CP501265490 Rev1

NOTICE: This document contains references to Varian.
Please note that Varian, Inc. is now part of Agilent

Technologies. For more information, go to
www.agilent.com/chem.
Varian BV
Herculesweg 8
4330 EA Middelburg
The Netherlands
Micro-GC
User Manual
North/South America Europe Australia/East Asia
2700 Mitchell Drive P.O. Box 8033 679 Springvale Road
Walnut Creek 4330 EA Middelburg Mulgrave, Victoria 3171
94598 California, USA The Netherlands Australia
Tel: ++(1)9259392400 Tel: ++(31)118671000 Tel: ++(61)395607133
Fax: ++(1)9259452360 or Fax: ++(31)118623193 Fax: ++(61)395607950
++(1)9259452344
© 2009 Varian, Inc. All Rights Reserved Printed in the Netherlands CP501265490 Rev:1 November 2009
Warranty Information
Varian Analytical Instrument Warranty

HARDWARE PRODUCTS
All analytical instruments sold by Varian are warranted to be free from defects in material and workmanship for the
periods specified and in accordance with the terms on the face of Varian's quotation or as otherwise agreed upon in
writing between Varian and the Customer. The warranty period begins on the date of shipment from Varian to the
original Customer. However, where installation is paid for by the Customer or included in the purchase price, the
warranty period begins upon completion of installation. If the Customer schedules installation to start later than 30 days
after delivery or if such delay is caused through the Customer's inability to provide adequate facilities or utilities or
through failure to comply with Varian's reasonable pre-installation instructions or through other omissions by Customer,
then the warranty period starts on the 31st day from date of shipment. Moreover Varian will charge the Customer for
labor and other expenses involved in making multiple or follow-up installation service calls.
SOFTWARE PRODUCTS
Where software is provided within the frame of a license agreement concluded between the Customer and Varian, any
warranty shall be strictly in accordance with the terms of such agreement.
In the absence of a license agreement and unless an alternate warranty period is agreed upon in writing between Varian
and the Customer, the warranty period is as specified on the face of Varian's quotation. Varian warrants such software
products, if used with and properly installed on Varian hardware or other hardware as specified by Varian to perform as
described in the accompanying Operator's Manual and to be substantially free of those defects which cause failure to
execute respective programming instructions; however, Varian does not warrant uninterrupted or error-free operation.
REMEDIES
The sole and exclusive remedy under hardware warranty shall be repair of instrument malfunctions which in Varian's
opinion are due or traceable to defects in original materials or workmanship or, at Varian's option, replacement of the
respective defective parts, provided that Varian may as an alternative elect to refund an equitable portion of the
purchase price of the instrument or accessory.
Repair or replacement under warranty does not extend the original warranty period.
Repair or replacement under warranty claims shall be made in Varian's sole discretion either by sending a Customer
Support Representative to the site or by authorizing the Customer to return the defective accessory or instrument to
Varian or to send it to a designated service facility. The Customer shall be responsible for loss or damage in transit and
shall prepay shipping cost. Varian will return the accessory or instrument to the Customer prepaid and insured. Claims
for loss or damage in transit shall be filed by the Customer. To correct software operation anomalies, Varian will issue
software revisions where such revisions exist and where, in Varian's opinion, this is the most efficient remedy.
LIMITATION OF WARRANTY
This warranty does not cover software supplied by the Customer, equipment and software warranted by another
manufacturer or replacement of expendable items and those of limited life, such as but not limited to: Filters, glassware,
instrument status lamps, source lamps, septa, columns, fuses, chart paper and ink, nebulizers, flow cells, pistons, seals,
fittings, valves, burners, sample tubes, probe inserts, print heads, glass lined tubing, pipe and tube fittings, variable
temperature dewars, transfer lines, flexible discs, magnetic tape cassettes, electron multipliers, filaments, vacuum
gaskets, seats and all parts exposed to samples and mobile phases.
This warranty shall be void in the event of accident, abuse, alteration, misuse, neglect, breakage, improper operation
or maintenance, unauthorized or improper modifications or tampering, use in an unsuitable physical environment, use
with a marginal power supply or use with other inadequate facilities or utilities. Reasonable care must be used to avoid
hazards.
This warranty is expressly in lieu of and excludes all other express or implied warranties, including but not
limited to warranties of merchantability and of fitness for particular purpose, use or application, and all other
obligations or liabilities on the part of Varian, unless such other warranties, obligations or liabilities are
expressly agreed to in writing by Varian.
LIMITATION OF REMEDIES AND LIABILITY

The remedies provided herein are the sole and exclusive remedies of the Customer. In no case will Varian be
liable for incidental or consequential damages, loss of use, loss of production or any other loss incurred.
Page II User Manual Micro-GC Varian, Inc.

Safety Information
Safety Information
INFORMATION
In accordance with Varian’s commitment to customer service and safety, this instrument and its
accompanying documentation (NEN 5509) complies with the CE specifications and the safety
requirements for electrical equipment for measurement, control, and laboratory use
(CEI/IEC 1010-1), cCSAus and FCC-b.
This device has been tested and found to comply with the limits for a Class A digital device,
pursuant to part 15 of the FCC rules. These limits are designed to provide reasonable protection
against harmful interference when the equipment is operated in a commercial environment. This
equipment generates, uses, and can radiate radio frequency energy and, if not installed and used
in accordance with the instruction manual, may cause harmful interference to radio
communications.
Operation of this equipment in a residential area is likely to case harmful interference in witch case
the user will be required to correct the interference at his own expense.
To prevent any injury to the user or any damage to the instrument it is essential that you read the
information in this chapter.
If this manual is not in your native language and if you have problems understanding the text, we
advise you to contact your Varian office for assistance. Varian cannot accept responsibility for any
damage or injury caused by misunderstanding of the information in this manual.
OPERATING INSTRUCTIONS
This instruction manual is provided to help you establish operating conditions, which will permit
safe and efficient use of your equipment.
Special considerations and precautions are also described in the manual, which appear in the
form of NOTES, CAUTIONS, and WARNINGS as described below (next page).
It is important that you operate your equipment in accordance with this instruction manual and
any additional information, which may be provided by Varian. Address any questions regarding
the safe and proper use of your equipment to your local Varian office.
Varian, Inc. User Manual Micro-GC Page: III

Safety information
CAUTION WARNING
Information to aid you in Alerts you to situations that Alerts you to potentially
obtaining optimal performance may cause moderate injury hazardous situations that
from your instrument. and/or equipment damage, could result in serious injury,
and how to avoid these and how to avoid these
situations. situations.
Warning Symbol Warning Description

WARNING: Indicates dangerous voltage: (terminals fed from the interior
Shock hazard by voltage exceeding 1000V must be so marked).
WARNING: Indicates parts that may cause burns when touched.

Burn hazard
Instruction Indicates that the user should refer to the manual before
Manual operating the equipment.
Protective For protection against electrical shock in case of a fault. Used
Conductor terminal with field wiring terminals to indicate the terminal, which must
be connected to ground before operating equipment.
Radioactive Indicates that the instrument contains radioactive
hazard components, which may cause personal injury when handled
incorrectly.
Indicates sharp or suddenly moving parts such as injection
Skin puncture needles that may cause injury.
Static discharge Indicates instrument contains parts that can be damaged by
Warning electrostatic discharge. Take care for proper grounding
before handling.
Touching this item may result in damage to the instrument
Do not touch
or personal injury.
Page IV User Manual Micro-GC Varian, Inc.

Safety Information
GENERAL SAFETY PRECAUTIONS
Follow these safety practices to ensure safe equipment operation.

 Perform periodic leak checks on all supply lines and pneumatic
plumbing.
 Do not allow gas lines to become kinked or punctured. Place lines
away from foot traffic and extreme heat or cold.
 Store organic solvents in fireproof, vented and clearly labeled
cabinets so they are easily identified as toxic and/or flammable
materials.
 Do not accumulate waste solvents. Dispose of such materials
through a regulated disposal program and not through municipal
sewage lines.
NOTICE: This instrument has been tested per applicable requirements of EMC
Directive as required to carry the European Union CE Mark. As such, this
equipment may be susceptible to radiation/interference levels or
frequencies, which are not within the tested limits.
This instrument is designed for chromatographic analysis of appropriately
prepared samples. It must be operated using appropriate gases and/or
solvents and within specified maximum ranges for pressure, flows, and
temperatures as described in this manual. If the equipment is used in a
manner not specified by the manufacturer, the protection provided by the
equipment may be impaired.
It is the responsibility of the Customer to inform Varian Customer Support
Representatives if the instrument has been used for the analysis of
hazardous biological, radioactive, or toxic samples, prior to any
instrument service being performed or when an instrument is being
returned to the Service Center for repair.
CAUTIONS
1. Disconnect the instrument from all power sources before removing protective panels to
avoid exposure to potentially dangerous voltages.
2. When it is necessary to use a non-original power cord plug, make sure the replacement
cord adheres to the color-coding and polarity described in the manual and all local
building safety codes.
3. Replace faulty or frayed power cords immediately with the same type and rating.
4. This instrument should be placed in a suitable location with sufficient ventilation to
remove gases and vapors. Space around the instrument must be sufficient to
enable cooling of the instrument.
Varian, Inc. User Manual Micro-GC Page: V

Safety information
5. Before plugging the instrument in or turning the power on, always make sure that
the voltage and fuses are set appropriately for your local power source.
6. Do not turn on the instrument if there is a possibility of any kind of electrical damage.
Instead, disconnect the power cord and contact your Varian office.
7. The supplied power cord must be inserted into a power outlet with a protective earth
ground connection. When using an extension cord, make sure that the cord is also
properly grounded.
8. Do not change the external or internal grounding connections as this could
endanger you and/or damage the instrument.
9. The instrument is properly grounded when shipped. You do not need to make any
changes to the electrical connections or to the instrument chassis to ensure safe
operation.
10. When working with this instrument, follow the regulations for GLP (Good Laboratory
Practice). Take care to wear safety glasses and appropriate clothing.
11. Do not place containers with flammable liquids on this instrument. Spillage of the
liquid over hot parts may cause fire.
12. This instrument may use flammable or explosive gases e.g. hydrogen under
pressure. Be sure to be familiar with and to follow accurately the operation
procedures prescribed for those gases before operating the instrument.
13. Never try to repair or replace any component that is not described in this manual
without the assistance of a Varian service engineer. Unauthorized repairs or
modifications will result in rejection of warranty claims.
14. Always disconnect the AC power cord before attempting any type of maintenance.
15. Use proper tools when working on the instrument to prevent danger for you and/or
damage to the instrument.
16. The customer should not attempt to replace battery(s) or fuse(s) in this instrument
other then specified in the manual.
17. Damage can result if the instrument is stored under unfavorable conditions for
prolonged periods (e.g., subject to heat, water, etc.).
18. Do not shut off column flow when the oven temperature is high this may damage
the column.
19. This unit has been designed and tested in accordance with recognized safety
standards and designed for use indoors.
20. If the instrument is used in a manner not specified by the manufacturer, the
protection provided by the instrument may be impaired.
21. Substituting parts or performing any unauthorized modification to the instrument
may result in a safety hazard.
22. Changes or modifications not expressly approved by the responsible party for
compliance could void the user’s authority to operate the equipment.
Page VI User Manual Micro-GC Varian, Inc.
Safety Information
SPARE PARTS AVAILABILITY SERVICE AVAILABILITY

