SpeedVac™ SPD1030/2030

Vacuum Concentrator

Installation and Operation

80302051 • Revision C • June 2018
IMPORTANT Read this instruction manual. Failure to follow the instructions in this manual can result in
damage to the unit, injury to operating personnel, and poor equipment performance.

CAUTION All internal adjustments and maintenance must be performed by qualified service personnel.

DISCLAIMER Thermo Fisher Scientific Inc. does not accept any responsibility for any damage caused to its
products by unauthorized personnel.

Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the
product operation. This document is copyright protected and any reproduction of the whole or any part of this
document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.

The contents of this document are subject to change without notice. All technical information in this document
is for reference purposes only. System configurations and specifications in this document supersede all
previous information received by the purchaser.

© 2018 Thermo Fisher Scientific Inc. All rights reserved.

Contents
Introduction ................................................................. 1

Safety Precautions ....................................................... 2

Operating Standards.................................................... 3
Product Specifications ............................................. 3
Environmental Conditions......................................... 4

Installation.................................................................... 5
Contents .................................................................. 5

Operation..................................................................... 6
Description of Control Panel ..................................... 7
Manual Run.............................................................. 8
Auto Run.................................................................. 9
Drying Rate .............................................................. 10
Preset Program Settings .......................................... 10
Exporting Live Run Data........................................... 10
HyperTerminal Configuration .................................... 11
Lid Stay Mechanism................................................. 11
Other Topics ............................................................ 11
Simple System Integrity Test .................................... 12

Application................................................................... 13
Devising Protocols/Application ................................. 13
Secondary Vapor Trapping....................................... 13
Accessories ............................................................. 13

Appendix 1: Troubleshooting Guide ............................. 15

Warranty ...................................................................... 17
Introduction
Thermo Scientific Integrated SpeedVac™ Systems are
complete systems for solvent evaporation, sample
concentration and drying. SPD systems use a technique that
combines centrifugal force, vacuum and applied heat to
eliminate sample bumping and foaming. Application of
thermal energy to the sample during concentration
counteracts the natural evaporative cooling effect that slows
the drying rate.
SPD1030 and SPD2030 systems integrate a SpeedVac™
concentrator, an oil-free vacuum pump, and a refrigerated
vapour trap into a single compact package. The SPD2030 is
a high capacity system for processing up to four 500 ml
samples. The SPD1030 features a smaller chamber capable
of processing up to four 100 ml samples. Both units feature
an advanced front panel with dual timer for automatic or
manual control of run conditions, it also features preset and
user defined programs which enables user to retrieve and
store application protocols for future use.

SpeedVac™ SPD1030/2030 Introduction | 1

Safety Precautions
In this manual, the following symbols and conventions are Below are important safety precautions that apply to this
used: product:

This symbol when used alone indicates WARNING: Disconnect the unit from all power
important operating instructions which reduce sources before cleaning, troubleshooting, or
the risk of injury or poor performance of the unit. performing other maintenance on the product or
its controls.
CAUTION: This symbol, in the context of a
CAUTION, indicates a potentially hazardous WARNING: Do not use this device in
situation which if not avoided could result in radioactive, highly reactive or explosive
minor to moderate injury or damage to the atmosphere.
equipment. Do not use this device to process any explosive,
radioactive, highly reactive or explosive
WARNING: This symbol, in the context of a
atmosphere creating substances.
WARNING, indicates potentially hazardous
situations which, if not avoided, could result in
serious injury or death.

This symbol indicates situations where

dangerous voltages exist and potential for
electrical shock is present.

The snowflake symbol indicates extreme low

temperatures and high risk of frostbite. Do not
touch bare metal or samples with unprotected
body parts.

This symbol indicates possible pinch points

which may cause personal injury.

This symbol indicates a need to use gloves

during the indicated procedures. If performing
decontamination procedures, use chemically
resistant gloves.

Before installing, using or maintaining this

product, please be sure to read the manual and
product warning labels carefully. Failure to follow
these instructions may cause the product to
malfunction, which could result in injury or
damage.

This symbol represents protective conductor

terminal.

2 | Safety Precautions SpeedVac™ SPD1030/2030

Operating Standards
Product Specifications
SPD1030 SPD2030

Capacity Moderate Large

115 VAC; 60 Hz; 12 amps 220 VAC; 60 Hz; 8 amps

Operative Power*
230 VAC; 50 Hz; 6 amps 230 VAC; 50 Hz; 8 amps

Vacuum Chamber TEFLON® coated aluminium casting TEFLON® coated aluminium casting

Powder coated steel - includes a Powder coated steel - includes a

Cover
safety interlock safety interlock

Induction Motor Maintenance free Maintenance free

35°C to 80°C, 35°C to 80°C,

Chamber temperature
5°C increments 5°C increments

-50°C (approx.) -50°C (approx.)

