Triplex
Triplex
Triplex
adds to the attractiveness of integrated photonic solu- of requirements for all photonic applications. Therefore,
tions [14, 15]. Nowadays, waveguide-based optical sensors the integration of complementary technologies is often
reach the detection limit of 10-7/refractive index unit (RIU) pursued.
[14], which covers most interesting applications. Current At present, three technology platforms are commer-
research focuses on creating sensor arrays and cost price cially available in multi-project wafer (MPW) runs: the
reduction by further miniaturization [16]. Recent progress III-V InP technology, silicon photonics, and the TriPleX
in miniaturization of spectrometers for Raman detection platform. Customers have access to a library contain-
and optical coherence tomography (OCT) [17–19] demon- ing basic building blocks, allowing complex functional
strates the potential of photonics technology for point-of- designs. Several design houses [22, 23] support these plat-
care diagnostics. The requirements and technology needs forms. Fabrication facilities for these platforms are avail-
for these application fields are, however, hard to gener- able: InP [24–27], silicon (Si) photonics [28–30], TriPleX
alize. The applicable wavelengths, for example, cover the [31–33]. The key property performances of these technolo-
spectrum of light ranging from UV-VIS for environmen- gies are summarized in Figure 2.
tal monitoring and absorption spectroscopy, from VIS to As indicated in Figure 2, the InP technology is applied
near-IR for clinical investigation techniques such as Raman in the full range of active functionalities yielding a large
spectroscopy and OCT, up to the mid-IR for gas sensing variety of photonic applications, such as laser (array)s,
and space exploration (wavelength ranges based on (fast) modulators, and detectors. Si-photonics and TriPleX
astronomy division and sensor response division schemes are both silicon based and can, therefore, rely on CMOS-
as addressed in [20] and references therein). Adding active compatible fabrication technology enabling low-cost
functions (light sources, detectors, switches, etc.), micro- volume manufacturing [11]. Silicon photonics has com-
fluidic components, and/or nonreciprocal elements such bined its passive platform with significant progress in
as circulators increases the functional and technological the realization of on-chip detectors and modulators. Most
complexity beyond the integration of passive circuitry. applications can be found in datacom [35]. TriPleX has
Therefore, one of the main challenges remains to be the focused on passive performance (i.e., no on-chip gain
access to cost-efficient (hybrid) assembly and packaging media or high-frequency tuning) with ultralow loss over a
techniques. wide wavelength range including the visible range down
Materials and technologies applied in integrated to near UV. TriPleX is widely applied for microwave pho-
optics research and development vary over a wide range, tonics, sensors, and visible light applications [36, 37].
e.g., doped silica, polymers, silicon-on-insulator, III-V For all three platforms, tight curvature of waveguide
semiconductors, chalcogenides, lithium niobate and bends enabling cascading of multiple structures and
dielectric materials such as Si3N4 or Al2O3. In Figure 1, a reduction of optical footprint is mandatory. Therefore, a
(non-exclusive) overview of known optical materials is large refractive index contrast between waveguide core
given, showing their applicability as function of wave- and cladding is needed. On the other hand, very efficient
length. Although many material systems have been suc- coupling to low-contrast optical fibers has to be accom-
cessfully applied in some of the application fields, none plished implying completely opposite requirements on the
of the technologies is capable to fulfill the complete set index contrast of the channel waveguide. For the TriPleX
Figure 1: Overview on various materials applied in integrated optics and their corresponding transparency ranges [21].
