Water- Grade of
(kg/m3) Cement Concrete
Ratio
1 Mild 300 0.55 M20
2 Moderate 300 0.50 M25
3 Severe 320 0.45 M30
4 Very Severe 340 0.45 M35
5 Extreme 360

Refer the table given below (As per IS-456) to choose right type of environment depending upon
different exposure conditions to concrete.
 Sl. No. Environment Exposure condition

1 Mild Concrete surfaces protected against weather or aggressive

conditions, except those situated in coastal areas.

2 Moderate Concrete surfaces sheltered from severe rain or freezing whilst wet
Concrete exposed to condensation and rain

Concrete continuously under water

Concrete in contact or buried under non aggressive soil/ground

water

Concrete surfaces sheltered from saturated salt air in coastal area

3 Severe Concrete surfaces exposed to severe rain, alternate wetting and

drying or occasional freezing whilst wet or severe condensation
Concrete completely immersed in sea water
Concrete exposed to coastal environment

4 Very severe Concrete surfaces exposed to sea water spray, corrosive fumes or
severe freezing condition whilst wet Concrete in contact with or
buried under aggressive sub-soil/ground water
5 Extreme Surface members in tidal zone Members in direct contact with
liquid/solid aggressive chemicals
STEP 5 - SELECTION OF WATER CONTENT

Selection of water content depends upon a number of factors such as

 Aggregate size, shape & texture

 Workability
 Water cement ratio
 Type of cement and its amount
 Type of admixture and environmental conditions.
Factors that can reduce water demand are as follows

 Using increased aggregate size

 Reducing water cement ratio
 Reducing the slump requirement
 Using rounded aggregate
 Using water reducing admixture

Factors that can increase water demand are as follows

 Increased temp. at site

 Increased cement content
 Increased slump
 Increased water cement ratio
 Increased aggregate angularity
 Decrease in proportion of the coarse aggregate to fine aggregate

The quantity of maximum mixing water per unit volume of concrete may be selected from the
table given below.

Maximum water content per cubic meter of concrete for nominal maximum size of
aggregate

Sl. No. Nominal maximum size of aggregate Maximum water content

1 10 208

2 20 186

3 40 165
The values given in the table shown above is applicable only for angular coarse aggregate and
for a slump value in between 25 to 50mm.

Do the following adjustments if the material used differs from the specified condition.

Type of material/condition Adjustment required

For sub angular aggregate Reduce the selected value by 10kg

For gravel with crushed stone Reduce the selected value by 20kg

For rounded gravel Reduce the selected value by 25kg

For every addition of 25mm slump Increase the selected value by 3%

If using plasticizer Decrease the selected value by 5-10%

If using super plasticizer Decrease the selected value by 20-30%

Note - Aggregates should be used in saturated surface dry condition. While computing the
requirement of mixing water, allowance shall be made for the free surface moisture contributed
by the fine and coarse aggregates. On the other hand, if the aggregate are completely dry, the
amount of mixing water should be increased by an amount equal to moisture likely to be
absorbed by the aggregate

STEP 6 - CALCULATING CEMENTIOUS MATERIAL CONTENT

From the water cement ratio and the quantity of water per unit volume of cement,
calculate the amount of cementious material. After calculating the quantity of cementious
material, compare it with the values given in the table shown in Step-4. The greater of the two
values is then adopted.

If any mineral admixture (such as fly ash) is to be used, then decide the percentage of
mineral admixture to be used based on project requirement and quality of material.

STEP 7 - FINDING OUT VOLUME PROPORTIONS FOR COARSE AGGREGATE &

FINE AGGREGATE

Volume of coarse aggregate corresponding to unit volume of total aggregate for different
zones of fine aggregate is given in the following table.

Nominal Volume of coarse aggregate per unit volume of total

aggregate for different zones of fine aggregate
Maximum

Sl. No. Size of

Aggregate Zone IV Zone III Zone II Zone I

(mm)

1 10 0.50 0.48 0.46 0.44

2 20 0.66 0.64 0.62 0.60

3 40 0.75 0.73 0.71 0.69

The values given in the table shown above is applicable only for a water-cement ratio of 0.5 and
based on aggregates in saturated surface dry condition.

If water-cement ratio other than 0.5 is to be used then apply correction using the rule given
below.

Rule- For every increase or decrease by 0.05 in water-cement ratio, the above values will be
decreased or increased by 0.01, respectively.
If the placement of concrete is done by a pump or where is required to be worked around
congested reinforcing steel, it may be desirable to reduce the estimated coarse aggregate content
determined as above, up to 10 percent.

After calculating volume of coarse aggregate, subtract it from 1, to find out the volume of fine
aggregate.