It is the policy of Varian to provide operational spare parts for any instrument and Varian provides a variety of
major accessory for a period of seven (7) years after shipment of the final services to support its customers
production run of that instrument. Spare parts will be available after this seven (7) after warranty expiration. Repair
year period but on an as available basis. Operational spare parts are defined as service can be provided by
those individual electrical or mechanical parts that are susceptible to failure during attractively priced service
their normal operation. Examples include relays, lamps, temperature probes, contracts or on a time and
detector elements, motors, etc. Sheet metal parts, structural members or material basis. Technical
assemblies and castings, printed circuit boards, and functional modules are support and training can be
normally capable of being rebuilt to like-new condition throughout their useful life provided by qualified personnel
and therefore will be supplied only on an as available basis after the final on both a contractual or as-
production run of the instrument. needed basis.
Varian Analytical Instruments Sales Offices

For Sales or Service assistance and to order Parts and Supplies, contact your local Varian
office.
Argentina France Russian Federation

Buenos Aires Les Ulis Cédex Moscow United States
Tel. +54.11.4.783.5306 Tel. +33.1.6986.3838 Tel. +7.095.937.4280 Walnut Creek, California,
USA
Australia Germany Spain Tel. +1.800.926.3000
Mulgrave, Victoria Darmstadt Madrid (GC and GC/MS)
Tel. +61. 3.9560.7133 Tel. +49.6151.7030 Tel. +34.91.472.7612
Tel. +1.800.367.4752 (LC)
Austria India Sweden
Poettelsdorf Mumbai Solna
Tel. +43.2626.20090 Tel. Tel. +46.8.445.1620
+91.22.2570.8595/97
Benelux Switzerland
Middelburg Italy Steinhausen
Tel. +31.118.671500 Torino Tel. +41.848.803.800
Tel. +39.011.997.9111
Brazil and Latin America (S) Taiwan
São Paulo Japan Shih-Chi
Tel. +55.11.3845.0444 Tokyo Tel. +886.22.698.9555
Tel. +81.3.5232.1239
Canada United Kingdom and http://www.varianinc.com/
Mississauga, Ontario Korea Ireland
Tel. 800.387.2216 Seoul Oxford
Tel. +82.333.665.5171 Tel. +44.1865.291500
China
Beijing Mexico and Latin Venezuela
Tel. +86.106310.8550 America (N) Caracas
Mexico City Tel.
Europe Tel. +58.212.285.0320/2494
Middelburg, The Netherlands +52.5.55.5239465/026
Tel. +31.118.671.000
Varian, Inc. User Manual Micro-GC Page: VII

Table of contents
Table of contents
VARIAN ANALYTICAL INSTRUMENT WARRANTY.................................................................. II

HARDWARE PRODUCTS ............................................................................................................... II
SOFTWARE PRODUCTS ................................................................................................................ II
REMEDIES ................................................................................................................................... II
LIMITATION OF WARRANTY ........................................................................................................... II
LIMITATION OF REMEDIES AND LIABILITY ....................................................................................... II
SAFETY INFORMATION............................................................................................................. III
INFORMATION ............................................................................................................................. III
OPERATING INSTRUCTIONS ......................................................................................................... III
GENERAL SAFETY PRECAUTIONS .................................................................................................V
CAUTIONS................................................................................................................................V
SPARE PARTS AVAILABILITY .......................................................................................................VII
SERVICE AVAILABILITY ...............................................................................................................VII
TABLE OF CONTENTS................................................................................................................ 1
PREPARING FOR INSTALLATION ............................................................................................. 6

GAS SUPPLY ............................................................................................................................... 6
GAS SAMPLES ............................................................................................................................. 6
MICRO-GC INSTALLATION ........................................................................................................ 7
INSPECTION ................................................................................................................................ 7
UNPACKING................................................................................................................................. 7
PACKING LIST .............................................................................................................................. 8
Micro-GC .............................................................................................................................. 8
Accessories .......................................................................................................................... 9
INSTALLATION............................................................................................................................ 10
Install Gas Regulators and Set pressures .......................................................................... 10
Carrier gas .......................................................................................................................... 10
Connect data handling peripherals..................................................................................... 10
Sample................................................................................................................................ 10
Heated Sample line ........................................................................................................ 10
Connect to Power ............................................................................................................... 11
Turn power ON ................................................................................................................... 11
Factory default states and settings..................................................................................... 11
INSTRUMENT OVERVIEW ........................................................................................................ 12
FRONT VIEW .............................................................................................................................. 12
BACK VIEW .............................................................................................................................. 13
INSIDE VIEW .............................................................................................................................. 14
CARRIER GAS CONNECTION........................................................................................................ 15
SAMPLE GAS ............................................................................................................................. 16
Varian, Inc. User Manual Micro-GC Page 1
Table of contents
Handling a sample .............................................................................................................. 16

Unheated Injector Systems ................................................................................... 16
Heated Injector Systems ................................................................................................ 17
HEATED SAMPLE LINE ................................................................................................................ 18
Connect a heated sample line ............................................................................................ 18
POWER ..................................................................................................................................... 20
SHUT DOWN PROCEDURE ........................................................................................................... 20
LONG STORAGE RECOVERY PROCEDURE ................................................................................... 21
INITIAL OPERATION .................................................................................................................... 22
INITIAL RUN ............................................................................................................................... 22
SETTING UP THE TEST METHOD .................................................................................................. 22
INJECTING THE SAMPLE .............................................................................................................. 22
COLUMN CP-SIL 5 CB 6 METER UNHEATED ................................................................................ 23
COLUMN CP-SIL 5 CB 4 METER HEATED .................................................................................... 24
COLUMN CP-SIL 5 CB 8 METER HEATED .................................................................................... 25
COLUMN CP SIL13CB TBM 12 METER HEATED ......................................................................... 26
COLUMN HAYESEP 40CM HEATED ............................................................................................. 27
COLUMN MOLSIEVE 5Å 20 METER UNHEATED ............................................................................. 28
Conditioning of Molsieve columns ...................................................................................... 29
COLUMN PPQ 10 METER HEATED .............................................................................................. 30
REFERENCE .............................................................................................................................. 31
INSTRUMENT DESCRIPTION ................................................................................................... 31

CARRIER GAS ............................................................................................................................ 31
MICRO ELECTRONIC GAS CONTROL (EGC).................................................................................. 32
INJECTOR .................................................................................................................................. 32
COLUMN ................................................................................................................................... 33
DETECTOR ................................................................................................................................ 34
TCD..................................................................................................................................... 34
DMD.................................................................................................................................... 34
IN/OUTPUTS............................................................................................................................... 35
EXTERNAL DIGITAL I/O............................................................................................................... 36
Ready/not ready signal ....................................................................................................... 36
COMMUNICATION PORTS (COM) ................................................................................................ 37
EXTERNAL ANALOG I/O.............................................................................................................. 38
THE DIFFERENTIAL MOBILITY DETECTOR ........................................................................... 39
GENERAL .................................................................................................................................. 39
General functionality ........................................................................................................... 39
Micro-GC DMD Channel..................................................................................................... 41
GENERAL OPERATION ................................................................................................................ 42
Tuning the DMD.................................................................................................................. 42
PROTOCOLS .............................................................................................................................. 43
Different Types of Protocols: .......................................................................................... 43
The Internet Protocol Suite............................................................................................. 43
IP Addresses .................................................................................................................. 43
Page 2 User Manual Micro-GC Varian, Inc.
Table of contents
The Internet protocol suite.............................................................................................. 43

MICRO-GC AND NETWORKS ...................................................................................................... 44
Network Requirements of the Micro-GC ........................................................................ 44
FAQ (FREQUENT ASK QUESTIONS)............................................................................................ 44
GLOSSARY OF NETWORK TERMS ................................................................................................ 45
BNC connector ................................................................................................................... 45
Crossover Cable ................................................................................................................. 45
Domain................................................................................................................................ 45
Ethernet Address ................................................................................................................ 45
Gateway.............................................................................................................................. 45
Host name .......................................................................................................................... 45
Hub ..................................................................................................................................... 45
IP Address .......................................................................................................................... 45
Patch Cable ........................................................................................................................ 46
RJ45 Connector.................................................................................................................. 46
TCP/IP ................................................................................................................................ 46
WORKSTATION SOFTWARE.................................................................................................... 47
EZCHROM ELITE ....................................................................................................................... 48
CONTROL INSTRUMENT .............................................................................................................. 48
SERIAL COMMUNICATION ........................................................................................................... 49
ETHERNET COMMUNICATION ...................................................................................................... 50
Peer-to-peer: single instrument .......................................................................................... 50
Multiple instrument (local network) ..................................................................................... 51
Global network: Multiple instruments.................................................................................. 52
COMMUNICATION SETUP ............................................................................................................ 53
Serial communication (EZCrom only)................................................................................. 53
Ethernet communication (Galaxie) ..................................................................................... 53
ASSIGN NEW IP ADDRESS VIA ETHERNET CONNECTION ............................................................... 54
ASSIGN NEW IP ADDRESS VIA SERIAL CONNECTION .................................................................... 55
REMOTE ACCESS INSTRUMENT STATUS ..................................................................................... 56
GENERAL ERROR STATE............................................................................................................ 58
VARIAN USERLINK APPLICATIONS ............................................................................................... 60
External Relays................................................................................................................... 60
instrument status including analog inputs........................................................................... 61
UserDataStore addresses of Varian userlink applications ................................................. 61
EXTERNAL DEVICES ................................................................................................................... 63
CYCLE WITH STATIC (ELECTRONIC) PRESSURE ................................................................ 65
CYCLE WITH ELECTRONIC PRESSURE CONTROL.............................................................. 66
COLUMN MODULE CONDITIONING ........................................................................................ 67
BACKFLUSH OPTION ............................................................................................................... 68

Description.......................................................................................................................... 69
Tuning ................................................................................................................................. 70

Table of contents
SHIPPING INSTRUCTIONS ....................................................................................................... 71
CLEANING INSTRUCTIONS...................................................................................................... 71
DISPOSAL INSTRUCTIONS ...................................................................................................... 71
ERROR LIST............................................................................................................................... 72
ERROR HANDLING...................................................................................................................... 72
ERROR LIST: ............................................................................................................................. 73

Introduction and Initial Operation
Introduction
Congratulations and thank you for purchasing the Varian, Inc. Micro-GC.
The Micro-GC is a powerful single or dual or quad channel high speed Micro GC suited for
analyses of gaseous samples. This instrument is tailored to meet your needs. The columns are
installed and the instrument as a whole has been thoroughly tested at our factory.
The Micro-GC incorporate technical advancements in Micro electronic gas control (EGC).
The unique advantages of the allow column head pressure settings to become part of the GC
method and can be programmed electronically.
The Varian, Inc. Micro-GC with Micro EGC allows you to optimize your analysis. Apart from the
constant pressure mode, the Micro EGC in the Micro-GC allows you also to program the
pressure over your column. Pressure programming improves not only the speed of the analysis,
but it will give you the opportunity to run new and more extended applications.
The Micro-GC analytical channels can optionally be equipped with backflush and Micro-Gasifier
capabilities thus optimizing the analysis even further.
For problems or questions about your Micro-GC, please contact your nearest
Varian, Inc. subsidiary or Varian, Inc. representative.