K. Wörhoff et al.: TriPleX: a versatile dielectric photonic platform 191
Figure 2: Qualitative performance comparison of the three commercially available technology platforms [34].
platform, a monolithic spotsize converter technology commercially available basic waveguide geometries,
has been developed. This technology allows for on-chip which can be obtained by modification of individual
modal field size conversion and, therefore, enables highly steps in the generic fabrication flow [42]. The geometries
efficient fiber-to-chip coupling over the full accessible are categorized by their shape: box shell (I), double stripe
wavelength range while maintaining a large flexibility in (II), and filled box (III), whereas type II is subdivided into
waveguide geometry being inherent to the TriPleX pho- the symmetric double stripe (IIa), the asymmetric double
tonic platform. stripe (IIc), and the single stripe (IIb) being a special
In this paper, we provide a comprehensive review on case of IIc. The schematic layouts of the geometries and
the TriPleX photonic waveguide platform. In Section 2, SEM micrographs of realized structures are depicted in
the properties, technological and design aspects will be Figure 3. The generic process flow covering the fabrica-
discussed with emphasis on the different commercialized tion steps of all TriPleX types is given in Figure 4.
TriPleX geometries, integration aspects, fabrication con- While the overall geometrical dimensions of the
cepts, and basic building blocks. Section 3 will focus on waveguide cores of these shapes are typically in the order
the applications and performance of TriPleX-based com- of 1 μm2, their waveguide characteristics and potential
ponents for communications, biomedicine, and sensing application areas differ greatly. Some key characteristics
as well as a few special fields of photonics. are effective index of the waveguide mode Neff and group
index Ng (for TE-polarized light), channel propagation
loss αch [dB/cm], polarization-dependent loss PDL [dB],
2 TriPleX photonic platform minimum bending radius Rb [μm], mode field diam-
eter MFD [μm] (TE00 mode), fiber-chip coupling loss αf-c
[dB/facet], and waveguide birefringence ΔNeff.
2.1 TriPleX technology and design The box shell layout is highly suited for telecom appli-
cations: due to its symmetrical shape, the polarization
TriPleX waveguide technology is based on alternating dependence is largely reduced [43]. The box shell is availa-
well-defined and highly stable silicon oxide (SiO2) and ble in a low [39] and high [44] index contrast variant based
silicon nitride (Si3N4) layers [38, 39]. The CMOS-compat- on different ratios of the Si3N4 and SiO2 thicknesses in the
ible fabrication equipment based on batch processing by core region. In the low contrast version, a 1 × 1-μm2 SiO2
low-pressure chemical vapor deposition (LPCVD) enables core is surrounded by 50-nm-thick Si3N4, while the high
volume production as well as good reproducibility [32, contrast is achieved with SiO2 and Si3N4 core dimensions
40]. TriPleX waveguides are transparent for wavelengths of 0.5 × 0.5 μm2 and 170 nm, respectively. The waveguide
from 0.4 up to 2.35 μm and exhibit very low optical propa- propagation loss of the high-contrast box shell geometry
gation losses. This technology combines good integration is below 0.2 dB/cm and reduces to 0.06 dB/cm for the
potential with high design flexibility allowing for tailor- low-contrast variant [45]. The main difference in the char-
ing of the waveguide properties [41]. We distinguish three acteristics of both versions can be found in the bending
192 K. Wörhoff et al.: TriPleX: a versatile dielectric photonic platform
Figure 3: Schematic layout of the TriPleX geometries and SEM images of realized structures: box shell (I), symmetric double-strip (IIa),
single stripe (IIb), a-symmetric double stripe (IIc), filled box (III).
radius, which is designed to fulfill the 0.01 dB/cm bend wavelength and the group index are 1.535 and 1.72, respec-
loss criterion, and the mode field diameter of the circular tively, while the waveguide birefringence is 5.3 × 10-2. The
mode shape: Rb = 500 μm, MFD = 3.6 μm (low contrast), and waveguide attenuation is ≤ 0.1 dB/cm [46]. The tight
Rb = 150 μm, MFD = 1.4 μm (high contrast). bending radius allows for functional complexity at VLSI
The symmetric double stripe layout is typically level. As shown in Figure 5, waveguide propagation loss
applied in components requiring tight bending radii and as low as 0.095 dB/cm was measured in optical ring res-
large polarization birefringence. The optimized geom- onator (ORR) structures with a bending radius down to
etry is composed of two 170-nm-thick and 1.2-μm-wide 70 μm [46]. The circular mode of this waveguide geom-
Si3N4 layers separated by a 500-nm-thick SiO2 interlayer. etry has a mode field diameter of ∼1.5 μm. To enable low-
The effective index of the waveguide mode at 1.55 μm loss coupling to standard single-mode fibers (SMF28),
K. Wörhoff et al.: TriPleX: a versatile dielectric photonic platform 193
Figure 5: Waveguide propagation loss as function of ORR bending radius (inset: measurement and fit of ORR frequency responses) [46].
