US Army Medical Course MD0954-100 - X-Ray Film Processing
US Army Medical Course MD0954-100 - X-Ray Film Processing
US Army Medical Course MD0954-100 - X-Ray Film Processing
X-RAY FILM
PROCESSING
ADMINISTRATION
COMMANDER
AMEDDC&S
ATTN MCCS HSN
2105 11TH STREET SUITE 4192
FORT SAM HOUSTON TX 78234-5064
Approved students whose enrollments remain in good standing may apply to the
Nonresident Instruction Section for subsequent courses by telephone, letter, or e-mail.
Be sure your social security number is on all correspondence sent to the Academy of
Health Sciences.
When used in this publication, words such as "he," "him," "his," and "men" are intended
to include both the masculine and feminine genders, unless specifically stated otherwise
or when obvious in context.
.
USE OF PROPRIETARY NAMES
The initial letters of the names of some products are capitalized in this subcourse. Such
names are proprietary names, that is, brandnames or trademarks. Proprietary names
have been used in this subcourse only to make it a more effective learning aid. The use
of any name, proprietary or otherwise, should not be interpreted as an endorsement,
deprecation, or criticism of a product. Nor should such use be considered to interpret
the validity of proprietary rights in a name, whether it is registered or not.
.
TABLE OF CONTENTS
Lesson Paragraphs
INTRODUCTION
Exercises
Exercises
Exercises
Exercises
MD0954 i
CORRESPONDENCE COURSE OF THE
U.S. ARMY MEDICAL DEPARTMENT CENTER AND SCHOOL
SUBCOURSE MD0954
INTRODUCTION
Subcourse Components:
Credit Awarded:
MD0954 ii
You can enroll by going to the web site http://atrrs.army.mil and enrolling under
"Self Development" (School Code 555).
MD0954 iii
LESSON ASSIGNMENT
LESSON OBJECTIVES After completing this lesson, you should be able to:
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Section I. INTRODUCTION
1-1. SCOPE
a. The chemistry of x-ray film and the chemistry of film processing (Lesson 1).
b. The processing room, its facilities and its equipment (Lesson 2).
c. The activities involved in the processing of x-ray film (Lessons 3 and 4).
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1-2. GENERAL
X-ray film must be characteristically different from film used in photography, since
x-ray exposure is different from light exposure. Because of its importance to medicine,
x-ray film is manufactured with consistent uniformity and quality, which facilitates
standardization of exposure and processing.
a. Film Base. The film base supports the emulsion and provides the correct
degree of stiffness for handling purposes. It is composed of either cellulose acetate or
polyester, both of which are transparent and blue-tinted.
(2) Polyester. The polyester base is made by "cracking" crude oil forming
the substance parazylene. When this substance is mixed with methyl alcohol and other
chemicals, a product of dimethyl-terebthalate (DMT) is formed. This DMT is one-half of
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the final preparation. Ethylene glycol is the other major ingredient. This is commonly
called antifreeze. It is produced from oil and natural gas in a process of oxidizing and
hydrolizing ethylene gas. When DMT and ethylene glycol are mixed in heat for a long
period of time, polyester is formed. The polyester is reheated and given a two-way
stretch until its thickness is .007 inch.
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NOTE: The black particles represent small quantities of black metallic silver.
a. When the x-ray film emulsion is sensitized during manufacture, the silver
bromide crystals are left in a state of suspended animation awaiting the x-ray stimulus
to start them on their way to becoming a radiographic image. The potentiality for
this activity exists in the tiny sensitization "specks" at the surface of the crystal
(A, figure 1-6). When x-ray exposure occurs, the latent image is produced.
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Figure 1-5. Composition of a-ray film.
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Figure 1-6. Changes occurring within silver bromide crystal upon exposure to x-rays
and subsequently developer.
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b. The generally accepted theory as to the nature of changes occurring in the
production of the latent image is that, when the silver bromide crystals are atomically
activated by exposure to x-rays (and usually, the fluorescent light of intensifying
screens), electrons fly out of their normal atomic orbits and wander at random
throughout the crystals. These are known as photoelectrons (B, figure 1-6), one of
which (in dotted box, B, figure 1-6) is theoretically represented in C through I, figure 1-6.
Normally, the silver bromide crystal is a nonconductor of electricity. Upon exposure to
x-rays or light, however, it becomes a weak conductor and the photoelectrons, released
from the individual atoms in the crystal flow within the crystal as a tiny electric current
(C, figure. 1-6). Ultimately, some of these electrons are trapped or acquired by the
"speck" (D, figure 1-6). A negative electrostatic field is now set up around the "speck."
Other activities also occur in the crystal for the slower-moving silver ions with a positive
charge travel (E, figure 1-6) to the negatively charged "specks" where they are
neutralized (F, figure 1-6) to form tiny particles of atomic silver, while the bromide
portions of the crystal are absorbed elsewhere. As more silver ions are neutralized, the
"speck" grows with silver (G, figure. 1-6). In I, figure 1-6, the silver has been reduced to
metallic silver by the action of the developer.
c. The latent image cannot be seen or detected by ordinary physical means, but
it can be changed into a visible silver image by chemical processing.
a. Periapical Film. The periapical film is used to radiograph the crown root and
supporting structure of the teeth. It is particularly useful to determine abscesses, cysts,
or granulomas located at the root apices. Additionally, periapical film has great value in
diagnosing bone loss caused by periodontal disease. Full mouth periapical series are
also used as a record of the progression of such diseases.
c. Occlusal Film. The occlusal film is a larger film, which is placed horizontally
between the occlusal (chewing) surfaces of the upper and lower teeth. The occlusal
film provides a general view of the maxillary (upper jaw) and mandibular (lower jaw)
arches, so it is especially useful in locating foreign bodies in the floor of the oral cavity
and impacted teeth, cysts, et cetera, in the palate. There are usually two films in the
occlusal packet, which allow for different developing times. In medical radiography,
occlusal film is also used for examination of the nasal bones and to demonstrate stones
in the salivary tracts.
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1-6. PHOTOFLUOROGRAPHIC FILM
At the time of manufacturing, the manufacturer determines not only the speed of
sensitivity of the film, but also other characteristics such as density, contrast, detail, and
inherent film fog. The characteristic of film is important since it has a bearing on the
quality of the finished radiograph. Manufacturers express the characteristics of their
films through a "characteristic curve" which is commonly referred to as an "H and D
curve," so named after Hurter and Driffield who first used it to describe the response of
the film to varying amounts of radiation.
a. Activator. The activator (or alkali), sodium carbonate, softens the gelatin of
the emulsion and provides the necessary alkaline medium to the solution so that the
reducing agents can diffuse into the emulsion and attack the exposed silver bromide
crystals. In general, the more alkaline the developer, the more powerful and rapid is its
action. A disadvantage of sodium carbonate is that when a film is processed in an x-ray
developer containing it and then transferred to a warm acid-fixing bath, tiny bubbles of
carbon dioxide gas may form in the soft gelatin. As the bubbles escape, they form tiny
craters or pits in the emulsion, thereby breaking up the normal character of the silver
image. The finished film or radiograph is blistered. To overcome this effect, the
temperature of the developer, rinse, and fixer solutions should be approximately the
same.
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b. Reducers.
(2) Reducing agents. The agents commonly used are Elon™ (another trade
name is Metol™) and hydroquinone. The activity of these chemicals requires their
presence in an alkaline solution. Chemical functions differently in attacking the
emulsion. The Elon™ starts development by attacking the exposed silver bromide
crystals swiftly with resultant production of gray tones in the image. Elon™ is
unpredictable above 75ºF and hydroquinone ceases its activity below 60ºF. The activity
of the hydroquinone is slower, but it serves to build up the black tones required in the
image. The reducers, acting as a team, produce a good image with satisfactory
contrast in a minimum of time, as long as the temperature of the solution remains in the
optimum range. Reducers are not too stable in the presence of oxygen, which they can
readily absorb from the air or from the water.
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used are different. The automatic developer consists of five chemicals: an activator,
reducers, a restrainer, a preservative, and a hardener.
d. Preservative. The preservative is once again the same chemical with the
same function as in the annual developer. It prevents rapid oxidation of the chemicals
and prolongs their useful life.
f. Solvent. The chemicals in both kinds of developer solutions are all dissolved
in water. This is necessary both for the action of the chemicals and for the softening of
the emulsion.
Although the concentration of the fixer solution varies for the two methods of
processing, the chemicals used are basically the same. The fixer has four chemical
agents: an acidifier, a clearing agent, a hardener, and a preservative. All of the
chemicals are mixed with water, which serves as the solvent.
a. Acidifier. The acidifier (acetic acid) neutralizes any alkaline developer that
may be carried over from the developing solution and provides the required acidity for
the other chemicals to function. The acidifying action quickly stops development and
prevents formation of stains.
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b. Clearing Agent. The clearing agent (sodium thiosulfate or ammonium
thiosulfate) dissolves the residual unexposed silver bromide crystals in the emulsion
without damage to the silver image. The unexposed crystals have of course, been
unchanged by the developer. If the film is not properly cleared, the remaining
unexposed silver bromide crystals will darken on exposure to light and obscure the
radiographic image. These chemicals are commonly known as "hypo." The clearing
action of hypo involves a chemical reaction between the sodium or ammonium
thiosulfate and the silver bromide in the emulsion, wherein silver thiosulfate is formed
and remains in solution.
1-11. GENERAL
X-ray film is packaged in hermetically sealed foil and paper wrappings to protect
it from light and moisture in quantities of 25 and 75 sheets. Each film is in a folder of
chemically pure interleaving paper. (Some manufacturers omit the interleaving paper.)
Each quantity of either 25 or 75 sheets is placed between cardboard, wrapped in
protective paper, and placed in a metal foil bag sealed to ensure approximately 50
percent relative humidity inside the package. The package is then wrapped in paper
and placed in a metal foil bag sealed to ensure approximately 50 percent relative
humidity inside the package. The package is then wrapped in paper and placed in a
cardboard carton. Packed in this manner, x-ray film will be free from any defects due to
excessive humidity as long as it remains in the unopened foil wrapping. For overseas
shipments, each carton is sealed in heavy waterproof paper for additional protection.
1-12. HANDLING
X-ray film is delicate and should not be handled carelessly or roughly. Avoid
touching its surfaces, holding it as near the edges as possible with clean, dry hands. It
is sensitive to maltreatment of any kind; heat and light adversely affect the emulsion. It
can be handled safely and rapidly for all radiographic purposes as long as the x-ray
specialist uses precaution to avoid the production of foreign marks (artifacts) on the film.
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(Radiographically, an artifact is a mark on the film which is foreign to the x-ray image
and which is not necessarily imposed on the film by the action of x-ray.) Artifacts
caused by bending and crinkling will be dark.
(2) If stored at 60F, it can be kept six months; at 50ºF, for one year.
b. X-Rays. Film must be suitably protected from the unwanted actions of x-rays
or radium by lead-lined walls or chests. Film bins located in the processing room should
be protected by sheet lead.
c. Fumes. X-ray film must never be stored in drug rooms or other places
containing fumes of any kind. Illuminating gas, formalin, ammonia, volatile oils, sewer
gas, and similar substance will fog film, which is stored in an atmosphere containing
them.
e. Expiration Date. All film should be used before its expiration date.
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opened, it should be used as soon as possible. If unexposed boxes of x-ray film must
be stored in refrigerators, the refrigerators should contain nothing else and some kind of
dehydrator should be used to reduce the humidity.
Any form of white light creeping into a processing room through cracks around
the edges of partitions or doors may fog x-ray film, casting a dark veil over it. Only that
light from a properly constructed safelight equipped with a filter that is compatible with
the screen/film system that is being permitted to fall on the film during its handling, but
even this light may fog film if permitted to shine on a particular area too long. No film
should be exposed to the safe light for longer than it takes to unload a film and place it
in the automatic processor.