Preparing for Installation
Refer to the Pre-Installation Instructions (CP501289) for site

preparation and unpacking information.
GAS SUPPLY
Gas quality specifications are listed in the reference document “Pre-Installation

requirements Micro-GC CP501289”.
GAS SAMPLES
- Do not introduce liquid samples into your Micro-GC.
- Type of samples: non-condensing gas
- Samples other than non-condensing gases (wet, vapors, particles and
polymers) must be filtered in advance.
- Sample conditions: Non condensing gas between 0 and 110C.
- Sample pressure between 0 and 100 kPa (1 bar, 15 psi)
- Outlet of sample container must fit to a stainless steel capillary of 1/16"
outside diameter, provided with a Swagelok® female nut.

Micro-GC Installation
INSPECTION
The Micro-GC will arrive packed in one large box and one or more smaller cartons.
Inspect the cartons carefully for damage or signs of rough handling. Report damage to
the carrier and to your local Varian office.
UNPACKING
Unpack the Micro-GC and accessories carefully and transfer to the work area, using
proper handling techniques. Inspect the Micro-GC and accessories carefully for damage
or signs of rough handling. Report damage to the carrier and to your local Varian office.
Avoid back strain or injury by following all safety precautions when

lifting (heavy) objects.
The instrument has been protected during shipment by protection caps.

Prior to operating, remove:
 At the back of the system all (plastic) caps (see picture below).

PACKING LIST
Micro-GC
Check the packing list to see if you have received all that you require.
Item Part number

External sample filter kit CP736729
Filters 5x for external filter assy. CP736467
CD-ROM user manual Micro-GC CP505532490
Ethernet cross over cable 2.8 m CP740292
Locking nut
CP420200 x 4
Male Luer
CP420100 x 4
Front and back ferrule 1/16” SS x 2 CP471201

Capillary tubing SS 1/16” x 1.0 mm, 10 cm CP4008
Capillary Ext. Filter CP736879
Power supply 110V or CP49PWR110
Power supply 220V or CP49PWR220
Power supply 240V CP49PWR240

Accessories
Item Qty Part number

Spare filters (5 pieces) for external filter 5 CP736467
Manual Micro-GC (hard copy) 1 CP501265490
Manual Micro-GC power supply (hard copy) 1 CP501267
Heated sample inlet elbow with frit 5 CP740434
Ethernet crossover cable 10 meter 1 CP740293
Ethernet crossover cable, 2 meter 1 CP740292
Combo card (Ethernet and Com ports), including 3
1 CP740292
meter crossover cable (not for HUB)
Aux power car cigarette lighter DC adapter 1 CP740291
Charger for battery pack 1 CP740427
Battery pack NiMH (rechargeable) 1 CP740328
Micro Gasifier 110 Volt 1 CP740431
Genie 170 BTU filter complete 1 CP739535
Genie 101 BTU filter complete 1 CP739534
Genie 170 standard filter complete 1 CP739536
Genie 170 BTU membrane 1 CP739531
Genie 170 standard membranes 5 392590004
Genie 101 BTU standard membranes 5 392590005

INSTALLATION
Install Gas Regulators and Set pressures
Carrier gas supplied from cylinders should have a two-stage pressure assembly to
adjust the carrier gas pressure to 550 ± 10 % (80 ± 10 %). Set cylinder regulator
pressure to match the Micro-GC gas inlet pressure
(see Carrier_gas_connection on page 15).
Carrier gas
The most commonly used carrier gas for the Micro-GC is either He or N2. The
recommended purity for carrier gas is 99.995% minimum.
See Carrier_gas_connection on page 15
Connect data handling peripherals
The Micro-GC must be connected to an external Workstation, on page 47 both to set up

the method and to acquire data.
Workstations and other data handling devices are connected to the cable connectors
inside the Micro-GC (see Cable_connectors on page 14 for more details).
 Hardware connection between the Micro-GC and Workstation (computer) is done

by Ethernet connection. For additional information look here Cable_connectors on
page 14.
Sample
Connect the sample to the using the sample-in connector situated at the front of the
instrument (see front view on page 12).
Read chapter Sample Gas on page 16 for more important information!
Heated Sample line

To connect heated sample lines refer to Heated Sample line chapter on page
18.

Connect to Power
First, connect the power connector to the Micro-GC, then plug the power cord into an
appropriate source of power.
Turn power ON
Turn on the Micro-GC using the power switch on the lower front of the instrument. The
“READY” LED should light (after two minutes) when ready. (see Front_view on page
12).
Factory default states and settings
Your Micro-GC is shipped from the factory with default settings. The following is
relevant information on the factory default states and settings:
 When the Micro-GC is turned on, the power LED will light up and the system will
begin the Flush cycle procedure. The Flush cycle is a 2-minute cycle in which the
various valves are activated and deactivated in order to flush the entrapped air from
the manifold, valves, and tubing.
 After the flush cycle is finished, the method (the default method in this case), which
was last active before the instrument was shutdown, is activated:
 All heated zones will be set at 30°C.

 The Detector filaments will be set to OFF.
If your system is supplied with a DMD (Differential Mobility Detector) detector all
settings are factory installed. The complete DMD method for the instrument (customer)
specific application is tested en installed inside the DMD.

INSTRUMENT OVERVIEW
FRONT VIEW
READY led
Led OFF: System NOT ready

Led ON: System ready
RUN led
Led OFF: No run

Led blinking: Run in progress
ERROR led
Led OFF: No error

Led blinking: Error present
See here for the complete list on
page 72
POWER led
Led OFF: No power

Led ON: Power OK
Led blinking: Voltage < 10 Volt
SAMPLE 1 and SAMPLE 2
Sample gas inlet connector

See here for more details on page 16
POWER ON/OFF SWITCH
Switch the Micro-GC ON or OFF

BACK VIEW
VENTS
It is possible to connect long vent lines to these fittings in order to safely

guide hazardous fumes to a fume hood or other appropriate vent.
DMD CONNECTOR
In DMD channel used as connector for
transport gas.
CARRIER 1 CONNECTOR POWER CONNECTOR
Carrier gas input connector Power IN connector (male).

See here for more details on page 15. See here for more details on page 20

INSIDE VIEW
Open the cover and the cable connectors will be visible.
ASSIGN IP-ADDRESS BUTTON
Holding down this button during power-up will set

the “assign IP-address mode”
See Assign_new_IP_address on page 54
Red led: Transmit data
Green led: Receive data
ETHERNET
Ethernet RJ45 connector for Ethernet

installations.
COM 2 & COM 3
RS232 (2-wire) and RS485 (4-wire)-

communication interface.
COM 1
RS232-communication interface.
ANALOG I/O
External Analog I/O signals.

DIGITAL I/O
Digital in and output signals.


CARRIER GAS CONNECTION
The carrier gas line is connected from a carrier gas connection to the Micro-GC at the
rear panel CARRIER GAS 1 or 2 port.
Do not use any kind of plastic tubing since air will diffuse through the tubing,
which may cause noisy baselines and decreased sensitivity. The metal
tubing should be clean for GC use. Buy either flamed or chromatographically
clean tubing.
Specifications for the carrier gas used on Micro-GC:
Pressure: 550 kPa ± 10 % (80 psi ± 10 %)

Purity: 99.995% minimum
Dry and free of particles: CP-Gas Clean filters are recommended
CP-Gas Clean filters are recommended to remove any traces of moisture and oxygen.
For low-level analysis a better grade of carrier gas should be considered. The type of
analysis you want to perform determines the type of carrier gas used. The difference
between the relative thermal conductivity of the carrier gas and the sample components
should be as high as possible. Refer to the table for several relative thermal
conductivities.
Hydrogen 47.1 Ethane 5.8

Helium 37.6 Propane 4.8
Methane 8.9 Argon 4.6
Oxygen 6.8 Carbondioxide 4.4
Nitrogen 6.6 Butane 4.3
Carbon monoxide 6.4
Your Micro-GC is configured either for carrier gas He (or H2) or it is

configured for N2 (or Ar). Make certain that the carrier gas selection in the
controlling Workstation corresponds to the carrier gas connected to your
Micro-GC. Use carrier gas corresponding this configuration. Changing
type of carrier gas must only be carried out using the mandatory
procedure in the Workstation software
If you are using hydrogen as carrier gas, pay particular attention to

possible leaks at connections inside and outside the Micro-GC (use an
electronic Leak Tester).
CP-Gas Clean filters are filled with nitrogen. If you are not using nitrogen
as the carrier gas, flush filters and gas lines after installation of a new
filter.

1HSAMPLE GAS
The Micro-GC is an analyzer built for the analysis of gases and vapors only. You are
advised to prepare a non-condensing gaseous samples standard sample for routine
check up of the instrument. Sample pressure should be between 0-100 kPa (0-15 psi),
the temperature between 0 and 40C ± 5°C of the analyzer ambient temperature and it
must be filtered, preferably through a 5 m filter. Varian, Inc. ALWAYS recommends the
use of the external filter kit part number CP736729.
Click here for more details about the heated sample line on page 18.
Liquids will seriously damage the instrument and should be avoided!
Handling a sample
If possible, filter and dry the sample before introducing it to the Micro-GC. It is advised
to use an External Sample Filter Unit between the injector and the sampling device.
The Filter, male must be hand tightened into the Filter Female, followed by a 1/8th turn
with a 7/16" wrench. The arrow on the Filter Female should be directed towards the
Fingertight Fitting. Replace the External Filter Unit on page 9 dat regular intervals.
Whenever possible remove moisture from samples introduced to the

Micro-GC.
Unheated Injector Systems

Heated Injector Systems

HEATED SAMPLE LINE
A heated sample line is always combined with a heated injector.

A heated injector and sample line is an option for a channel unit and is chosen in case
condensable samples need to be analyzed and condensation in the sample lines needs to be
prevented.
The heated sample and injector can be controlled between 30°C and 110°C.
Connect a heated sample line
Before connecting a heated sample line, allow the sample line heater to cool
down to ambient temperature. The metal surfaces of the sample line heater
are very hot and could burn your skin.
- Open the side panel, the heater will be visible.
- Remove the insulation.
Sample line heater
- The sample line connector will be visible.
- Connect the sample line.

Insulate the sample line coming into the Micro-GC, this to prevent damage to the
in/out coming cables.
Must be insulated!

2HPOWER
The Micro-GC requires 12.0 VDC, 130W maximum.

Refer to the User manual power supply for more information part number CP501267.
Only use the power supply that has been supplied with the instrument.
SHUT DOWN PROCEDURE
When the instrument is shut down for more then a few days please,
carry out the procedure mentioned below
Create a method for all channels with the following settings:
 Filaments switched OFF.
 Column temperature set at 30°C.
 Injector temperature set at 30°C.
 Pressure set at 50 kPa (7 psi).
 Wait until the temperature of the column and injector is < 40°C (to protect the column),
before switching off the Micro-GC.
 Remove the carrier gas tubing and plug all the vents/carrier gas connections with 1/8”
brass nut or plastic cap.
 When the instrument is going to be used again then follow the procedure on page 21

LONG STORAGE RECOVERY PROCEDURE
Follow the recovery procedure below if your Micro-GC has been stored for a
long period of time
 Remove the 1/8” brass nuts & plastic caps from all the vents/carrier gas
connections.
 Connect carrier gas tubing and apply pressure on the Micro-GC, according
the pre-installation requirements.
 Wait, at least 10 minutes, before switching ON the Micro-GC.
 Check immediately if the detector filaments are switched OFF, switch OFF if
necessary .
 Set the column(s) temperature to the maximum allowed temperature.
 Condition the column module, preferably overnight. This will ensure that all
the water has been removed from the column module and no damage will
occur to the TCD filaments.