multimode, and an additional tapering section is required trench etching (into the thermal oxide layer) and trench
for adiabatic widening of the channel width [51]. filling (by LPCVD Si3N4 deposition) in combination with
Finally, the filled-box geometry was developed for chemical mechanical polishing (CMP) was applied for the
applications requiring ultrahigh confinement of the fabrication of crack-free waveguides (see also Figure 4).
modal field in the core layer. In this geometry, core widths The optical propagation loss of these waveguides at 1.55
of 0.8–1.0 μm and thicknesses varying from 0.8 to 1.2 μm μm wavelength was 0.4 dB/cm [53].
were realized [53]. The waveguide channel is multimodal;
up to three modes exist. For the 1.55-μm wavelength and
TE-polarized light, the corresponding effective index of
2.2 Technology integration aspects
the mode and MFD of the fundamental mode (TE00) are
around 1.79 and 1 μm, respectively. A minimum bending
The high design flexibility provided by the TriPleX plat-
radius of 12.5 μm was calculated for the TE00 mode taking
form is prerequisite to boost photonic integration. The
the 0.01 dB/cm loss criterion into account. As stoichio-
availability of low- and high-contrast regions on a single
metric LPCVD Si3N4 films exhibit high tensile stress, the
chip easily enables interposer functionality in photonic
layer thickness growth is limited to < 500 nm. Therefore,
assemblies. The large freedom in pitch and spotsize con-
version is, for example, utilized in low-loss connections
between optical fiber arrays and high-confinement wave-
guide technologies such as InP or silicon on insulator
(SOI) [54]. In return, active functionality (light generation,
detection, and modulation) available on those platforms
is efficiently joined with the TriPleX circuitry. Various
complementary functionalities such as high-Q resona-
tors, arrayed waveguide gratings, tunable delay lines, and
devices for polarization control available in the ultralow
loss silicon nitride waveguide technology and in silicon
photonics are reviewed [55, 56]. On the SOI side among
others, modules based on hybrid integration with the
III-V InP technology and magneto-optical materials add
to the functionality portfolio. The proposed integration
Figure 6: Red light propagation in a high-aspect ratio spiral-shaped concepts for silicon nitride waveguides with the silicon
waveguide with minimum bending radius of 165 μm [51]. photonic platform are based on a hybrid bonding process
K. Wörhoff et al.: TriPleX: a versatile dielectric photonic platform 195
utilizing an SiO2 interface layer with a controlled thickness controlled by design rather than solely by the process-
[57, 58]. The integration concept and an SEM micrograph specific etch profile [60]. The preliminary results based on
of a fabricated device are shown in Figure 7. insertion loss measurements of waveguides with multiple
Currently, a novel assembly concept for integrating tapering sections indicate a taper loss reduction by about
InP and TriPleX chips on a carrier platform is being devel- one order of magnitude.
oped by a European consortium: PHASTFlex [59]. Besides Last but not the least, the TriPleX platform is also
addressing low-cost, high-volume assembly, the approach well suited for lab-on-a-chip applications. Manufactur-
focuses on bridging the gap between typical flip-chip able concepts (Figure 8) for the integration of microflu-
placement accuracies ( ≤ 1 μm) and the sub-100-nm align- idic systems as well as the assembly of VCSEL arrays and
ment precision required by high-contrast coupling inter- detectors have been developed [42, 61].
faces by monolithically integrated MEMS-based fine
tuning.
