Celdas - Electroquimicas
Celdas - Electroquimicas
Celdas - Electroquimicas
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Components of VC-2/VC-3 cell can be provided separately. In that case, each sample vials (A-010343) includes 10 pieces of them per the sales unit Catalog No. Description A-001052 VC-2 Voltammetry cell Components A-001056 Sample vial(20ml)7pcs A-002222 Pt counter electrode for VC-2 cell A-009028 Teflon cap for VC-2 A-010537 Purging tube
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Catalog No. Description A-011224 VC-4 Voltammetry cell Contents A-011504 Sample vial(5ml)7pcs A-011226 Teflon cap for VC-4 A-011227 Cell holder for VC-4 A-002222 Pt counter electrode for VC-2 cell A-010537 Purging tube Components of VC-4 cell can be provided separately. In that case, each sample vials (A-011504) includes 10 pieces of them per the sales unit
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Catalog No. Description A-010914 SVC-3 Oxygen-free Voltammetry cell Contents A-001056 Sample vial(20ml)7pcs A-002233 5cm Platinum counter electrode for VC-3 cell A-011811 Teflon cap for SVC-3 A-010537 Purging tube
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To lower electric resistance, please soak the Vycor frit of sample holder into supporting electrolyte solution at least for one hour prior to use. These frits need to be kept immersed in solution all of time. If obtained data is shifted, IR drop may be caused. In that case, please increase the supporting electrolyte as much as five times or add approx. 0.5M of NaCl Catalog No. Description A-011520 MCA Micro cell kit Components A-001052 VC-2 Voltammetry cell A-012177 Sample holder dia 9mm (2pcs)
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This product is utilized to do complete electrolysis. As mentioned in below, carbon working electrode is formed into reticulated that provides with sufficient surface area to gain the rate in electrolysis. The water jacketed cell can be purchased separately. The platinum mesh electrode is also available as a custom order. The platinum counter electrode equips a separating chamber. The progress of an electrolysis can be investigated by inserting additional indicator electrode (required be prepared by users themselves). That insertion need to be plugged with a port plug when the indicator electrode is not used suitable for: Quantification of mass transfer of the electron per molecule Measuring the absolute quantity of the analyte Electrolytic synthesis of new materials (generally in quantity of milligram) etc.
Catalog No. Description A-001197 Bulk Electrolysis Cell Contents A-001195 100ml Glass cell A-010530 Porous carbon electrode A-002234 Platinum counter electrode 23cm A-001198 Lid for counter electrode A-001196 Chamber for counter electrode A-001236 O-ring for counter electrode A-009131 Port plug A-000178 Stirrer bar A-001199 Teflon Cap (for bulk) A-010537 Gas purging tube Optional components Catalog No. Description A-001194 Water Jacketed Glass cell (for bulk) A-002250 Platinum mesh 80 electrode A-002251 Gold mesh 100 electrode
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Cell vials
Various shapes and sizes of PYREX glass cell vials are available for users' purposes. Please be referred to their capacity as well
Catalog No.
Description
A-001056 Sample vial A-011504 Sample vial A-001051 Water Jacketed Glass cell
Sample Quantity Application Volume 20 mL 10 pcs VC-2, VC-3, VC-5, SVC-3, MCA 5 mL 10 pcs VC-4 20 mL 1 pc VC-2, VC-3, VC-5, SVC-3, MCA
Catalog
Description
Quantity 1 pc 1 pc
Catalog No.