In today's modern radiology clinic, generally the cardboard film holder will not be
utilized. There may be situations when the radiographer may encounter the use of the
cardboard, and should have the knowledge of the proper loading and unloading
technique.
b. In loading, the film with the paper around it is placed in the open holder, the
large flap of the envelope is turned down, and then the side flaps are brought together
and clipped.
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c. Since the backs of holders (and cassettes) contain thin sheets of lead to
prevent backscatter fogging, you should take care not to use the folder upside down.
If you do this, the lead will absorb most of the radiation, leaving the film underexposed.
Be sure to place the side marked "tube side" facing the x-ray tube and you will avoid
this problem.
In taking the film (to be used in a cassette) from the carton, always remove the
film slowly. Rapid movement can cause a build-up of static electricity. When the film is
removed from its carton, it should be held vertically at the middle of the top border with
the fingertips of the right hand and placed in the cassette. Careful handling will prevent
many kinds of marks on the film.
a. Loading. When loading a cassette, the film is placed in the bottom of the
cassette on the front intensifying screen. The lid carrying the back screen is gently
closed and locked by means of the back springs. When placing the film in the cassette,
care should be exercised to avoid scraping or sliding the film over the edges of the
cassettes or the surface of the screen. The procedure for correctly loading a cassette is
illustrated in figure 1-7.
b. Unloading. The correct procedure for removal after exposure of the x-ray
film cassette it is to be sure hands are dry and not come in contact with the screens.
Since dental x-ray films are in sealed individual wrappings, a special procedure
for removing these wrappings is required. A dental film hanger consists of a bar of
metal, which is affixed to film-holding clips for insertion of exposed dental x-ray films for
processing. Care should be taken not to make any finger marks on the film.
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Using both hands to avoid kink marks, place the film carefully in the cassette.
Gently close and latch the cassette.
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1-21. IMMERSION OF HANGERS IN SOLUTIONS
When placing hangers loaded with film in solutions, dip them quickly and
carefully. After complete immersion, raise and lower the films about two inches several
times to remove air bells and completely bathe the surfaces of the film. Make sure
hangers are separated by about three-fourths inch. Do not remove them entirely from
the solution until you are ready for the next operation. By keeping the level of the
solutions one-inch below the tops of the tanks, the crossbars of the hangers are not
covered by the developer of fixer solutions. However, the crossbars should be
immersed in the wash water.
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EXERCISES, LESSON 1
After you have completed all the exercises, turn to "Solutions to Exercises," at the end
of the lesson and check your answers.
a. Silver bromide.
b. Emulsion.
c. Cellulose acetate.
d. Gelatin.
a. Cotton cellulose.
b. Cellulose acetate.
c. Silver iodine.
d. Gelatin.
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4. When x-rays are taken using intensifying screens, __________________
account(s) for most of the exposure.
a. X-rays.
b. Gamma rays.
c. Beta rays.
d. Fluorescent light.
5. The emulsion x-ray film is coated with a thin, transparent material to:
a. Exposure.
b. Manufacture.
c. Development.
d. Fixing.
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8. Which type of dental film is used to show cavities between the teeth?
a. Periapical.
b. Occlusal.
c. Panarex.
d. Interproximal.
9. Which of the following types of dental film would be useful in locating an impacted
tooth?
a. Periapical.
b. Interproximal.
c. Occlusal.
d. Photofluorographic.
11. Reducing agents in the developer change silver bromide crystals to black metallic
silver and also act as electron donors to the latent image site. In this latter
function, their action results in a:
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12. Because of the chemicals released by the developing process, which of the
following ingredients included in a fresh developer solution is not used in the
replenisher?
a. Elon™.
b. Potassium bromide.
c. Sodium sulfite.
d. Hydroquinone.
13. In the developer solution, sodium sulfite works well as preservative because it:
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SOLUTIONS TO EXERCISES, LESSON 1
1. b (para 1-2)
2. c (para 1-3a(1))
3. d (para 1-3c(2))
4. d (para 1-3b)
5. c (para 1-3c)
6. b (para 1-4a)
7. d (para 1-4c)
8. d (para 1-5b)
9. c (para 1-5c)
End of Lesson 1
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LESSON ASSIGNMENT
LESSON OBJECTIVES After completing this lesson, you should be able to:
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Section I. PROCESSING ROOM, ITS FACILITIES, AND ITS EQUIPMENT
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Figure 2-1. A schematic diagram of an automatic processing darkroom and
adjacent light room area.
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NOTE: Dotted workflow line indicates course of exposed film during the processing
procedure.
Figure 2-2. Plan for a processing room showing tank and loading bench sections.
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2-3. LIGHTPROOF ENTRANCES
An entrance, which provides easy accessibility while at the same time providing
complete protection from outside white light, is essential. Commonly used entrances are
of three general types: the single door, the lightlock (double doors), and the labyrinth or
maze. The one best suited for a particular situation will be determined largely by the
number of people using the processing room and by the floor space available.
a. Single Door. If the radiologist and x-ray specialists are the only persons who
routinely use the processing room, a single lightproof door with an inside bolt or lock will
usually suffice. (Figure 2-3).
b. Lightlock. This type of entrance may consist of a small hall with two doors, one
opening into the processing room and one to the outside. Electric or mechanical
interlocking devices can be installed to prevent the accidental opening of both doors
simultaneously. However, safety releases must be incorporated into the interlock so that
both doors can be opened at the same time to allow the movement of supplies into the
processing room or in case of an emergency. If interlocks are not provided, warning lights
or buzzers are useful. A lightproof louver should be installed to accommodate changes in
air pressure caused by opening and closing the doors and to provide some ventilation. All
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of these arrangements can be used with either hinged or sliding doors. If a lightlock opens
directly into the exposure room, the lightlock must be equipped with lead-lined doors.
Thus, it is simpler if it opens into the control booth, where protection is already provided.
The color of the walls in the lightlock is unimportant. Safelight may be used if desired.
Minimum dimensions for a lightlock are determined by door size, the smallest practical
door being about two and one half feet by seven feet. One door normally swings inward
with sufficient room to close it before opening the other.
c. Labyrinth. The labyrinth, or maze, is not provided with doors. It prevents the
entrance of white light yet provides air circulation. Since it requires at least twice as much
floor space as a lightlock, it is seldom used. The height of the entrance should be limited
to seven feet to admit the minimum amount of light. The walls and ceiling should be
painted with a flat paint and safelight illumination should be provided. A straight passage
into the processing room should be made possible by placing a lightproof door in the
baffle.
2-4. ILLUMINATION
Illumination of the processing room can be broken down into several individual
aspects: white light, safelight, wet film illumination, and wall finish. Each of these
elements must be taken into consideration in the design of a processing room.
a. White Light. White light is necessary for many operations such as mixing
chemicals, cleaning tanks, caring for intensifying screens, and general maintenance of the
darkroom. Fixtures for white light should be strategically located and of sufficient intensity
to provide general illumination.
b. Safelight Illumination. Since x-ray films are sensitive to white light, they must
be handled either in darkness or under safelight illumination of the proper quality. Films
exposed with intensifying screens are approximately eight times more sensitive to safelight
than unexposed film. Therefore, safelight illumination must be designed to give enough
visibility in the processing room for the specialist to accomplish his duties, yet be subdued
enough to avoid harming unprocessed film.
(1) Light source and filters. A safelight consists of a light source and a suitable
filter combined in a lamp housing and giving light of an intensity and spectral quality which
will not fog film exposed to it for a reasonably short time. A combination that is
recommended and widely used is a 15-watt tungsten bulb with a Wratten 68 filter or Kodak
GBX. Light from such safelight is in the yellow or yellow-red portion, not in the same
spectral range as the film sensitivity. The wattage is sufficient to provide illumination
without undue fogging of the film.
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which will depend upon the amount of illumination desired and the angle of which it must
fall. An indirect safelight should be used at the loading bench because of the possibility of
fairly long exposure o the film to this light.
(3) Safety standards. No safelight is safe if film is left under it too long. Film
that cannot be processed immediately should be kept in a lightproof container. Films
awaiting processing should be protected by screens, not piled near a safelight.
(4) Checking safelight illumination. A simple method for checking the safety of
illumination is to cover part of a film with cardboard and then expose the remainder for one
minute at a distance of three feet. This test film is then developed. If no fog shows on the
exposed part as compared with covered part, the lighting may be assumed safe. If fog
appears, the safelights are not functioning properly. All safelights should be tested
periodically for light leaks, fading of the filter, and excess wattage.
d. Wall Finish. If the quality of the light from a safelight is "safe," the illumination
reflected from any surface is also "safe" regardless of the color or finish of the surface.
However, the finish should be an attractive color and should reflect the maximum amount
of safelight illumination. To avoid glare, flat paint should be used. Maximum reflection is
achieved by choosing a color within the same color spectrum as that of the safelight. In
permanent installations, the ceilings and the upper 18 inches of sidewalls should be
painted white. The remaining wall surfaces should be a warm, light color.
2-5. VENTILATION
b. When not properly controlled, temperature and humidity have adverse effects on
both the worker and the film. For comfort, humidity between 40 and 50 percent,
temperature between 67º and 83ºF, and air movement between 15 and 25 feet per minute
should be maintained. Greater air velocity would be tolerable at temperatures above 80°.
The air in the processing room should be maintained at a positive pressure, that is, air
should be pumped in, not out. This helps prevent the entry of dust. The dryer should
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have a duct vented outside so that it may be used to exhaust air from the room. Incoming
air should be pumped through filters and should be sufficient in volume to change the air in
the room from 6 to 10 times each hour.
c. When ventilating ducts are absent, fans with lightproof intakes may be installed
in the wall. Doors may be equipped with lightproof louvers to permit passage of air.
b. All outlets, switches, sockets, and similar devices should be insulated and
grounded. Despite safety devices, always follow the "one-hand" rule, that is, when
operating electrical apparatus with one hand, avoid grounding yourself with the other.
Foot switches eliminate the use of hands in operating electrical equipment, but special
care must be taken in grounding them because of the likelihood of moisture on the floor.
c. A safelight installed in the ceiling of the entrance lightlock should have its switch
at a convenient height on the right side of the inner entrance. The white-light circuit
switch, however, should be high on the wall above the safelight switch so it will not be
turned on inadvertently. All safelights should be on the same circuit, but should have
individual switches. In manual processing, the film dryer should be on a separate circuit of
ample capacity. As an extra precaution, it is advisable to have all three main circuits (for
white light, safelight, and dryer) controlled by a single heavy-duty disconnecting switch in
addition to their individual switches.
a. General. The loading bench is the primary component of the "dry" side
(manual) and "dark side" (automatic) of the processing room. It contains an area for
loading and unloading film holders, a cassette transfer cabinet, a film bin, compartments
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for cassettes and exposure holders, storage for hangers, a wastepaper receptacle, and
storage for processing materials. Generalized layouts for a loading bench are shown in
figures 2-4 and 2-5. In figure 2-4, the racks for storing dry film hangers are above the
loading bench and storage compartments are beneath the bench.
b. Loading Area. The length of the loading bench depends on the volume of work
and the space available. The minimum length of the working surface should
accommodate two 14 by 17-inch cassettes, side by side, to permit unloading and
reloading of two cassettes. Preferably, it should be long enough to accommodate at least
four 14 by 17-inch cassettes, side by side, to preclude piling of cassettes. The working
surfaces shown in figures 2-4 and 2-5 require approximately 96 inches, exclusive of
transfer cabinet and dryer space. The bench should be about 36 inches high and 24
inches deep. A strip of one-half by one-inch molding placed lengthwise and six inches
from the back edge of the bench anchors the cassettes while they are being opened and
closed and keeps them at the front of the bench within the working area of maximum
efficiency.
c. Film Bin. It is customary to keep a supply of opened boxes of film sufficient for
immediate needs underneath the loading bench. The most convenient method is to use a
lightproof film bin having compartment in which opened film boxes can be kept upright.
e. Storage Cabinets. As shown in figures 2-4 and 2-5, closed cupboards for such
items as packaged chemicals, solution-mixing accessories, and towels may be located
either above or below the loading bench.
