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    Inorganic and Analytical Chemistry CH-102 Engr. Muhammad Arslan Haider

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    inam ullah
    1) The document outlines the safety rules and procedures for an inorganic and analytical chemistry laboratory. It details proper attire, chemical handling techniques, emergency equipment use, and cleanup responsibilities. 2) Students are informed of attendance requirements, assignment policies, and lab coat/shoe dress code. Proper techniques are outlined for various procedures like heating, smelling chemicals, and pipetting. 3) The safety rules aim to prevent accidents through policies like adding acids to water, working under fume hoods, inspecting glassware, and knowing hazard information. Students are responsible for cleaning work areas and storing chemicals and equipment properly.

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    © All Rights Reserved
    Download as PPT, PDF, TXT or read online from Scribd

    Inorganic and Analytical Chemistry CH-102 Engr. Muhammad Arslan Haider

    Uploaded by

    inam ullah
    41 views38 pages
    1) The document outlines the safety rules and procedures for an inorganic and analytical chemistry laboratory. It details proper attire, chemical handling techniques, emergency equipment use, and cleanup responsibilities. 2) Students are informed of attendance requirements, assignment policies, and lab coat/shoe dress code. Proper techniques are outlined for various procedures like heating, smelling chemicals, and pipetting. 3) The safety rules aim to prevent accidents through policies like adding acids to water, working under fume hoods, inspecting glassware, and knowing hazard information. Students are responsible for cleaning work areas and storing chemicals and equipment properly.

    Original Title

    UPDATED Lab safety inorganic-2019

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    1) The document outlines the safety rules and procedures for an inorganic and analytical chemistry laboratory. It details proper attire, chemical handling techniques, emergency equipment use, and cleanup responsibilities. 2) Students are informed of attendance requirements, assignment policies, and lab coat/shoe dress code. Proper techniques are outlined for various procedures like heating, smelling chemicals, and pipetting. 3) The safety rules aim to prevent accidents through policies like adding acids to water, working under fume hoods, inspecting glassware, and knowing hazard information. Students are responsible for cleaning work areas and storing chemicals and equipment properly.

    Copyright:

    © All Rights Reserved
    Download as PPT, PDF, TXT or read online from Scribd
    Download as ppt, pdf, or txt
    41 views38 pages

    Inorganic and Analytical Chemistry CH-102 Engr. Muhammad Arslan Haider

    Uploaded by

    inam ullah
    1) The document outlines the safety rules and procedures for an inorganic and analytical chemistry laboratory. It details proper attire, chemical handling techniques, emergency equipment use, and cleanup responsibilities. 2) Students are informed of attendance requirements, assignment policies, and lab coat/shoe dress code. Proper techniques are outlined for various procedures like heating, smelling chemicals, and pipetting. 3) The safety rules aim to prevent accidents through policies like adding acids to water, working under fume hoods, inspecting glassware, and knowing hazard information. Students are responsible for cleaning work areas and storing chemicals and equipment properly.

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    © All Rights Reserved
    Download as PPT, PDF, TXT or read online from Scribd
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    You are on page 1of 38

    Inorganic and Analytical Chemistry

    CH-102

    Engr. Muhammad Arslan Haider


    Rules of lab
    • No retake of Assignment and quiz
    • 75% attendance is mandatory
    • Copy should be completed in the Lab
    • No entry in lab without lab coat and close
    shoes
    Chemistry Laboratory Safety
    Rules
    Protect Your Eyes
    • Appropriate eye
    protection must
    be worn at all
    times!
    Wear appropriate protective
    clothing

    • Your clothing should cover your legs to the


    knees – shorts are not appropriate for the
    laboratory
    • Lab aprons can be used to protect good
    clothing
    • Loose clothing should not be worn because it
    may dip into chemicals or fall into a flame and
    catch fire
    Wear shoes that cover your feet.
    Do not apply cosmetics, eat, or drink
    in the lab.
    • These activities are ways by which you
    can accidentally ingest harmful
    chemicals
    Do not taste any chemical!
    Pour from large containers to smaller
    ones.
    Always ADD ACID to water

    acid

    water

    “Do not spit into acid!” – a good phrase to


    remember this rule.
    Hold your hand over the label while pouring.
    Work with volatile chemicals under a fume
    hood.
    Check glassware for stars or cracks.
    Heat test tubes at an angle, directing
    the opening oppositely to you and
    other people in the laboratory.
    Handle hot glassware with gloves or beaker
    tongs.
    First light the match

    THEN

    Turn on the gas!