Refrigerated trap 4 litre 4 litre
CFC-free CFC-free

Vacuum Pump Displacement

30/36 litres/min 30/36 litres/min
(50/60 Hz)

Maximum vacuum <10 Torr (13 mbar,1.3 kPa) <10 Torr (13 mbar,1.3 kPa)

Vacuum Level Control 30 to 5.1 Torr in 0.1 increments 30 to 5.1 Torr in 0.1 increments

Vacuum Ramp Setting 1 to 5 1 to 5

158 lbs 205 lbs

Weight
72 kg 93 kg

25 in x 26 in x 16 in 31 in x 28 in x 21 in
Size (W x D x H)
64 cm x 66 cm x 41 cm 79 cm x 71 cm x 53 cm

12 A, 250 VAC, Time-lag 8 A, 250 VAC, Time-lag

Fuse
6 A, 250 VAC, Time-lag 8 A, 250 VAC, Time-lag

*Dependent upon ambient temperature, line voltage fluctuation, and load capacity.

SpeedVac™ SPD1030/2030 Operating Standards | 3

Environmental Conditions
Indoor use only, in the absence of hoarfrost, dew, percolating water, rain and solar radiation.

Maximum altitude 2000 meters above mean sea level

Ambient temperature range 17°C to 32°C
Humidity 20% to 80% non-condensing
Pollution degree 2

Main supply voltage fluctuations not to exceed ±10% of the nominal voltage.
Transient overvoltages per Installation Categories II.

4 | Operating Standards SpeedVac™ SPD1030/2030

Installation
IMPORTANT NOTE: Before operating the unit, read Section
Contents Operation, and Section Application Information, to deter-
mine your specific application requirements.
1. Thermo Scientific Savant SPD1030/SPD2030
SpeedVac™ Concentrator
2. Cover Lock Emergency Release Tool
3. Line Cord
Unpacking. Open the shipping cartons. Carefully remove the
instrument and accessories. Lift and carry with two
people, holding securely underneath with both hands.
Use proper lifting technique (lift with the legs, not the
back) to avoid personal injury. Compare the contents with
the packing list. If there is a discrepancy, call Thermo
Scientific technical service.
Inspection. Inspect the unit and accessories for damage that
may have occurred during shipment. Should there be any
damage, report it to the carrier and contact Thermo Scientific
immediately. Make sure the carrier inspects the damage and
leaves an inspection report. Register any claims for shipping
damage against the carrier or his agent. Save the shipping
carton in the event a return is necessary. Call Thermo
Scientific technical service for further assistance.
Site preparation. The SPD1030/SPD2030 requires a stable,
level surface for proper operation. The SPD1030 units
configured for 115 VAC, 60 Hz, should be plugged into a
circuit rated for at least 12 amps. The SPD1030 units
configured for 230 VAC, 50 Hz, should be plugged into a
circuit rated for at least 6 amps. The SPD2030 units are
configured for 220 VAC, 60 Hz, or 230 VAC, 50 Hz,
operation. Both configurations require a circuit rated for at
least 8 amps.

CAUTION: Be sure to leave at least 4 inch

clearance on all sides of the unit. Verify that the
unit is on a levelled and stable platform. Level
operation is important to ensure proper flow of
refrigerant. If necessary, move the unit to a more
suitable location.

WARNING: Before connecting the unit to an

electrical outlet, make certain that voltage,
frequency, and amperage match the
requirements indicated on the product label/
name plate of the instrument. Use sockets with a
protective earth conductor and correct mains
cable.

Note: Do not use any detachable power cord that is not ade-
quately rated for the unit.

