2000 FRM
2000 FRM
2000 FRM
Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please
consult your local sales representative for details.
Thermo Fisher Scientific has contracted with one or more recycling/disposal companies in each EU Member
State, and this product should be disposed of or recycled through them. Further information on Thermo Fisher
Scientific’s compliance with these Directives, the recyclers in your country, and information on Thermo Fisher
Scientific products which may assist the detection of substances subject to the RoHS Directive are available at:
www.thermo.com/WEEERoHS.
Revision B.003
Notice is hereby given that the EPA in accordance with 40 CFR 40 Part 53 has
designated a new reference method for the measuring mass concentrations of
particulate matter as PM-2.5 in ambient air. The new reference method is a
gravimetric method which utilizes a specially designed PM-2.5 sampler for particle
collection the designated method is as follows:
This method is available from Rupprecht & Patashnick Company, Inc. (R&P).
PAGE I
Revision B.003
This instrumentation from Rupprecht & Patashnick Co., Inc. (R&P) is covered by
pending patents in the United States of America and other countries.
Partisol® and the “rp” logo are registered trademarks of Rupprecht & Patashnick Co.,
Inc. Other trademarks are the property of their respective holders. Mention of specific
product names (other than R&P products) in this manual does not constitute an
endorsement or recommendation by R&P of that equipment.
PAGE II
Revision B.003
Safety Notice
The Partisol stand must be anchored when installed outdoors to prevent tipping of the
sampler and/or stand in high winds.
Some assembly of the sample inlet and WINS impactor is required for installation and
regular maintenance. Care should be taken when assembling the WINS impactor or
inlet to prevent pinching fingers between the assembly parts.
The seller cannot foresee all possible modes of operation in which the user may
attempt to utilize this instrumentation. The user assumes all liability associated with
the use of this instrumentation. The seller further disclaims any responsibility for
consequential damages. Use of this product in any manner not intended by the
manufacturer will void the safety protection provided by the equipment, and may
damage the equipment and subject the user to injury.
PAGE III
Revision B.003
Warranty (U.S.)
R&P warrants that the R&P-supplied equipment shall be free from defects in material
or workmanship for a period of three-hundred sixty-five (365) days after the date of
shipment. Subject to the conditions of this provision, R&P agrees to repair or replace,
free of charge, any components of the equipment found to be defective in material or
workmanship during the warranty period. Purchaser shall notify R&P of any detected
defects and shall return any equipment believed to be defective to R&P, suitably
insured and at the purchaser’s expense. In the event R&P determines the equipment
returned for warranty correction is not defective within the terms of the warranty,
purchaser shall be responsible for all costs of handling and return transportation.
R&P’s sole responsibility under the warranty shall be, at R&P’s option, to either
repair or replace any component that fails during the warranty period due to a defect
in workmanship and/or material, provided purchaser has promptly reported same to
R&P and R&P has, upon inspection, found such components to be defective.
The above warranty is contingent upon the proper use of the equipment (i.e., operation
and maintenance in accordance with the procedures set forth in the provided operation
manual(s)) and does not cover equipment that has been modified without R&P’s
approval, or which has been subjected to abuse or unusual physical or electrical stress.
This warranty does not cover any optional personal computer equipment or operating
system software supplied with the equipment beyond the warranty period provided by
the manufacturer of the computer. The customer is responsible for obtaining a local,
third party service agreement for computer service requirements beyond the warranty
term of the computer.
PAGE IV
Revision B.003
Equipment Rating
The following information can be used to determine the power service requirements
of this product.
Line Voltage
115 V ~ 60 Hz 380 VA
230 V ~ 50 Hz 380 VA
Only reach as far as needed to adjust the mass flow controller (MFC) in the pump
compartment. There may be a hazardous line (wire) accessible in the rear of the pump
compartment.
There are two fuses in the transformer wiring harness. Both fuses are in the Secondary
of the Transformer. The fuse values are T 4A 250V and T 5A 250V.
FUSE TABLE
PAGE V
Revision B.003
This product has been tested by Intertek Testing Services, and has been documented
to be in compliance with the following U.S. and Canadian standards:
UL Standard 3101-1
CAN/CSA C22.2 NO. 1010.1
Rupprecht & Patashnick Co., Inc. certifies that this product operates in compliance
with the EC Directive 89/336/EEC in reference to electrical emissions and immunity.
Specifically, the equipment meets the requirements of EN50081-1:1992, Class B
(Emissions) and EN50082-1:1997 (Immunity).
In addition, the hardware has been tested for personal or fire safety hazards, and meets
the requirements of EN61010-1 (Safety) in fulfillment of EC Directive 73/23/EEC.
PAGE VI
Revision B.003
The operating manual includes references to U.S. EPA 2.12 Quality Assurance
Handbook Volume II, Part II. Partisol-Plus Model 2025 Air Samplers which are
installed as part of a U.S. EPA monitoring network, or which must meet U.S. EPA
monitoring requirements must follow the procedures found in the 2.12 Quality
Assurance Handbook. If there is any conflict between the instructions or procedures
in this operating manual and those found in the 2.12 Quality Assurance Handbook,
the 2.12 specifications and procedures take precedence.
A copy of U.S. EPA 2.12 Quality Assurance Handbook may be obtained from the
AMTIC web site: http://www.epa.gov/ttn/amtic/pmqa.html or the QC coordinator at
any EPA Regional Office, or the Monitoring and Quality Assurance Group (MD-14),
U.S. EPA, Research Triangle Park, NC 27711.
PAGE VII
Revision B.003
To help our customers keep track of the changes to the Partisol-FRM Model 2000 PM-
2.5 Air Sampler and its operating manual, following is a list of the manual sections
with their respective revision numbers:
PAGE VIII
Revision B.003
PAGE IX
Revision B.003
Table of Contents
PAGE X
Revision B.003
PAGE XI
Revision B.003
Section 1: Introduction
The Partisol-FRM Model 2000 PM-2.5 Air Sampler (Figure 1-1) is designed to
conform to the U.S. EPA Federal Reference Method for fine particulate sampling.
Specifically, Rupprecht & Patashnick (R&P) has designed the hardware to exceed or
meet the requirements of CFR 40 Part 50 Appendix L and related drawings supplied
by the U.S. EPA.
This addition to the Partisol family of samplers builds upon the extensive experience
gained by R&P in the design and manufacture of the original Partisol PM-10 Air
Sampler. This popular sampling platform holds the U.S. EPA reference designation
for PM-10 sampling. Many of the design features adopted by the U.S. EPA in the
proposed PM-2.5 Federal Reference Method were first introduced into a reference-
designated air sampling method by R&P in the original Partisol Sampler. These
include the following:
✔ The Partisol-FRM • The use of standard 47 mm sample filters with a convenient filter exchange
Sampler builds upon the mechanism.
features first introduced
with the original Partisol
PM-10 Air Sampler. • Full microprocessor control and data handling.