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Figure 2-4. Loading bench section with hangers mounted above bench.
Figure 2-5. Loading bench section with hangers mounted below bench.
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2-8. PROCESSING TANKS
a. General. Processing tanks are used for such operations as developing, rinsing,
fixing, washing, and drying x-ray films. Tanks as well as mixing vessels are usually made
of stainless steel. These tanks are the "wet side," and are usually used in manual
processing. In automatic processing, all of the processing tanks are in a closed
compressed unit, and require less maintenance than the manual tanks. The following
information will generally apply to manual processing.
(1) Master tank. The master tank serves as a water jacket for holding insert
tanks and usually provides space between the insert tanks for washing and rinsing. If a
washing tank is available, washing will be done in it.
(2) Insert tanks. Insert tanks are removable containers for individual solutions,
which are placed in the master tank. The stainless steel insert tanks are standardized at a
five-gallon capacity. The American Standards Association gives the inside dimensions of
a standard 5-gallon tank as 20-1/32 inches deep, 14-1/2 inches long, and four inches
wide. To check a tank of unknown size, use the following formula:
When the inside dimensions of the tank are correct, the solution level is one inch below
the crossbar ledge.
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Figure 2-6. Conventional arrangement of a small tank unit (top view).
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e. Cascade Wash Tank. Cascade washing of radiographs is the most efficient
method because it rinses the fixer solution off the film with a minimum amount of water.
Although an additional operation is required for moving the films from one compartment to
the next, the cascade system is especially useful in installations handling a continuous
volume of films. The tank (figure 2-8) consists of two washing compartments and an
overflow well. The fresh water flows into the bottom of compartment "A," passes upward
over the partition into the compartment "B," under the end wall of the tank proper, and
through the outlet "C" in the overflow wall.
(2) Overflow well. The chief purpose of the overflow well in a cascade system
is to permit the draining of water from the bottom of the adjacent washing compartment
through a standard standpipe or through an overflow pipe in the back of the tank.
NOTE: Arrows indicate water flow from inlet over both film surfaces and to outlet.
f. Temperature Control. The temperature of the solutions should be controlled
closely. The ideal situation would be to maintain both the air and the tap water at 68ºF,
which would keep the washing water constant with the solutions. Since this is seldom the
case, some method of temperature control becomes necessary.
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(2) Heating unit. In the laboratory, the hot water tap may be utilized. In the
field, a suitable immersion-heating unit can readily raise the temperature of the solution
above 60ºF, the minimum processing temperature.
(3) Thermometer. Processing of radiographs requires that an accurate check
on the temperature of the solutions be maintained at all times by the use of a reliable
thermometer. The temperature should always be checked when the work is first begun
and at intervals throughout the day. The optimum temperature of 68ºF, recommended by
the American Standards Association, has been adopted. Do not attempt to judge the
temperature of a solution by dipping a finger into it.
(4) Tank insulation. The master tank may require insulation, especially when
there are wide differences between ambient air temperature and the optimum processing
temperature. If the air is much warmer than the processing solutions, an uninsulated tank
might condense enough moisture to be annoying and it could be difficult to hold the
solutions at the right temperature. Air conditioning solves this problem very effectively. In
the field, however, the specialist may find it necessary to improvise insulation with
blankets.
g. Drainage Facilities. The drain line must be large enough to accommodate the
maximum simultaneous flow of water from both the water jacket and the washing tank.
Both size and pitch (slope) of the line affect the rate of flow. The pipe should be at least
two inches in diameter and the pitch at 1/4 inch per foot. Flushing the drain with rapidly
flowing water after old processing solutions have been discarded through it will help
prevent corrosion and deposits. In the field, drainage should be into a seepage pit or
ditch.
2-9. MAINTENANCE OF TANKS
Trays, tanks, and other processing equipment frequently become discolored and
encrusted through use. Frequent rinsing and drying is the best prevention for these
conditions. Strong cleaners should be used only when really needed. Exercise care when
using these cleaners, because they usually possess strong acids or alkalines.
a. Oxidized developer stains (brown or yellow-brown) can often be removed with
soap and water. If not, tray cleaner formula or some similar product will be needed. An
effective tray cleaner can be prepared by mixing 32 ounces of water, three ounces of
potassium bichromate, and three ounces of concentrated sulfuric acid.
CAUTION: Always add the sulfuric acid to the water and potassium chromate solution,
stirring constantly. Never add the solution to the acid as it may cause boiling
and spattering, leading to serious burns.
To use, pour a small amount of the solution into the vessel, rinse it around to be sure it
reaches all surfaces, pour it out, and wash the vessel six to eight times with water. Do not
use the solution on your hands.
b. Developer tanks accumulate a scale of basic calcium sulfite, which is difficult to
scrub off. This scale is soluble in acids, but ease of removal varies according to the
MD0954 2-14
conditions under which the scale was formed. Fill the tank with stop-bath solution and
allow to stand overnight. A strong stop-bath solution can be prepared by adding
16 ounces of 28-percent acetic acid to one gallon of water. To make 28-percent acetic
acid, combine three parts alcohol acetic acid with eight parts water. If this stop-bath
solution does not loosen the scale, try a five percent solution of hydrochloric acid. Be very
careful, as the acid solution can pit stainless steel.
c. Wash tanks often become coated with algae that may stick to the film.
Thorough cleaning and weekly treatment with commercial bleach solution consisting of
one part bleach to six parts water, removes algae. Be sure to cover the inside of the
intake and overflow pipes with the solution, since algae often grows there. Leave the
solution in the tank overnight; drain, scrub, with a stiff brush; and rinse four or five times.
2-10. THE FILM DRYER
a. The drying of radiographs is always important. The dryer is fitted with heating
elements and a large fan, both on the same circuit. The dryer duct should vent outside the
building to prevent excessive humidity.
b. The small processing room in which only a few films are processed daily usually
does not justify installation of a dryer. In such a case, a commercial drying rack is
adequate. When a commercial rack is not available, a one-by three-inch board can be
drilled with three-eighths inch holes, about four inches apart and mounted on a high wall.
c. The drying unit may be installed along the wall at one end of the processing
room or underneath the loading bench. The drying of films is usually considered a "wet
film" operation, but with reasonable care can be carried out at a low location on the "dry"
side of the room.
d. When air is drawn in rather than blown through the dryer, a uniform air flow
results. Airflow should be at least 450 to 500 cubic feet per minute. Air temperature inside
the dryer should be maintained at the coolest temperature that will dry the film--never
more than 120ºF. Heating elements and the fan should be on the same circuit.
e. Suitable insulation is placed around the dryer so that the temperature of the
room is not unduly affected. The drip pan underneath each film drawer should be kept
clean and free of dust and debris.
Section II. PROCESSING ACCESSORIES
2-11. ARRANGEMENT
Processing accessories should be kept near the section of the processing tank
where they are used. Time-temperature guides, exhaustion charts, and other processing
information are readily referred to when fastened to a chart board placed near the
developing tank. A shelf for the interval timer and thermometers should be located near
the developer section. Other accessories may be placed on shelves above and behind
the processing tanks.
MD0954 2-15
2-12. PROCESSING HANGERS
(1) Sheet film hanger. The sheet film hanger holds the x-ray film taut during
processing. It consists of a crossbar and rigid frame to which are attached four clips, two
of which are mounted on a bow spring welded to the crossbar (figure 2-9).
(2) Dental film hanger. The dental film hanger consists of a bar to which film
clips are attached.
(3) Roll film hanger. When it is necessary to process roll film and a special
processing tank is not available, a special adjustable processing hanger may be used. It
will accept 35, 45, 50, 60, and 70 mm film widths and any length up to 11 feet. The outer
frame is approximately the size of a 14 by 17-inch hanger and can be used in the regular
processing tanks. For four by 10-inch short film and 70 mm roll film, there are special
hangers, which will fit the same five-gallon tanks.
(1) Acetic acid treatment. Soak the hangers or clips for an hour in a tray filled
with a 10-percent solution of acetic acid to nine parts water or one part 28-percent acetic
acid to two parts water). Then wash with clear water and a stiff brush.
MD0954 2-16
(2) Trisodium phosphate treatment. Boil the equipment for several minutes in
a 10-percent solution of trisodium phosphate, wash it with a stiff brush. This method is
especially useful for cleaning deposits mixed with gelatin.
(3) Acid bichromate treatment. Tray cleaner formula may be required if silver
deposits remain. Dilute the regular formula, one part to two parts water. Soaking for
10 minutes is usually sufficient. Rinse well and brush off any reddish scale. Use a glass
or hard rubber tray as enamel is etched by this solution. In addition, this solution should
not be used on chromium-plated articles.
The interval timer is used to regulate the period of development of the exposed x-
ray film. The dial face should be marked in minutes, usually up to and including 30, with
each minute subdivided into quarter-minute intervals. The timer most commonly supplied
is spring wound, usually by depressing the winding lever.
a. Mixing Equipment. Two 2-gallon stainless steel pails for solutions, a stainless
steel or plastic funnel, and two stainless steel mixing paddles are the usual items of mixing
equipment supplied.
b. Filler and Drainer Pump. When circulating water is available, a small filler and
drainer water pump is useful for emptying and filling solution tanks not equipped with
outlets. This device consists of a three-branched rubber hose, one for connecting to a
water faucet, one for the solution tank, and one for the sink. When the faucet is turned on,
the tank drains rapidly because of the suction.
MD0954 2-17
EXERCISES, LESSON 2
After you have completed all the exercises, turn to "Solutions to Exercises," at the end of
the lesson and check your answers.
2. In a processing room, the minimum distance between the "dry side" and the "wet
side" is:
a. Three feet.
b. Six feet.
c. Four feet.
d. Two feet.
a. Lightlock.
b. Single door.
c. Maze.
d. Labyrinth.
MD0954 2-18
4. The labyrinth requires____________________ floor space as a lightlock.
5. Which filter is normally used in a darkroom safelight with a 15-watt tungsten bulb?
a. 5A.
b. 6A.
c. 6B.
d. 8B.
c. A densimeter.
7. What effect, if any, does a light-colored wall have on indirect safelight illumination?
MD0954 2-19
8. Hanger bow springs lose tension through:
a. A lifetime tension.
b. Moisture.
c. Dryness.
d. Prolonged use.
9. What protective measures should be used to prevent possibly fatal electric shock i in
the film processing room?
10. Which piece of equipment listed below would be located on the "dry side" of a
processing room.
a. Loading bench.
b. Film dryer.
c. Timer.
d. Sink.
11. For convenience, the cassette transfer cabinet should open onto the end of the
loading bench and outside into:
MD0954 2-20
12. Which of the materials listed below would be used in containers for mixing x-ray film
processing chemicals?
a. Tin.
b. Aluminum.
c. Galvanized iron.
d. Stainless steel.
13. Which equipment or functions, listed below would be likely to be located on the "wet
side" of a processing room?
a. Loading bench.
b. Processing tanks.
c. Film bins.
d. Hanger storage.
14. A processing tank has the following dimensions: four inches wide, 14-1/2 inches
long, and 20 1/32 inches deep. Using the formula in the text (para 2-8b(2)) what is
the capacity of the tank?
a. 4.7784 gallons.
b. 4.9840 gallons.
c. 5.0000 gallons.
d. 5.1001 gallons.
MD0954 2-21
15. In manual processing of x-ray films, which of the following methods permits the
complete washing of films with a minimum amount of water?
b. Aeration tank.
c. Tray.
d. Cascade.