SpeedVac™ SPD1030/2030 Installation | 5

Operation
Connect the power cord to the power inlet on the right side of CAUTION: Load the rotor and close the lid.
the unit and plug it into the appropriate outlet. Turn on the Always balance rotor loads. An imbalanced rotor
main power switch located on the front of the unit in the lower causes vibration that will damage the system’s
right to energize the unit. The safety lid locking mechanism will bearings and equipment. Load the rotor
automatically disengage. Do not attempt to open the lid symmetrically. There need not be a tube in each
unless the unit is plugged in. holder, but the load must be evenly distributed.
When using a rotor with aluminium tube holders,
CAUTION: Immediately verify by touch that the insert all the tube holders.
product is drawing air through the vent on the
right side. If you cannot feel the air suction, Glass Condensation Flask Installation. Prepare the
switch the product OFF at once. Operating the refrigerated stainless steel trap chamber by adding
product without a working fan, or with the air flow approximately 750 ml of CryoCool™ Heat Transfer Fluid. A
blocked, will damage the refrigeration system. line scribed on the wall of the stainless-steel trap indicates the
minimum appropriate level. CryoCool™ conducts heat away
Start-of-day procedure. At the start of each day, ensure from the Glass Condensation Flask, allowing vapours to
that the refrigerated trap contains a clean, dry, Glass condense on the flask walls. Gently put a clean Glass
Condensation Flask (GCF400) and that the supply of Thermo Condensation Flask into the refrigerated chamber. As you
Scientific CryoCool™ Heat Transfer Fluid is sufficient. press the flask into the chamber, the CryoCool™ level rises.
Verify that the final CryoCool™ level is 10 to 15 mm below the
The CryoCool™ in the refrigerated trap must be cold before
rubber seal. If low, carefully pour more CryoCool™ into the
drying runs can begin. Turn unit on at least 45 minutes before
chamber while holding down the flask.
starting the drying run.
Immediately wipe clean any CryoCool™ that spills onto the
For best results, maintain electrical power to the system (the
rubber seal.
main power switch on the front of the unit in the lower right is
“ON” and the front display is illuminated) at all the times to Fit the white insulating Flask Seal over the glass flask to
keep the refrigerated trap cold and ready for use. secure the flask in the chamber. Its bevelled side faces
upward to admit the Flask Cap.
CAUTION: Do not switch OFF and ON with in a Snap the black rubber Flask Cap over the mouth of the glass
short period of time as this could cause pressure flask. This provides easy tubing connection and a vacuum
to build up within the system and lock the system seal while also securing the Glass Condensation Flask and
that could trigger the fuse. After switching OFF, insulating Flask Seal in the refrigerated chamber.
allow sufficient time (minimum 15 minutes) for the
pressure to stabilize before switching the system Glass Condensation Flask Defrosting and Cleaning.
ON again. Thermo Scientific Glass Condensation Flasks should be
defrosted and cleaned after each day’s use, or more often if
CAUTION: Use appropriate Thermo fisher greater than one-fourth the rated volume has condensed on
Scientific designed rotors recommended for the the walls. Failure to follow this procedure can prevent the
Product. system from achieving high vacuum levels and could cause
flask breakage. Flasks with cracks shall not be used.

Rotor installation. Open the lid of the rotor chamber. CAUTION:

Visually align the pin on the drive shaft with the groove on the
bottom of the rotor. Carefully lower the rotor onto the drive 1. Use gloves while handling Glass
shaft. Rotate the rotor by hand to ensure alignment of the pin condensation flask to avoid pain, local
with the groove. Secure the assembly by screwing the frostbites due to extreme low temperature.
retaining knob into the drive shaft above the rotor. Tighten it 2. Handle fully filled Glass condensation flask
firmly but not excessively. with care to avoid risk of injury.
3. Use face masks if required while cleaning the
flask for protection against toxic chemicals
and bio hazards.

6 | Operation SpeedVac™ SPD1030/2030

Description of Control Panel

1. Lid locked - Indicates whether or not the lid of the 4. Temperature display - Indicates the set temperature or
concentrator is locked, the indicator will be illuminated the actual temperature during run in °C. The temperature
when locked. set point can be set from 35°C to 80°C at a 5°C interval.
In addition, it is possible to set the temperature to “no”
2. Preset buttons - Preset programs that are not
which means that heating will not be applied during the
modifiable.
run. The temperature setting of “no” can be reached
Loading a preset is achieved by pressing the under 35°C or over 80°C.
corresponding Preset button. The following parameters
5. Time display - Indicates the heat timer or the run timer
are automatically loaded on to the screen.
set points. During a run, it indicates the elapsed or
• Temperature set point remaining run time or the remaining heat time left. The
range for these timers is from 0.01 [1 min.] to 9.59 [9
• Heat time
hours, 59 minutes] at a 1-minute interval. In addition, it is
• Run time possible to set the heat time to “CCC” (continual heating),
which represents a continuous heating throughout the
• Vacuum pressure
execution of a run.
• Vacuum ramp
The setting of “CCC” can be reached under 0.01 [1 min.]
3. Program buttons - 3 programs that are modifiable. or over 9.59 [9 hours, 59 minutes].
Loading a user-defined program is achieved by pressing 6. Vacuum display - Indicates either the vacuum pressure
the corresponding Program Button. The following set point (in torrs or millitors) or the selected vacuum
parameters are automatically loaded on to the screen. ramp based on the vacuum type setting (see point 12).
During a run, it indicates either the actual vacuum
• Temperature set point
pressure or the selected vacuum ramp.
• Heat time
Note:
• Run time
• The atmospheric pressure is represented by “HPr”
• Vacuum pressure
• A decimal point indicates a vacuum pressure in Torr
• Vacuum ramp
• No decimal point indicates a vacuum pressure in
Saving a user defined program is achieved by pressing mTorr
and holding down corresponding Program button for 3
7. Select - Press this button to select the parameters to be
seconds. The parameters displayed in the screen are
modified. The selection is from left to right, in a cyclic
stored into the program and can be loaded for use at a
manner. The selected parameters are shown by the
later time.
corresponding indicator that is illuminated.