As with other manual sampling devices, the filters used in the Partisol-
FRM Sampler must be conditioned and weighed before exposure, and then
conditioned and weighed again after use to determine the mass of the
particulate matter collected during the 24-hour exposure time. The Partisol
hardware stores the data relevant to each 24-hour collection period in its
internal data logger for viewing and/or retrieval after the fact. Such information
includes the total volume sampled (in volumetric m³), total collection time, and the
average ambient temperature and pressure during the collection period. In addition,
the device stores interval data records every five minutes to keep a record of the
temperature of the ambient air and sample filter.
The following is a listing of some of the advanced features contained in the Partisol-
FRM Air Sampler:
• Interval data are stored every five minutes, and include the five-minute
averages of the filter temperature, ambient temperature, and ambient
pressure. Data storage continues both during and after the exposure of the
collection filter. The sampler has a capacity of 14 days of five-minute
interval data.
• A record of filter data is stored for each filter used in the device, and
includes all U.S. EPA-specified values such as the volume sampled, error
condition flagging, and average temperatures and pressures. The sampler
has a capacity of 25 filter data records.
• The sampler is easily transported due to its compact form and lightweight
design. Its low noise level makes it appropriate for indoor monitoring.
• The sampler ships with UL-, CSA- and CE-equivalent electrical and
safety approvals.
• An analog output of 0-5 VDC indicates the current flow rate and the
existence of any status conditions.
This manual is divided into sections, with each treating a different topic. The first parts
deal with the setup of the system's hardware and software, while the later sections
describe the more-advanced features of the Partisol-FRM Sampler. The user should
read and implement the procedures discussed in the earlier sections before using the
functions detailed later in the manual. The following listing provides an overview of
the topics handled in each section of this manual:
Section 1: Introduction
This section introduces the user to the advanced features of the Partisol-FRM Sampler
and describes the flow configuration of the system. It also discusses the flow control
scheme used in the hardware.
The system flow schematic provides an overview of the hardware's flow and
electronic connections (Figure 1-2). The schematic shows a PM-10 inlet that is
followed by a down tube and WINS PM-2.5 Impactor. The WINS Impactor is located
inside the sampler enclosure. A 47 mm Teflon filter is housed in a filter cassette that
the user installs in a single-filter tray. The tray makes the easy exchange of filters
Figure 1-2. System flow possible in the sampler's filter exchange mechanism, and minimizes the chances of
schematic.
fingers coming into contact with the collection filter.
An in-line filter downstream of the sample filter protects the mass flow controller from
any particles that may remain in the air flow. The mass flow controller operates under
✔ The Partisol-FRM the control of the sampler’s microprocessor, and maintains the sample stream at a
Sampler actively maintains constant volumetric flow rate (16.7 l/min default) through the use of ambient
a constant volumetric flow temperature and pressure sensors. The accumulator minimizes pulsations caused by
rate at the user-defined set the vacuum pump, while the pump built into the Partisol-FRM Sampler is the same
point (16.7 l/min by default).
highly-reliable model built into the original Partisol Model 2000 Air Sampler.
The Partisol-FRM Sampler maintains a constant volumetric flow rate at the set point
entered by the user (usually 16.7 l/min), and reports sampled volumes (m³) in
volumetric terms in accordance with new U.S. EPA guidelines.
The sampling system determines the ambient temperature and pressure for flow rate
calculations through the use of sensors that continually provide updated information
to the microprocessor system.
where:
Flow RateSTP = Control set point of the mass flow meter (equivalent
flow at 0 °C and 1 atmosphere).
Flow RateVol = Volumetric flow rate set point (l/min) as entered by
the user in the Setup Screen (Section 5). This value
is 16.7 l/min (1 m3/h) for most applications.
Ave Temp = The current temperature (°C) as measured by the
temperature sensor mounted on the down tube of the
sampler.
Ave Pres = The current pressure (mm Hg) as measured by the
pressure transducer in the sampler's enclosure.
Mass concentration data reported to the U.S. EPA must be in volumetric m³, which
simply involves integrating the above volumetric flow rate over the sampling period,
without any further adjustment. The Partisol-FRM Sampler automatically determines
the sampled volume in volumetric m³ for each filter exposed, and stores this
information internally for later viewing or downloading (Section 7).
This section describes the installation of the Partisol-FRM Sampler, along with the
setup of the optional support stand. This part also covers a number of operational
considerations.
The following is a listing of the standard components provided with a Partisol hub
unit:
Partisol-FRM enclosure with WINS PM-2.5 impactor and filter ex-
change mechanism
PM-10 sample inlet
3 rain hoods and associated hardware
Sample tube
Ambient temperature sensor and cable
Dual filter transport container with cassettes and carriers
Flow audit adapter
Box of 25 glass filters, 37 mm diameter
Bottle of WINS impactor oil, 30 ml
Analog input calibration cable
Mating cable connector for four-pin user-output connector
AKCOMM software diskette
9-to-9 pin computer cable
2 Operating Manuals
1 Service Manual
1 Quick Start Guide
NOTE: The Partisol-FRM Sampler should be fitted with its optional insulating
jacket (10-004146) in the wintertime for locations at which temperatures are
expected to drop below -30 °C on a regular basis. Refer to Appendix F for a
complete listing of part numbers.
1) When moving the instrument, be sure to lift the unit by using the
two handles.
2) Cut any tie wraps and remove any transport restraints from inside
the sampler enclosure.
3) Install the large rain hood on the right side of the enclosure (Fig-
ure 2-1). The rain hood should cover both air filters.
a) Peel back the paper facing of the larger gasket and apply it to the larger rain
hood.
b) Place the large rain hood with its gasket attached on the enclosure.
c) Secure the rain hood to the unit using four (4) #10-32 x 1/2" thumb screws.
4) Install the two small rain hoods (Figure 2-1). One rain hood is
installed on the left side of the enclosure and the other on the
back. Each rain hood covers one fan opening.
a) Peel back the paper facing of one of the smaller gaskets and apply it to one
of the smaller rain hoods.
b) Place the small rain hood with its gasket attached hood on the enclosure.
c) Secure the rain hood to the unit using four (4) #10-32 x 1/2" thumb screws.
d) Repeat this procedure for the other small rain hood.