16. If a developer tank coated with a scale of basic calcium sulfite cannot be cleaned
with a stop bath solution, what should be used?
a. Tray cleaner.
17. The operating temperature for a film dryer should not exceed:
a. 101°F.
b. 120°F.
c. 180°F.
d. 212°F.
18. Spongy deposits of silver on metal film hangers must be periodically removed or they
may:
MD0954 2-22
19. Which of the following is most efficient for regulating the period of development of an
exposed film?
20. The filler and drainer pump has one branch of its base to the sink and one branch in
the solution tank. For the pump to properly drain the solution tank, the third branch
must be:
MD0954 2-23
SOLUTIONS TO EXERCISES, LESSON 2
1. b (para 2-2a)
2. c (para 2-2c)
3. a (para 2-3b)
4. a (para 2-3c)
5. c (para 2-4b((1))
6. a (para 2-4b((4))
7. d (para 2-4b)
8. d (para 2-5b)
9. c (para 2-6a)
= 4 X 14.5 X 19.03)
231
MD0954 2-24
15. d (para 2-8e)
End of Lesson 2
MD0954 2-25
LESSON ASSIGNMENT
LESSON OBJECTIVES After completing this lesson, you should be able to:
MD0954 3-1
Section I. AUTOMATIC FILM PROCESSING
3-1. INTRODUCTION
MD0954 3-2
c. The rollers of the crossovers and racks move by means of a main drive shaft
run by a drive motor. Through a series of cogwheels and gears, the energy is
transferred to the rollers from this drive shaft.
d. No attempt will be made to cover all the mechanics of the crossovers and
racks because of the great variation between models. If a breakdown occurs,
maintenance personnel or the manufacturer will repair the processor.
The roller-transport system squeezes the chemicals into and out of film emulsion,
providing an agitating action, which promotes even processing and increases the speed
of reactions. A circulation-filtration system is used to boost this action. The circulation
pump recirculates the solutions through filters, keeping the chemicals properly mixed
and clean as well as in a state of agitation.
a. As each film passes through the automatic processor, the chemicals are
changed slightly. To offset the resulting deficiencies, new developer and fixer in
measured amounts are pumped into the solutions. This is called replenishment.
b. There are two tasks, called replenisher tasks, in which fixer and developer are
stored. The tanks are protected by dust covers and a floating lid in the developer tank
helps to reduce oxidation.
c. When a film is initially fed into the processor, it activates the micro switch
previously mentioned. The micro switch turns on the replenisher pumps and new
solutions are pumped into the system, which filter out dirt from the replenisher solutions.
MD0954 3-3
b. The wash water temperature is controlled by a mixing valve, which mixes the
hot and cold water. A thermometer gauge is located between the mixing valve and the
wash tank near the mixing valve. Usually a shutoff valve is located between the
thermometer and the mixing valve so that readjustment of the mixing valve is not
necessary each time the water flow is shut off.
To dry the film, there is a heater to heat the air and a blower to move the air.
There must be a good exhaust system to remove the warm, moist air so that only hot,
dry air is directed over the films as they move through the roller-transport system.
There are holes at the ends and slits along the sides of the air tubes to direct the air
onto the films.
3-8. CHEMISTRY
a. Starting.
MD0954 3-4
(3) Allow 15 minutes for solutions to warm.
(4) Remove crossovers. Turn sun gear and wipe crossover rollers with
damp sponge or cloth. Wipe stainless steel feed rollers and the guide plates of
developer rack(s). This should be done whenever the machine has been idling long
enough for chemicals to dry on the roller, even if the machine has been turned on.
(5) Check solution level in processor and replenisher tanks. Check wash
water flow.
(7) Insert film between stainless steel feed rollers and adjust flow meters for
correct replenishment rate.
(8) Reinstall crossovers and visually check operation of racks and dryer
rollers.
(10) Run enough clean-up film to clean rollers, which are out of solution. Do
not reuse clean-up sheets.
b. Feeding Film.
(1) Place film on feed table and push in until rollers pull it forward. (See
manufacturer's recommendations for detailed instructions.)
c. During Operation.
d. Stopping.
(2) Remove crossovers and wipe with damp sponge or cloth. Use a
nonmetallic pad for stubborn dirt and chemicals.
MD0954 3-5
(3) Wipe stainless steel feed rollers and check that they turn freely and then
reinstall crossovers.
(8) To prevent rusting, leave dryer and processor covers open slightly when
machine is not running.
e. Standby Position.
(1) To allow for emergency work at night or during other slack periods, leave
only heat and cool switches on. Then, when other switches are turned on, machine will
be ready for processing within 10 minutes.
(2) Also leave the valve(s) open in the cold water supply line to heat
exchanger.
(c) Remove film at this point to avoid further pile-up. Put films in a tray
of water to prevent them from sticking together.
(d) Clear the film jam. Turn off circulation if a rack is removed.
(e) Feed the removed films into the rack nearest the point of jamming
to complete cycle.
MD0954 3-6
(b) Cut the film at the feed.
3-11. MAINTENANCE
(1) Remove the crossbars and wipe with damp sponge or clothe. Use a
nonmetallic pad for stubborn dirt and chemicals.
(2) Clean the stainless steel feed rollers and be sure they turn freely.
(3) Remove the solution racks. Check the tanks for foreign matter. Rinse
the racks with running water and clean off any chemical deposits and dirt. Use a
nonmetallic pad for stubborn deposits.
(4) Check spring tension on the racks. Be sure roller bearings are free.
Operate each rack manually to check for binding. Check for loose setscrews. Lay the
rack on a flat surface and be sure it is square. Use a fiber or nylon brush to clean gear
teeth. Replace worn gears and springs. Reinstall the racks and crossovers.
(6) Clean dryer air tubes by removing and agitating vigorously in warm
water.
b. Miscellaneous.
(1) Clean developer rack(s) whenever a soil pattern transfers to film. When
normal cleaning is not adequate, use chemical dissolving solutions according to
directions. Be careful not to drip solutions into an adjacent tank when removing a rack.
Reinstall racks slowly so that solutions will not overflow. Do not interchange developer
and fixer racks.
MD0954 3-7
(4) When solutions are changed, remove and clean screen in bottom of
replenisher tanks. Swirl the screen through solution to remove trapped air bubbles.
(5) When changing solutions, drain tanks and flush thoroughly before
refilling.
(6) At least once a month, flush replenisher systems with hot water--not
over 150ºF. Give special attention to check valves and flow meters, which should be
removed and disassembled during cleaning.
(7) Clean the solenoid valve periodically; the frequency of cleaning will
depend upon the cleanliness of the water supply.
3-12. INTRODUCTION
This section will discuss the techniques of applied chemistry used by the x-ray
specialist in manual processing of x-ray films. Although most hospitals now use
automatic processors, there may be times when knowledge of manual processing
procedures is required.
MD0954 3-8
chemicals, turn off electric fans for chemicals may be blown about the room and
contaminate the loading bench, screens, or other equipment. Hands that are wet with
chemicals should never be used for handling films, screens, or other accessories.
Since water is the solvent for all processing solutions, same care should be
exercised in choosing its source. Most city water supplies are suitable, but they should
be checked for high concentrations of various salts before use. In general, any water
that is good to drink should be satisfactory.
a. Pure Water. Distilled water, since it does not contain dissolved chemicals, is
pure and therefore ideal for mixing purposes. Rainwater and water melted from clean
snow are good substitutes.
b. Water Impurities. The chief kinds of impurities usually found in water are as
follows:
(2) Some solid chemicals found freely in nature are often dissolved by
water. These chemicals cause hardness of the water and are composed of calcium and
magnesium salts in the form of bicarbonates, chlorides, and sulfates. These salts are
not injurious to the image but may produce a scum on the surfaces of the film that
reduces its transparency. It must and can be removed before drying by squeegeeing
the faces of the radiograph with cotton or a photographic sponge. Circulating the water
through a water softener may eliminate the hardness of the water. In general, most
metropolitan areas use water containing some minerals, but experience few, if any,
problems.
MD0954 3-9
3-17. MIXING PROCEDURE
Water should always be poured into the tank and the chemicals added slowly
while the mixture is stirred vigorously. In this way, the chemicals dissolve rapidly. (To
ensure the proper concentration of solution, the volume in gallons of the tank used
should be determined mathematically.) Sufficient water should be added to bring the
solution to the correct volume and temperature; thorough stirring is necessary to mix the
cool water with the chemical-laden solution. Solutions should not be used until all the
chemicals are thoroughly mixed and at the optimum temperature of 68°F.
If the solution is not for immediate use, it should be placed in a clean brown
bottle of the proper size, well stoppered, and labeled plainly. Developer should be
stored away from radiators, as heat may cause deterioration of the solution.
The tank method of processing is efficient and convenient. Its most important
advantage is that it provides facilities for maintaining constant temperatures and for
preserving the solutions. Tanks containing the processing solutions are located in a
master tank containing water at the prescribed temperature and sufficient space is
provided for film rinsing and washing. Water should be circulated in the master tank at
a temperature that is controlled by a mixing valve situated in the hot and cold water
supply. If the volume of radiographic work justifies it, a separate tank used only for
washing purposes should be provided.
As the film is first lowered into the developer solution, it should be rapidly moved
up and down a few times to remove the air bells (small air bubbles) from the film. If
these were not removed, the film would not correctly be processed at those points.
After an exposed x-ray film is placed in the developer, the gelatin in the emulsion
becomes swollen and porous due to the presence of water and the activity of the alkali
in the developer solution. The exposed silver bromide crystals have become ionized
and the reducing agents can attack them. The x-ray exposure causes the sensitization
MD0954 3-10
specks to acquire atomic (photolytic) silver ions form the disintegrating silver bromide
crystals are exhausted. The bromine ions are freed from the emulsion and react with
the potassium ions form other completion of development; the exposed silver bromide
crystals have been reduced to bock metallic silver, which constitutes the image. The
unexposed and undeveloped silver bromide crystals remain largely unaffected, but are
removed by a later treatment (fixing).
a. When using the replenisher system, film should be removed from the
developer quickly and the excess solution should not be drained back into the developer
tank, but rather into the waste outlet. Normally, this procedure will remove about the
proper amount of solution for efficient use of this system. Approximately one gallon of
replenisher should be added for every forty 14 x 17-inch films or the equivalent. If
sufficient solution has not been drained to waste by the films, it may be necessary to dip
a measured quantity of developer from the tank and to add a comparable amount of
replenisher to maintain normal developing activity. However, by the frequent addition of
small quantities of replenisher solution, the proper level of the developer and the activity
of the solution can be easily maintained. This procedure relieves the specialist of the
responsibility for computing the actual quantities needed for replacement; however, a
record of the volume of replenisher used must be maintained.
b. It is important that you never add replenisher solution to the developer while
films are developing. This may ruin the films with streaks of very high density.
MD0954 3-11
3-24. RINSING PROCESS
When the film is removed from the developer, the gelatin emulsion is swollen and
like a sponge, saturated with all the soluble chemicals of the developer solution. Also,
the gelatin contains the black metallic silver image and unexposed, undeveloped silver
bromide crystals. The bulk of the soluble developer chemicals should be removed from
the film before it is placed in the fixing bath and these chemicals replaced by either
fresh or acidified water. Such treatment is necessary to stop the reaction of
development, to neutralize the alkalinity of the residual developer, and to remove the
oxidation products of development. There are two methods of removing these
chemicals--rinsing the film in fresh water and rinsing the film in acidified water.
After development, the film should be rinsed for 30 seconds in circulating fresh
water and drained before being placed in the fixer. This rinse should remove the
soluble developer chemicals form the surface of the film and the pores of the emulsion.