SpeedVac™ SPD1030/2030 Operation | 7

8. Minus (“-”) - Decrements the valve of the selected you want to set a fixed run time.
parameter.
16. Stop - Terminates a “Manual” or “Auto” run.
9. Plus (“+”) - Increments the value of the selected
parameter.
10. View - During a run, pressing view shows the set run Audible Notification
parameters. When no run is ongoing, pressing view
displays the actual live parameters. The time display
The concentrator will play tones depending on the user
shows either ''0.00'' or the end status of the last
actions. Below is a description of these tones.
executed run (e.g. “End”, “Err”).
11. Pre-heat - Use to pre-heat the chamber to 45°C prior to Table 1. Audible Notifications
beginning a run or between runs. Once a run is initiated,
the pre-heat automatically stops. Event Sound Description
Note that the pre-heat function is only enabled if the Start-up 5 beeps
temperature set point is different than “No”.
Starting a run (manual
12. Vacuum Type - Select either “Level”, or “Ramp”, in the 1 single beep
or automatic)
vacuum display.
Level: Allows users to select a preset vacuum level. Manually stopping a
During a run, the vacuum level will be automatically manual or automatic 3 beeps
regulated and maintained at the select preset value. run

Ramp: The rate at which vacuum is achieved can be set Automatically

1 beep that is repeated until the
for preventing bumping. There are 5 adjustable levels that stopping an automatic
user pushes the Stop button or
can be set as required, depending upon your solvent. run
opens the cover of the
concentrator

Setting Vacuum Rate (Approximate) Program saved 3 beeps

5 70 Torr/min (Maximum setting) 1 long beep that lasts for 1

User input error
second
4 50 Torr/min
1 long beep that lasts for 1
3 40 Torr/min second and that is repeated
System error until the user pushes the Stop
2 30 Torr/min button or opens the cover of the
1 5 Torr/min concentrator

13. RL (Radiant Lamp) on/off - Adds radiant heat to

chamber by activating the radiant lamp of the
concentrator. The radiant lamp can be activated and
Manual Run
deactivated manually by pressing the button at any point
during a run. If enabled, the radiant lamp will remain 1. Connect the unit to its required voltage.
powered as long as the heat timer has not expired. The 2. Turn the power switch located on the front of the UNIT, to
indicator will be illuminated when the radiant lamp is on. the ON position, (light on switch indicates ON). The cover
Note that this feature is disabled if the temperature set lock, disengages, allowing the top cover to be opened.
point is set to “no”.
The display lights up and shows the following in
sequence:
CAUTION: Do not use radiant heat with
microplates. Improper use may result in melting • Name of the concentrator
or deformation.
• Software revision number

14. Manual run - Starts a “Manual” run based on the • Default values:
parameters loaded in the screen, use manual run - Temperature 45°C
function if you do not want to set a fixed run time.
- Run Time 2.00 hours
15. Auto run - Starts an “Automated” run based on the
parameters loaded in the screen, use auto run function if - Vacuum Pressure 5.1 Torr

8 | Operation SpeedVac™ SPD1030/2030

3. Select a run configuration using one of the following
method: Auto Run
• Load a present program
1. Refer to the Manual Run section for start-up.
• Load a user defined program
2. To execute an AUTOMATIC RUN, execute the following
• Directly modify values that are loaded on the screen, steps:
using the Select button and the “+”/ “-” buttons.
a. Use the Select button and the “+”/ “-” buttons to
4. Set the temperature set point between 35°C and 80°C, select and modify the Temperature, “Heat Time and
or “no”, for no heat. “Run Time” parameters. The Run and Heat Time can
be set from 0.01 to 9.59 hours (Heat Time also has
5. Using the Select button and the “+”/ “-” buttons select
“CCC” for continuous use).
and modify “Heat Time” to between 0.01 and 9.59 hours
or “CCC” (for continual heating). When the heat timer b. To select a vacuum level, press Vacuum Type to
expires, the heater will shut off, no matter what the illuminate “Level”. Use the “+”/ “-” buttons to set the
temperature set point reads (except if “CCC”). vacuum to the desired level. To select a vacuum
6. Select Run Time: Since this a manual run no time ramp rate, press Vacuum Type to illuminate “Ramp”
adjustment is needed”. and use the “+”/ “-” buttons to set a ramp rate
(5=highest, 1=lowest).
7. To select a VACUUM LEVEL, press Vacuum Type to
illuminate “Level” and “+”/ ”-” buttons to set vacuum to 3. Place the sample tubes in the rotor so that the load is
desired level. To select a vacuum ramp rate, press balanced. Secure the rotor with the supplied knob (hand
Vacuum Type to illuminate ''Ramp'' and use the “+”/ ”-” tight). Close the cover.
buttons to set a ramp rate (5=highest, 1=lowest). a. Press the Auto Run button to start the run. The
8. Place sample tubes in rotor so load is balanced. Secure cover locks and the lid locked indicator is illuminated.
rotor with the supplied knob (hand tight). Close cover. The rotor starts spinning. The run time display is
counting down in 1 minute Intervals. The heat time is
9. Pre-heat may be selected at this time, to apply a 45°C counting down if the set point is not set to “CCC” and
heat to the chamber. if the temperature set point is not “no” (use the
10. Press the Manual Run button. The cover locks and the Select button to view “Heat Time”). The temperature
lid locker indicator is illuminated. The rotor starts rises in 1°C increments to set temperature. The
spinning. The “Run Time” display counts up. The vacuum pressure begins decrementing down from
temperature rises to the set temperature. The “Heat “HPr” (atmospheric pressure), after both SAV valves
Time” will count down if set point is not set to “CCC” and actuate, applying vacuum to the chamber.
if the temperature set point is not “no” The vacuum will be
b. The vacuum display will indicate vacuum pressure in
applied to the chamber and the level begins falling.
the chamber.
Note: If the cover is not closed, the display will show “Lid”
and the run will not start. Note: If the cover is not closed, the display will show
“Lid” and the run will not start.
11. Press RL On/Off for radiant chamber heat. Press at any
time to turn OFF and ON. (As long as there is time left in Press the RL On/Off for radiant chamber heat. Press
the heat timer and if the temperature set point is not set at any time to turn OFF and ON. (As long as there is
to “no”). time left in the heat timer and if the temperature set
point is not set to “no”).
12. To end the manual run, press Stop button. The unit will
sound three audible beeps. The display will show “End”, c. Once the run time expires, the run will automatically
the valves will click, isolating the chamber from the stop, the display will show “End”, the SAV valves will
vacuum pump and allowing air to bleed into the chamber. click, also allowing air to bleed into the chamber. The
unit will sound 1 beep that will be repeated until the
13. After the rotor stops spinning, the cover lock disengages user acts on it.
and the lid locked indicator is turned off. The display
reverts to last set parameters. d. After the rotor stops spinning, the cover unlocks and
the lid locked indicator is turned off. The display
14. Open the cover and remove samples.
reverts to last set parameters.
GENERAL: During the run, display shows actual parameters.
To check set parameters, press View button and Select. The e. Open the cover and remove samples.
display will revert temporarily to set points for approximately 5 GENERAL: During the run, display shows actual parameters.
seconds. To check set parameters, press View button and Select