Description
A-012062 Sample vial for RRDE-3 A-012018 Water Jacketed Cell vial
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SpectroElectrochemical Cell
Spectroelectrochemistry(SEC) is aimed at the investigation of electrochemical reaction mechanism and the interface structure between electrolyte solution and electrode. Remarkable progress in this field and related technology enables SEC to be applied in wide areas. Nowadays, the relation between absorbance and potential for reversible or quasi-reversible system is theoretically elucidated, on which basis the analysis of electrochemical characteristics becomes possible for the system otherwise difficult with only the result of voltammogram. Typical example is redox enzyme cytochrom c and methylene-blue
Analysis of the charge transfer at the electrode/liquid surface Spectrometric measurement of near/surface of electrodes
Catalog No. Description A-011240 SEC-C Thin Layer Quartz Glass Spectroelectrochemical cell Kit Components A-011498 SEC-C Pt Gauze working electrode A-011499 SEC-C Pt counter electrode A-011500 SEC-C Thin Layer Quartz Glass cell Light pass length: 1 mm A-011501 SEC-C Teflon Cap A-010537 Purging tube
Reference Electrode can be chosen optionally from below: Catalog No. Description
Length: OD: 6.0mm 80.0 mm Length: A-012171 RE-7 Non Aqueous reference electrode(Ag/Ag+) OD: 6.0mm 70.0 mm A-012167 RE-1B Silver-Silver chloride reference electrode We can provide also UV-Visible spectrophotometers with diode Array detection (please contact your local representative)
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Applications: Study of charge transfer mechanism on the interface between electrode and electrolyte.
Analysis of concentration, diffusion coefficient, life time so on Schematic view of flow cell (thin layer flow channel, light pass and working electrode) is shown below left. The working electrodes ( ITO, platinum mini-grid, and gold mini-grid) are replaceable. UV or visible light is introduced via optical-fiber from light source and absorbed light is transferred into CCD via optical-fiber. Example of spectrum change during oxidation-reduction of ferrocene by CV is shown below right
Description Cat No. A-011320 SEC-F Spectroelectrochemical flow cell Components A-011329 SEC-F flow cell base A-011330 SEC-F flow cell block(A) A-011331 SEC-F flow cell block(B) A-011495 SEC-FT500 Teflon gasket (2pcs) A-010562 74-UV UV/VIS Collimating Lens, 200-2000 nm -----Dynaseal PEEK fingertight(2pcs) -----Teflon Tubing (80cm) -----Silicon Tubing (30cm) -----Stainless Tubing OD 1/16" (50mm) Optional Products Cat No. Description A-011810 FIA-P1000-SR 1000 m optical fiber A-011496 SEC-F Pt grid electrode for flow cell A-011497 SEC-F Au grid electrode for flow cell A-011519 SEC-F ITO electrode for flow cell (4pcs) RE-3V Silver-silver chloride Reference A-012169 electrode Screw type RE-7V Non Aqueous reference A-012173 electrode(Ag/Ag+) Screw type
Fiber optic spectrometer was used in this measuring system; Lights is transmitted by optic fibers over a proper wavelength through electrode. The lights absorption, which occurred by electrolysis on the electrode, can be detected by spectrometer
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This quite handy cell was developed in order to evaluate plate material such as metal or semiconducting plate etc.. In evaluation, a sample plate is sandwiched in between block of the cell. Catalog No. Description Quantity 1 A-011951 Plate Material Evaluating Cell Components Teflon Cell [Body] 1 Teflon Cell [Base] 1 O-ring 1 Screw 20 mm 2 Purging tube 1m 1 A-002222 Pt counter electrode for VC-2 cell 1 PLEASE CHOOSE SEPARATELY YOUR REFERENCE ELECTRODE How to Set Up 1. Place a plate sample on a lower side Teflon block of the cell. Applicable plate dimensions: W: 10-20 mm, T: ~3 mm 2. Put another Teflon block on the sample, drive two screws evenly to fix the plate. Liquid contact area depends on inner diameter of the o-ring. Deliver approximately 1 ml of electrolyte after confirm if the plate is fixed. 3. Attach a Pt counter electrode and a reference electrode to the cell by setting them onto a cell cap. We would recommend you to twist up the Pt part appropriately if that counter electrode was longer.
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Or EL-CORR-2
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Accessories options: Thoses cells accept a lot of options like a corrosion sample holder, double jacket, Pt100 for temperature control (ask for connector type) with magnetic stirrer or for external bath, telescopic support or different king size reference electrode, bridge tube and platinum electrodes (see page 21)
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