    Do not smell any chemicals directly!

    • If absoluteley
    necessary to
    smell, use your
    hand to fan the
    vapor to your
    nose.
    Do not pipet solutions by mouth!

    • Use a rubber
    suction bulb or
    other device to
    fill a pipet.
    Wash your hands with soap and
    water before leaving.

    • This rule applies


    even if you have
    been wearing
    gloves!
    Know the hazards of the materials being
    used.
    • Read and reread
    labels carefully to
    make sure that you
    are using the right
    chemical.
    Tie Back Loose Hair
    • Dangling hair can
    fall into the
    Bunsen burner
    and catch fire or
    can fall into a
    chemical solution

    • P.S. Burning hair


    REALLY STINKS!
    Know the safety equipment
    • Eye wash fountain

    • Safety shower

    • Fire extinguisher

    • Emergency exits
    Know how to use the safety equipment
    • Eye wash Fountain

    • Safety Shower

    • Fire extinguisher

    • Emergency Exit
    Don’t work alone in the lab

    • In case of a
    problem, you may
    need another
    person to prevent
    injury or even
    save your life!
    Remember that the lab is a place for
    serious work!
    Careless behavior may endanger yourself
    and others and will not be tolerated!
    Demonstrate safe behavior
    • Obey all safety instructions.
    • Clean up spills immediately; IF you
    know how. If you are uncertain how
    to clean up a spill or if a large spill
    occurs, notify persons in
    accordance to the emergency
    procedure.
    Demonstrate safe behavior
    • Before leaving the lab:
    – Return equipment and chemicals to
    their proper places
    Demonstrate safe behavior
    • Before leaving the lab:
    – Return equipment and chemicals to
    their proper places

    – Be sure to replace the lids to all


    containers
    Demonstrate safe behavior
    • Before leaving the lab:
    – Return equipment and chemicals to
    their proper places

    – Be sure to replace the lids to all


    containers

    – Clean up your work area


    Report any accidents or unsafe
    conditions immediately!
    Program Learning Outcomes(PLOs)
    1) Engineering Knowledge
    2) Problem Analysis
    3) Modern Tool Usage
    4) The Engineer and Society
    5) Environment and Sustainability
    6) Ethics
    7) Design/Development of Solutions
    8) Individual and Team Work
    9) Investigation
    10)Communication
    11)Project Management
    12)Lifelong Learning
    Laboratory CLOs
    Learning level
    No. CLO PLO