SpeedVac™ SPD1030/2030 Operation | 9

button. The display will revert temporarily to set points for
approximately 5 seconds. Exporting Live Run Data
The unit is equipped with a USB port to enable
communication with an external computer. The USB port is
Drying Rate located on the rear panel of the unit and can be used to
connect to a computer via a standard USB type A or B cable.
Thermal energy can be applied to the concentrator chamber
to counteract the cooling effect of evaporation, maintain the CAUTION: USB lead length less than 3 meters
samples in the liquid state, and accelerate the concentration shall be used to connect to the computer.
run. Select 80°C if you desire accelerated drying. To ensure
against over drying of samples, and possible denaturing, it is
recommended that the Radiant heat timer be set for only a
portion of the total run time (e.g., 50%–75% of total run time).

Preset Program Settings

The table below shows the values attributed to the present
programs parameters.

Preset Application Settings

Temperature: 45°C
Heat time: 0.30
When a run is ongoing, the unit exports the following
Preset 1 Water Run time: 2.00 information via the USB port every minute.
Vacuum level: 14 Torr • The live temperature applied to the samples chamber
Vacuum ramp: 5
• The remaining heat time for the run (“CCC” indicates con-
Temperature: 65°C tinuous heating)
Heat time: 0.30 • The remaining or elapsed run time, depending on the run
“Low Boiling” type (manual or automatic)
Preset 2 Run time: 2.00
ACN/MEOH
• The vacuum pressure in the samples chamber
Vacuum level: 5.1 Torr
Vacuum ramp: 5 The data are sent at a fixed baud rate of 115200 and are
comma-separated as shown in the format: <temperature>,
Temperature: “no” <heat time>, <run time>, <vacuum pressure>
HPLC Heat time: 0.01* • The temperature is represented as a 2-digit integer in °C
Preset 3 H2O + Low Boil Run time: 2.00 • The heat time is expressed as a 3-digit integer in minutes
solvent +.1% (or “CCC” for continuous heating)
acid Vacuum level: 5.1 Torr
Vacuum ramp: 5 • The runtime is expressed as a 3-digit integer in minutes
• The vacuum pressure is represented as a floating-point
*When the temperature is set to “no”, the heat time is
number in Torr (or as “HPr” to represent a high pressure).
defaulted to “0.00” while executing the run.

Note: The preset programs are for convenience In case of a communication failure between the
only. Prior to use, users are advised to conduct a monitoring program of the computer and the
risk assessment to confirm that the preset product, user can re-establish the connection by
program parameters meet the user’s application disconnecting and reconnecting the USB cable.
specific needs and conditions. Users accept the Note: The following section details the step-by-step proce-
risks associated with using the preset programs. dures for configuring Microsoft® HyperTerminal running on a
host computer using Windows® XP. These instructions may
need to be modified to be used with a different terminal emu-

10 | Operation SpeedVac™ SPD1030/2030

lator program and/or operating system. Contact Technical secure the lid and maintain it open, allowing the user to
Services if further assistance is required. operate the unit with both hands.
Note: The picture shown below is for SPD2030 and this
would be slightly different in SPD1030 as it uses a different lid
HyperTerminal stay mechanism.