On-chip adiabatic tapering sections are key elements 2.3 Technology access
for many integration aspects. Therefore, the optimization
of the taper design and technology was emphasized. Verti- Low-threshold access to the TriPleX platform is, among
cal tapers are usually fabricated by standard lithography others, enabled through MPW services [62]. The MPW
and isotropic etching of the silicon nitride layers. Meas- approach provides a solution for researchers and entre-
urements of propagation losses through such tapering preneurs to prototype their design at affordable cost and
sections resulted in ≤ 0.5 dB/taper [47]. The most critical time levels. The designs of several participants are inte-
part of the tapering path is at the starting position of the grated on a single mask and fabricated in a shuttle run.
taper (thin side), where the propagation of the weakly con- Circuitry simulation and mask design can be carried out
fined mode is extremely sensitive to geometrical changes. by PhoeniX software tools [22]. A prerequisite to the suc-
Therefore, LioniX has developed a novel ultrataper pro- cessful implementation of such an approach is the avail-
cedure, in which the shape of the tapering section can be ability of well-defined and verified design elements.
Fluidic wafer
Optical wafer
A
Therefore, a library of standard optical components was Light coupling to the toroidal cavities is usually real-
established and implemented as basic building blocks ized through tapered fibers because on-chip integration
(BBBs) in the licensed design kit of the PhoeniX software. of access waveguides is challenging. The integration of
In the past MPW services, components for the box shell high-Q ring resonators in the ultralow-loss TriPleX plat-
geometry were applied, while in currently active MPW form is an attractive approach, as access waveguides,
calls, the double-stripe geometry is offered. The BBB cavities, and directional couplers can be monolithi-
libraries include the following main elements: waveguide cally integrated. In the TriPleX single stripe geometry
straight, bent waveguide, Y-junction, directional coupler, (40 nm × 11 μm), add-drop ring resonators, with a 9.65-mm
spotsize converter, and heater section. This allows for the bending radius and a 3.3-GHz FSR at 1580 nm wavelength,
easy design of integrated functions such as interposers, have been integrated [65, 66]. Several directional coupler
microring resonators (MRRs), several types of interfer- concepts (symmetric, straight, pulley, and tapered) have
ometers (multimode, Michelson, Young, Mach-Zehnder), been implemented to assess and minimize the coupler
arrayed waveguide gratings, multiplexers, frequency, and excess loss. An intrinsic Q-factor of 0.81 × 108 was meas-
modal filters, mode and polarization converters as well ured with a weakly tapered directional coupler design.
as implementation of thermo-optic tuning or sensing Round trip and propagation losses of 0.019 dB and
windows. The library kit for the asymmetric stripe geom- 0.0032 dB/cm were extracted, respectively. Upon further
etry is under preparation. coupler optimization and full exploitation of the low-loss
TriPleX services as well as its combination with other TriPleX platform (i.e., αch < 0.0005 dB/cm) Q-factors as
photonic platforms and technologies are also available high as 6 × 108 are predicted.
through the European initiative ACTPHAST [63], which A range of ring resonators suited for application
has created a unique one-stop-shop European access over a wide wavelength range (1060, 1310 and 1550 nm)
center for photonics innovation solutions and technology was studied in [67]. Based on single-mode TE propaga-
support. tion in two different TriPleX single stripe geometries
(50 nm × 5.3 μm and 80 nm × 2.8 μm with bending radii of
5 and 2 mm, respectively), Q-factors of 19, 28, 7 × 106 were
3.2 Biophotonics
Reference arm
SLED Polarization Collimating
Fiber array
controller lens Sample
Power
monitor
X-Y
Galvo scanner
A Spectrometer Integrated interferometer chip
A
Integrated interferometer chip Scan lens
Fiber
array
B
Collimating lens B
Figure 13: Schematic layout of the OCT setup with the integrated
TriPleX-based interferometer chip (A) and photograph of test setup
with fiber array, integrated interferometer chip and scan lens (B) [45].
