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    Preparation and Study of Optical, Thermal, and Antibacterial Properties of Vanadate - Tellurite Glass

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    This document discusses the preparation, optical, thermal, and antibacterial properties of vanadate-tellurite glass. Specifically, it prepared glass samples with varying amounts of V2O5 from 5-20 mol% and analyzed their physical properties using XRD, density measurements, and UV-VIS absorption. It found that the optical band gap decreased and refractive index increased with higher V2O5 content. Thermal analysis showed stability and fragility increased with more V2O5. pH and antibacterial tests demonstrated the glass had significant antibacterial effects against various pathogens, with highest against L.monocytogenes, and that antibacterial potential increased with higher V2O5 and glass dissolution rates. This study is among the

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    Preparation and Study of Optical, Thermal, and Antibacterial Properties of Vanadate - Tellurite Glass

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    anti girlz
    24 views9 pages
    This document discusses the preparation, optical, thermal, and antibacterial properties of vanadate-tellurite glass. Specifically, it prepared glass samples with varying amounts of V2O5 from 5-20 mol% and analyzed their physical properties using XRD, density measurements, and UV-VIS absorption. It found that the optical band gap decreased and refractive index increased with higher V2O5 content. Thermal analysis showed stability and fragility increased with more V2O5. pH and antibacterial tests demonstrated the glass had significant antibacterial effects against various pathogens, with highest against L.monocytogenes, and that antibacterial potential increased with higher V2O5 and glass dissolution rates. This study is among the

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    This document discusses the preparation, optical, thermal, and antibacterial properties of vanadate-tellurite glass. Specifically, it prepared glass samples with varying amounts of V2O5 from 5-20 mol% and analyzed their physical properties using XRD, density measurements, and UV-VIS absorption. It found that the optical band gap decreased and refractive index increased with higher V2O5 content. Thermal analysis showed stability and fragility increased with more V2O5. pH and antibacterial tests demonstrated the glass had significant antibacterial effects against various pathogens, with highest against L.monocytogenes, and that antibacterial potential increased with higher V2O5 and glass dissolution rates. This study is among the

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    24 views9 pages

    Preparation and Study of Optical, Thermal, and Antibacterial Properties of Vanadate - Tellurite Glass

    Uploaded by

    anti girlz
    This document discusses the preparation, optical, thermal, and antibacterial properties of vanadate-tellurite glass. Specifically, it prepared glass samples with varying amounts of V2O5 from 5-20 mol% and analyzed their physical properties using XRD, density measurements, and UV-VIS absorption. It found that the optical band gap decreased and refractive index increased with higher V2O5 content. Thermal analysis showed stability and fragility increased with more V2O5. pH and antibacterial tests demonstrated the glass had significant antibacterial effects against various pathogens, with highest against L.monocytogenes, and that antibacterial potential increased with higher V2O5 and glass dissolution rates. This study is among the

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    Preparation and study of optical,

    thermal, and antibacterial properties of


    vanadate–tellurite glass

    N. Elkhoshkhanya, Ali Reda, Amira M. Embaby


    Institute of Graduate Studies and Researches
    Introduction

    • Tellurite glass .
    • Vanadium improves the semi-conducting
    properties ) .
    • Sodium oxide soda (Na2O) , Calcium
    oxide lime (CaO) network modifiers.
    • antibacterial agents like (silver (Ag+),
    copper (Cu2+), and zinc (Zn2+) ) .
    Glass preparation , XRD and Physical
    measurements

    • (90-X) TeO2- 5 CaO -5 Na2O- X V2O5) where x=5, 10, 15 and 20 mol% was prepared by
    conventional melt cast-quenching technique (800–850 °C).

    • Samples were identified by X-ray diffraction technique (XRD) to ensure the glassy
    state.
    • The density (ρ)and the number of bonds per unit volume(𝒏𝒃 ) decreased while molar
    ഥ ) increased
    volume , oxygen packing density (OPD) and stretching force constant (𝑭
    with increasing V2O5 mol %.

    5.2 34
    molar volume (cm3)

    5.15 33.5
    Density (g\cm3)

    5.1 33
    5.05 32.5
    5 Density
    32
    4.95
    31.5
    4.9 Molar volume
    4.85 31
    4.8 30.5
    4.75 30
    4.7 29.5
    0 5 10 15 20 25
    V2O5 content (mol%)
    UV/VIS absorption spectra and DSC
    measurements

    • Optical measurements proved that optical energy band gap decreased while Urbach
    energy and refractive index increased with V2O5 mol% increases .

    • The thermal stability (S), and glass factor tendency (Kg) were found to increase and
    the thermodynamic fragilities F decrease with the increasing of V2O5 mol% while,
    generally activation energies decreased due to the formation of non-bridging
    oxygen NBO's.
    pH measurements and Antibacterial properties

    • The antibacterial potential of V2O5 added in all TVCN increased significantly (P < 0.01)
    by increasing the concentrations of V2O5 for all tested bacterial pathogens. All TVCN
    showed the highest antibacterial effect on L.monocytogenes in comparison with the
    other tested bacterial strains.
    • It was found that the magnitude of the pH drop increases with the increase in glass
    dissolution rate and vanadium content.
    • So far, V2O5 is not reported yet as an
    antibacterial agent in combination with any
    type of glass.
    • Antibacterial potential of tellurite glass and
    non-tellurite glass incorporated with metals
    against S. enterica serovar Typhimurium had
    not been reported yet.

    • To the best of knowledge, present data


    concerning the antibacterial activity of all
    TVCN is considered the first finding verifying
    its antibacterial potential against broad
    spectrum Gram-ve bacteria (e.g., S.enetrica
    serovar Typhimurium, E.coli, and
    P.aeruginosa) and Gram +ve bacteria (e.g.,
    E.faecalis and L.monocytogenes).
    Thanks

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