INITIAL OPERATION
A test method has been provided. This method has been designed to determine if the
instrument is functioning properly and comes together with test chromatograms on
which the test conditions are stated.
If you ordered a Molsieve column, make sure it is conditioned before use.

See conditioning_Molsieve_columns on page 29 for parameters.
INITIAL RUN
SETTING UP THE TEST METHOD
To enter the method parameters, refer to the method set-up portion of the data-handling
package manual.
Send the instrument parameters from the data-handling package software to the Micro-
GC. You can watch the Micro-GC status in the instrument status tab.
INJECTING THE SAMPLE

Connect the sample by means of a 1/16" line
to the Micro-GC. You are advised to put an
external 5 m filter between the sample and N2 0.77 % Nitrogen
the Micro-GC for additional filtering (see CH4 89 % Methane
Sample_Gas on page 16 for more details). C2H6 8% Ethane
C3H8 1% Propane
Following are a few results on commonly IC4H10 0.14 % Isobutane
used columns. CP-Sil 5 CB and CP-Sil 19 NC4H10 0.2 % N-butane
CB, HayeSep A and Molsieve. The sample is IC5H12 0.007 % Isopentane
natural gas, which provides a convenient NC5H12 0.001 % N-pentane
standard for testing the instrument in any
configuration of these columns.

COLUMN CP-SIL 5 CB 6 METER UNHEATED
Instrument parameters
Column temperature : 50°C
Injector temperature : NA
Column pressure : 150kPa (21PSI)
Sample time : 30s
Injection time : 40ms
Run time : 60s
Detector sensitivity : Auto
Peak identification
ID Component Concentration
1 Composite Balance
2 Ethane 8.1%
3 Propane 1.0%
4 i-Butane 0.14%
5 n-Butane 0.20%
The natural gas components, mostly hydrocarbons, separate in the same order on the
non-polar and medium-polar CP-Sil CB columns. Nitrogen, methane, carbon dioxide,
and ethane are not separated on these columns. They produce a composite peak. For
separation of these components a HayeSep A column is advised.

COLUMN CP-SIL 5 CB 4 METER HEATED
Injector temperature : 110°C
Sample time : 30s
Run time : 30s
Peak identification
1 Composite Balance
2 Ethane 8.1%
3 Propane 1.0%
4 i-Butane 0.14%
5 n-Butane 0.20%

COLUMN CP-SIL 5 CB 8 METER HEATED
Sample time : 30s
Run time : 60s
Peak identification
1 Composite Balance
2 Ethane 8.1%
3 Propane 1.0%
4 i-Butane 0.14%
5 n-Butane 0.20%

COLUMN CP SIL13CB TBM 12 METER HEATED
Instrument parameters Peak identification

Column temperature : 40°C ID Component Concentration
Injector temperature : 50°C 1 Methane Balance
Column pressure : 250kPa (38PSI) 2 TBM 6.5ppm
Sample time : 30s
Run time : 80s

COLUMN HAYESEP 40CM HEATED
Sample time : 30s
Run time : 60s
Peak identification
1 Nitrogen 0.77%
2 Methane Balance
3 Ethane 8.1%
The HaySep A column separates oxygen, methane, carbon dioxide, ethane, acetylene,
ethylene, and selected sulfur gases. Nitrogen coelutes with oxygen. Components with a
higher molecular weight than propane have long retention times on this column.
Maximum allowable column temperature: 160 C

COLUMN MOLSIEVE 5Å 20 METER UNHEATED

Injector temperature : NA 1 Neon 18ppm
Column pressure : 200kPa (28PSI) 2 Hydrogen 1.0%
Sample time : 30s 3 Argon 0.2%
Injection time : 40ms 4 Oxygen 0.2%
Run time : 210s 5 Nitrogen 0.2%
The Molsieve 5Å column is designed to separate: hydrogen, carbon monoxide,

methane, nitrogen, oxygen, and some noble gases. Higher molecular weight
components have much higher retention times on this column.

Conditioning of Molsieve columns
On a properly activated column nitrogen and oxygen will be very well separated.
However, in time you will find that these two peaks will start to merge together. This is
caused by water, present in the sample or carrier gas, adsorbing to the stationary
phase. To restore the columns efficiency it will suffice to raise the oven temperature to
180 C (max. column oven temperature) and, with the normal operating pressure on the
column head, leave it to condition for about an hour. You are advised to switch the
detector filaments off during this period. After reconditioning you can test the column
performance by injecting plain air. If you have a proper separation between nitrogen
and oxygen again the column separation power has been restored. If the Micro-GC's
frequency of use is very high, you might adopt a standard reconditioning procedure of
leaving the instrument with the oven temperature at 180C overnight. The longer the
re+onditioning period the better the column performance without damage.

COLUMN PPQ 10 METER HEATED

Injector temperature : 110°C 1 Composite Balance
Column pressure : 150kPa (21PSI) 2 Ethane 8.1%
Sample time : 30s 3 Propane 1.0%
Injection time : 40ms 4 i-Butane 0.14%
Run time : 50s 5 n-Butane 0.20%

Reference
REFERENCE
INSTRUMENT DESCRIPTION
CARRIER GAS
The Varian, Inc. Micro-GC is configured for the use with either He (or H2) or N2 (or Ar).
Having chosen one option definitely rules out the use of the other without the
instrument undergoing internal changes prior to any switching of carrier gas
type.
It is recommended to use gases with a minimum purity of 99.995%. Since the injection
valve is operated pneumatically, there is a limit of 550 kPa ± 10 % (80 psi ± 10 %) to the
main gas supply.
Your Micro-GC is configured either for carrier gas He (or H2) or it is

configured for N2 (or Ar). Use the carrier gas type, for which your instrument
is configured, otherwise the detector filaments can be damaged.

Reference
GAS CLEAN UNIT

(OPTIONAL) Micro- Injector Column & Detector
electronic reference (TCD)
gas control
(EGC)
CARRIER GAS
SAMPLE COLUMN/REFERENCE
IN OUT VENT
MICRO ELECTRONIC GAS CONTROL (EGC)
The Micro-GC has built-in Micro EGC regulators that can be adjusted to get a constant
or programmed pressure control, which result in a constant or programmed flow through
the injector, column and detector. The pressure range of the Micro EGC is between 50-
350 kPa (7 - 49 Psi). This pressure sets a continuous flow of carrier gas of about 0.2-
4.0 mL/min.
A typical pressure rise is 200 kPa/min, which will give a significant pressure increase
during the run, without excessive baseline disturbance. In most cases baseline
subtraction may improve the quality of chromatograms that suffer from baseline drift.
INJECTOR
The injector has a built-in 10l sample loop that is filled with the gaseous sample. The
pressure of the sample should be between 0-100 kPa (0-15 psi) and the sample
temperature within 5-40 °C ±5 C of the analyzer.
By start “Run” within the data-handling package, a vacuum pump will draw the gas
sample through the loop and then the injector will inject the gas sample from the sample
loop into the gas stream. The minimum pressure required by the injector is 550 kPa ±
10 % (80 psi ± 10 %). A typical injection time is 40 milliseconds (ms). This equals an
average injection volume of 200 nL. Injection time will be rounded to a multiple of 5 ms.
A practical minimum value is 40 ms.
In most cases a value of 0 - 20 milliseconds will result in no injection.

Reference
COLUMN
A variety of column configurations are possible on the Micro-GC . The columns you
require for your specific analysis have been installed at our factory. Other configurations
are, of course, possible, but changing the column modules is a delicate matter that can
only be handled by one of our service engineers. Table I shows several standard
columns as supplied in the Micro-GC and selected applications. Other columns are
available by contacting Varian, Inc.
Column/Phase type Target components

Permanent gases, methane, CO, NO ,etc.(H.R. for O2-Ar
Molsieve 5Å baseline separation). Optional Retention Time Stability (RTS)
configuration
Hayesep A Hydrocarbons C1-C3, N2, CO2, air, volatile solvents.
CP-Sil 5 & 8 CB Hydrocarbons C3-C10, aromatics, organic solvents.
CP-Sil 19 CB Hydrocarbons C4-C10, high boiling solvents, BTX.
CP-WAX 52 CB Polar higher boiling solvents.

Light hydrocarbons C1-C5 saturated and un-saturated.
PLOT Al2O3/KCl
Optional Retention Time Stability (RTS) configuration.
Hydrocarbons C1-C6, Freons, Anesthetics, H2S, CO2, SO2,
Pora Plot U
volatile solvents.
Hydrocarbons C1-C6, Freons, Anesthetics, H2S, CO2, SO2,
Pora Plot Q
volatile solvents.
CP-COX CO, CO2, H2, Air, CH4.
THT column THT and C3-C6 + in Natural Gas Matrix.
TBM column TBM and C3-C6+ in Natural Gas Matrix.
CP-Poraplot Specially tested for H2S in natural gas (10 to 50 ppm)

Unique column specially tested for MES in natural gas (1
MES column
ppm)
For all compounds not present in this list contact you nearest Varian office
All columns except the HayeSep A (160 C) and MES (110 C) (TCEP) column
can be used up to 180 C, the maximum temperature of the column oven. The
HayeSep A will deteriorate above 160 C. Exceeding this temperature will
cause the column to lose efficiency instantly and the column module will
need replacement.

Reference
DETECTOR
TCD
The Micro-GC is equipped with a thermal conductivity detector (TCD). This detector
responds to the difference in thermal conductivity between the carrier gas and the
sample components. The construction of a TCD is such that the changing thermal
conductivity of the carrier gas stream, due to components present, is compared to the
thermal conductivity of a constant reference gas stream.
DMD
The Differential Mobility Detector, DMD, is fully integrated into a Analytical channel.
Differential Mobility Detection is an advanced form of Ion Mobility Spectroscopy (IMS). It
uses a drift tube under atmospheric and thermally constant conditions. See for more
details chapter The difference mobility detector on page 39.

Reference
IN/OUTPUTS
The Micro-GC has several in/output ports accessible inside the instrument for
interfacing with external devices.
Open the cover.
At the front of the Micro-GC, the external device connectors will be visible.
Close the cover after connecting the cables!

Reference
EXTERNAL DIGITAL I/O
Connection between Micro-GC and external devices is made with the appropriate cable
to the External Digital I/O port (see also External_devices on page 63).
CP-4900 Pin 1 Digital IN1 (not definied)

2 Digital IN2 (not definied)
3
4 Digital OUT1 (not definied)
5 Digital OUT2 (not definied)
6
Not used
7
8
Micro-GC will only start in external ready mode when
9 Start-IN Start-IN detects a contact closure pulse
10 External Ready-IN
11 External system reset
12 Not used
* 13
OUT Relay 1
14
* 15
OUT Relay 2
16
* 17
OUT Start 500 ms contact closure when injection will take place
18
* 19
OUT Ready/not ready
20
21 Reserved
22 +5 VDC out (electronic fused max 500 mA)
23
24 +12 VDC out ( electronic fused max 500 mA)
25
GND External Digital I/O

* Relay contacts maximum 24 Volt 1 Ampere
Ready/not ready signal
The Instrument Ready/not Ready output will follow instrument status (Ready LED in the
front of the instrument).