5) Install the sample tube and PM-10 inlet (Figure 2-2).
NOTE: Examine the sample tube. Some sample tubes are machined down to a
smaller diameter on both ends. The machining on one end extends for 5 cm (2
inches), while the machining on the opposite end extends only 3 cm (1.25
inches).
a) Insert the end of the sample tube with the 5 cm (2 inches) machined section
into the bulkhead of the sampler. Ensure that the tube is pushed into the enclosure
through the final O-ring until it hits a stop.
b) Turn the dome connector on the bulkhead to ensure a tight grip.
c) Place the PM-10 inlet on the end with 3 cm (1.25 inches) of machining.
Ensure that the tube is pushed past the inlet’s two O-rings, which provide some
resistance, and hits a stop.
In its final sampling configuration, the entrance to the inlet must be approxi-
mately 2 m above the ground (6 to 7 feet). An optional stand (57-004644)
described in Section 2.3 provides a convenient means of installing the sampler.
6) Connect the hub to the electric supply in a manner that meets all
safety and regulatory requirements for the hardware’s intended
use.
The wires inside the power cord are defined by the following colors, which are
different for 115 and 230 VAC configurations:
115 VAC 230 VAC
Line Black or Brown Brown
Neutral White or Blue Blue
Common Ground Green or Green/Yellow Green/Yellow
For 115 VAC configurations of the Partisol system, the standard three-pronged
U.S. plug is provided at the end of the power cord. This plug is intended only for
some types of indoor installations, and may have to be replaced by other
connecting hardware for certain types of indoor and outdoor locations to meet
electrical and other safety requirements.
WARNING: Use of the supplied 115 VAC three-prong plug out of doors or in
and uncontrolled interior environment may present a severe electrical shock
hazard.
For 230 VAC configurations of the Partisol system, the standard two-pronged
European plug is provided at the end of the power cord. This plug is intended only
for some types of indoor installations, and may have to be replaced by other
connecting hardware for certain types of indoor and outdoor locations to meet
electrical and other safety requirements.
WARNING: Use of the supplied 230 VAC two-prong plug out of doors or in and
uncontrolled interior environment may present a severe electrical shock hazard.
7) Install the ambient temperature sensor.
a) Locate the two screws installed on the left side of the enclosure.
b) Remove the two screws, being careful not to lose the washers, if installed.
This will expose two holes.
c) Locate the ambient temperature probe assembly in the compilation package.
d) Place the ambient temperature probe assembly over the two holes in the left
side of the sampler enclosure (Figure 2-3).
e) If R&P supplied the sampler with washers, secure the assembly to the
enclosure using the screws and washers previously removed. Place the washers
between the ambient temperature bracket and the enclosure – not under the head
of the screw – then insert the screws into the bracket. The washers provide a
watertight seal to prevent leakage of water into the electronics compartment.
f) If R&P supplied the sampler without washers, secure the assembly to the
enclosure using the screws previously removed. In this case, leak tightness is
achieved on the inside of the electronics compartment through the use of self-
sealing components.
g) Plug the ambient temperature probe into the connector on the back panel of
the sampler labeled “TEMPERATURE SENSOR” (Figure 2-4).
8) Prepare the WINS PM-2.5 impactor for use (Appendix H).
9) Install a 47 mm filter in the sampler (Section 3). Ensure that the
sampler is not powered up.
10
10)) After the system is powered up according to the instructions in
Section 4, perform the leak check described in Section 10.2.
The Partisol Stand (R&P part number 57-004644) aids in the installation of the
Partisol-FRM Sampler, and ensures that the inlet is at the appropriate height. Figure
2-5 shows the mounting of the unit on the stand.
Figure 2-6 contains a listing of parts, as well as other assembly information for the
stand. Put this hardware together in accordance with the diagram shown in this figure.
The sample pump is always on when sampling takes place. When the device is not
sampling, the sample pump turns on under the cold-weather conditions listed below.
In such a case, the flow through the pump enters the system through a valve that
regulates the bypass stream to the flow controller.
If the temperature measured on the interface board drops below a certain level, the
system electronics cannot be guaranteed to operate reliably, and the device enters a
standby condition. This occurs according to the following rule:
Turn the knob on the on the lower left-hand side of the keypad to adjust the contrast
of the sampler’s liquid crystal display. This knob may be turned both clockwise and
counterclockwise (Figure 2-7).
This section covers the initial inspection of 47 mm filters used in the Partisol-FRM
Sampler, as well as the equilibration and weighing before and after use. Further, it
covers their installation and removal in the sampling unit, as well as the computation
involved in calculating the 24-hour mass concentration average of PM-2.5 as found
in U. S. EPA 2.12 Quality Assurance Handbook Volume II, Part II Section 7 (Filter
Preparation and Analysis, Section 8 (Field Operation) and Section 11 (Calculations,
Validation and Reporting of PM2.5 Monitoring Data). Use the filter log in Appendix
G as an aid in record keeping.
The only filter media currently approved by the U.S. EPA for reference method
sampling of PM-2.5 in the proposed regulations is Teflon material in a 47 mm
diameter size. This is available from R&P in the following form:
✘ Never touch filters with Teflon Filters, 2.0 µm pore size, Box of 50 R&P part number 10-002322-0050
fingers.
The user must be careful to keep filters clean and never to touch filters with fingers.
Filters should be stored at the laboratory in petri dishes, and should be transported to
and from the sampling site in the filter transport system supplied by R&P. Only non-
serrated forceps should be used to handle the 47 mm filters used in the sampler.
Inspect each filter visually for integrity before use. Check for the following:
• Pinholes
• Chaff or flashing
• Loose material
• Discoloration
• Non-uniformity
Perform this procedure to equilibrate 47 mm filters before use. Be sure to use petri
dishes to store filters in the laboratory.
NOTE: Refer to the U.S. EPA 2.12 Quality Assurance Handbook, Section 7, for
further information.
1) Place a label on the cover of each petri dish and number each
dish.
2) Place the petri dish cover under the bottom half of the dish.
3) Place each inspected filter into a separate petri dish.
4) Record the filter number, relative humidity, temperature, date and
time at the beginning of equilibration.
5) Equilibrate each filter for at least 24 hours under the following
conditions:
The equilibration room must be held at a constant relative humidity between 30
and 40% with a variability of not more than ±5% relative humidity.
The equilibration room must be held at a constant temperature between 20 and
23 °C with a variability of not more than ±2 °C.
Follow this procedure to weigh the 47mm collection filters (tare weight) before
sampling.
NOTE: Refer to the U.S. EPA 2.12 Quality Assurance Handbook, Section 7, for
further information.