Figure 15: Photograph of Hyperion laser light engine [37]: modular interior with TriPleX LCB chip in blue pig-tailed package (A) and commer-
cial product with software in action (courtesy XiO photonics) (B).
stripe TriPleX geometry with 35 nm and 85 nm lower and Absorption sensing: TriPleX-based chips have been
upper silicon nitride layer thickness, respectively [94]. designed and realized for a range of absorption-based
Challenges with respect to power budget aspects in mul- applications in fluidic environments.
tichannel operations are addressed by a grating-based The development of processes in a microreactor
vertical VCSEL coupling concept in combination with an largely benefits from integrated UV/VIS spectroscopic
optimized 1 × 8 multimode interference (MMI) coupler. detection allowing for real-time analysis under segmented
flow. An optofluidic chip optimized for evanescent field
sensing based on a 65-nm-thick Si3N4 waveguide layer and
Gas/liquid specific absorption window: an operational wavelength range from 488 to 632 nm was
Interaction length (L) developed for the monitoring of gold nanoparticle produc-
Evanescent tail tion [61]. Segmented flow detection at integration times as
low as 2 ms was demonstrated.
Cover nc
Fluorescence sensing: A sensitive and low-cost
Waveguiding film nf detection scheme for molecular biomarkers has been
demonstrated [95, 96] in TriPleX chips of 10 mm × 10 mm.
Bottom cladding nb
One of the applied chip layouts yielding a matrix of 100
sensing wells is depicted in Figure 18. Light of 642-nm
Silicon support
wavelength is coupled from a low-cost diode laser
array into the excitation waveguides of the chip. In
Figure 16: Sensing principle [42]. each sensing well, analyte molecules can be captured.
202 K. Wörhoff et al.: TriPleX: a versatile dielectric photonic platform
Excitation waveguides
Sensing wells
Collection waveguides A
the optical signal is split by a 1 × 11 MMI. The optical and ratio between the original channel width and the sidewall
fluidic modules are connected by a bonding process and gratings. High grating reflectivity was measured in the
diced to a chip size of 52 mm × 16 mm. 1550-nm wavelength range. On top of the passive Si3N4
platform an erbium (Er3+)-doped aluminum oxide film
with an Er3+ concentration of 1.3 × 1020 cm-3 was integrated
3.4 Special applications by reactive co-sputtering [99]. The laser performance of
several DBR and DFB grating configurations was meas-
Besides the above-discussed conventional application ured applying 974-nm pumping. Pump thresholds, laser
fields, the technology platform has also entered emerging output powers, conversion efficiencies, and side mode
areas of photonics and special applications such as inte- suppressions of 11 mW, 2.1 mW, 5.2%, and 50dB, respec-
grated light sources, nonlinear optic devices, components tively, were achieved.
for space, and quantum computing. Ultra-narrow linewidth laser components have been
The active/passive integration potential of the silicon realized by hybrid integration of III-V laser diodes with a
nitride technology was, for example, demonstrated by TriPleX cavity in a so-called waveguide-based external
the monolithic implementation of optically pumped cavity semiconductor laser (WECSL) configuration [100].
DFB lasers (Figure 19). For this purpose, side wall grat- The design is based on the box shell geometry and exploits
ings with 520-nm period have been etched by stepper the response of two integrated MRRs acting as external
lithography into the 4.6-μm-wide silicon nitride channel mirror and having radii of 50 and 55 μm, respectively. The
waveguides [98]. The grating coupling constant can be layout of the frequency-selective mirror component realized
controlled between 13 and 310 cm-1 by adjusting the aspect in TriPleX technology is shown in Figure 20. A laser diode
equipped with only one mirror is connected to the input
port (IN) of the chip. To monitor the laser and mirror perfor-
mance in greater detail, three output ports (OUT) are added
to the design, whereas OUT3 provides the actual response
of the WECSL. The measured FWHM laser linewidth and
side mode suppression ratio of the WECSL are 25 kHz and
50 dB, respectively. Wavelength tuning over the full tel-
ecommunications C-band (1530–1565 nm) is demonstrated.