Reference
COMMUNICATION PORTS (COM)
The instrument can communicates serially with the computer via an RS-232 port
(COM 1) accessible inside the instrument. (see also Serial communication on page 49).
In the table below an overview is given of the communication possibilities.
Function Galaxie (Standard) EZchrom

COM 1 - RS-232-interface
COM 2 RS-232-interface RS-232-interface
COM 3 RS-485-interface RS-485-interface
Ethernet 10Mbit 10Mbit
Video output VGA (not used) VGA (not used)
COM 1 DCD data carrier detect

COM 2
Pin 1 Pin 1
2 TXD transmitted data RXD received data
2
3 RXD received data TXD transmitted data
3
DTR data terminal ready
4 4
5 GND ground GND ground
5
DSR data set ready
6 6
7 CTS clear to send RTS request to send
7
RTS request to send
8 8
RI ring indicator CTS
9 9
RS-232 RS-232
COM 3
Pin 1
2
3
RXA(+)
4
RXB(-)
5
6
7
TXB(-)
8
TXA(+)
9
RS-485

Reference
EXTERNAL ANALOG I/O
This external analog I/O port can handle six (6) analog inputs (input 0-10 Volt)
The User Interface receives this analog information, and translates this information into
actions to be taken by the local user interface and/or events/data to be shown/stored in
the remote user interface (see also External_devices on page 63).
490-GC
GND Pin
1
2 EXT-Analog IN1
3 EXT-Analog IN2
4 EXT-Analog IN3
5 EXT-Analog IN4
6 EXT-Analog IN5
7 EXT-Analog IN6
8
10
11 -15 VDC out (electronic fused max 100 mA)
12
14
Analog GND
External Analog I/O

Reference
THE DIFFERENTIAL MOBILITY DETECTOR
GENERAL
This detector contains a Ni63 beta-emitting radioactive

WARNING: isotope plated onto a metallic foil for ionization of the
RADIATION SOURCE carrier gas.
For details about procedures governing the handling, leak testing, repair,
storage, shipping and maintenance of records for the Ni63 DMD detector as a
radioactive sealed source please refer to the Ni63 Radiation Safety Manual.
General functionality
Varian has extended its Micro Gas Chromatography product line with a new detector.
The Differential Mobility Detector, DMD, integrated into the chassis is a joint
development of Sionex Corporation and Varian Instruments.
Differential Mobility Detection is an advanced form of Ion Mobility Spectroscopy (IMS). It

uses a drift tube under atmospheric and thermally constant conditions. The advantage
over IMS is that DMD uses additional sets of RF modulation voltages, which results in
selective performance, which is tuneable depending on the compounds of interest and
the matrix.
Ions generated by a Ni63 radioactive ionization source are transported through a drift
tube by means of a high velocity transport gas, usually Zero-Air or Nitrogen. The drift
tube basically consists of two parallel plates, approximately 500 microns apart. Over
these plates a RF modulated electric field is applied by setting a fixed Voltage of 2-500
Volts/cm and a Scanning Voltage (or Compensation Voltage). The RF modulation
frequency is 1.3 Megahertz.
Isolation results from the interaction between the ion and the net applied field that
alternates between high and low electric field strength. Trajectory of the target ions will
be tuned so that the ions of interest straight through the filter without colliding with the
electrode plates, when they would be neutralized and not detected. The Compensation
Voltage is used for ‘tuning’ the trajectories of ions in order to get the ‘desired’ ions
towards the detector.

Reference
Figure: DMD set-up showing different voltages applied.
As illustrated in Figure 1, the net voltage applied results from three independent
settings:
1. A fixed voltage, or RF-Voltage,
2. A scanning voltage, also referred to as Compensation Voltage,
3. A RF modulated voltage.

Reference
Figure 2:Separation principle of DMD
As illustrated in Figure 2, the DMD is equipped with two detectors, one for positive ions
and one for negative ions. Yet, the data produced by the DMD show a ‘normal’ two-
dimensional representation as the system will be ‘tuned in time’ to detect certain
species by setting compensation voltages to accommodate transmission of the
compound of interest in that particular part of the chromatogram. This ‘time-segmented’
detection thus leads to maximum selectivity for the application of interest as the matrix
is eliminated. The application specific method is saved inside the DMD hardware.
Micro-GC DMD Channel
The DMD channel is always located in the last position (against the backpanel)
Position 2 DMD channel
The firmware recognises the DMD channel as a detector only, and automatically sets
the controls accordingly.

Reference
A complete instrument, the DMD consists of a basic cabinet, a column module with its
pneumatic system, its standard µ-TCD and an additional DMD. The standard channel’s
µ-TCD output is in series with the DMD inlet via a heated transfer line. The temperature
of this heated transfer line is controlled from the DMD electronics.
From a control point of view, the DMD has no control of a column temperature or
column head pressure or the optional injector temperature as needed for the GC
channel. No carrier gas type needs to be selected in the configuration.
Furthermore, the DMD method is factory tuned and ready to perform the appropriate
application. This requires the Micro-GC method to be identical throughout its use with
respect to chromatographic column and settings.
GENERAL OPERATION
Within the workstation package, the DMD will be handled as a separate channel. With
respect to the operation of the DMD note the following:
 In instrument configuration, selection of carrier gas type and heated injector has
been removed.
 In method development for the DMD channel, GC-channel specific information has
been left out. Instead, the Transfer line temperature and the detector tuning
capabilities are added.
 In instrument status for the DMD channel, GC-channel specific information has
been left out. Instead, the Transfer line temperature and the detector tuning
capabilities are added.
Tuning the DMD
The complete DMD method for the instrument specific application has been tested and
is loaded inside the DMD. Generally no modification or changes are required in case
the factory-supplied method is used throughout.
In case of a suspected misalignment of the method, where retention time or

compensation voltage may be out of tune, a tuning run may be needed.
Please contact for more information your local Varian Inc. subsidiary or Varian, Inc.
representative.

Reference
PROTOCOLS
A protocol is a set of rules that govern how computers send and receive information.
Different Types of Protocols:
AppleTalk, ATM, Banyan Protocols, CDPD, DECnet Protocols, Frame Relay, GPRS,
H.323, IBM Protocols, ISDN, ISO Protocols, LAN Data Link Layer Protocols, MPLS
Novell Protocols, PPP Suite, Bridge/Router Internetworking Protocols, SNA, SS7
Suite Sun Protocols, Tag Switching Protocols, TCP/IP Suite, UMTS Telephony, V5,
Voice over IP#(VoIP), WAP, X.25, XNS
The Internet Protocol Suite
 Developed to allow cooperating computers to share resources across a network.

 TCP and IP are the two best-known protocols in the Internet Protocol Suite.
 Other protocols / services are FTP, Remote Login (Telnet), Mail, SMTP.
IP Addresses
 Uniquely identify a computer on the Network / Internet.

 Are made up of four 8-bit numbers and each of these numbers are separated by a
point.
 Each of the 8-bit numbers can represent a decimal value of 0-255.
 Each part of an IP address can only be in that range (e.g., 198.12.253.98).
The Internet protocol suite
Starting IP Ending IP Subnet Mask Type

0.0.0.0 255.255.255.255 N/A Public
10.0.0.0 10.255.255.255 255.0.0.0 Private
172.16.0.0 172.31.255.255 255.255.0.0 Private
192.168.0.0 192.168.255.255 255.255.0.0 Private
Note: never use 0.0.0.0. or 255.255.255.255

Reference
MICRO-GC AND NETWORKS
Network Requirements of the Micro-GC
 Customer Cable type should be Cat3 or Cat5 UTP / STP.

 Customer network should comply with Standard Ethernet (IEEE 802.3).
 The network must have either 10BASE-T or 10/100BASE-TX compatible HUB or
Switch.
 TCP-IP should be used on the network.
FAQ (FREQUENT ASK QUESTIONS)
Q: Can I connect the Micro-GC to my Network?

A: Yes, if the network is standard Ethernet and uses TCP-IP with UTP cabling.
Q: I’m using a DHCP server; can I use this to assign the GC with an IP-Address?
A: No, The GC works with static IP-addresses only, so an IP-address will have to be
reserved on the DHCP server and marked as static.
Q: How do I assign the GC with an IP-address?

A: Connect the GC via a UTP crossover cable to the pc running Workstation software.
Then define the network-settings, and restart the GC with the Service button
pushed.
Q: Are the network settings saved if the GC is restarted, or with loss of power?
A: Yes, the Network Settings of the GC are stored in Flash Memory, and will not be
erased at loss of power.
Q: Can I control my Micro-GC from anywhere in the world via the Internet?
A: Yes, if the customer network is designed for this, and has Internet access or remote
access facilities (the ports 4900,4901 and 4902 must be open).

Reference
GLOSSARY OF NETWORK TERMS
The following brief glossary of terms may be useful:
BNC connector
This is a bayonet style connector used for a two-conductor style hardware connection.
BNC connectors are used with the CP-3800 GC.
Crossover Cable
A cable is used to connect two, and only two, Ethernet devices together.
Domain
This is one of several settings that reside within the TCP/IP configuration that identifies
paths that are used to establish connections with Ethernet devices. The Domain is an IP
address.
Ethernet Address
This is a unique identifier that every Ethernet communication device has assigned to it.
Typically, the Ethernet address cannot be changed and is the permanent way of
identifying a particular hardware device. The Ethernet address consists of 6 pairs of
hexadecimal digits.
Gateway
This is one of several settings within the TCP/IP configuration that identifies paths that
are used to establish connections with Ethernet devices. The Gateway is assigned an
IP Address.
Host name
The host name is an alternate way of identifying a device that is friendlier to people.
Frequently the host name and the IP address may be used interchangeable.
Hub
A device that allows many Ethernet devices to be interconnected. Several hubs may be
interconnected to increase the number of Ethernet connections. For 10Mbits/second
network connections (10BaseT), no more than four (4) hubs may be connected in
series. For 100M bits/seconds network connections (100BaseT), no more then two
hubs may be connected in series.
IP Address
This is a unique number for each Ethernet device within the set of connected devices.
Two PCs may have identical IP addresses so long as they are not interconnected to
each other either through the Internet. The IP Address consists of a series of four sets
of decimal numbers (between 1 and 255) that provide routing information used by the
TCP/IP protocol to establish a reliable connection. Without the IP Address,
communications would be bogged down trying to establish connections to Ethernet
addresses at unknown locations.
Reference
Patch Cable
A cable that is used to connect Ethernet devices to hubs, switches, or your company
network.
RJ45 Connector
This is a telephone jack style connector used for a Universal Twisted Pair (UTP)
hardware connection for 10/100BaseT Ethernet connections.
RJ45-style connectors are used by the Micro-GC.
TCP/IP
An international standard protocol used by the Internet. We use this protocol for
communication to the Micro-GC. You may find several network protocols, such as
IPX/SPX and NetBEUI, installed on you computer.

