TRANSFORMER TESTING LAB

MEASUREMENT UNCERTAINTY
CALCULATION
Job Description: Standard Gas Mixture
Test Name: Dissolved Gas Analysis (Hydrogen)
Equipments used: DGA Test Kit Syringe
Make AGILENT AGILENT
S.No SL CN 16483114 NABL/LAB/EQ/082
Range: H2: 0.5-5000 ppm Upto 10 ml
Accuracy: 1.0000% 1.00%
Uncertainty from calibration certificate: 3.90000% 0.12%
Resolution: 0.001 1

No. of measurements:(n) : 6 Unit of measurement: PPM

Sr No. Measured value

1 10.212
2 10.345
3 10.398
4 10.091
5 10.022
6 10.021

1 n
Avg measurement: X 
n
i 1
X i
10.18161

Type A Estimation

Standard deviation ( S ) 
n
x i  X 2 0.163655421444
 i 1

n 1

Std deviation of mean (= S/√n) 0.06681204603

UA in % ( = std deviation of mean/Avg Measurement*100) 0.6562030%

Type B Estimation
DGA Test Kit
Ub1( = Uncertainty from calibration certificate/2) Type B, Normal 1.950000%
Ub2 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub3 (= resolution/(2*√3) Type B, Rectangular 0.002835%
Syringe
Ub4( = Uncertainty from calibration certificate/2) Type B, Normal 0.060000%
Ub5 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub6 (= resolution/(2*√3) Type B, Rectangular 2.886751%

UB in % (= √Ub1*Ub1+Ub2*Ub2+Ub3*Ub3) 3.57856%

Combined uncertainty Uc (= √UA*UA+UB*UB) 3.63823%

In terms of abosolute value:( % value*mean/100) 0.370430357292 Unit: PPM

Veff (= (n-1)*Uc4/UA4 ) 4724.73 Infinity

K 2

Expanded uncertainty in% 7.27646%

Expanded uncertainty in value 0.740861 Unit: PPM

Preapred by : Testing Engineer Reviewed & Approved by : Technical Manager

Issue Date: 01.10.2019 Retention: TIll Change F No:PML/TTL/F/7.6/01 Rev 0

 TRANSFORMER TESTING LAB
MEASUREMENT UNCERTAINTY
CALCULATION
Job Description: Standard Gas Mixture
Test Name: Dissolved Gas Analysis (Carbon Dioxide CO2)
Equipments used: DGA Test Kit Syringe
Make AGILENT AGILENT
S.No SL CN 16483114 NABL/LAB/EQ/082
Range: 5-50000 ppm Upto 10 ml
Accuracy: 5.0000% 1.00%
Uncertainty from calibration certificate: 0.67000% 0.12%
Resolution: 0.001 1

No. of measurements:(n) : 6 Unit of measurement: PPM

Sr No. Measured value

1 103.60007
2 104.68728
3 104.84054
4 103.60000
5 103.94375
6 103.77274

1 n
Avg measurement: X 
n
i 1
X i
104.07406

Type A Estimation

Standard deviation ( S ) 
n
x i  X 2 0.551489655557
 i 1

n 1

Std deviation of mean (= S/√n) 0.22514470909

UA in % ( = std deviation of mean/Avg Measurement*100) 0.2163312%

Type B Estimation
DGA Test Kit
Ub1( = Uncertainty from calibration certificate/2) Type B, Normal 0.335000%
Ub2 ( = accuracy/√3) Type B, Rectangular 2.886751%
Ub3 (= resolution/(2*√3) Type B, Rectangular 0.000277%
Syringe
Ub4( = Uncertainty from calibration certificate/2) Type B, Normal 0.060000%
Ub5 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub6 (= resolution/(2*√3) Type B, Rectangular 0.002887%

UB in % (= √Ub1*Ub1+Ub2*Ub2+Ub3*Ub3) 2.96353%

Combined uncertainty Uc (= √UA*UA+UB*UB) 2.97141%

In terms of abosolute value:( % value*mean/100) 3.092470959343 Unit: PPM

Veff (= (n-1)*Uc4/UA4 ) 177969

K 2

Expanded uncertainty in% 5.94283%

Expanded uncertainty in value 6.184942 Unit: PPM

Preapred by : Testing Engineer Reviewed & Approved by : Technical Manager

Issue Date: 01.10.2019 Retention: TIll Change F No:PML/TTL/F/7.6/01 Rev 0

 TRANSFORMER TESTING LAB
MEASUREMENT UNCERTAINTY
CALCULATION
Job Description: Standard Gas Mixture
Test Name: Dissolved Gas Analysis (Carbon Monoxide CO)
Equipments used: DGA Test Kit Syringe
Make AGILENT AGILENT
S.No SL CN 16483114 NABL/LAB/EQ/082
Range: 1-50000 ppm Upto 10 ml
Accuracy: 5.0000% 1.00%
Uncertainty from calibration certificate: 1.30000% 0.12%
Resolution: 0.001 1