1) Ensure that each filter has been equilibrated for at least 24 hours
✔ Record the initial filter
weight as Wi. before weighing.
2) Filters must be weighed on a microbalance with a resolution of at
✔ The pre-sampling
weighing must take place least 1 µg (0.001 mg). Ensure that the balance has been allowed
within 30 days of the to warm up before performing any weighings.
sampling period.
3) Weigh each filter at least once (three times recommended), re-
cording the mass in grams (Figure 3-1). The average mass
reading is the initial filter weight, Wi. Use appropriate techniques
to neutralize static charges on the filter. This pre-sampling weigh-
ing must take place within 30 days of the sampling period, as
specified in 2.12 Quality Assurance Handbook, Section 7.
5) Place the filter cassette with its 47 mm filter installed into the filter
cassette carrier (55-004847), and place the entire assembly into
the metal transport container (Figure 3-3) as specified in 2.12
Quality Assurance Handbook, Section 7. The container should be
identified appropriately using a sticker or other system, and
should contain a foam liner to ensure a snug fit.
✘ Do not exchange sample 1) Determine from the Main screen (Section 4.3) whether the unit is
filters until their sampling still sampling, i.e., whether it is in the Sampling Operating Mode
program is complete. (SAMP in the upper right-hand corner of the screen, Section 5.3).
The Main screen displays the current time/date, as well as the
programmed starting and ending time/date. If the device is still in
its Sampling Operating Mode, allow it to complete its current
✔ The sampler must be in sampling program before executing the steps below.
its Stop Operating Mode
when removing the cur- 2) If the device is in the Stop or Error Operating Mode, press <F4:
rently-installed filter. Run/Stp> in the Main screen to return the sampler to the Stop
Operating Mode (Section 5.3). This causes the sampler to write
the final information to the current record of filter data, and must
take place before removing a currently-installed filter.
3) Pull the handle of the filter exchange mechanism toward the front
of the instrument to lower the filter platform and expose the filter
cassette in its carrier (Figures 3-4 and 3-5).
11) Press <F4: Run/Stp> to leave the Stop Operating Mode and enter
either the Wait or Sampling Operating Mode (Section 5.3). The
unit will automatically execute the sampling program defined in
the Filter Setup screen of step 9 above.
12) If an exposed filter was removed from the sampler in step 4
above, press <F3: Data> in the Main screen to view the data for
the removed filter in the Filter Data screen (Section 8.1). Press
<F2: ->, if necessary, to view the appropriate record of filter data.
13) Record the information required for data computation and quality
assurance purposes. At a minimum, this would usually include
the volume sampled (Vol), the flow rate coefficient of variation
(%CV), the total sampling time (Tot), the largest difference be-
tween the ambient and filter temperatures (TempDiff), and the
status code (Stat).
14) When in the Filter Data screen, press <F4: PwrDat> to view power
outage and filter ID information in the Power Outages screen
(Section 8.1), or press <F5: IntvDat> to gain access to 5-minute
averaged temperature and pressure data in the Interval Data
screen (Section 8.2).
NOTE: The information contained in the Filter Data screen, Power Outages
screen and Interval Data screen may be downloaded electronically into a laptop
personal computer (PC) using software and a cable provided with the Partisol-
FRM Sampler (Section 8.3).
1) Ensure that the filter has been equilibrated for at least 24 hours
before weighing (Section 3.5).
2) Filters must be weighed on a microbalance with a resolution of at
least 1 µg (0.001 mg). Ensure that the balance has been allowed
to warm up before performing any weighings.
NOTE: U.S. EPA regulations require that the post-collection weighing be
performed immediately following post-collection conditioning and within 10
days of sampling, and that it be performed by the same person and on the same
balance as the initial filter weighing as found in 2.12 Quality Assurance
✔ Record the final filter Handbook, Section 7 and Section 11.
weight as Wf.
3) Remove the filter from its petri dish.
4) Weigh each filter at least once (three times recommended), re-
cording the mass in grams (Figure 3-7). The average mass
✔ The change in filter
weight involves the Wi and reading is the final filter weight, Wf.
Wf weights computed
above.
5) Return the filter to its petri dish, place the petri dish cover over it,
and store it for archival purposes.
6) Document the relative humidity, temperature, date and time of the
post-collection weighing.
Compute the average mass concentration (MC) of PM-2.5 during the sampling period
using the following formula with the information assembled above, refer to 2.12
Quality Assurance Handbook, Section 11:
∆W x 106
MC = ––––––––––
V
where:
DW = the net change in the mass (g) of the 47 mm filter between the initial
weighing and the post collection weighing, as computed in step 8 of Section 3.6 above.
For 24-hour PM-2.5 concentration averages to be valid without adjustment for U.S.
EPA reporting purposes, the total sampling time (Tot in step 12 of Section 3.4) must
be between 23 and 25 hours, and other requirements must also be met as referenced
in 2.12 Quality Assurance Handbook, Section 8. The value of the Stat field recorded
in step 12 of Section 3.4 indicates whether the sampler encountered any adverse
operational conditions (Section 7.1).
This section describes the steps involved in turning on the Partisol-FRM Sampler,
navigating through its basic screens, and in interacting with the device as a user. The
software’s menu structure and a complete listing of screens may be found in Appendix
A.
Implementation of the subject matter covered in this section should only be attempted
once the sampler is set up in accordance with Sections 2 and 3.
✔ Ensure that all applicable Follow the procedures outlined in Sections 2 and 3 carefully before attempting
safety standards are met operation of the Model 2000 sampler. Once the sampling system has been wired to a
before applying power to
the hardware.
main electrical source of the proper voltage in accordance with local standards, power
can be applied to the unit.
1) Press the power switch on the main panel to its “on” (1) position
to activate the sampler (Figure 4-1).
Once the power switch is pressed, the pump in the hub unit may start up momentarily.
This is the default setting of the unit in case it is being turned on under extreme cold
conditions where additional heat is necessary to warm the electronics.
The Title screen appears on the display of the sampler momentarily to identify the
model number of the hardware and the revision number of the installed software
(Figure 4-2). During the time that the sampler displays this screen, the user has a
chance to reset the hardware by pressing the appropriate keys on the keypad (Section
12).
After a few seconds, the Title screen is automatically replaced by the Main screen
(Figure 4-3). This screen shows summary information regarding the sampling
program currently defined by the user, the current operating mode, the existence of
any status conditions, as well as certain operational information.
Status Code The value of the status code in the upper left-hand
corner of the Main screen indicates whether or not
the hardware is operating properly (Section 7.1). A
value of “Ok” indicates that all functions are pro-
ceeding normally.