The emulsion on a 14 by 17-inch film holds at least three ounces of developer. To stop
development, the residual developer must be quickly diluted with water. If films are
insufficiently rinsed and repeatedly placed directly in the fixing bath, the chemical
balance of the fixer is eventually upset and its useful life materially shortened. Poor
rinsing causes the acidity of the fixer to be rapidly reduced, the hardening action to be
destroyed, and stains to appear on radiographs. Still, water should not ordinarily be
used for rinsing. An accumulation of developing solution in the rinse bath eventually
oxidizes and when it is carried over to the fixing solution, it streaks and stains
radiographs because of fixing solution contamination.
a. Acid rinse baths prolong the life of the fixer and ensure maintenance of the
hardening action. An acid rinse bath eliminates the need for running water (required by
a water rinse bath). The most efficient rinse (stop) bath is one consisting of a dilute
solution of acetic acid in water made according to the following procedure. Add two and
one-half quarts of 28-percent acetic acid to one gallon of water. Stir thoroughly. Add
sufficient water to make five gallons of solution. This bath can be made in a five-gallon
tank and placed between the developer and fixer tanks. The bath immediately stops
development of the emulsion and neutralizes the alkali in the developer contained in the
emulsion.
b. Radiographs should be rinsed in the acid bath for 30 seconds but they may
be left in the bath for as long as one and one-half minutes. Do not overwork the acid
rinse bath. When the activity of the solution is reduced, it will accentuate rather than
prevent stains and streaks. The acid rinse bath will operate satisfactorily within the
normal range of processing temperature when the rapid x-ray developer is used.
During this useful life, the acid rinse bath will rinse about 200 14 by 17-inch films or their
equivalent per five gallons of solution.
MD0954 3-12
3-27. FIXING PROCESS
c. The duration of the fixing process is dependent upon several factors. These
include the strength and nature of the fixer; the temperature of the solution, the amount
of film agitation, the volume of fixing agitation is related to the number and surface area
of films being fixed, and the emulsion thickness. The minimum fixing time is that
needed to clear and harden the film. For best results, the film should remain in the
fixing bath three times as long as necessary to clear the film.
d. Although radiographs may be left in the fixer for a slightly longer period, it is
not wise to do so, for it will only take longer to wash them free of residual silver and
fixing bath salts. The hardness of the emulsion in a given fixing solution decreases with
solution exhaustion and the initial fixing time must be extended as the solution is used
to maintain normal hardening.
e. Also, the higher the temperature, the greater the speed of fixation; however,
the optimum range of temperatures is from 60º to 75ºF. With higher temperatures, a
fixing solution tends to sulfurize, thereby shortening its life. Therefore, it must be
specifically treated when high temperatures prevail.
a. Most processing tank systems only provide for a single tank of fixing solution.
The use of a single bath is not the most efficient nor economical method for fixing. The
gradual accumulation of silver salts in the bath makes longer washing times necessary
because of the difficulty in replacing these salts with pure water.
b. Normally, the usefulness of a single tank fixer ends when the bath loses its
acidity or when more than twice the normal times is required to remove the unexposed
silver from the film. The bath should then be discarded, especially if it has become
turbid. An exhausted fixing bath permits abnormal swelling of the emulsion due to
deficient hardening action. Consequently, drying is prolonged and reticulation or
MD0954 3-13
sloughing of the emulsion may take place. Neutralization of acid in the bath invariably
causes certain kinds of stains on the radiographs. A good rule to follow is to change the
fixing bath when fresh developer is made, if the fixer tank is twice as large as the
developer tank and proper temperatures are maintained. When exceptionally high
temperatures prevail, the fixing bath should be changed twice during the life of the
developer. This assures maximum hardening of the emulsion and freedom from "hot
weather troubles."
c. When the volume of the fixing solution is the same as that of the developing
solution, the fixing solution should be changed twice during the life of the developer to
ensure satisfactory clearing and hardening of the emulsion. Table 3-1 is a guide for
determining the clearing time, fixing time, and exhaustion point.
Table 3-1. Life of five gallons of unreplenished fixing solution in a single tank
at temperature range 60º to 75ºF.
A fixing solution gradually loses its acidity because of the carryover of the
alkaline developer by the film. It also becomes diluted by water carried over from the
rinse bath. Consequently, its hardening properties and fixing rate are gradually
affected. The exhaustion of the thiosulfate reduces its ability to dissolve silver salts.
The loss in function of the fixing solution can in some measure be restored by
replenishment.
MD0954 3-14
normally used to make five gallons of solution can be dissolved in 12-1/2 quarts of water
and stored in bottles for future use. The rate of replenishment is illustrated in Table 3-2.
NUMBER 14 X 17
FIXING
INCH FILMS CLEARING
TIME REPLENISHMENT
FIXED PER TIME (MIN)
(MIN)
5 GALLONS
Remove 2 qts old solution; replace with
0-50 1½-2¾ 5
2 qts replenisher. *
Remove 2 qts old solution; replace with
51-100 1¾-3 5
2 qts replenisher. *
Remove 2 qts old solution; replace with
101-150 2-3 5
2 qts replenisher. *
Remove 2 qts old solution; replace with
151200 2-3½ 5
2 qts replenisher. *
Remove 2 qts old solution; replace with
201-225 2½-3¾ 7
2 qts replenisher. *
Discard fixer solution; make new
226-250 3-4 8
solution. *
* Replenisher is made by dissolving concentrated fixer in less water than is used in
preparing the fixing bath. RESULT: Replenisher is stronger than the fixing bath. See
manufacturer's instructions for proper dilution.
Table 3-2. Replenishment of x-ray fixing solution (five gallons) in a single tank.
a. Method. One of the quickest and most economical ways to remove silver
salts from radiographs is the use of the two-tank fixing bath. This bath consists of two
equal sized tanks of fixing solution. The first tank is reserved for clearing the film and
the second tank for hardening of the emulsion. Radiographs are taken from the rinse
bath and placed in the first tank where most of the silver salts removed. When the film
is cleared, it is removed to the second bath where the emulsion is hardened. Because
of this procedure, the second bath has a very low concentration of salts and the
diffusion of the reminder of these salts is exceedingly rapid. Since very few silver salts
are carried over to the washing tank, the washing time can be materially reduced.
MD0954 3-15
tank has hardened the equivalent of 180 14 by 17-inch films and then when used as the
number one tank can be used for another 180 of the same size films or their equivalent
for clearing purposes. Once the routine has been established, this system of rotation
between tanks will assure the production of well-fixed films indefinitely.
a. General. The time required for adequate washing depends principally upon
the type of film, the rate of water flow through the tank, and the temperature of the
water. If circumstances demand, a shorter washing time may be used. As long as the
film is not subjected to high heat and humidity conditions, it may be thoroughly washed
at a later time (within three to six months). Generally, if a radiograph is to remain in a
temperate zone, less washing is necessary than for those kept in a tropical or
subtropical region. However, every effort should be made to wash the film properly
during its initial processing, since it is unlikely that at this time the area of ultimate
storage can be determined.
b. Washing in a Single Tank. If the hourly flow of water through a single tank
is four times the capacity of the tank, 30 to 40 minutes is required for washing x-ray film
MD0954 3-16
at a water temperature of about 70Fº. When the flow is eight times the tank's capacity
per hour, the washing time is 25 to 30 minutes. Shorter washing times than these
should not be used no matter how frequently the water in the tank is changed. If the
flow of water through the tank is very slow, the films should remain in the water even
longer than the above specified times. The washing time should be measured from the
immersion of the last film in the wash water, since washed and partly washed films
fixing bath chemicals rinsed into water from newly added films.
The temperature of the wash water is important. It should range between 68º
and 70ºF, if possible. This range is about 40 percent more efficient than 40º would be,
for instance, and temperatures above 75ºF tend to soften the emulsion, leaving it open
to damage. In general, the temperature of the wash water should approximate that of
the other processing solutions.
3-35. USING SEAWATER FOR WASHING
Film may be washed in seawater, but they should receive an additional final
washing in fresh water for at least five minutes. Otherwise, the film may attract excess
moisture and the image may fade rapidly. Seawater does remove the chemicals more
rapidly than fresh water and washing time may be cut in half. Washing in seawater or
other salt water may be done at lower temperatures, even at 5º0F or lower. When
processing solutions have been mixed with seawater, it is advisable to wipe the
surfaces of the radiograph with a soft, wet cloth after washing.
The success of any drying operation lies in the rapid removal of the water from
the emulsion. The most common procedure is the use of a rapid flow of air (with or
without the aid of heat) over the edges of the film surfaces. Drying often takes more
than all the other operations together, so it is often a bottleneck in the flow of
radiographs through the processing room. The radiographs are wet and vulnerable to
damage, so they should not be removed from their hangers. If they are not handled
carefully, dust may become embedded in the emulsion or the film may get scratched
and abraded.
MD0954 3-17
3-37. DRYING AIDS
a. Prevention of Emulsion Swelling. The speed with which x-ray film dries is
dependent upon the quantity of water that must be evaporated from the emulsion. This
speed is proportional to the combined thickness of the emulsions. It is, therefore,
necessary to prevent excessive emulsion swelling. The use of a good fixing bath will
keep swelling to a minimum by shrinking and hardening the emulsion. The emulsion
should be hardened before excessive swelling can occur. Hardening of a swollen
emulsion raises its melting point but does not necessarily reduce its thickness.
Consequently, developing and fixing solutions should be within the optimum
temperature range. These precautions should especially be observed when processing
is done in hot, humid climates where drying always tends to be prolonged. Washing of
the film should be adequate but not excessively long. When processing temperatures
are above 75ºF, special treatment keeps the emulsion hard, provided that short washing
times are used.
c. Alcohol. The use of alcohol for drying is recommended only where some
emergency requires the use of a dried radiograph in a minimum of time after
processing. Any good grade denatured alcohol may be used for drying films, provided
that when diluted with water it does not turn milky. The alcohol concentration should be
no greater than 70 percent by volume if opalescence of the emulsion or deformation of
the base is to be avoided. After washing, the radiograph is thoroughly drained. Then,
the film is immersed in a tray of alcohol for two minutes at temperatures under 70ºF.
The tray should be rocked to assure uniform bathing of both film surfaces and to
prevent the film from sticking to the bottom of the tray. This operation causes the water
to diffuse from the pores of the emulsion, and the water is replaced by the alcohol. With
the bulk of the water removed, the film is immersed in a second and final tray of alcohol
to remove any residual water. The film is then drained. The alcohol will evaporate
rapidly to leave a dry emulsion.
d. Dryers. X-ray departments are usually provided with cabinet dryers equipped
with a fan and heating elements. The dryer should always be vented to the outside of
the processing room to prevent excessive humidity. Drawers are provided in which the
films are hung in their hangers. Ordinarily, radiographs should be dried with air
moderately warm. Heat should be used cautiously when drying films in hot, humid
MD0954 3-18
weather because the water-laden gelatin emulsion may soften and distort the
radiographic image. Under these conditions, it is safest to use only the dryer fan.
Overheating of the dryer should be avoided because very rapid drying is apt to cause
distortion of the radiograph.
e. Drying Rack. When a small number of films are to be dried each day and a
cabinet dryer is not available, film hangers may be inserted in a wall drying rack. The
rack may be simply a board in which holes have been drilled into which one end of the
hanger crossbar can be inserted while the film is drying.
The time required to dry a film is dependent upon the efficiency of the hardener
in the fixing solution, the amount of water retained in the gelatin emulsion after washing,
the velocity and temperature of the drying absorption is reduced to a minimum by the
use of a reasonably fresh fixing solution which will assure proper hardening of the
emulsion. Ideally, the humidity should be below 50 percent and the temperature under
90ºF. When films are dried in cabinet dryers, they should be adjusted so that drying
takes place in 10 to 20 minutes. The use of infrared lamps is not recommended, since
they cause unequal drying of the film surfaces.