No. of measurements:(n) : 6 Unit of measurement: PPM

Sr No. Measured value

1 60.00036
2 60.27323
3 60.14674
4 60.43428
5 60.54423
6 60.59261

1 n
Avg measurement: X 
n
i 1
X i
60.33191

Type A Estimation

Standard deviation ( S ) 
n
x i  X 2 0.232886480107
 i 1

n 1

Std deviation of mean (= S/√n) 0.095075507376

UA in % ( = std deviation of mean/Avg Measurement*100) 0.1575874%

Type B Estimation
DGA Test Kit
Ub1( = Uncertainty from calibration certificate/2) Type B, Normal 0.650000%
Ub2 ( = accuracy/√3) Type B, Rectangular 2.886751%
Ub3 (= resolution/(2*√3) Type B, Rectangular 0.000478%
Syringe
Ub4( = Uncertainty from calibration certificate/2) Type B, Normal 0.060000%
Ub5 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub6 (= resolution/(2*√3) Type B, Rectangular 0.002887%

UB in % (= √Ub1*Ub1+Ub2*Ub2+Ub3*Ub3) 3.01542%

Combined uncertainty Uc (= √UA*UA+UB*UB) 3.01954%

In terms of abosolute value:( % value*mean/100) 1.821744827864 Unit: PPM

Veff (= (n-1)*Uc4/UA4 ) 673978

K 2

Expanded uncertainty in% 6.03908%

Expanded uncertainty in value 3.643490 Unit: PPM

Preapred by : Testing Engineer Reviewed & Approved by : Technical Manager

Issue Date: 01.10.2019 Retention: TIll Change F No:PML/TTL/F/7.6/01 Rev 0

 TRANSFORMER TESTING LAB
MEASUREMENT UNCERTAINTY
CALCULATION
Job Description: Standard Gas Mixture
Test Name: Dissolved Gas Analysis (Ethylene C2H4)
Equipments used: DGA Test Kit Syringe
Make AGILENT AGILENT
S.No SL CN 16483114 NABL/LAB/EQ/082
Range: 0.1-50000 ppm Upto 10 ml
Accuracy: 1.0000% 1.00%
Uncertainty from calibration certificate: 4.80000% 0.12%
Resolution: 0.001 1

No. of measurements:(n) : 6 Unit of measurement: PPM

Sr No. Measured value

1 5.08774
2 5.13003
3 5.13620
4 5.12000
5 5.16768
6 5.12312

1 n
Avg measurement: X 
n
i 1
X i
5.12746

Type A Estimation

Standard deviation ( S ) 
n
x i  X 2 0.025895198332
 i 1

n 1

Std deviation of mean (= S/√n) 0.01057167045

UA in % ( = std deviation of mean/Avg Measurement*100) 0.2061775%

Type B Estimation
DGA Test Kit
Ub1( = Uncertainty from calibration certificate/2) Type B, Normal 2.400000%
Ub2 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub3 (= resolution/(2*√3) Type B, Rectangular 0.005630%
Syringe
Ub4( = Uncertainty from calibration certificate/2) Type B, Normal 0.060000%
Ub5 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub6 (= resolution/(2*√3) Type B, Rectangular 0.002887%

UB in % (= √Ub1*Ub1+Ub2*Ub2+Ub3*Ub3) 2.53580%

Combined uncertainty Uc (= √UA*UA+UB*UB) 2.54417%

In terms of abosolute value:( % value*mean/100) 0.130451491173 Unit: PPM

Veff (= (n-1)*Uc4/UA4 ) 115929

K 2

Expanded uncertainty in% 5.08835%

Expanded uncertainty in value 0.260903 Unit: PPM

Preapred by : Testing Engineer Reviewed & Approved by : Technical Manager

Issue Date: 01.10.2019 Retention: TIll Change F No:PML/TTL/F/7.6/01 Rev 0

 TRANSFORMER TESTING LAB
MEASUREMENT UNCERTAINTY
CALCULATION
Job Description: Standard Gas Mixture
Test Name: Dissolved Gas Analysis (Ethane C2H6)
Equipments used: DGA Test Kit Syringe
Make AGILENT AGILENT
S.No SL CN 16483114 NABL/LAB/EQ/082
Range: 0.1-50000 ppm Upto 10 ml
Accuracy: 1.0000% 1.00%
Uncertainty from calibration certificate: 4.20000% 0.12%
Resolution: 0.001 1

No. of measurements:(n) : 6 Unit of measurement: PPM

Sr No. Measured value

1 4.87012
2 4.82413
3 4.92804
4 4.83460
5 4.86818
6 4.89334

1 n
Avg measurement: X 
n
i 1
X i
4.86973

Type A Estimation

Standard deviation ( S ) 
n
x i  X 2 0.038140580882
 i 1

n 1

Std deviation of mean (= S/√n) 0.015570826942

UA in % ( = std deviation of mean/Avg Measurement*100) 0.3197469%

Type B Estimation
DGA Test Kit
Ub1( = Uncertainty from calibration certificate/2) Type B, Normal 2.100000%
Ub2 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub3 (= resolution/(2*√3) Type B, Rectangular 0.005928%
Syringe
Ub4( = Uncertainty from calibration certificate/2) Type B, Normal 0.060000%
Ub5 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub6 (= resolution/(2*√3) Type B, Rectangular 0.002887%