STEP 8 - MIX CALCULATIONS

The mix calculations per unit volume of concrete shall be done as follows.

1 Volume of concrete 1m3

(Mass of cement/specific gravity of

2 Volume of cement
cement)*(1/1000)

(Mass of water/specific gravity of

3 Volume of water
water)*(1/1000)

(Mass of admixture/specific gravity of

4 Volume of admixture
admixture)*(1/1000)

5 Volume of total aggregate (C.A+F.A) [a-(b+c+d)]

e*Volume of coarse aggregate*specific

6 Mass of coarse aggregate
gravity of coarse aggregate*1000

e*Volume of fine aggregate*specific gravity

7 Mass of fine aggregate
of fine aggregate*1000

STEP 9 - TRIAL MIXES

Conduct a trial mix as per the amount of material calculated above.

STEP 10 - MEASUREMENT OF WORKABILITY (BY SLUMP CONE METHOD)

The workability of the trial mix no.1 shall be measured. The mix shall be carefully
observed for freedom from segregation and bleeding and its finishing properties.

STEP 11 - REPEATING TRIAL MIXES

If the measured workability of trial mix no.1 is different from stipulated value, the water
and/or admixture content shall be adjusted suitably. With this adjustment, the mix proportion
shall be recalculated keeping the free water-cement ratio at pre-selected value.

Trial-2 – increase water or admixture, keeping water-cement ratio constant

Trial-3 – Keep water content same as trial-2, but increase water-cement ratio by 10%.

Trial-4 – Keep water content same as trial-2, but decrease water-cement ratio by 10%

Trial mix no 2 to 4 normally provides sufficient information, including the relationship between
compressive strength and water-cement ratio.

ACI METHOD CONCRETE MIX DESIGN

American Concrete Institute Method of Mix Design 11.3 - this method

of proportioning was first published in 1944 by ACI committee 613. In 1954 the method was
revised to include, among other modifications, the use of entrained air. In 1970, the method of
ACI mix design became the responsibility of ACI committee 211. The latest is the ACI
Committee 211.1 method.
It has the advantages of simplicity in that it:
1. Applies equally well
2. With more or less identical procedure to rounded or angular aggregate
3. To regular or light weight aggregates
4. To air entrained or non-air-entrained concretes.
The ACI Standard 211.1 is a ―Recommended Practice for Selecting Proportions
for Concrete‖.
The procedure is as follows:
Step 1 - Choice of slump
Step 2 - Choice of maximum size of aggregate
Step 3 - Estimation of mixing water and air content
Step 4 - Selection of water/cement ratio
Step 5 - Calculation of cement content
Step 6 - Estimation of coarse aggregate content
Step 7 - Estimation of Fine Aggregate Content
Step 8 - Adjustments for Aggregate Moisture
Step 9 - Trial Batch Adjustments

Step 1 - Choice of slump

If slump is not specified, a value appropriate for the work can be selected from the below
Table which is reproduced from the text book below*, (note that the table numbers are given
from the text book rather than the ACI standard).
Slump
Type of Construction
(mm)
(inches)
Reinforced foundation walls and footings 25 - 75 1-3
Plain footings, caissons and substructure
25 - 75 1-3
walls
Beams and reinforced walls 25 - 100 1-4
Building columns 25 - 100 1-4
Pavements and slabs 25 - 75 1-3
Mass concrete 25 - 50 1-2

Step 2 - Choice of maximum size of aggregate

Large maximum sizes of aggregates produce fewer voids than smaller sizes. Hence,
concretes with the larger-sized aggregates require less mortar per unit volume of concrete, and of
coarse it is the mortar which contains the most expensive ingredient, cement. Thus the ACI
method is based on the principle that the maximum size of aggregate should be the largest
available so long it is consistent with the dimensions of the structure.
ACI 211.1 states that the maximum CA size should not exceed
 One-fifth of the narrowest dimension between sides of forms,
 One-third the depth of slabs,
 3/4th of the minimum clear spacing between individual reinforcing bars, bundles of bars,
or pre-tensioning strands.
Special Note: When high strength concrete is desired, best results may be obtained with reduced
maximum sizes of aggregate since these produce higher strengths at a given w/c ratio.