Configuration
1. Power up the host computer and close any running
applications.
2. Open the HyperTerminal application by clicking on Start \
“Programs” \ “Accessories” \”Communications” \
“HyperTerminal.”
3. In the “Connection Description” box, enter the name
“SPD1030 or SPD2030” based on the model and
choose an icon and click OK.
4. Connect to the virtual COM port that is linked with the
SpeedVac™ concentrator attached to the computer
(USB virtual com port). WARNING: Device lid can crush your fingers.
5. In the “COM Port Properties” box \ “Port Settings” folder Keep away: Do not reach between the device
select the following options: and lid when opening or closing the device lid.
Bits per second: _ 115200
Data bits: _ 8 Other Topics
Parity: _ None
Chamber Cover. The cover must be closed before
Stop bits: _ 1 beginning a run. If you press Manual Run or Auto Run and
Flow control _ None the cover is open, the display shows “lid” to remind you to
close the cover. The run will start immediately after closing the
After verifying the above settings, click OK. cover.
6. In the main dialog box click on File \ Save. If a user tries to open the lid at the start of the run, when the
7. Exit the program by clicking on File \ Exit \ Yes. lid has already been locked, the unit will automatically abort
the run and signal the user with the ''Lid'' message on the
8. Verify the program was saved by going to Start \ display and an error tone. Otherwise, during a run the user
“Programs” \ “Accessories” \ “Communications” \ cannot open the cover due to vacuum in the concentration
“HyperTerminal” \ “SPD1030 or SPD2030” based on the chamber. The cover is locked down at all times during a run
model and whenever power to the unit is interrupted.
9. This completes the configuration of HyperTerminal. The cover lock is an additional safety feature that reduces the
10. Turn on SpeedVac™ system and connect to the virtual risk of injury or damage from the spinning rotor. Do NOT
COM port that is linked with the SpeedVac™ attached to bypass the cover lock to conduct a run with the cover open.
the computer. If removal of samples from the concentrator chamber during
11. Start HyperTerminal by clicking on SPD1030 or a power failure is required, insert cover lock emergency
SPD2030 based on the model. release tool into the vertical slot at the base of the front of the
unit. Press the object gently into the slot until the lock
12. Initiate the run and SpeedVac™ will screen print releases. The cover can then be opened.
<temperature>, <heat time>, <run time>, <vacuum
pressure>

Lid Stay Mechanism

The unit is equipped with a lid-stay mechanism that will assist
the user in opening and closing the cover of the unit. It will

SpeedVac™ SPD1030/2030 Operation | 11

 Routine checks:
1. Check all the hoses to ensure that they are secure.
2. Ensure all glass condensation flask in emptied, cleaned
and checked for crack before every run.
3. Clean the cover, cover seal and chamber with a soft lint
free cloth with one of the following
• Mild detergent solution
• Diluted Methanol (50%)
• Diluted Ethanol (50%)

CAUTION: WARNING: Burns due to hot device parts:

When the concentrator is set to a temperature of
List of Solvent and Solvent Combinations: 60°C and above the rotor and the sample tubes
will be hot, do not touch the wall of the rotor
chamber, use suitable auxiliary to remove the
Solvent & Solvent sample tubes
SPD1030 SPD2030
Combination

Acetonitrile Yes Yes

Ethanol Yes Yes Simple System Integrity

Methanol Yes Yes Test
Methylene chloride Yes No
You can use this simple system test to verify periodically the
Water Yes Yes operational integrity of the vacuum pump and refrigerated
vapour trap.
Acetonitrile & Water Yes Yes
1. Install a clean dry Glass Condensation Trap.
Methanol & Water Yes Yes
2. Allow the refrigerated vapour trap to operate for 45
minutes.
Typical Application- Both Models
3. Open the chamber lid and remove the rotor.
1. HPLC fractions with water/0.1% trifluoracetic acid
4. Fill a plastic beaker that will fit in the chamber, with 50 ml
2. Reversed-phase SPE elements
of water and place it in the chamber. Close the lid.
In the event that your choice of solvents and applications are
5. Set the temperature to “no”.
unique and not listed above, please contact Thermo Scientific
Customer Support for advice. 6. Set the Run Time for 15 minutes.
7. Press the Auto Run button.
WARNING: Do not use this device in radioactive,
highly reactive or explosive atmosphere. 8. At the end of the run, immediately open the lid and
measure the water sample temperature.
Do not use this device to process any explosive,
radioactive, highly reactive or explosive A properly functioning system will reduce the sample
atmosphere creating substances. temperature to within the range of +3°C to +7°C (+37°F to
+45°F).
CAUTION: Product Maintenance:
Maintenance of product only permitted to be
performed by trained service staff using suitable
measuring and auxiliary equipment as well as
detailed service instruction.

CAUTION: Wear gloves, eye protection, masks

and lab coats while working on the system.