UB in % (= √Ub1*Ub1+Ub2*Ub2+Ub3*Ub3) 2.25395%

Combined uncertainty Uc (= √UA*UA+UB*UB) 2.27652%

In terms of abosolute value:( % value*mean/100) 0.110860543773 Unit: PPM

Veff (= (n-1)*Uc4/UA4 ) 12848

K 2

Expanded uncertainty in% 4.55304%

Expanded uncertainty in value 0.221721 Unit: PPM

Preapred by : Testing Engineer Reviewed & Approved by : Technical Manager

Issue Date: 01.10.2019 Retention: TIll Change F No:PML/TTL/F/7.6/01 Rev 0

 TRANSFORMER TESTING LAB
MEASUREMENT UNCERTAINTY
CALCULATION
Job Description: Standard Gas Mixture
Test Name: Dissolved Gas Analysis (Methane CH4)
Equipments used: DGA Test Kit Syringe
Make AGILENT AGILENT
S.No SL CN 16483114 NABL/LAB/EQ/082
Range: 0.1-50000 ppm Upto 10 ml
Accuracy: 1.0000% 1.00%
Uncertainty from calibration certificate: 4.40000% 0.12%
Resolution: 0.001 1

No. of measurements:(n) : 6 Unit of measurement: PPM

Sr No. Measured value

1 4.90039
2 4.90060
3 4.89811
4 4.77953
5 4.88019
6 4.98214

1 n
Avg measurement: X 
n
i 1
X i
4.89016

Type A Estimation

Standard deviation ( S ) 
n
x i  X 2 0.064923904997
 i 1

n 1

Std deviation of mean (= S/√n) 0.026505073225

UA in % ( = std deviation of mean/Avg Measurement*100) 0.5420083%

Type B Estimation
DGA Test Kit
Ub1( = Uncertainty from calibration certificate/2) Type B, Normal 2.200000%
Ub2 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub3 (= resolution/(2*√3) Type B, Rectangular 0.005903%
Syringe
Ub4( = Uncertainty from calibration certificate/2) Type B, Normal 0.060000%
Ub5 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub6 (= resolution/(2*√3) Type B, Rectangular 0.002887%

UB in % (= √Ub1*Ub1+Ub2*Ub2+Ub3*Ub3) 2.34740%

Combined uncertainty Uc (= √UA*UA+UB*UB) 2.40917%

In terms of abosolute value:( % value*mean/100) 0.117812092693 Unit: PPM

Veff (= (n-1)*Uc4/UA4 ) 1952

K 2

Expanded uncertainty in% 4.81833%

Expanded uncertainty in value 0.235624 Unit: PPM

Preapred by : Testing Engineer Reviewed & Approved by : Technical Manager

Issue Date: 01.10.2019 Retention: TIll Change F No:PML/TTL/F/7.6/01 Rev 0

 TRANSFORMER TESTING LAB
MEASUREMENT UNCERTAINTY
CALCULATION
Job Description: Standard Gas Mixture
Test Name: Dissolved Gas Analysis (Acetylene C2H2)
Equipments used: DGA Test Kit Syringe
Make AGILENT AGILENT
S.No SL CN 16483114 NABL/LAB/EQ/082
Range: 0.1-5000 ppm Upto 10 ml
Accuracy: 1.0000% 1.00%
Uncertainty from calibration certificate: 4.00000% 0.12%
Resolution: 0.001 1
.
No. of measurements:(n) : 6 Unit of measurement: PPM

Sr No. Measured value

1 4.84060
2 4.84048
3 4.83966
4 4.90024
5 4.95656
6 4.92433

1 n
Avg measurement: X 
n
i 1
X i
4.88365

Type A Estimation

Standard deviation ( S ) 
n
x i  X 2 0.0508
 i 1

n 1

Std deviation of mean (= S/√n) 0.0207

UA in % ( = std deviation of mean/Avg Measurement*100) 0.4245775%

Type B Estimation
DGA Test Kit
Ub1( = Uncertainty from calibration certificate/2) Type B, Normal 2.000000%
Ub2 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub3 (= resolution/(2*√3) Type B, Rectangular 0.005911%
Syringe
Ub4( = Uncertainty from calibration certificate/2) Type B, Normal 0.060000%
Ub5 ( = accuracy/√3) Type B, Rectangular 0.577350%
Ub6 (= resolution/(2*√3) Type B, Rectangular 0.002887%

UB in % (= √Ub1*Ub1+Ub2*Ub2+Ub3*Ub3) 2.16109%

Combined uncertainty Uc (= √UA*UA+UB*UB) 2.20240%

In terms of abosolute value:( % value*mean/100) 0.107557510954173 Unit: PPM

Veff (= (n-1)*Uc4/UA4 ) 3620

K 2

Expanded uncertainty in% 4.40480%

Expanded uncertainty in value 0.215115 Unit: PPM

Preapred by : Testing Engineer Reviewed & Approved by : Technical Manager

Issue Date: 01.10.2019 Retention: TIll Change F No:PML/TTL/F/7.6/01 Rev 0