After the radiograph has been dried, the sharp and/or punctured corners caused
by the hanger clips should be trimmed with a corner cutter or scissors. This enhances
the appearance of the radiograph, facilitates its insertion into an envelope, and
precludes its scratching other radiographs with which it may come in contact. After its
corners are trimmed, the radiograph should be placed in a heavy manila envelope of
proper size and all essential identification written legibly in the space provided on the
face of the envelope. Given to the radiologist in this condition, it is ready for subsequent
filing.
MD0954 3-19
film under step number six. Therefore, upon development, the quantity of silver
deposited in area number six is less than that under number one. A deposit of silver
that is proportional to the exposure represents each step.
b. Upon development (D), the latent image silver bromide is reduced to metallic
silver and the unexposed silver bromide (thin diagonal lines) is not affected. (Mixed with
the metallic silver deposits are some unexposed and undeveloped silver bromide
crystals.)
c. After the film has been fixed (E), all the unexposed and undeveloped silver
bromide is dissolved from the emulsion and the metallic silver remaining on the film
constitutes the radiographic image of the step wedge shown in (A).
d. When the radiograph (F) is later viewed on an x-ray illuminator, all the various
deposits representing the steps of the wedge are seen in their proper concentrations
and various degrees of translucency. To obtain an optimum density, full development is
required.
MD0954 3-20
e. In the preceding diagrammatic examples, the amount of silver deposited by
development depended upon length of exposure of the silver bromide crystals to x-rays,
the length of time of development, and the temperature of the developing solution. As
the development time and/or temperature of the developer increases, the amount of
silver deposited increases, and vice versa. Radiographic density and other film
characteristics are influenced by the time of development and the temperature of the
solution, adequate density control may be obtained by standardization. Once this is
achieved, radiographic density as influenced by development may be considered a
constant.
a. There are several ways that a film may be developed, but the standard time-
temperature method is almost universally used. This method is virtually foolproof and
provides an excellent means for checking x-ray exposures. The quality of a radiograph
depends upon full development of the x-ray film within a limited temperature range.
Variations from the optimum must be carefully compensated to maintain quality. Once
standardized, processing rules are established and followed, overall changes in density
and contrast can be attributed to exposure factors. Standardized processing of the film
can then become a constant as long as a reasonable measure of discipline is exercised
in the processing room.
MD0954 3-21
3-43. DEVELOPER CONTRAST
The type of developer solution used produces a degree of image contrast that is
considered optimum by the manufacturer. Therefore, developer contrast may be
considered a contrast when the solution is used according to the directions outlined by
its manufacturer. Full advantage of this constant is usually obtained when complete
development of the image takes place.
The time of development given to an exposed x-ray film materially affects the
amount of silver deposited on the radiograph. As the time development increases up to
a certain point, the amount of silver increases. In general, the time required to develop
a film in a given developer depends upon the emulsion and its thickness. To assure
accurate timing of all processing procedures, it is necessary to use a properly
functioning interval timer. A series of correctly exposed hand radiographs was made
using identical x-ray exposure factors, but each film was developed for a different period
of time at temperature of 68ºF.
a. The radiograph developed for one minute shows only slight traces of silver
deposit. Image detail is lacking and the contrast is low. The streaked background
density is characteristic of the underdeveloped radiograph.
b. The radiograph developed for two minutes shows some of the important
features of the image and a greater overall deposit of silver (B, figure 3-8). Image detail
and contrast are somewhat improved.
MD0954 3-22
c. The radiograph developed for three minutes shows more silver deposited, but
the image is still somewhat weak.
d. The radiograph developed for four minutes shows a fairly well defined image.
e. The radiograph developed for five minutes shows all essential details, for the
maximum amount of silver has been deposited on the film. The exposure was such as
to provide a satisfactory radiograph when development times are not sufficient to justify
extension of the development time beyond the basic five-minute period.
Development time has a direct relation to the activity of the developer. The
reliability of the recommended normal development intervals for an x-ray film is valid
only as long as the solution has a reasonable measure of its original developing power.
When using the replenisher system, the time should remain the same as long as the
activity is restored by frequent additions of a replenisher solution.
Development time intervals should never be guessed at. There are two basic
times of development for each type of developing solution. One produces an image
with normal speed and contrast, while the other provides maximum speed and contrast.
The first basic development time provides a short time that is compensated for by
25 percent more x-ray exposure. The second is longer in time, but the x-ray exposure
is 25 percent less than the other. When employing rapid x-ray developer, normal speed
and contrast are obtained by the basic development time of three minutes at 68ºF. To
obtain maximum contrast, the time is five minutes at 68ºF. The longer basic
development period will always provide better radiographic quality than the shorter
interval because full development is assured. (See Table 3-3).
MD0954 3-23
3-50. TIME COMPENSATION FOR TEMPERATURE CHANGES
MD0954 3-24
3-51. LOW TEMPERATURES
Temperatures below 60ºF inhibit the activity of one of the reducing agents. If the
x-ray specialist is not certain of the temperature, the appearance of the film may lead
him to believe that insufficient exposure has been given. Hence, the exposure time is
usually increased in a futile effort to increase radiographic density and a cycle of
overexposure and underdevelopment occurs, resulting in poor radiographic quality. If
solutions gradually warm up to a more normal temperature and the fact are not
observed, the sequel is that no compensating reduction in exposure time is made. Over
development of an overexposed film ensures and results in deposits of excessive
density on the radiograph. Know the correct temperature at all times so that optimum
developing times and correct exposures can be used.
A developer at 80ºF requires less time to produce a satisfactory image, but the
density of the image is likely to be excessive. This high temperature will cause rapid
oxidation of the solution, which will then produce an underdeveloped, fogged
radiograph. Besides all this, the emulsion may melt from the film unless the solutions
are specially treated. When development must take place with temperatures of 75ºF
and above, the special procedures described later in this subcourse must be used.
Developer begins to age as soon as it is mixed and is fresh only while the active
chemicals are still in approximately the same concentrations as when the solution was
originally mixed. Each film developed not only removes solution by absorption and
surface cohesion, but also weakens the developer in the tank. The developer solution
should never be used after three months, because a weakened solution will produce
weak images and may cause chemical stain or fog. During development, chemical
reactions take place, which exhaust the solution. The developing agents are destroyed
by their action in reducing the exposed silver bromide crystals in the emulsion to and
bromide, as well as oxidation products, slow up the speed of development. Other
factors that shorten the usefulness of the developer are high temperatures, dilution with
water, and contamination.
The nature and concentration of the reducing agents and the effective alkalinity
of the solution affect the composition of the developer.
MD0954 3-25
3-56. DILUTION OF DEVELOPER
a. To assure uniform activity over the entire surface of the x-ray film during
processing, it is necessary after a period of activity to stir the developer and fixer
solutions thoroughly, using different paddles. Stirring is particularly important in the
case of the developer. When the developer solution is not stirred in the tank, there is a
tendency for the lower areas of the film to receive less development than the upper
areas because the temperature of the solution is usually lower at the bottom of the tank
than it is at the top. Also, the reaction products of development that tend to restrain
development are heavy and settle to the bottom of the tank. The lower temperature and
higher concentration of reaction products at the bottom of the tank cause unequal
development of the film.
MD0954 3-26
3-59. SOLUTION LEVEL
(1) Low activity. Low activity may be the result of incorrect mixing, an error
in dilution, or low temperature. An unusual drop in activity may be attributed to the
addition of water instead of fresh developer to raise the solution level, contamination
from fixing solution or acid rinse bath, or inadequate replenishment. The remedy is
adherence to a correct processing routine.
(2) High activity. High activity is seldom encountered, but it may occur
because of high temperature or the addition of more replenisher than is necessary. The
remedy is to follow time-temperature processing and a correct replenishment routine.
MD0954 3-27
(4) Sludge. As the developer is used, sludge gradually accumulates at the
bottom of the tank. This sludge may consist of insoluble calcium and magnesium salts
originally obtained from the water source; metallic silver reduced and removed from the
emulsion by the developer, gelatin, and dirt particles. The sludge does not interfere with
development unless it is present in large quantities. It can be easily siphoned from the
bottom of the tank.
(5) Slime. Some kinds of bacteria grow on the accumulated gelatin in the
developing solution despite its alkalinity. Evidence of this growth is slime on the walls of
the tank. Sometimes the slime floats in the solution and adheres to the surfaces of films
being developed. The remedy is to thoroughly clean the tank before making new
solution. After scrubbing, use a solution of sodium hypochlorite, then rinse thoroughly.
(2) Chemical fog and stain. Chemical fog and stain are usually the result of
using exhausted developer solution, contaminated fixing bath, or dirty developing
hangers.
a. Sludging. An excess of developer carried over into the fixer solution tends to
participate some of the hardening agent. The result may be a white sludge in the
solution or a white scum on the films. This sludging may be prevented if films are
thoroughly rinsed in flowing water between developing and fixing. The films should then
be adequately drained so that a minimum of developer-contaminated rinse water is
transferred to the fixer.
MD0954 3-28
development of the film may continue unevenly in the fixer solution, resulting in streaks.
The importance of adequate rinsing cannot be too strongly emphasized.
MD0954 3-29
EXERCISES, LESSON 3
After you have completed all the exercises, turn to "Solutions to Exercises" at the end of
the lesson and check your answers.
1. The micro switch in an automatic processor, used to detect the presence of more
than one film, also activates the:
a. Filtration system.
b. Transport system.
c. Replenisher system.
d. Dryer system.
c. Call a nurse.
a. Higher temperatures.
b. Lower temperatures.
c. Fast rollers.
d. Filtered solutions.
MD0954 3-30
4. When the automatic processor has been idle long enough for drops of chemical
solution to dry, you should not operate it until you wipe off the:
a. Crossovers.
b. Feed tray.
c. Main drive.
d. Cog wheels.
5. When clearing a film jam in an automatic processor, the power should be turned
_________ if sheet film is involved and ________ if roll film is involved.
c. Off, on.
d. On, off.
a. Image distortion.
b. Underdevelopment.
7. The time needed to dry x-ray film is determined by the amount of emulsion
swelling. Swelling can be controlled by using:
a. A stop bath.
b. Fresh developer.
MD0954 3-31
8. In the course of manual processing, what is the recommended time for leaving film
in the acid rinse bath?
a. 10 seconds.
b. 15 seconds.
c. 20 seconds.
d. 30 seconds.
9. When mixing x-ray film replenisher, the amount of fixer normally used for one
gallon of fixer solution is mixed with _____ quarts of water.
a. One.
b. Two.
d. Three.
10. There may be times in the field when cold weather makes washing of films difficult.
Under such conditions, it may be desirable to use:
a. Salt water.
b. Boiled water.
c. Gasoline.
d. Alcohol.
11. If the film dryer overheats, what effect can this have on the film?
d. A milky image.
MD0954 3-32
12. After manually processing and washing x-ray film, what would be the fastest way
to dry it?
13. What determines the amount of silver deposited on a processed x-ray film?
b. Development time.
d. Washing time.
14. What results when a film is developed in solutions that have been idle for a time
and are not stirred before use?
15. What chemicals should be used to control the bacterial growth that cause
slime in developing tanks?
a. Sodium sulfite.
b. Sodium carbonate.
c. Sodium thiosulfite.
d. Sodium hypochlorite.
MD0954 3-33
16. What undesirable result is most likely to occur when films are processed in
solutions with wide temperature differences?
b. Chemical fog.
c. Underdevelopment.
d. Crystallization.