Step 3 - Estimation of mixing water and air content

The ACI Method uses past experience to give a first estimate for the quantity of water per
unit volume of concrete required to produce a given slump. In general the quantity of water per
unit volume of concrete required to produce a given slump is dependent on the maximum CA
size, the shape and grading of CA and FA, as well as the amount of entrained air.
The approximate amount of water required for average aggregates is given in Table 1 below.
Table 1 - Approximate mixing water and air content requirements for different slumps and
maximum aggregate sizes.
Step 4 - Selection of water/cement ratio
The required water/cement ratio is determined by strength, durability and finishing. The
appropriate value is chosen from prior testing of a given system of cement and aggregate or a
value is chosen from Table 2 and/or Table 3
Table 2 - Water-Cement ratio and compressive strength relationship
Table 3 - Water-Cement Ratio and Compressive Strength Relationship

Step 5 - Calculation of cement content

The amount of cement is fixed by the determinations made in Steps 3 and 4 above.
Step 6 - Estimation of coarse aggregate content
The most economical concrete will have as much as possible space occupied by CA since
it will require no cement in the space filled by CA.

Notes
 These values can be increased by up to about 10 percent for pavement applications.
 Coarse aggregate volumes are based on oven-dry-rodded weights obtained in
accordance with ASTM C 29
The ACI method is based on large numbers of experiments which have shown that for
properly graded materials, the finer the sand and the larger the size of the particles in the
CA, the more volume of CA can be used to produce a concrete of satisfactory workability.

Step 7 - Estimation of Fine Aggregate Content

At the completion of Step 6, all ingredients of the concrete have been estimated except
the fine aggregate. Its quantity can be determined by difference if the ―absolute volume‖
displaced by the known ingredients-, (i.e., water, air, cement, and coarse aggregate), is subtracted
from the unit volume of concrete to obtain the required volume of fine aggregate. Then once the
volumes are know the weights of each ingredient can be calculated from the specific gravities.
Step 8 - Adjustments for Aggregate Moisture
Aggregate weights Aggregate volumes are calculated based on oven dry unit weights, but
aggregate is typically batched based on actual weight. Therefore, any moisture in the aggregate
will increase its weight and stockpiled aggregates almost always contain some moisture. Without
correcting for this, the batched aggregate volumes will be incorrect.
Amount of mixing water If the batched aggregate is anything but saturated surface dry it will
absorb water (if oven dry or air dry) or give up water (if wet) to the cement paste. This causes a
net change in the amount of water available in the mix and must be compensated for by adjusting
the amount of mixing water added.

Step 9 - Trial Batch Adjustments

The ACI method is written on the basis that a trial batch of concrete will be prepared in
the laboratory, and adjusted to give the desired slump, freedom from segregation, finishing,
unit weight, air content and strength.

TESTING, EVALUATION AND CONTROL OF CONCRETE QUALITY

Satisfactory concrete construction and performance requires concrete with specific
properties. To assure that these properties are obtained, quality control and acceptance testing are
indispensable parts of the construction process. Test results provide important feedback used to
base decisions regarding mix adjustments. However, past experience and sound judgment must
be relied on in evaluating tests and assessing their significance in controlling the design, batching
and placement processes that influence the ultimate performance of the concrete.
Specifiers are moving toward performance-based specifications (also called end-result or
end-property specifications) that require the final performance of concrete be achieved
independent of the process used to achieve the performance. Physical tests and concrete
properties are used to measure acceptance. Such specifications may not have acceptance limits
for process control tests such as slump or limits on the quantities of concrete ingredients as do
prescriptive specifications. The end result of compressive strength, low permeability,
documented durability, and a minimal number of cracks, for example, would be the primary
measure of acceptance. Of course, even though process control tests may not be specified, the
wise concrete producer would use them to guide the product to a successful end result.
Project specifications may affect

 Characteristics of the mixture, such as maximum size of aggregate, aggregate

proportions, or minimum cement content;
 Characteristics of the cement, water, aggregates, and admixtures; and
 Characteristics of the freshly mixed and hardened concrete, such as temperature, slump,
air content, and compressive or flexural strengths.
Cementitious materials are tested for their compliance with CSA (ASTM) standards to
avoid any abnormal performance such as early stiffening, delayed setting, or low strengths in
concrete. Standards for Cementitious materials are contained in CSA A-3000-98, Cementitious
Materials Compendium.

Tests of aggregates have two major purposes:

 To determine the suitability of the material itself for use in concrete, including tests for
abrasion, soundness against saturated freeze-thaw cycles, harmful materials by petro
graphic examination, and potential alkali-aggregate reactivity; and
 To assure uniformity, such as tests for moisture control, relative density, and gradation of
aggregates.
 To determine their potential alkali-aggregate

Tests of concrete are:

 To evaluate the performance of available materials,
 To establish mixture proportions, and
 To control concrete quality during construction
Slump, air content, and strength tests are usually required in project specifications for
concrete quality control, whereas density is more useful in mixture proportioning. The slump,
air-content, and temperature tests should be made when strength specimens are made.