Reference
Workstation software
For detailed driver information visit the help-file(s) in the used Workstation
software.
EZChrom Elite Galaxie
Communication Ethernet and RS232 Ethernet only
IP Settings BootP/RS232 BootP/RS232
Com 1 RS232 Not available
Stream selection on Stream selection on

Com 2
Com-2 Com 2 *
Com 3 Not available Not available
Yes
Analog I/O Capturing
(via Analog Board)
External start in: Yes External start in: Yes

Digital I/O
External Ready: Yes External Ready: Yes
Timed Relay: Yes Timed Relay: Yes

Relay Control
Alarm Relay: Yes Alarm Relay: Yes
* Only one Vici valve possible in Galaxie

Reference
EZCHROM ELITE
Multiple Micro-GCs can be controlled serial or Ethernet.
The maximum number of Micro-GCs controlled by (one computer) serial communication is two.
For Ethernet this is limited by your license.
The 490-GC driver scope
CONTROL INSTRUMENT
Ethernet control on page 50 (TCP/IP) is standard.
Even if the instrument is equipped with Ethernet it is possible to control the instrument serially.
In that case the instrument will accept the first incoming connection type (serial or Ethernet) and
will lock the other connection type. There can never be a connection on the two different ports
at the same time.

Reference
SERIAL COMMUNICATION
To control the Micro-GC via serial communication, just connect the serial cable (supplied with
the instrument) to a free serial port of your computer configured as RS232, and plug the other
side into port COM 1 of the Micro-GC (see Inside View on page 14).
Avoid cable lengths longer than 15 meter while this can cause communication
problems due to high communication speed (baud rate 115200 bits/sec).
The maximum number of Micro-GCs controlled by serial communication is two.

Choose Ethernet communication in case more than two Micro-GCs must be
controlled by one computer or setup a second computer with EZChrom Elite
installed. If RS485 is required, an RS232-RS485 converter (optional) must be used.
RS485 is only possible via two RS232-RS485 converters, one on Workstation
(computer) side and either one at Micro-GC side on Com 1.
Com 1: RS232 Serial Cable Com 1
Com 2: RS232
Serial Cable
EZChrom Elite
490-GC
Com 1
490-GC

Reference
ETHERNET COMMUNICATION
An Ethernet crossover cable (RJ-45 connector, 2.8 meter) is included with the Micro-GC.
The crossover cable must be used to control the Micro-GC in a peer-to-peer communication
(see Inside View on page 14).
This requires IP addresses in the same range for computer and Micro-GC. Only the most right
IP segment must be different.
In case both the computer as well as the Micro-GC are connected to a (local) network this cable
cannot be used for control of the Micro-GC.
However this crossover cable must be used if a new IP address has to be assigned to the
Micro-GC. Once the IP address is assigned you can disconnect the crossover cable and
connect computer and Micro-GC both to a (local) network.
Peer-to-peer: single instrument
Crossover Cable
Workstation
Any IP-address allowed
490-GC
Multiple 490-GCs connected to a local
workstation. IP-address in same range
as computer IP-address.

Reference
Multiple instrument (local network)
Switch
Patch
Cable
Workstation
Any IP-address allowed
EZChrom Elite maximum connections are limited by

the computer speed, license and network
performance.
490-GC
Multiple 490-GCs connected to a local
workstation. IP-address in same range
as computer IP-address.

Reference
Global network: Multiple instruments
Switch
Subnet
EZChrom Elite
IP-address in range of subnet 1
Router
490-GC
Multiple 490-GCs connected to a
Internet
companies network. IP-address in
same range of subnet 1.
Switch
Subnet 2
EZChrom Elite
IP-address in range of subnet 2 IP-address in range of
490-GC in subnet 1 can also be controlled subnet 2

Reference
COMMUNICATION SETUP
In the Workstation window select the type of communication for instrument control.
Serial communication (EZCrom only)
For serial communication select a free serial port on your computer which is configured
as RS232. You need an RS485-RS232 converter to control the instrument via RS485.
Com1 on the Micro-GC is fixed configured as RS232. The baud rate is fixed at 115200
bit/sec.
Ethernet communication (Galaxie)
For Ethernet communication select “Configure system”, followed by the “Network

Parameters” in order to setup the IP address for the instrument. If the IP address is
already known (and in the right subnet range) only the IP address has to be typed in.
It’s also possible to change the IP address (Assign new IP address on page 54) with
BootP and to view all the Micro-GCs connected to the subnet.

Reference
ASSIGN NEW IP ADDRESS VIA ETHERNET CONNECTION
If for the network the Micro-GCs IP address is unknown or invalid, a new IP address must be
assigned.
To assign a new IP address the following steps are required:
1. Make sure the computer and the Micro-GC are connected to the same subnet or use the
supplied Ethernet crossover-link cable to connect computer and Micro-GC (peer to peer
connection).
2. Setup the IP address for the computer in case the computer wasn’t connected to a network
before. For a global network, the system administrator must be contacted.
3. Enter the IP address that must be assigned to the Micro-GC. This IP address must be in the
same range as the computers IP address. The three left IP segments must be identical.
4. Enter the Subnet Mask. This will be in most cases 255.255.255.0.
5. Enter the Gateway IP address if this is required. In most small local network this is not
required.
6. Enter the Domain if this is required. In most local network this is not required.
7. Enter a Host name for the Micro-GC.
8. Do now reboot the Micro-GC in the assign IP-address mode. Hold down the push button
located just above the Ethernet RJ-45 connector in the Micro-GC on page 14 and power up
the Micro GC. Hold down this button till the instrument is started. This will take
approximately 1 minute. The Micro-GC is now in assign IP-address mode and starts
broadcasting on the net “Waiting for IP address assignment”. There is a BOOTP/DHCP
server running in the Micro GC when it is started in service mode.
9. Press now the “Assign IP address” button. The Micro-GC driver does now assign the
defined IP address to the first received BOOTP/DHCP request. This will take maximally 2
minutes.
10. Switch the Micro-GC off and then on again (Reboot).
Never startup two Micro-GCs in the assign IP-address service mode at the same
time. This to avoid assigning an IP address to the wrong Micro-GC.

Reference
ASSIGN NEW IP ADDRESS VIA SERIAL CONNECTION
1. Make sure this computer and the Micro-GC are connected via a serial RS232 cable
(peer to peer connection).
2. Start the Micro-GC configuration in Serial mode (see communication setup) on page 53
3. Click on the button “Serial Setup IP-address”, the “Serial Setup Ethernet Settings”
window appears.
4. Enter the IP address that must be assigned to the Micro-GC. This IP address must be in
the same range as the computers IP address. The three left IP segments must be
identical.
5. Enter the Subnet Mask. This will be in most cases 255.255.255.0.
6. Enter the Gateway IP address if this is required. In most small local network this is not
required.
7. Click now on the button “Assign IP address” of the “Serial Setup Ethernet Settings”
window.
8. Switch the Micro-GC off and then on again (Reboot).
9. Change the Micro-GC configuration from Serial mode to Ethernet mode and proceed as
described in the section Ethernet communication on page 50.

Reference
REMOTE ACCESS INSTRUMENT STATUS
The Instrument status of the Micro-GC can be accessible for other applications like Varian
userlink applications: Mlink32, I/O Control, PCI1000Com or any other self written program
capable to collect instrument status from the UserDataStore database.
It is required that this application runs on the same computer together as EZChrom-Elite. Read
the user-manual of Mlink32, I/O Control or PCI1000Com in order to import the instrument status
into these applications. Find more information in topic Varian Userlink applications. on page 60.
To enable remote access of instrument status, select a unique “Instrument” number and
“Remote Access status” In the Automation Tab of the Instrument Configuration.
The following instrument status parameters are available for other applications running:
UserDataStore
Parameter description
Address
1200 Serial number Main board
1201 Serial number Channel 1 Controller
1205 Serial number Channel 1 Analytical Module
1209 Part number Channel 1 Analytical Module
1213 Reserved for Tx com2 Don’t use this
1214 Reserved for Tx com3 Don’t use this
1215 Reserved for Rx com2 Don’t use this
1216 Reserved for Rx com2 Don’t use this
1218 Instrument State (0=Initializing, 1=Flushing, 2=Running, 3=Stabilizing,
4=Ready, 5=Error, 6=Recovery error, 7=Broken, 8=Not ready)
1219 Instrument general Error State. Find error description in next table
1220 Error State
1221 Sample Line temperature in Celsius
1222 Ambient pressure in kPa
1223 Ambient temperature in Celsius
1224 Power Supply in Voltage
c1226 Auto Sampler position
1227 Auto Sampler position at start of run
402 Current stream position
Reference
1230 Instrument external Ready-In state

1231 External Analog Input #1 in units determined by the scaling and offset
factors
factors
factors
factors
factors
factors
1237 External Analog Input #1 at start of run (copied from address 1231)
1243 Column temperature channel 1 in Celsius
1244 Column temperature channel 2 n Celsius
1247 Injector temperature channel 1 in Celsius
1251 Column pressure channel 1 in kPa

Reference
GENERAL ERROR STATE
The General Error State as stored in UserDataStore address 1219 is composed of the following
items:
The error must be handled as ‘CLNNN’ in which C=error class, L=location and NNN=error
number or event number.
The Error class contains of the following values: 0=diagnostic error, 1=advisory error, 2=critical
error, 3=fatal error.
There are five locations: 0=main board, 1=channel 1, 2=channel 2, 3=channel 3 and 4=channel
4.
Error number NNN Error Description

1 Init passed (event)
2 Pressure restored
3 Start flush cycle
4 Flush cycle passed
5 TCD calibrating
6 Too low pressure
7 Pressure fault
8 Low battery 1
9 Low battery 2
10 Sample line sensor fault
11 Sample line temperature fault
12 Injector temperature fault
13 Column temperature fault
14 TCD Temperature limit activated
15 EDS logging error
16 Low power supply
17 Injector sensor fault
18 Column temperature sensor fault
19 TCD control error
20 TCD calibration failed
21 Hardware reset"
22 Pressure too high
23 Initialization error
24 Internal communication error
25 Instrument EDS incorrect
26 EDS incorrect
27 Internal power failure
28 Flush cycle aborted
29 GC module changed
30 TCD Gain calibrated
31 TCD Offset calibrated
32 Null String

Reference
33 ADC reading out of range

34 EDS Analytical Module incorrect
35 EDS Config checksum incorrect
36 EDS Logbook checksum incorrect
37 EDS Protected checksum incorrect
38 EDS C.C. Config checksum incorrect
39 EDS C.C. Logbook checksum incorrect
40 EDS C.C. Protected checksum incorrect
41 EDS A.M. Config checksum incorrect
42 EDS A.M. Logbook checksum incorrect
43 EDS A.M. Protected checksum incorrect
44 EDS Config SVER incorrect
45 EDS Protected SVER incorrect
46 EDS C.C. Config SVER incorrect
47 EDS C.C. Protected SVER incorrect
48 EDS A.M. Config SVER incorrect
49 EDS A.M. Protected SVER incorrect
50 Pressure Offset calibration complete
51 Pressure Offset calibration Failed
52 Unable to store pressure offset
53 Temperature sensor disconnected
60 DMD control to temperature setpoint
61 DMD start run
62 DMD stop run
63 DMD start tuning
64 DMD case temperature error
65 DMD sensor temperature error
66 DMD method file error
67 DMD sensor voltage error
68 DMD RF voltage error
69 DMD Vc voltage error
70 DMD sensor pressure error
71 DMD tuning process error
72 DMD gas flow error
73 DMD system voltage error
74 DMD communication error
75 DMD sensor error

Reference
VARIAN USERLINK APPLICATIONS
The schedule describes the data transfer between applications.
External Relays
The switch condition for the external Relays of the can be setup out of almost any parameter
available in all application part of this schedule. Everything stored in the shared UserDataStore
database can be used to setup a switch condition, since every Varian userlink application is
capable to store its specific results into this database. To store CP-Maitre Elite 3.2
concentrations into the UserDataStore database look at topic Common Tab of Instrument
Method Setup.