Current Time The local time and date are displayed on the second
line of the Main screen. These variables should be
set to their proper values in the Setup screen (Sec-
tion 5.1) before commencing operation of the
sampler. The Partisol-FRM Sampler expresses time
as “hh.mm” and dates as “yy/mm/dd” in accordance
with U.S. EPA requirements.
Sample Start The Sample Start line indicates the time and date at
which the sampler is currently programmed to begin
sample collection. Press <F1: FiltSet> from the
Main screen to enter the Filter Setup screen (Section
5.2). With the device in the Stop Operating Mode
(Section 5.3), the user can change the sampling
program from this screen.
Sample Stop The Sample Stop line indicates the time and date at
which the sampler is currently programmed to stop
sample collection. Press <F1: FiltSet> from the
Main screen to enter the Filter Setup screen (Section
5.2). With the device in the Stop Operating Mode
(Section 5.3), the user can change the sampling
program from this screen.
Flow Rate This field contains the current sample flow rate
(volumetric l/min). The value of this field is “0” if
the sample flow is currently turned off.
Sampling Time This field contains the total elapsed sampling time
(hh.mm). This field is reset to “0” whenever the user
advances from the Done to the Stop Operating
Mode (Section 5.3) by pressing <F4: Run/Stp>. The
user may view stored data by entering <F3: Data>
from the Main Screen (Section 8.1).
The function keys labelled “F1” to “F5” activate the commands shown on the bottom
line of virtually every screen in the system. The following parts of this section describe
how to navigate among the screens of the system software, as well as how to switch
between the “Browse Mode” and “Edit Mode” to change the value of system
parameters.
The system software allows the user to navigate easily through the use of soft function
keys (<F1> to <F5>) and the <ESC> key (Figure 4-4). The depth of the sampler’s
menu structure is shallow, making it relatively easy to switch from one display to
another (Figure 4-5). From the Main screen, simply press the soft key labelled <F1:
FiltSet>, <F2: Stats>, <F3: Data> or <F5: Setup> to drop down one level in the screen
✔ Use function keys to structure. Pressing the <ESC> key causes the current display to be replaced by the next
drop down by one layer in higher screen in the hierarchy. For example, pressing <ESC> when in the Filter Setup
the structure of screens.
Pressing <ESC> returns the screen returns the user to the Main screen. The definition of the soft function keys
user to the next highest changes as different screens appear on the display and different functions are required.
level. Appendix A contains an overview of all screens included in the Partisol-FRM
software.
Main Screen
Power Outages
Screen
Interval Data
Screen
Flow Calibration
Screen
The <F1: Edit> key is common to many screens. The function of this command, which
causes the sampler to leave the Browse Mode and enter the Edit Mode, is described
in the following parts of this section.
The <SHIFT> key plays a special role in accessing soft function keys. Certain
displays, such as the Setup screen (Figure 4-6), have a “>” or “<” indicator on the right-
most position of the bottom line. The appearance of these symbols indicates that the
soft key menu for the current screen is two lines long, and that <SHIFT> can be pressed
to toggle between the lines of the menu. This is the case both in the Browse Mode and
the Edit Mode.
The following describes the use of the <SHIFT> key to switch between soft key menu
lines:
✔ Press the <SHIFT> key > The first line of the soft key menu is currently being displayed. Press
to toggle between the two
lines of the soft key menu, <SHIFT> to toggle to the second line of the soft key menu. Once this
as indicated by “>” and “<.” occurs, the “<” symbol appears in its place. This procedure applies when
in the Browse Mode and Edit Mode.
< The second line of the soft key menu is currently being displayed. Press
<SHIFT> to toggle to the first line of the soft key menu. Once this occurs,
the “>” symbol appears in its place. This procedure applies when in the
Browse Mode and Edit Mode.
For the descriptive purposes of this manual, the soft keys on the second line of the soft
key menu are identified as “F6” to “F10.”
The Partisol Sampler normally operates in the Browse Mode, which enables the user
to navigate among all of its screens, but does not allow any changes to be made to
system parameters.
To enter the Edit Mode, press the <F1: Edit> key. Because many screens contain
information, such as flow rate set points that can only be changed when the sampler
is in the Stop Operating Mode, the hardware beeps if it cannot enter the Edit Mode.
In such a case, the user must return to the Main screen and press <F4: Run/Stp> before
attempting to enter the Edit Mode in the desired screen.
The cursor changes from an underline when it is in the Browse Mode to a large square
shape when the sampler is in the Edit Mode.
Many screens, such as the Setup screen (Figure 4-6), contain soft keys to decrement
by larger or smaller amounts (<--> and <->, respectively) and to increment by larger
or smaller amounts (<++> and <+>, respectively).
Numeric values can also be entered directly from the keypad. The <Bksp> (back-
space) key erases previously typed characters.
Times expressed as “hh.mm” (or “hh.mm.ss”) are edited as two (or three) separate
sections, and can be edited using the <-->, <->, <+> or <++> keys, or through direct
keypad entry. Use the arrow keys on the keypad to move from one part of the time field
✔ Use the arrow keys to to another.
move from one field to
another while remaining in Dates expressed as “yy/mm/dd” are edited as three separate sections, and can be
the Edit Mode.
changed using the <-->, <->, <+> or <++> keys, or through direct keypad entry. Use
the arrow keys on the keypad to move from one part of the date field to another.
To edit multiple parameters while remaining in the Edit Mode, press the arrow keys
on the keypad after making each change. This moves the cursor to a new field and
keeps the Model 2000 unit in its Edit Mode. This does away with the need to toggle
between the Browse Mode and Edit Mode for each parameter edited.
The following two keystrokes cause the software to leave the Edit Mode and return
to the Browse Mode:
✔ Leave the Edit Mode by
pressing <ENTER> to save
changes or <ESC> to
<ENTER> Changes made while in the Edit Mode are retained,
disregard changes. and the sampler then returns to the Browse Mode.
The cursor reverts to its underline shape when the software returns to the Browse
Mode.
The Filter Setup screen (Figure 4-7) makes special function keys available when the
user is in the Edit Mode. The <F8: <-- > and <F9: --> > keys move the editing cursor
to the left and right, respectively, when making changes to the ID1 and ID2
parameters. New numbers entered by the user overwrite any character that already
resides in the current cursor position.
This section describes the basic setup and operation of the Partisol-FRM Sampler. Do
not attempt the procedures described in this section until carrying out the steps in
Sections 2, 3 and 4. Appendix A displays all of the sampler’s screens, while Appendix
B contains a listing of the hardware’s most important Program Register Codes.