For nonlinear optic applications, high modal confine-
ment in the photonic waveguide is of importance. There-
fore, the filled box geometry of the TriPleX platform with
core cross sections of 1.2 μm × 0.8 μm is highly attractive.
In ongoing research, this technology is implemented for
the design and realization of components for supercon-
tinuum generation with over 700 nm spectral bandwidth
[101] and four-wave mixing in the 800–1500 nm wave-
length range [102].
The specific requirements of several applications
for space research can be met by the TriPleX technology.
4 Conclusions
LioniX’ TriPleX technology is a versatile photonics plat-
form suited for applications over a wide wavelength range
covering the transparency window from 0.4 to 2.35 μm.
Ultralow-loss channel waveguides with propagation losses
down to 0.0005 dB/cm have been demonstrated. The mon-
olithic integration of low- and high-contrast waveguides
on the same chip enables the realization of low-loss spot-
size converters. Therefore, TriPleX chips are suitable joints
between different high-index platforms such as III-V or SOI
and standard optical fibers giving access to the ‘outside
world’. Currently, substantial effort is put into the devel-
opment of low-cost integration and assembly techniques
A
for adding complementary functionalities of the different
photonic platforms into a single package.
In this paper, we have reviewed a wide range of appli-
cation examples that have been realized in or enabled by
TriPleX technology. In the area of communications, com-
ponents for telecommunication networks and microwave
photonics operating in the 1.3- and 1.5-μm wavelength
window are discussed. High-performance filtering and
true time delay concepts are surveyed, and components
with high functional complexity for optical beam-form-
ing networks are introduced. Milestones in the develop-
ment of miniaturized biomedical devices can be mainly
found in the field of optical coherence tomography and
integrated Raman spectroscopy. The results addressed in
this paper cover functional devices operating over a broad
spectral range, from VIS to 1.3 μm. Although results in this
field are still preliminary, the potential of integrated optics
solutions becomes clear. Finally, sensor devices and sub-
systems are addressed. Main application fields are envi-
ronmental control, food/water safety, and security. The
B
spectral range of interest is at a visible wavelength and
at 850 nm due to access to low-cost VCSEL light sources.
Figure 21: MRR-based in-flight calibration module for earth-orbiting
satellites; optical chip propagation inspection with VIS light (A) and State-of-the-art sensing concepts developed on the TriPleX
module assembly (B) [21]. platform allow for detection limits around 10-7 RIU.
The functionality of the TriPleX platform is captured
In general, components for space missions need to be by verified basic building blocks and incorporated in the
highly compact, robust, lightweight, and low on power library of a design kit developed by LioniX and PhoeniX
consumption. One example of a realized module for Software. The availability of this library in combination
the ExoMars mission was discussed in the fluorescence with affordable manufacturing through MPW shuttle runs
sensing section of this paper. Another application is lowers the threshold for researchers and entrepreneurs to
addressed by the development of spectroscopic tech- enter and exploit photonics technology.
niques on earth-orbiting satellites where an in-flight cali-
bration module for the 2.3- to 2.4-μm wavelength range Acknowledgments: The authors would like to thank
was designed with thermally tunable MRR building R. Duer (iNDX Lifecare Inc.), C. Roeloffzen (SatraX BV),
blocks based on the asymmetric stripe geometry [21, 103]. and J. van Kerkhof (XiO Photonics BV) for providing pho-
The packaged module (Figure 21) has an insertion loss as tographs of their commercial products based on TriPleX
low as 2.4 dB. chip technology. Co-workers of the following research
K. Wörhoff et al.: TriPleX: a versatile dielectric photonic platform 205
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