Reference
instrument status including analog inputs
The instrument status and analog inputs can be stored into the UserDataBase database.
Applications like Mlink32, PCI1000Com and I/O Control can retrieve these from the database.
UserDataStore addresses of Varian userlink applications
Find below a table of relevant UserDataStore addresses, which can be used, for alarming
purposes. The addresses are all part of the Varian Userlink applications: ISOCAL32, BTU32,
InstrumentNorm32 and Mlink32.
The addresses are specific for each instrument (maximal four instruments)
ISOCAL32 BTU32 ValveControl32

Address Parameter Address Parameter Address Parameter
0 Calib.Level 200 Calib.Level 402 Current Stream
Position
1 Total-ESTD 201 Total-ESTD 404 Calib.Level
2 Total- 202 Total-
Estimates Estimates
3 Hs_MJ/m3 203 Hv_actual InstrumentNorm32
4 Hi_MJ/m3 204 Hv_dry Address Parameter
5 Rel.Density 205 Hv_saturated 0 Calib.Level,
SampleID
6 Density 206 Hv_act._MJ/m 1 Total-ESTD
3
7 Wobbe_MJ/m3 207 Wobbe 2 Total-Area
8 MoleWeight 208 MoleWeight 20 ESTD Peak1
9 MoleWeight 209 MoleWeight 109 ESTD Peak90
ratio ratio
10 Hs_KW/m3 210 Rel.Density 110 ESTD% Peak1
11 Wobbe_KW/m 199 ESTD% Peak90
3
20 ESTD Peak1 220 ESTD Peak1
109 ESTD Peak90 309 ESTD Peak90
110 ESTD% Peak1 310 ESTD%
Peak1
199 ESTD% 399 ESTD%
Peak90 Peak90

Reference
EliteExport.dll
Address Parameter
501 Calib.Level and SampleID
511 Stream Position from CP-Maitre Elite
512 Total ESTD summed of all channels
EliteExport.dll or Mlink32
520 and User defined parameters as defined in the UserDataStore sheets output section of
up Mlink32 or as defined in the EliteExport.ini file.

Reference
EXTERNAL DEVICES
The is equipped with several external I/O’s in order to control external devices or to synchronize
with external devices. External devices can be external pump(s), alarms, Auto Sampler, etc.
The following I/O’s are standard available:
1. Two external serial ports (Com2: RS232, Com3: RS485)

The driver supports control of the VICI electric actuated multi positional valve via Com2
(see also COM_port_details on page 37).
2. Two external relays (contact closures)
The driver supports alarming purposes, Auto-Sampler control via solenoids and external
pump control (see also External_digital_IO on page 36).
3. External Start In
The driver supports the start of the Micro-GC by an external device (Flow computer or
PLC). The Micro-GC processes this event (start run) and passes the event to the driver
(see also External_digital_IO on page 36).
4. External Start Out
The “External Start Out” signal is directly controlled from the Micro-GC (see also
External_digital_IO on page 36).
5. External Ready In
The “External Ready In” signal is not processed in the Micro GC. The driver acquires
this event. It can be used to synchronize with an external device (see also
6. External Ready Out
The “External Ready Out” signal is directly controlled from the Micro-GC (see also
7. Six External Analog Input signals
The driver supports the acquisition and processing of the External Analog Input signals
(see also External_Analog_IO on page 36).
The VICI electric actuated multi positional valve

Reference

Reference
Cycle with static (electronic) pressure

This time diagram will help you to understand the Static (electronic) pressure cycle of the Micro-GC .
Pressure
 After the run sampling is  Pressurisation  During NOTE: This description is only for one channel. In most
cases a dual-channel system is used; in this situation the
begun. This means that the delay (120 mS), used injection time sequence is the same, but the timing-settings can differ. If the
sample is (mostly) sucked into the to pressurize the the sample is sample-time on channel A and channel B are different, the
sample-loop. sample to the same transported to longest time is used for both channels. Also the run-time can be
pressure as the the column by specified per channel; the data-acquisition stops per channel as
column head the carrier gas soon as the run-time has elapsed. The total analysis-time
pressure. depends on the longest run-time.
initial pressure
time
download pressurisation
Sample Time inject time run time
method time
equilibration time
run started
inject start data acquisition run finished
 Before a run is  The run can be started,  Fixed  The real  After the
started all used when the is ready (Ready equilibration-delay analysis (run) specified run-time
method- LED is lit). of 40 ms. This and data- has elapsed, the
parameters must The Workstationsoftware will time allows the acquisition is run is finished.
be downloaded wait until data is received sample to settle in started.
via the from the Micro-GC. the sample-loop
Workstation

Reference
Cycle with electronic pressure control
This timing diagram will help you to understand the electronic pressure control (EGC) cycle of the Micro-GC .
The diagram shows the situation in the Micro-GC , using electronic (programmed) pressure control. The timing before the
injection is identical to the static pressure cycle.
The remaining final time depends on the total run time, the duration of the initial time and the
pressure rise. This means that it is possible that the final time is zero. Another situation is that
the final pressure is limited, because of these settings. The software will check all parameter-
values and change them into realistic values.
Pressure
NOTE: During the run-time there can be only one pressure-ramp to higher pressure.
not ready
final pressure
 The pressure rise is started,
the duration is depending on pressure rise pressure relieve
two (2) parameters:
 Pressure rise
 Final pressure
ready
ready
initial pressure
 Stabilization
time for the
pressure after it
has been
time
returned to the
initial pressure
Fixed 500 mS
download pressurisation relieve stabilisation
Sample Time inject time initial time rise time final time
method time time time
equilibration time
run started inject start data acquisition run finished
run time
 During initial time  As soon as the final-pressure is  Relieve time, the time needed to
the column head reached, the rise stops and the decrease the column head pressure
pressure remains the final-time begins. The pressure from the final pressure to the initial
same. remains the same. pressure.

Reference
COLUMN MODULE CONDITIONING
Follow this procedure to make sure that any “water” that might be present
inside the analytical column is removed before the TCD is switched on.
Also follow this procedure if the Micro-GC or Micro-GC module has been
stored for a long period.
The detector filaments may be damaged if this procedure is not followed!
1. Switch off the TCD filaments in the method.
2. Set the column temperature of the module to the maximum temperature.

Leave the filaments off!!
3. Download this method to the Micro-GC.
4. Condition the column module, preferably overnight.
This will insure you that all the “water” has been removed from the column
module and no damage will occur to the TCD filaments.

Reference
Backflush option
Backflush to vent is an advanced technique, which is used to prevent later
eluting compounds to reach the analytical column and detector. The main
reason for applying this technique is to keep the analytical column clean and
reduce analysis time.
The Varian Micro-GC is optionally available with GC modules that incorporate
backflush capabilities.
A backflush system always consists of a pre-column and an analytical column.

The two columns are coupled with a so-called pressure point, which makes it
possible to invert the carrier gas flow direction through the pre-column at a
preset time, the "backflush time".
Restriction
Pressure point
System Analytical
Pre-column column Detector
pressure
Pressure
regulator
Injector Backflush
vent

Reference
Foreflush Restriction
Pressure point
System Analytical
pressure
Pressure
regulator
Injector Backflush
vent
Description
The injector, two columns, and detector are set in line.

The sample is injected onto the pre-column where a pre-separation takes place;
injection takes place in "foreflush" mode (see foreflush diagram).
Backflush
Restriction
Pressure point
System Analytical
pressure
Pressure
regulator
Injector Backflush
vent
When all compounds which are to be quantified are transferred to the analytical column,
the backflush valve switch (at the backflush Time) On the pre-column the flow is
inverted and all compounds left on the pre-column are now (back) flushed to the vent
(see backflush diagram). On the analytical column the separation goes on, because as
there the flow is not inverted!

Reference
The standby mode for the is to be in the backflush configuration (if the instrument is
equipped with the optional backflush valve).
Back flushing will ensure that the pre-column will be in good condition for the next run.
Tuning
Tuning of the backflush time is done by trial and error. Reducing the backflush time will
transfer fewer compounds to the analytical column.
How to Tune
Obtain a chromatogram in foreflush. Check out the retention times of the compounds
you have to quantify. Start at a backflush time of 10 seconds. Obtain a second
chromatogram. Adjust the Backflush time (increments of 0.1 seconds are possible) until
all components of interest are transferred to the analytical column and that all unwanted
peaks are backflushed.
Be aware that a small pre-column is used. It is not always possible to cut between 2
peaks!
Backflush Time range 0.5 seconds until maximum run time.
Special value
BACKFLUSH TIME = 0 this puts the system in FOREFLUSH mode during run the entire
run.

Reference
SHIPPING INSTRUCTIONS
If your Micro-GC for any reason must be sent back to the factory, it is very
important to follow these additional shipping preparation instructions:
1. Add all the vent caps at the back of the Micro-GC.
2. Always include the power supply.
3. Include, if used, the inlet filter(s).
CLEANING INSTRUCTIONS
To keep the Micro-GC surface clean, refer to the remarks given below:
 Switch the Micro-GC off.

 Remove the power cable.
 Put protection plugs on the sample and carrier gas inlets.
 Put protection plugs on the Column vents.
 Use a soft (no hard or abrasive) brush to carefully brush away all dust and
dirt.
 If the outer case is dirty (never clean the inside!) clean it with a soft, clean
cloth dampened with mild detergent.
 Never use alcohol or thinners to clean the Micro-GC, these chemicals can
damage the case.
 Be careful not to get water on the electronic components.
 Do not use compressed air to clean.
DISPOSAL INSTRUCTIONS
When the lifetime of the Micro-GC or parts of it has reached the end of its
useful life, disposal must be carried out in accordance with all (environment)
regulations applicable in your country.

Reference
ERROR LIST
ERROR HANDLING
During operation a series of events and error messages are generated indicating start
or finishing of certain actions and procedures as well as smaller and fatal errors
somewhere in the instrument. This section describes how micro-GC reacts to these
events or messages.
The following error classes as well as the subsequent actions are available:
Class 0 Internal event.

Basically these are only events indicating a certain procedure has started or finished. In
no way do they influence the proper functioning of the instrument.
Class 1 Advisory fault; the instrument continues.

These are the less-critical errors, advisory errors not requiring immediate action from
the user. The ongoing run may be minimally effected by it and thus need not to be
stopped. Class 2 error messages indicate certain malfunctions of the instrument. Some
errors of this type keep the instrument from becoming ready.
Class 2 Critical errors for logging; error LED ON.

These are critical errors for which the user needs immediate warning (window-pop at
workstation! as well as Error-LED). The run in progress is to be stopped since its results
will definitely be wrong. Corrective action by the user or instrument service may be
required.
Class 3 Fatal errors for logging; instrument shut-down, error LED and buzzer ON.
These are fatal errors for which the user needs immediate warning! (Error-LED). An
instrument shut-down will be generated. Corrective action by the user or service is
required.
All errors, independent of class are to be transferred to reader (PROstation or web

browser) connected for display (trouble shooting information) under instrument status.
All Class 1 and above errors will be logged on flash.
Individual numbers identify all errors; these numbers are built using the error class and
a number. Events are not numbered.