The Setup screen (Figure 5-1) allows the user to define global parameters for the
operation of the Partisol-FRM Sampler, such as the current time and date, default flow
rate, and default sampling time parameters. The user must make the desired entries
for the current time, current date and default flow rate in the Stop Operating Mode in
the manner described in Section 5.3.
Press <F5: Setup> when in the Main screen (Figure 4-3) to enter the Setup screen. All
of the fields in the Setup screen with the exception of the software version number are
editable when the instrument is in the Stop Operating Mode.
Cur Time The Cur Time parameter is the current local time (or other
standard time selected by the user) expressed as hh.mm.ss.
✔ The sampler only allows
When editing this parameter, treat each part of the time as a
changes to these param- separate field.
eters if it is in the Stop
Operating Mode (Section Cur Date The Cur Date parameter is the current local date expressed
5.3). as yy/mm/dd. When editing this parameter, treat each part of
the date as a separate field.
Set Flow The Set Flow parameter defines the flow rate (volumetric l/
min) at which the device draws a sample when it is in the
Sampling Operating Mode (Section 5.3). This is identical to
the Set Flow field in the Filter Setup Screen (Section 5.2).
Def Start The Def Start parameter sets the default start time (hh.mm)
of samples collected by the unit. The sampler uses this
parameter to simplify sample programming in the Filter
✔ The DefStart and DefDur Setup screen (Section 5.2). The default value of 0 causes
parameters simplify the sampling to begin at midnight by default.
definition of sampling
programs in the Filter Setup Def Dur The Def Dur parameter establishes the default sampling
Screen (Section 5.2).
duration (hh.mm) of samples collected by the Partisol unit.
The sampler uses this parameter to simplify sample pro-
gramming in the Filter Setup Screen (Section 5.2). The
default value of 24 causes the sampling duration to be 24
hours by default.
FTS Const m The FTS Constant parameter is the Streamline Flow Trans-
fer Standard "m" calibration constant. The Streamline FTS
can be used for verifying and calibrating the Partisol-FRM
sampler flow. The sampler uses this constant to convert flow
from inches H2O into l/min.
Soft Ver R&P increments the software version number when it issues
new releases of the Partisol-FRM operating software. Refer
to Appendix E for instructions to upgrade the system soft-
ware. This field is not editable.
Ser Num The Ser Num field contains a shortened version of the
sampler’s serial number or other identifying information.
✔ Password protection
prevents inadvertent
changes to system opera- The Setup Screen enables users to turn on password protection by pressing <F6:
tions. Passwd> when in the Browse Mode. Refer to Section 5.7 for instructions to turn
password protection on and off.
The Setup screen also provides users access to a variety of other hardware functions
such as system calibrations (Section 1), diagnostics (Section 7), RS232 setup (Section
9), and audits (Section 10).
The Filter Setup screen (Figure 5-2) provides a straightforward way for users to define
the sampling program to be executed by the sampler. Press <F1: FiltSet> when in the
Main screen (Figure 4-3) to enter the Filter Setup screen. Ensure that the sampler is
in the Stop Operating Mode (Section 5.3) before making any changes to the
parameters contained in this screen.
The Filter Setup screen contains the following fields to define the sampling program
✔ The sampler automati-
of the Partisol-FRM unit:
cally ensures that the
ending time/date is greater
than the beginning time/ Start Time The Start Time parameter defines the time of day (hh.mm)
date. It beeps if it makes at which sampling is to begin. When editing this parameter,
any adjustments to the treat each part of the time as a separate field.
user's inputs.
Start Date The Start Date parameter sets forth the date (yy/mm/dd) on
which sampling is to begin. When editing this parameter,
✔ Midnight is represented treat each part of the date as a separate field.
by time 0.
End Time The End Time parameter defines the time of day (hh.mm) at
which sampling is to end. When editing this parameter, treat
each part of the time as a separate field.
End Date The End Date parameter sets forth the date (yy/mm/dd) on
which sampling is to end. When editing this parameter, treat
each part of the date as a separate field.
Set Flow The Set Flow parameter determines the flow rate (volumet-
ric l/min) at which the hardware samples when in the
Sampling Mode (Section 5.3). This is identical to the Set
Flow field of the Setup screen (Section 5.2).
ID1, ID2 The Filter Setup screen contains two user-definable identi-
fication fields that are each 32 characters long. Use the
special Edit Mode function keys <F8: <-- > (Shift F3:) and
<F9: --> > (Shift F4::) to make changes to these fields. The
sampler stores these fields in each record of filter data
(Section 7.1).
A number of function keys in the Browse Mode simplify the process of defining the
✔ The Browse Mode sampling program:
function keys of the Filter
Setup screen simplify the
<F2: Next Hr> Pressing this key causes the sampler to revise the values of
programming of the
sampler. the Start Time, Start Date, End Time and End Date param-
eters. In this case, the start time and date are set so that the
unit begins sampling at the start of the next whole hour. It
automatically sets the ending time and date so that sampling
takes place for the period defined by Def Dur in the Setup
screen (Section 5.1).
<F3: NextDay> Pressing this key causes the sampler to revise the values of
the Start Time, Start Date, End Time and End Date param-
eters. In this case, these parameters are automatically set so
that the unit begins sampling at the time specified by Def
Start and samples for the period defined by Def Dur in the
Setup screen (Section 5.1). The unit uses the next available
time slot that meets these requirements.
<F4: + Day> Pressing this key advances the values of Start Date and End
Date by one day.
<F5: Set Def> Pressing this key causes the sampler to revise the Def Start
and Def Dur parameters of the Setup screen (Section 5.1) in
accordance with the starting time and sampling duration
currently set in the Filter Setup screen.
The Partisol-FRM Sampler displays its current operating mode in the upper right-
hand corner of the Main screen (Figure 4-3), as well as in the same position of certain
✔ Pressing <F4: Run/Stp>
in the Main screen toggles
other screens. Press <F4: Run/Stp> when in the Main screen to switch between the
the sampler between the non-sampling Stop Operating Mode and the sampling program execution modes
Stop Operating Mode and (Wait, Sampling, Done, Error).
the system's operational
states. The unit’s operating modes (Figure 5-3) are defined as follows:
Stop Mode In the Stop Operating Mode (STOP), the user exchanges
filter cassettes and defines the sampling program using the
Filter Setup screen. As this is the only non-operational
mode, all user-definable system parameters may be edited
with the sampler in this state. Pressing <F4: Run/Stp> in
the Main screen with the hardware in this mode causes the
sampler to advance to the Wait or Sampling Operating
Modes.