MD0954 3-34
SOLUTIONS TO EXERCISES, LESSON 3
1. c (para 3-3a)
2. d (para 3-3d)
3. a (para 3-6a)
4. a (para 3-10a(4))
6. c (para 3-31)
7. c (para 3-37a)
8. d (para 3-26b)
9. c (para 3-29b)
End of Lesson 3
MD0954 3-35
LESSON ASSIGNMENT
LESSON OBJECTIVES After completing this lesson, you should be able to:
MD0954 4-1
Section I. X-RAY FILM PROCESSING UNDER ADVERSE FIELD
CONDITIONS AND OTHER SPECIAL METHODS
4-1. INTRODUCTION
a. Efficient processing of x-ray film under field conditions is often difficult. This is
particularly true when, in amphibious or airborne operations, an x-ray laboratory is
established in strange terrain proximate to combat operations. Under these conditions,
casualties are awaiting medical attention and the hospital's surgical and radiographic
functions should be established as soon as possible.
Since electric power is not needed and a small quantity of fresh water can be
included with the equipment, processing of radiography can begin as soon as the
equipment is landed and assembled. The amount of water needed for the first 24 hours
can be contained in a 50-gallon drum. This will be enough to mix solutions and
accomplish the film washing process. After solutions are made, the water for washing
purposes will average 15 gallons per 480 14 by 17-inch films or the equivalent.
Treatment of the x-ray film during the processing procedure assures protection of the
emulsion by good hardening characteristics and freedom from residual salts after the
film is dry. The elimination of conventional processing apparatus is offset by using a
processing system that chemically controls the processing procedure within a
temperature range of the prevailing solution temperatures--one is used for the range 60°
to 75ºF and the other for 75º to 90ºF. The method of developer replenishment requires
the maintenance of the correct solution level by frequent additions of replenisher. The
volume of replenisher needed to process 600 14 by 17-inch films, or their equivalent, is
about equal to four times the original volume of the developer. This system makes
possible the use of a constant development time for a given temperature.
4-3. EQUIPMENT
Seven stainless steel (Alloy number 316) tanks are needed for this method of
processing. Each tank should be of approximately five gallons capacity. A frame upon
which tanks may be grouped for convenient use by the x-ray specialist may be
improvised (figure 4-1)
MD0954 4-2
Tank 1--Developer. Tank 4--Second fixing solution.
Figure 4-1. Diagram of tank (five gallon) arrangement in seven tank processing
procedure.
TEMPERATURE (FAHRENHEIT) 60 62 64 66 68 70 72 74 75
MD0954 4-3
a. Development. Development is by time and temperature in tank one,
according to table 4-2. After development, the film is removed quickly and drained to
waste for 15 seconds (do not drain into the developer tank). The waste can be a trough
in the back of the tanks leading to a drainage pit outside the processing room structure.
b. Rinsing. The film is next placed in tank two containing an acid rinse bath
(stop bath) made by mixing 2-1/2 quarts of 28-percent acetic acid with five gallons of
water. Exhaustion of this bath occurs when 200 14- by 17-inch films, or their equivalent,
have been passed through the solution. If an acid rinse bath is not available, a fresh
water rinse bath can be used, but it must be changed after 40 14- by 17-inch films have
been rinsed. The film should be rinsed in tank two for one minute with active agitation
or for two minutes without active agitation. After rinsing, it is removed and drained to
tank two for 15 seconds and then immersed in tank three for fixing.
c. Fixing. Tanks three and four are used for fixing solution. The fixing solution
should be mixed using a sodium thiosulfate formula. The film remains in tank three
from one to two minutes until clear. It is then removed and drained to tank three for 15
seconds before being placed in tank four, where it remains two minutes for hardening.
Be sure that the fixing solution from tank three does not drain into tank three. When 80
14- by 17-inch films have been passed through tank three, it is replaced with new
solution and tank four is moved into number three position. The new solution in tank
three then assumes the number four position.
d. Washing.
(1) Washing is a precise operation in this procedure and all the rules must
be observed if a radiograph of quality and permanence is to result. For this operation,
freely circulating water is not used. When the film is removed from tank four, it is
drained for 15 seconds to tank four, or to waste, and then immersed in tank five where it
is agitated for one minute (leave it in tank five for two minutes if it is not agitated). It is
then removed and drained for 15 seconds to tank five, or to waste, before being placed
in tank six. After agitation for one minute in this tank, it is removed to drain into tank 6,
or to waste, for 15 seconds. The film is then immersed in tank seven for one minute
while being agitated (or for two minutes if not agitated) and then removed to drain into
tank seven, or to waste, for 15 seconds. Tank seven also contains a wetting agent
(Table 4-2). In the process of transferring films between tanks five, six, and seven, if
the films are drained to the waste, be sure that each water level is maintained by the
frequent addition of fresh water to compensate for the water loss. The film may then be
placed in the dryer or viewed by the radiologist or surgeon.
MD0954 4-4
EXHAUS-
IMMER- TION
TANK PROCESSING QUANTITY DRAIN
SION RATE REMARKS
NO. SOLUTION SOLUTION TIME
TIME 14 X 17
INCH FILM
Replenishment
procedure
Developer 1 with 3 minutes 15 sec
1 5 gal 600 described on
replenisher at 68ºF (to waste)
label of chemical
container.
1 min If acid not
active available, use
agitation or 15 sec fresh water and
2 Acid rinse 5 gal 200
2 min (to tank 2) change after each
without 40 14X17" films.
agitation
1 to 2 min Discard; replace
15 sec
3 No 1 fixer1 5 gal or until 80 with tank 4.
(to tank 3)
clear
Move to tank 3.
15 sec Replace with tank
4 No 2 fixer 5 gal 2 min 160
(to tank 4) of fresh fixing
bath.
Discard; replace
1 min with
with tank 6.
No 1 stagnant agitation; 2 15 sec
5 5 gal 160 Maintain tank
wash min without (to tank 5)
water level with
agitation
fresh water
Move to tank 5;
1 min with
replace with tank
No 2 stagnant agitation; 2 15 sec
6 5 gal 320 7. Maintain tank
wash min without (to tank 6)
water level with
agitation
fresh water
Move to tank 6;
1 min with replace with fresh
No 3 stagnant
agitation; 2 15 sec water plus wetting
7 wash with wetting 5 gal 480
min without (to tank 7) agent. Maintain
solution2
agitation tank water level
with fresh water.
1
Data based on use of solution made from rapid x-ray developer and its replenisher, and
sodium thirosulfate x-ray fixer.
2
Mix 3 1/3 oz of wetting solution (if available) in tank 7 to eliminate drying marks and accelerate
drying of the radiograph.
MD0954 4-5
(2) The chief purpose of the washing done in tank five is to remove the bulk
of the residual fixing solution and silver salts. Therefore, the water soon becomes
charged with these chemicals and should be discarded when 160 14- by 17-inch films
have been washed. Since the rotation of fixing and washing tanks is necessary to
conserve water, tank five is removed, the old wash water is discarded, and tank five is
filled with fresh water. Tank six is moved into the position of tank five and tank seven to
the tank 6 position. The former tank 5 containing fresh water is put in the number 7
position. This system of rotation is repeated each time tank five washes 160 14- by 17-
inch films in number five position.
a. The sequence of processing steps is the same as the one just described
except for the use of the specially treated developing and rinse bath solutions (Table
4-3). Time and temperature processing is accomplished by reference to Table 4-4. To
ensure emulsion stability when processing at these higher temperatures, 50 ounces of
sulfate is added to the developing solution. The rinse bath is replaced by a hardener
solution made according to the following formula. Any quantity may be mixed, so long
as the proportions are observed.
Water 5 gallons.
Potassium chrome alum 20 ounces.
Sodium sulfate (desiccated) 2 1/2 pounds.
or Sodium sulfate (crystalline) 5 pounds, 10 ounces.
MD0954 4-6
EXHAUSTION
TANK PROCESSING QUANTITY IMMERSION DRAIN
RATE 14 X 17 REMARKS
NO. SOLUTION SOLUTION TIME TIME
INCH FILM
Replenishment
Developer 1 with
See time procedure
replenisher plus 15 sec
1 5 gal temperature 600 described on
50ozsodium (to waste)
table label of chemical
sulfate
container.
Discard daily
3 min active 15 sec
2 Hardner bath2 5 gal 80 whether used or
agitation (to tank 2)
not.
1 to 2 min or 15 sec Discard; replace
3 No 1 fixer1 5 gal 80
until clear (to tank 3) with tank 4.
Move to tank 3.
15 sec Replace with
4 No 2 fixer 5 gal 2 min 160
(to tank 4) tank of fresh
fixing bath.
Discard; replace
1 min with
with tank 6.
No 1 stagnant agitation; 2 15 sec
5 5 gal 160 Maintain tank
wash min without (to tank 5)
water level with
agitation
fresh water
Move to tank 5;
1 min with
replace with tank
No 2 stagnant agitation; 2 15 sec
6 5 gal 320 7. Maintain tank
wash min without (to tank 6)
water level with
agitation
fresh water
Move to tank 6;
replace with
fresh water plus
1 min with wetting agent.
No 3 stagnant
agitation; 2 15 sec Maintain tank
7 wash with wetting 5 gal 480
min without (to tank 7)
solution3 water level with
agitation fresh water.
1
Data based on use of solution made from rapid x-ray developer and its replenisher, and sodium
thirosulfate.
2
Above 90ºF double strength.
3
Mix 3 1/3 oz of wetting solution (if available) in tank 7 to eliminate drying marks and accelerate
drying of the radiograph.
MD0954 4-7
TEMPERATURE (FAHRENHEIT) 75 76 78 80 82 84 86 88 90
4-6. INTRODUCTION
Most radiographers in their careers will be faced with processing many different
types of film. Not all films are processed by placing the film into the automatic
processor or placement on a film hanger. The following information outlines different
types of film and the proper procedure for processing.
b. Both green and blue-sensitive roll films are available in 70-millimeter width for
use in the Fairchild Fluoro-Record Cameras, F-212. However, only the green-sensitive
film has been found useful in the 35-millimeter width. Single-coated x-ray film is
available in 2-11/16 by 6-1/2-inch sheet for use with both green and blue-fluorescing
screens. The blue-sensitive type of this film, however, is also available in 4 by 5-inch
and 4 by 10-inch sizes.
MD0954 4-8
4-9. CHEMICALS FOR PHOTOFLUOROGRAPHIC FILM PROCESSING
a. In processing roll film, the leader and trailer should not be left attached to the
ends of the roll while it is being processed. There are camera-activating perforations
along the edges of the leader and the trailer. If the film is rolled on spools in the tank so
that the first and last few frames will be in contact with the leader and trailer, the
perforations can be the source of oval areas of increased density on these frames. The
alternative to removing the leader and trailer prior to processing is not to make
exposures on the first and last three of four frames on a roll.
b. In transferring the film from the magazine of the camera to the spool of the
tank, great care must be exercised not to produce crimp marks or abrasions on the film.
In addition, static electricity will occasionally be created during this operation if the
humidity is low. This can lead to the creation of tree-like artifacts on the film. This can
be prevented if the magazine itself is placed temporarily on one of the spindles of the
tank cover assembly and the film threaded and started onto the processing spool. The
entire assembly can then be immersed in water and the transfer of the film to the spool
completed. The empty magazine reel is then removed and the other processing spool
put into place.
b. The motor-driven, rewind type tanks are designed with a spout so that if
necessary only, one tank can be used and the processing solutions poured in and out
as necessary. However, it is much more convenient to use two tanks so that the motor-
driven reel assembly can be removed from one solution and immersed in the next
solution in a second tank with a minimum loss of time.
MD0954 4-9
4-12. SOLUTIONS FOR ROLL FILMS
(1) One gallon of rapid x-ray solution will develop 200 feet of film.
(2) One gallon of acid rinse solution will stop development of about 100 feet
of film.
(3) One gallon of fixing solution will fix 300 feet of film. However, this
capacity will be lessened when short lengths of film are processed.