Reference
ERROR LIST:
The General Error State as stored in UserDataStore address 1219 is composed of the
following items:
The error must be handled as ‘CLNNN’ in which C=error class (severity),

L=location and NNN=error number or event number.
The Error class contains of the following values: 0=diagnostic error, 1=advisory
error, 2=critical error, 3=fatal error.
There are five locations: 0=main board, 1=channel 1, 2=channel 2, 3=channel 3

and 4=channel 4.
Error Error
Class number Event/Error code Description Action needed
©) (NNN)
0 1 Init passed (event) End of initialization phase NA
0 2 Pressure restored Pressure restored after Too Low Pressure NA
0 3 Start flush cycle Is a part of the initialization cycle NA
0 4 Flush cycle passed Is a part of the initialization cycle NA
Automatic generation after method activation or TCD off and temp.
0 5 TCD calibrating
download. control to default
1 6 Too low pressure Pressure drops below 35 kPa Check gas supply
Check gas supply
1 7 Pressure fault Pressure state not ready after 5 minutes or replace
manifold
1 8 Low battery 1 Battery 1 low power (portable Micro-GC only) Recharge battery
1 9 Low battery 2 Battery 2 low power (portable Micro-GC only) Recharge battery
2 10 Sample line sensor fault Sample line temperature sensor error Heater turned off
Temperature not reached within 35 min (heater Replace sample
2 11 Sample line temperature fault
error) line heater
Temperature not reached within 35 min (heater
2 12 Injector temperature fault Replace module
error)
Temperature not reached within 35 min (heater
2 13 Column temperature fault Replace module
error)
1 14 TCD Temperature limit activated Hardware protection activated NA
0 15 EDS logging error Unable to update EDS log Call service
1 16 Low power supply Voltage < 10 Volt Recharge battery
2 17 Injector sensor fault Injector temperature sensor error Replace module
2 18 Column temperature sensor fault Column temperature sensor error Replace module
2 19 TCD control error TCD voltage not or incorrectly set Call service
Replace module
2 20 TCD calibration failed Any error during TCD calibration or TCD controller
board
2 21 Hardware r”set" Instrument reset request from WS NA
2 22 Pressure too high Pressure > 450 kPa for at least 2 minutes Replace manifold
3 23 Initialization error During initialize Call service
During/after initialization, between MPU and
3 24 Internal communication error Call service
IOC/IOE
3 25 Instrument EDS incorrect Instrument Electronic Datasheet incorrect Call service
3 26 EDS incorrect Electronic Datasheet incorrect Call service
3 27 Internal power failure During/after initialization, internal supplies Call service
0 28 Flush cycle aborted Flush cycle stopped before completion NA
Reference
Error Error
©) (NNN)
Changing a channel (controller or module) and
0 29 GC module changed NA
restarting the instrument
0 30 TCD Gain calibrated End TCD Gain calibration NA
0 31 TCD Offset calibrated End of Offset calibration NA
0 32 Null String Not used NA
0 33 ADC reading out of range Analog Digital Control out of range NA
Electronic Data Sheet Analytical Module
0 34 EDS Analytical Module incorrect NA
incorrect
Electronic Data Sheet Configuration checksum
0 35 EDS Config checksum incorrect NA
incorrect
EDS Logbook checksum Electronic Data Sheet Logbook checksum
0 36 NA
incorrect incorrect
EDS Protected checksum Electronic Data Sheet Protected checksum
0 37 NA
incorrect incorrect.
EDS C.C. Config checksum Electronic Data Sheet Channel Control
0 38 NA
incorrect checksum incorrect.
EDS C.C. Logbook checksum Electronic Data Sheet Channel Control Logbook
0 39 NA
incorrect checksum incorrect
EDS C.C. Protected checksum Electronic Data Sheet Channel Control
0 40 NA
incorrect Protected checksum incorrect
EDS A.M. Config. checksum Electronic Data Sheet Analytical Module
0 41 NA
incorrect Configuration checksum incorrect
EDS A.M. Logbook checksum Electronic Data Sheet Analytical Module
0 42 NA
incorrect Logbook checksum incorrect
EDS A.M. Protected checksum Electronic Data Sheet Analytical Module
0 43 NA
incorrect Protected checksum incorrect
Electronic Data Sheet Configuration Structure
0 44 EDS Config SVER incorrect NA
Version incorrect
Electronic Data Sheet Protected Structure
0 45 EDS Protected SVER incorrect NA
Version incorrect
EDS C.C. Config SVER Electronic Data Sheet Channel Control Structure
0 46 NA
incorrect Version incorrect
EDS C.C. Protected SVER Electronic Data Sheet Channel Control
0 47 NA
incorrect Protected Structure Version incorrect
EDS A.M. Config SVER Electronic Data Sheet Analytical Module
0 48 NA
incorrect Configuration incorrect
EDS A.M. Protected SVER Electronic Data Sheet Analytical Module
0 49 NA
incorrect Protected Structure Version incorrect
Pressure Offset calibration Notification Pressure Offset calibration is
0 50 NA
complete completed
Pressure Offset calibration
0 51 Calibration offset out of range
Failed
0 52 Unable to store pressure offset Pressure off set is out of valid range (range??)
Temperature sensor
2 53 Temperature sensor not connect to instrument Call Service
disconnected
Issued by Safety Control Object in Hardware
1 54 Not ready to start run domain. Bridge Call to GC domain (Reporting Check Method
Not Ready To Start Run Error)
1 54 Stream selection failed Stream selector (VICI) failed switching Check Valve
Issued by Safety Control Object in Hardware
Ambient pressure or
1 55 domain whenever ambient temperature has
temperature alarm
passed a certain value.
1 56 Column cleaning Instrument in column cleaning state NA
Instrument stabilizing after column cleaning
1 57 Equilibrating temperature zones Wait till Ready
DMD control to temperature Wait for
60 Notification that DMD is warming up.
setpoint completion

Reference
Error Error
©) (NNN)
0 61 DMD start run NA
0 62 DMD stop run NA
0 63 DMD start tuning NA
Case Temperature reading is outside of
1 64 DMD case temperature error Cool down
acceptable tolerance range
Sensor temperature is outside of acceptable
2 65 DMD sensor temperature error tolerance range. If temperature was just reset, Call Service
please wait for stabilization
The method file is not loaded or the file data is Reboot
2 66 DMD method file error
corrupted
2 67 DMD sensor voltage error Saturated ± sensor readings Call service
RF voltage is outside of acceptable tolerance
2 68 DMD RF voltage error Call service
range
Compensation voltage is outside of acceptable
2 69 DMD Vc voltage error Call service
tolerance range
Sensor pressure reading is outside of acceptable
1 70 DMD sensor pressure error Call service
range
Confirm presence
Tuning process fail, previously calibrated values
0 71 DMD tuning process error of compound in
are kept for failed compounds
calibration gas
Check for empty
gas tank or gas
1 72 DMD gas flow error Startup gas flow diagnostic fail
line leakage/
blockage
Main supply voltage is outside of acceptable
2 73 DMD system voltage error Call service
tolerance range
2 74 DMD communication error Internal communication error Reboot
2 75 DMD sensor error Startup sensor diagnostic fail Call service
3 76 IOC Communication error MPU is not able to communicate with IOC Call service
3 77 Read main board EDS error Not able to read Main board EDS Call service
Read channel controller EDS
3 78 Unable to read EDS controller Call service
error
Read channel analytical module
3 79 Not able to read analytical module EDS Call service
EDS error
Watchdog Error: Store Internal Software Error, can’t store application
3 990 Auto reboot
Application report on flash error report on flash memory.
Watchdog Error: Store ErrorLog Internal Software Error, can’t store ErrorLog
3 991 Auto reboot
report on flash error reprt on flash memory.
Watchdog Error: Instrument
3 992 Internal Software Error, software hanging Auto reboot
frozen (hazardous error)
Watchdog Error: OOA Timer Internal Software Error, OOA Timer could not be
3 993 Auto reboot
error created.
Watchdog Error: ACE reactor
3 994 Internal Software Error, ACE reactor stopped. Auto reboot
stopped
Watchdog Error: Event pump
3 995 Internal Software Error, Event pump stopped. Auto reboot
stopped for 20 s
Watchdog Error: IOC Fatal error
3 996 Internal Software Error, IOC fatal error 0 Auto reboot
0)
1)
2)
3)

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NOTICE: This document contains references to Varian.

Please note that Varian, Inc. is now part of Agilent

Varian Analytical Instrument Warranty

LIMITATION OF REMEDIES AND LIABILITY

Page II User Manual Micro-GC Varian, Inc.

Varian, Inc. User Manual Micro-GC Page: III

Warning Symbol Warning Description

WARNING: Indicates parts that may cause burns when touched.

Page IV User Manual Micro-GC Varian, Inc.

GENERAL SAFETY PRECAUTIONS

Follow these safety practices to ensure safe equipment operation.

Varian, Inc. User Manual Micro-GC Page: V

SPARE PARTS AVAILABILITY SERVICE AVAILABILITY

Varian Analytical Instruments Sales Offices

Argentina France Russian Federation

Varian, Inc. User Manual Micro-GC Page: VII

VARIAN ANALYTICAL INSTRUMENT WARRANTY.................................................................. II

PREPARING FOR INSTALLATION ............................................................................................. 6

Handling a sample .............................................................................................................. 16

INSTRUMENT DESCRIPTION ................................................................................................... 31

The Internet protocol suite.............................................................................................. 43

CYCLE WITH ELECTRONIC PRESSURE CONTROL.............................................................. 66

COLUMN MODULE CONDITIONING ........................................................................................ 67

BACKFLUSH OPTION ............................................................................................................... 68

Varian, Inc. User Manual Micro-GC Page 3

SHIPPING INSTRUCTIONS ....................................................................................................... 71

DISPOSAL INSTRUCTIONS ...................................................................................................... 71

Page 4 User Manual Micro-GC Varian, Inc.

Varian, Inc. User Manual Micro-GC Page 5

Preparing for Installation

Refer to the Pre-Installation Instructions (CP501289) for site

Gas quality specifications are listed in the reference document “Pre-Installation

Page 6 User Manual Micro-GC Varian, Inc.

Avoid back strain or injury by following all safety precautions when

The instrument has been protected during shipment by protection caps.

Varian, Inc. User Manual Micro-GC Page 7

Item Part number

Front and back ferrule 1/16” SS x 2 CP471201

Page 8 User Manual Micro-GC Varian, Inc.

Item Qty Part number

Varian, Inc. User Manual Micro-GC Page 9

Install Gas Regulators and Set pressures

Connect data handling peripherals

The Micro-GC must be connected to an external Workstation, on page 47 both to set up

 Hardware connection between the Micro-GC and Workstation (computer) is done

Heated Sample line

Page 10 User Manual Micro-GC Varian, Inc.

Factory default states and settings

 All heated zones will be set at 30°C.

Varian, Inc. User Manual Micro-GC Page 11

Led OFF: System NOT ready

Led OFF: No run

Led OFF: No error

Led OFF: No power

SAMPLE 1 and SAMPLE 2

Sample gas inlet connector

POWER ON/OFF SWITCH

Switch the Micro-GC ON or OFF

Page 12 User Manual Micro-GC Varian, Inc.

It is possible to connect long vent lines to these fittings in order to safely