Wait Mode The Partisol system resides in this operating mode (WAIT)
until the user-defined starting time/date is achieved. At
that point, the device automatically enters the Sampling
Operating Mode and begins sample collection. Pressing
<F4: Run/Stp> in the Main screen with the hardware in
this mode causes the sampler to return to the Stop Operat-
ing Mode.
Sampling Mode While in this operating mode (SAMP), the sampler draws
ambient air through its sampling system at the volumetric
flow rate specified by the user (16.7 l/min by default).
Unless the sample flow rate deviates from its set point by
10% or more for more than 60 sec, sampling continues
until the ending time/date is reached. Pressing <F4: Run/
Stp> in the Main screen with the hardware in this mode
causes the sampler to return to the Stop Operating Mode.
Sample Collection
If the current time is between
Sampling (SAMP) the starting and ending time/
Operating Mode date, the device samples
ambient air.
Termination Conditions
In the absence of any status
conditions, the sampler enters
the Done Operating Mode after
the ending time/date is reached.
Otherwise, it enters the Error
Operating Mode.
Done Mode The sampler enters this mode (DONE) at the completion
of its sampling program if it encountered no status condi-
tions during sample collection (status code is “Ok”).
Pressing <F4: Run/Stp> in the Main screen with the
hardware in this mode causes the sampler to return to the
Stop Operating Mode.
Error Mode The sampler proceeds to this mode (ERR) at the comple-
tion of its sampling program if it encountered a status
condition during sample collection (status code is not
“Ok”), or if it encounters the flow rate deviation condition,
“X” (Section 6.1). Pressing <F4: Run/Stp> in the Main
screen with the hardware in this mode causes the sampler
to return to the Stop Operating Mode.
returning to this state, exchange the sample filter and define the sampling
program for the next filter to be exposed.
The sampler completes the information recorded for each exposed filter in the filter
storage buffer (Section 8.1) when the user returns the sampler to the Stop Operating
Mode from one of its operational modes (Wait, Sampling, Done, and Error).
• Anytime more than fifteen (15) minutes pass since the last keystroke was
entered on the keypad, the backlighting of the LCD (liquid crystal
display) dims. When this occurs, press any key to reactivate the screen’s
backlighting.
• If the sampler is left in the Edit Mode for more than five (5) minutes
without any user keystrokes, it automatically reverts to the Browse
Mode.
✔ The backlighting of the
LCD is turned off when the • Whenever the sampler remains in a screen other than the Main screen for
sampler is left unattended longer than fifteen (15) minutes without any user keystrokes, the hard-
for 15 minutes. ware automatically reverts to the Main screen.
The Partisol-FRM Sampler performs the following actions upon resumption of power
if the power failure occurs while the sampler is in its Sampling Operating Mode:
• If the power outage is longer than 60 sec, the hardware registers a “V”
✔ A large flow deviation status condition (Section 7.1) and stores the starting time of the power
spanning more than 60 failure in “hh.mm” format in the current record of filter data (Section 8.1).
seconds causes sampling to
be cut off prematurely. • If the ending time/date is not yet reached upon resumption of the power
supply, the sampler continues its sampling program in the Sampling
Operating Mode. Otherwise, it enters either the Done or Error Operating
Modes, depending upon the existence of any status conditions.
✔ Ensure that the sampler
is in the Stop Operating If the hardware is not in the Sampling Operating Mode at the time of the power failure,
Mode before turning off the the unit resumes operation in its pre-outage operating mode upon restoration of
power.
power.
With password protection turned on, the sampler restricts the user to the Main screen,
and does not allow entry into the Edit Mode.
Upon entering password protection, the unit jumps to the Main screen and does not
allow for any keypad interaction except for turning off password protection.
This section describes the steps involved in verifying sampler performance charac-
teristics prior to starting a sampling run, programming a sampling run and retreiving
data after a sampling run.
R&P recommends that the user perform the pre-sampling verification tests every
three months of routine operation and whenever the sampler is relocated. However,
individual monitoring organizations may abide by different standards.
NOTE: Refer to Section 6 of the U.S. EPA 2.12 Quality Assurance Handbook for
the U.S. EPA verification schedule requirements.
NOTE: Refer to Section 10 of this manual for more detailed information on
programming the sampler for performance verification.
1) Turn on the sampler by pressing the power switch on the main
panel to its “ON” position. The sampler must be in the Stop Mode
to perform the verification audits. If the sampler is not in the Stop
Mode, press <F4: Run/Stop> when in the Main screen.
2) Verify the sampler’s ambient temperature by pressing <F5: Setup>
to access the Setup screen, then press<F5:Audit> to access the
Audit screen (Figure 6-1). Determine the current ambient tem-
perature (°C) at the ambient temperature sensor using an external
thermometer. Verify that the value for the temperature displayed
by the Partisol-FRM in the Audit screen is within ±2 °C of the
measured temperature. If this is not the case, the sampler re-
quires calibration (Service Manual).
6) If you have a unit that supports the automatic leak check function
(Section 10), go to step 7. If you do not have a unit that supports
the automatic leak check function, go to Section 10.
7) Perform a leak check by pressing <F5: LeakCk>. Follow the in-
structions on the screen to begin the automatic leak check cycle.
(Turn off the manual shut off valve attached to the large air filter
on the left-hand side of the manifold in the hub. This corresponds
to location “A” in Figure 6.3. Wait for the automatic leak check
cycle to complete. The sampler will display a message at the end
of the cycle indicating the vacuum loss (mm Hg) during the 60
second leak check, and a pass or fail message. The criteria for a
successful leak test is a drop of less than 127 mm Hg in one
minute. Open the manual valve on the sampler then release the
vacuum (slowly) by opening the flow audit adapter valve. If the
leak check fails, refer to Section 10).
9) Press <F2: Pump>, then <F1: Valve>. If you are using the Stream-
line FTS, press <F1: Edit> then enter the pressure drop (inches
H2O), and then press the <ENTER> key. The Partisol-FRM will
calculate the flow in l/min. If you are not using the Streamline
FTS, determine the flow in actual (volumetric) l/min using the
external flow meter.
10) Verify either that the displayed Streamline FTS Flow or the mea-
sured flow is within ±5% of the value displayed in the “Flow Rate”
field of the Audit screen. If this is not the case, the sampler
requires calibration (Service Manual).
11) The performance verification is now complete. Return to the Main
screen by pressing the <ESC> key twice.
12) Restore the sampling hardware to its original state by removing
the flow metering hardware and reinstalling the PM-10 inlet on
the sample tube. Remove the filter cassette from the sampler and
discard the installed filter.