    3 Follows instructions by the teacher to PLO 5 P-3


    realize experiment

    4 Demonstrate an eagerness to work in a PLO 9 A-3


    team during the lab activities

    5 Complies lab instructions to ensure safe PLO 7 A-2


    environment in the lab

    6 Analyse experimental results in the view PLO 1 C-4


    of theoretical understanding developed
    during the class
    List of Experiments
    • To determine the melting point of a given solid sample by using
    Melting point apparatus.
    • To determine amount per liter of NaOH in a given sample by using
    standard oxalic acid solution.
    • To determine hardness due to the presence of calcium (Ca+2) in the
    given sample of tap water.
    • To determine the number of molecules of water of crystallization in
    a given sample of ferrous sulphate by permanganate titration.
    • To determine amount per liter of Mohr’s salt in the given solution
    by using standard KMnO4 solution.
    • To find the amount of total dissolved solids (TDS) in the given
    sample of tap water.
    • Given solution contains 6.9 grams of A2CO3 dissolved per 1000 ml.
    Calculate the atomic weight of metal “A” and name it using
    standard HCL solution.
    • To determine the amount per liter of (SO4-2) in the given sample by
    Gravimetric analysis.
    • To determine the amount of chloride (Cl-1) ions in a given sample of
    water by standard AgNO3 solution.
    Contd….
    • To determine the Refractive Index of a given sugar samples by using
    Abbe’s Refractometer apparatus
    • To determine the concentration of sodium (Na+) and Potassium (K+) ions
    in a given samples with the help of Flame photometer.
    • To determine the surface tension of liquids at room temperature by
    means of Stalagmometer.
    • Determination of caffeine/Chromium content in a given sample by UV/
    Visible spectrophotometer.
    • Ink analysis by using paper chromatographic technique.
    • Analysis of sample (solid /liquid) through FTIR.
    • Analysis of sample by High performance liquid chromatography (HPLC)
    technique
    • To compare the viscosity measurements for Newtonian and non-
    Newtonian fluids.
    • To determine the best conductor among 0.1 M solutions of 5 different
    electrolytes.
    Equipments
    Weeks Introduction to Chemistry Lab and lab safety
    Week 1 To determine amount per liter of NaOH in a given sample by using standard oxalic acid solution.

    Week 2 To determine the melting point of a given solid sample by using Melting point apparatus.

    Week 3 Given solution contains 6.9 grams of A2CO3 dissolved per 1000 ml. Calculate the atomic weight of
    metal “A” and name it using standard HCL solution.
    Week 4 To determine the Refractive Index of a given sugar samples by using Abbe’s Refractometer
    apparatus
    Week 5 To determine the amount of chloride (Cl ) ions in a given sample of water by standard AgNO3
    -1

    solution. + Quiz-1
    Week 6 To determine the concentration of sodium (Na+) and Potassium (K+) ions in a given samples with the
    help of Flame photometer.
    Week 7 Analysis of sample by High performance liquid chromatography (HPLC) technique

    Week 8 Mid Viva


    Week 9 To determine the number of molecules of water of crystallization in a given sample of ferrous
    sulphate by permanganate titration.
    Week 10 Determination of caffeine/Chromium content in a given sample by UV/ Visible spectrophotometer.

    Week 11 To find the amount of total dissolved solids (TDS) in the given sample of tap water.

    Week 12 To determine the surface tension of liquids at room temperature by means of Stalagmometer +
    Quiz-2
    Week 13 Analysis of sample (solid /liquid) through FTIR.
    Week 14 To determine hardness due to the presence of calcium (Ca+2) in the given sample of tap water.

    Week 15 Final Viva


    Groups Description
    ABDUL REHMAN FAROOQUI AQSA AMIR HASSAN RAFIQ
    AWAIS RIAZ
    AHMED ASAD ULLAH INAM ULLAH
    AYESHA NOOR
    ALEEZA AHMAD IQRA YOUNIS
    AZKA JAVED
    ALI HAIDER HADEEQ UZ ZAMAN JANNAT
    ALMAS AIJAZ HAFIZ MUHAMMAD HASNAIN MAHAM BASHIR
    AMNA KHALIL KHAN MANAHIL TARIQ

    MIAN AHSAN BARI


    MUHAMMAD ALI SARWAR MUHAMMAD MAAZ
    MUHAMMAD AMAAN MALIK MUHAMMAD OSAMA SHAHID
    MOHAMMAD HARIS ALI SIDDIQUI
    MUHAMMAD ASAD IJAZ MUHAMMAD SAQIB FAROOQ
    MUHAMMAD JUNAID
    MUHAMMAD FAHAD SIKANDAR MUNTAZIR MEHDI
    MUHAMMAD SAMEER
    MUHAMMAD HASAN RUBBA FATIMA SHAHID
    MUHAMMAD SUFYAN
    MUHAMMAD ADNAN IQBAL MUHAMMAD JAHANZEB SAAD UR REHMAN

    SHAHER YAR HASSAN USAMA AHMED KHAN


    SHEEZA RAZZAQ ZARFISHAN TAHIR JAVEED
    SIBT HASSAN MUHAMMAD BILAL HASSAN
    SYED SAFFI HADIR SHAH CHUDARY MUHAMMAD UMER EJAZ
    UMAIR MAJEED MUHAMMAD SAAD
    UMER IMTIAZ
    AHMAD RAZA

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