12 | Operation SpeedVac™ SPD1030/2030

Application
At the end of a run, you can determine your percentage
Devising Protocols/ solvent recovery by removing and measuring the volume of
solvent captured in the Glass Condensation Flask.
Application As solvent evaporates, samples remain cool due to the
effects of evaporative cooling. If you continue to apply radiant
Test runs are necessary to determine the correct run times for energy, the sample temperature rises. Therefore, a sample
given procedures. To obtain data for concentration, reducing drying operation using an expendable batch sample should
a large volume to a small volume, and drying, you will need to be run. Based on the results, determine an optimum time to
conduct manual test runs using containers, solvent and shut OFF the Radiant Lamp before the end of a run.
volumes t will be used for actual samples. Interrupt the run
every 15 minutes to measure remaining sample volume and Drying rates vary depending on the solvent being evaporated.
sample temperature. Continue the test until the samples are Temperature, sample volume, number and type of tubes,
completely dry or concentrated to an acceptable level. vacuum level, vacuum ramp rate and other factors can all
Conduct additional runs at different drying rates with and influence drying rate. The following chart provides a guide for
without the Radiant Lamp ON. determining approximate drying rates.

Heat Setting OFF 45°C 65°C

Initial Sample Volume 4 ml 20 ml 4 ml 20 ml 4 ml 20 ml

Drying Rate (ml/hr/vessel) WATER 0.35 2 0.5 2.5 1 5

Secondary Vapor Trapping The chemical trap requires periodic checking and
cartridge replacement to ensure its continued
effectiveness.
When processing solvents with a lower freezing point of -
55°C, it is recommended to install the Thermo Scientific CAUTION: Risk to health from escaping
SCT120 Chemical Trap on the exhaust port to capture substances, No vapours from toxic liquids and
residual evaporated solvent vapours. This trap, installed in pathogenic germs must escape, ensure sufficient
addition to the integral refrigerated trap, provides more separation of vapor via correct chemical trap.
complete solvent trapping. The SCT120 accepts a variety of
disposable cartridges that are designed to adsorb vapours
that may exhaust from the SpeedVac™. The Thermo
Scientific DTK120R Chemical Trap Kit, which includes the
trap, a disposable cartridge (DC120R), tubing and fitting, has
Accessories
an activated-charcoal cartridge that traps radioactive vapours
and is effective for containing residual quantities of organic DTK120R Chemical Trap. for drying samples containing
solvent vapours. (This is the same medium commonly used in radiolabelled biomolecules, the chemical trap with activated
fume hoods). The DTK120A Chemical Trap Kit is carbon cartridge is strongly recommended. Attach to the
recommended for low pH vapours from samples involving vacuum pump exhaust recovery vessel. This set-up traps
acid hydrolysis of peptides or other acidic samples. This kit volatile radioactivity, preventing its release to the laboratory
contains trap, tubing, fitting, and DC120A cartridge to environment.
neutralize acids. ANT100 Ammonia Neutralizing Trap, for drying samples
To install a trap on the SpeedVac™ exhaust, remove the such as synthetic oligonucleotides in ammonium hydroxide.
muffler and the rubber tubing from the SOLVENT VAPOR The ANT100 includes a cup-mounting bracket, which
EXHAUST PORT. Attach a piece of vacuum tubing to this attaches to the left side of the SPD SpeedVac ™ at the
fitting. Attach the other end to the chemical trap. exhaust port. The trap also includes four bottles of Ammonia
Neutralizing Solution (ANS121/4). This trapping system
Note: Refer to the manual shipped with each Chemical Trap effectively neutralizes ammonia gas, and eliminates exhaust of
Kit for full details and installation instructions. unpleasant odours.

SpeedVac™ SPD1030/2030 Application | 13

CC120/DX Deluxe Convenience Cart is a space-saving
accessory for the laboratory. When used with an SPD
SpeedVac™, the system resides on the top shelf, while any
additional trapping apparatus resides on the bottom shelf.
Addition of the cart produces an easily portable concentration
system.
CryoCool™ (SCC1 or SCC5) for use in SPD1030 and
SPD2030.

CAUTION: The use of accessories other than

those recommended by Thermo fisher Scientific
may impair the safety and function of the device.
Thermo fisher Scientific cannot be held liable or
accept any liability for damage resulting from the
use of incorrect or non-recommended
accessories and spare parts.

14 | Application SpeedVac™ SPD1030/2030

Appendix 1: Troubleshooting Guide
Table 2. Thermo Scientific SPD1030/SPD2030 SpeedVac™

Symptom Possible Causes Solution/Explanation

No current to the equipment. Check line cord for proper connections.

No response
Power failure at source. Check main circuit panel

System trips circuit Short circuit to ground in one of the Call Technical Service.
breaker or main line fuse. components.

Flask cap plugged with ice. Remove blockage and install a dry flask.

Internal vacuum pump needs servicing. Call Technical Service.

Vacuum leak. Check seal of cap on glass condensation flask.