(4) One gallon of wetting solution should be sufficient for 100 feet of film. It
should be discarded after each batch of 100 feet. For optimum results, these
recommended limits should not be exceeded. When the recommended amount of film
has been circulated through one of these solutions, the solution should be discarded.
a. Prewetting Roll Films. Unless the film has been wound onto the processing
tank spool under water, it should be wet with water at 68ºF before being placed in the
developer. This may be done by running the film through the water-filled tank for five
minutes.
b. Developing Time for Roll Films. It is important that the developing time be
measured from the time of immersion of the film in the developer to the time of
immersion in the rinse bath. The developing time at 68ºF for the first 100 feet of film in
one gallon of developer solution varies with the length of the roll being processed.
These times are listed in table 4-5. The developing time should be increased by one
minute for the second 100 feet of film processed in one gallon of developer solution.
c. Rinsing Roll Films. The film should be removed from the developer solution
and immersed in the stop bath as rapidly as possible. (To make the stop bath, add
16 ounces of 28-percent acetic acid to water to make one gallon of solution.) To stop
development quickly over the entire length of film, wind the film by hand through two
complete cycles in each direction.
d. Fixing Time for Roll Films. The fixing time for various lengths of roll film is
listed in Table 4-6.
MD0954 4-10
LENGTH OF FILM DEVELOPMENT AT 68°F
6-1/2 feet 6 minutes
25 feet 8-1/2 minutes
50 feet 9 minutes
100 feet 10 minutes
e. Washing Roll Films. To increase the flow of water through the motor-driven
tank during the washing procedure, one end of the cover assembly should be propped
up about one-quarter inch. The hose nozzle is inserted into the bottom of the solution
trap and the film should be washed for at least 25 minutes in rapidly running water.
g. Drying Roll Films. All photofluorographic film requires great care in drying.
Drying should be done in a room as free as possible from dust. After film has been
removed from the tank, excess water should be removed with a chamois, photographic
sponge, or squeegee. This should be done regardless of whether the film is to be dried
in loops or on a rack. If heat is used, the film should never be allowed to become bone
dry since it will tend to become brittle. Allowing the film to remain several hours in a
normal room atmosphere after drying will promote equilibrium between the moisture
content of the film and that of the room. When the film is dry, any residual spots or
fingerprints may be removed with film cleaner.
MD0954 4-11
adjustable processing hanger is especially designed for processing any length of
35millimeter or 70 millimeter film up to 11 feet. Adjustable film guides accommodate
strips of different widths, while sliding clips on the top and bottom bars hold the film
smooth. The number 11 processing hanger is of the channel type and holds five sheets
of 2-11/16 by 6-1/2-inch film. Other hangers are available for 4 by 5-inch and 4 by 10-
inch films.
If it is not possible to cool the solutions and wash water to 68ºF, a number of
general precautions may be exercised to lessen the difficulties of processing x-ray film
at higher temperatures. For temperatures up to 75ºF, the development time should be
shortened as indicated in the development time-temperature table (see Table 4-1). The
fixing solution should be renewed frequently. The film should be fixed for fully 15
minutes to ensure maximum hardening and the washing time should be limited to 15
minutes. A good practice is to use a fixing solution, which is twice the volume of the
developer, and to change the fixer when the developer is changed. Short development,
through fixing, and minimum washing all help to prevent excessive softening and
swelling of the emulsion gelatin.
DEVELOPMENT--RAPID
TEMPERATURE HARDENING BATH FIXATION
X-RAY DEVELOPER
80ºF 1 1/2 minutes 3 minutes 10 minutes
90ºF 1 1/2 minutes 3 minutes 10 minutes
95ºF 1 1/2 minutes 3 minutes 10 minutes
MD0954 4-12
4-17. TEMPERATURES ABOVE 90ºF
OUNCES OF
TEMPERATURE DESICCATED SODIUM
(FAHRENHEIT) SULFATE ADDED PER
GALLON OF SOLUTION
80ºF 0
Rapid X-Ray Developer 90ºF 10
95ºF 20
80ºF 0
Hardening Bath 90ºF 0
95ºF 7
a. General.
(1) When a tank is not available, films may be processed in trays, although
this method is not as efficient as the others that have been discussed.
MD0954 4-13
(2) At least four heavy, durable, white enamel trays are essential. They
should be of adequate size to accommodate the largest film normally exposed. One
tray each is used for developer solution, rinse water or stop bath, fixing solution, and
wash water. The tray used for washing should be fitted with an automatic tray siphon
so that the water will be kept in constant circulation.
(1) On removing the film from the cassette or exposure holder, attach a
dental x-ray film clip to one corner to facilitate handling. Immerse the film in the
developer solution with a quick sliding motion so that it is completely covered. Unduly
slow and uneven immersion will result in a dark line on the radiograph.
(2) Start the timer for the proper interval as indicated by the temperature
and activity of the solutions. Because of the more or less continuous agitation afforded
by this procedure, it requires 20 percent less development time than the tank system.
For example, using rapid developer and a basic three-minute development time at 68ºF,
normal contrast is provided in screen-type film with a 2-1/2-minute tray development.
During development, the film must be moved about frequently so that the underside
does not adhere to the tray and thereby retard the action of the developer on the
emulsion. It is also advisable to turn the film over several times during development.
The tray should be rocked to provide continuous redistribution of solution over both
surfaces of the film. This agitation can be accomplished by raising and lowering
alternate sides of the tray and must continue throughout the processing period.
(3) Rinse the film in fresh water or acid bath for 20 seconds and transfer it to
the fixing solution for 15 minutes. When the film is first placed in the tray, and at
intervals during fixation, the solution should be agitated by the method previously
described. The film must not be allowed to rest on the bottom.
(4) After fixing, the film should be washed in running water for not less than
20 minutes. The rate of flow should be rapid enough to replace the water in the tray at
least eight to 10 times an hour. If several films are developed in succession, the
washing time must be calculated from the time the last film was placed in the wash
water.
MD0954 4-14
(5) The developer and fixer solution should be returned to their respective
bottles promptly after use pr discarded because of aerial oxidation of the developer
solution and dust and other foreign matter collecting in uncovered trays.
b. Procedure.
(1) Two parts of stock solution are mixed with one part water, and the x-ray
film is developed in it for about 60 seconds at 68ºF. The development time may be
reduced to 45 seconds by decreasing to one ounce the potassium bromide in the above
formula. However, appreciable fog may result. The tray method of processing is
preferred because the keeping quality of the developer is poor when diluted as
recommended above. The solution should be discarded after it has been used. The
stock solution, however, will retain its properties for about two months if kept in a well-
stoppered brown bottle.
(2) Since caustic soda is one of the components of the developer, dental x-
ray film clips should be used for handling the films to protect the hands. It is important
that the films be rinsed well following development before being placed in the fixer. This
step is necessary to prevent the formation of stains or diachronic fog.
(3) If fresh fixer solution is used, the radiograph should be ready for viewing
after having been immersed, with frequent agitation, for approximately 10 minutes to
ensure thorough hardening of the emulsion. It may then be washed in the usual
manner.
MD0954 4-15
4-20. EMERGENCY PROCESSING MEASURES
Whenever possible, the x-ray specialist should strictly adhere to the rules of good
processing outlined in the preceding sections. However, emergencies may arise during
which it may be impossible for the x-ray specialist to know all the facts about the
developer and fixer. In such emergencies, the following rules of thumb may be helpful.
a. Sight Development.
(2) Sight development opens avenues of error through which the quality of
the finished radiograph may be impaired. It is a characteristic of x-ray film emulsions
that the silver bromide crystals are packed more closely together than in the usual
photographic emulsion. Depending upon the type of exposure given, the visual
appearance of the developing image may be comparatively different. In radiographs
exposed with intensifying screens, the exposure effect occurs chiefly in the crystals at or
near the surface of the emulsion because the exposure is made chiefly by the
fluorescent light emitted by the intensifying screens. The image appears to flash up
quickly in the developer and the developed crystals at the surface prevent estimation of
the degree of overall development in the body of the emulsion. Therefore, it is largely a
matter of guesswork as to the time that development may be judged complete.
Frequently, the radiograph is removed from the developer before complete development
of the entire image has taken place because the image appears to the eye to possess a
very high density. This results in underdevelopment. In direct exposure of the x-ray
film, the x-rays penetrate the entire emulsion layers fairly equally. Crystals at the
emulsion's surface as well as throughout the layers develop slowly. The developing
image is ill defined at first, gradually building up to the point where the well-
accommodated eye sees what may be construed to be a well-defined image.
Frequently, however, an error in judgment is made and full development is not given.
MD0954 4-16
(4) To sight develop a film, you may place a finger behind the densest part
of the film and then view it against a safelight. If the shadow of the finger cannot be
seen through the film, development should be terminated. To avoid causing aerial fog,
the x-ray specialist should be particularly careful not to keep the film out of the
developing solution for too long a time.
(1) It is not advisable to process films by the sight method if the temperature
and/or the strength of solutions are unknown. For consistency in film quality,
standardized processing times must be established for both the developer and the fixer.
This may be done by using the following methods.
(2) A simple test for proper development time can be carried out within a
few minutes. Using an eight by 10-inch, cassette, flash-expose half the film to x-rays
while covering the other half with lead. Then, in the darkroom, cut the exposed film into
strips so that each strip has one exposed and one unexposed end. Only one strip is
used in making the test, so the remainder of them should be stored in a lightproof
container. Using a stopwatch with a second hand, place the strip of film in the
developer so that it can be easily observed by the safelight illumination. The instant that
the exposed half of the film becomes different in appearance from the unexposed half,
note the time elapsed in seconds. Then, divide the number of seconds elapsed by 10;
the result gives a suitable development time in minutes. For example, if it took 35
seconds for a density to appear on the exposed half of the film, then the proper
development time for that solution at that temperature would be 35 divided by 10,
or 3-1/2 minutes.
(3) To estimate the proper fixing time, place a film in the fixer (the first film
processed will do satisfactorily) and note the time it takes for the film to clear. Triple this
time for the complete fixing of all films. For example, if it took six minutes to clear a film,
then all films left in the fixer for 18 minutes would be satisfactorily hardened.
MD0954 4-17
EXERCISES, LESSON 4
After you have completed all the exercises, turn to "Solutions to Exercises" at the end of
the lesson and check your answers.
d. Using chemicals.
a. Slow development.
b. Speed development.
a. Green, yellow.
b. Red, green.
c. Green, blue.
d. Blue, red.
MD0954 4-18
4. Suppose that a processed roll of photofluorographic film shows small oval areas
at the beginning and end of the roll. What is the cause?
a. 52ºF.
b. 68ºF.
c. 75ºF.
d. 82ºF.
a. Fixer.
b. Wetting solution.
c. Acetic acid.
d. Sodium sulfate.
MD0954 4-19
8. While a regular x-ray film is developed at 68ºF for three to five minutes, a segment
of blue-sensitive film requires minutes.
a. Two.
b. Six.
c. Eight.
d. Ten.
9. According to the subcourse, the absolute upper temperature limit at which x-ray
film can be hand processed is:
a. 65ºF.
b. 70ºF.
c. 80ºF.
d. 95ºF.
a. Adding chemicals.
11. Tray agitation requires _______ less development time than the tank system.
MD0954 4-20
12. When speed is quite important but manual procedures must be employed,
__________ may be added to the developer to speed its action.
a. Elon.
b. Sodium hydroxide.
c. Hydroquinone.
d. Potassium bromide.
13. In a time-strength solution test, the exposed filmstrip required forty seconds to
show a density change. What is the developing time?
a. Three minutes.
c. Four minutes.
d. Six minutes.
MD0954 4-21
SOLUTIONS TO EXERCISES, LESSON 4
1. d (para 4-5b)
2. a (para 4-5b)
3. c (para 4-7)
4. b (para 4-10)
5. a (para 4-10b)
6. b (para 4-13a)
7. c (para 4-13c)
8. c (para 4-14b)
9. d (para 4-16)
End of Lesson 4
MD0954 4-22