Sample does not dry, or Check cover gasket on sample chamber.
noticeable change in the
Insufficient thermal energy applied to Evaporative cooling retards evaporation:
drying rate.
the sample chamber. additional chamber heat counteracts this effect.

Refrigerated trap not reaching Call Technical Service.

operating temperature.

Condensation flask full past 3/4 mark. Replace with new dry flask.

Table 3. Thermo Scientific SpeedVac™ Chamber

Symptom Possible Causes Solution/Explanation

No current to the equipment. Check line cord for proper connections.

Rotor does not rotate or Corroded upper magnetic assembly Assembly requires replacement. Call
makes a grinding noise. Technical Service.

Lower drive magnet bound up on the Call Technical Service.

separation plate.

Rotor makes a loud clattering Hold-down knob has been over- Tighten knob only until it makes contact
noise on initial start-up. tightened. with rotor. Do not over-tighten.

Chamber does not seal Cracked or fouled cover gasket. Clean or replace cover gasket.
properly. Automatic bleeder valve malfunction Call Technical Service.

Chamber does not reach Radiant lamp burned out. Replace lamp or call Technical Service.
operating temperature. Heater control or element malfunction. Call Technical Service.

SpeedVac™ SPD1030/2030 Appendix 1: Troubleshooting Guide | 15

Table 4. Refrigerated Condensation Trap

Symptom Possible Causes Solution/Explanation

Leave at least 4 inch clearance on all sides. Clear

Insufficient air circulation.
Refrigerated trap not dust and debris from the condenser.
cooling.
Compressor system has lost its charge. Call Technical Service.

Noisy vibration and/or Cabinet housing has become loose or

excessive heat on top of circulation fan is rubbing an internal Call Technical Service.
cabinet. component.

Large ice build-up which expands during Change and clean the glass condensation flask
thawing. daily.
Glass condensation
flask breakage. Trap contents allowed to thaw and Leave the main power switch ON between runs
refreeze. and change the flask daily.

Use CryoCool™ instead of ethanol.

Glass condensation Excessive water and ice build-up in Remove the ice.
flask plugged with ice. thermal transfer fluid. CAUTION: Extreme cold may cause severe
blistering.

Flask cap sealed improperly. Verify that the cap is pressed securely over the
Vacuum leak at flask mouth of the glass condensation flask.
cap.
Flask cap worn or fouled. Replace cap.

16 | Appendix 1: Troubleshooting Guide SpeedVac™ SPD1030/2030

Warranty
All Thermo Fisher Scientific products mentioned in this
manual (excluding glassware) are warranted against defects
in workmanship for one year after the date of delivery to the
original purchaser. This warranty is limited to defective
materials and workmanship and does not cover incidental or
consequential damages.
Thermo Fisher Scientific will repair free of charge any
apparatus covered by this warranty. If a new component fails
to work, Thermo Fisher Scientific will replace it, absorb all
charges, and continue the one-year warranty period.
Warranty work is subject to our inspection of the unit. No
instruments, equipment, or accessories will be accepted
without a Return Material Authorization (RMA) number issued
by Thermo. Costs of shipping the unit are not covered under
warranty. The warranty obliges you to follow the precautions
in this manual.
When returning apparatus that may contain hazardous
material, you must pack and label them following U.S.
Department of Transportation (DOT) regulations applying to
transportation of hazardous materials. Your shipping
documents must also meet DOT regulations. All returned
units must be decontaminated (free of radioactivity,
biological, or chemical contamination).
Use of this equipment in manners other than those specified
in this manual may jeopardize personal safety. Under no
circumstances shall Thermo Fisher Scientific be liable for
damages due to the improper handling, abuse, or
unauthorized repair of its products. Thermo Fisher Scientific
assumes no liability, express or implied, for use of this
equipment.
Visit us online to register your warranty:
www.thermoscientific.com/labwarranty

SpeedVac™ SPD1030/2030 Warranty | 17

WEEE Compliance
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Waste Electrical & Electronic Equipment (WEEE) Directive 2012/19/EU. Thermo Fisher Scientific has
contracted with one or more recycling/disposal companies in each EU Member State, and this
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these Directives, the recyclers in your country, and information on Thermo Scientific products which
may assist the detection of substances subject to the RoHS Directive are available at
www.thermofisher.com/WEEERoHS under Services & Support.

WEEE Konformittät. Produkte mit diesem Symbol müssen der EU-Richtlinie für Elektro- und Deutschland
Elektronik-Altgeräte (WEEE) 2012/19/EU entsprechen. Thermo Fisher Scientific hat Vereinbarungen
getroffen mit Verwertungs-/Entsorgungsanlagen in allen EU-Mitgliederstaaten und dieses Produkt
muss durch diese Firmen widerverwetet oder entsorgt werden. Mehr Informationen über die
Einhaltung dieser Anweisungen durch Thermo Scientific, dieVerwerter und Hinweise die Ihnen nützlich
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Davantage d’informations sur la conformité de Thermo Fisher Scientific à ces directives, les recycleurs
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