This section describes the procedures for programming the sampler for a sampling
run. A filter cassette with a 47 mm filter must be installed in the hardware before
starting the sampling run.
1) If the sampler is not in the Stop Mode, press the <RUN/STOP> key
when in the Main screen to enter the Stop Mode.
2) Press <F5:Setup> to access the Setup screen.
3) Confirm that the correct time, date and set flow rate are displayed
on the Setup screen. If the correct time, date and set flow rate are
not displayed, re-set the sampler by pressing <F1: Edit>, then
enter the correct data using the keypad. Press the <ENTER> key.
4) Press the <ESC> key to return to the Main screen, then
<F1:Setup> to enter the Filter Setup screen (Figure 6-5).
5) Press <F1:Edit>, then enter the sample run start time and start
date, end time and end date, (and ID1 and ID2 if desired). Press
the <ENTER> key. Press the <ESC> key to return to the Main
screen.
6) Press the <RUN/STOP> key. The sampler should now enter the
Wait Mode. Verify that the correct sampler run data (start time
and date, etc.) is displayed on the Main screen.
7) When the clock time equals the sample start time, the sampler will
automatically enter the Sampling Mode and begin the sampling
run.
8) When the clock time equals the sample stop time, the sampler will
automatically end the sampling run, and enter the Done Mode. If
a status condition occurred during the sampling run, the Error
Mode will display instead of the Done Mode.
9) Press <F4: Run/Stop> to enter the Stop Mode before exchanging
filter cassettes or retrieving data on the sampling run.
This section describes the procedures for verifying the sampling run status and
retrieving the sampling run data.
Follow these steps to verify the sampling run and retrieve data from the
unit:
5) If there were any status codes other than “OK,” verify the validity
of the sampling run from the output of the Filter Data screen.
Press <F4: PwrDat> to view the Power Outage Data screen. Press
the <ESC> key to return to the Filter Data screen.
6) Download stored data from the sampling run onto a personal
computer (PC). Connect the PC to the sampler with the 9 pin-to-9
pin RS232 connector cable.
7) Use AKCOMM or any other data transfer program to transfer data
from the sampler to the PC.
8) Ensure that the sampler is in the Browse Mode.
9) When in the Filter Data screen, use the function keys <F1> to <F8>
to move to the first record of the sampling run. Press the <F5>
function key to access the <F10: Output> function key. All data
from the current record displayed in the screen to the last record
will automatically download from the sampler to the PC.
10) Press <F5:IntvDat> to access the Interval Data screen (Figure 6-8).
Use the function keys to move to the first record that you wish to
download. Press the <F5> function key to access the <F10:
Output> function key. All interval data from the current record
displayed in the screen to the last record will automatically
download from the sampler to the PC.
This section describes the status codes generated by the Partisol-FRM Sampler, as
well as the operating information contained in the Statistics and Diagnostics screens.
The sampler displays operational status codes in the upper left-hand corner of the
Main screen (Figure 4-3) next to “Stat,” as well as on several other screens. The
hardware resets the status to “Ok” (no current conditions) after the user presses <F4:
Run/Stp> from the Main screen to return the unit to the Stop Operating Mode.
With the occurrence of any status conditions, the sampler displays the single-letter
abbreviation for each flag that applies. The following list details the system’s status
codes and definitions:
X Flow Cutoff. The measured sample flow rate deviates by more than
10% from its set point for more than 60 sec.
✔ A heater in the instru- I Instrument Electronics Temperature. The temperature of the instru-
ment electronics ment electronics is outside of its usual operating range (less than
compartment ensures that
the control zone stays within -5 °C or greater than 60 °C).
limits under cold tempera-
ture conditions. V Power Outage (Voltage). A power outage of greater than 60 seconds
occurred during sample collection.
E Elapsed Sample Time. The elapsed time of the sample was less than
23 hours or greater than 25 hours.
✔ The current status code In the case of multiple status conditions, the sampler displays the single-letter
is made up of one or more
abbreviation of all applicable flags in the status field of the Main screen and other
single-letter abbreviations
or “Ok.” screens with a status condition field. For example, the sampler would display “FV”
in the case of simultaneous flow rate and power outage conditions.
The hardware stores all status conditions that apply to each exposed filter in the filter
data storage buffer (Section 8.1).
The Statistics screen (Figure 7-1) displays more detailed operational information than
is shown on the sampler’s Main screen. Press <F2: Stats> when in the Main screen to
display the Statistics screen. This screen does not contain any editable fields.
Current Time The current time and date, as determined by the system’s
battery-backed clock. The user may reset the time/date in the
Setup Screen (Section 5.1) in the Stop Operating Mode.
Filt Fan The current operating status of the fan in the filter compart-
ment (ON or OFF).
Encl Fan The current operating status of the fan in the pump compart-
ment (ON or OFF).
Press the <ESC> key to return to the Main screen from the Statistics screen.
The Diagnostics screen (Figure 7-2) displays more low-level operational information
about the Partisol-FRM Sampler. When in the Main screen, press <F5: Setup> and
then <F3: Diag> to display the Diagnostics screen. The Service Manual (42-004278)
of the Partisol-FRM Sampler contains routines that make use of the Browse and Edit
Mode function keys of the Diagnostics screen.
Pres The current analog input level (VDC) from the ambient
pressure sensor.
InsT The current analog input level (VDC) from the instrument
electronics temperature sensor.
AmbT The current analog input level (VDC) from the ambient
temperature sensor.
3 Not used.
FltT The current analog input level (VDC) from the filter tem-
perature sensor.
Flow The current analog input level (VDC) from the mass flow
sensor.
A/O1 The current analog output level (VDC) to the valve in the
mass flow controller.
A/O2 The current analog output level (VDC) to the user analog
output port on the back of the sampler (Section 8).
Val The current position of the flow cutoff valve (ON or OFF).
FnF The current operating status of the fan in the filter compart-
ment (ON or OFF).
FnP The current operating status of the fan in the pump compart-
ment (ON or OFF).
When in the Diagnostics screen, press the <ESC> key twice to return to the Main
screen.
✔ The Partisol-FRM The Partisol-FRM Sampler stores two types of data in its internal data logger: filter
Sampler has a capacity of data and interval data. This information is stored in two separate circular buffers
25 filter data records and
two weeks of interval data whose contents can be viewed on the screen of the sampler and/or downloaded
records. Data are stored in through the RS232 port. Once these buffers are filled, the oldest data points are
a circular buffer on a “first replaced with the most recent information (“first in, first out”). The following
in, first out” basis. describes the two types of data stored internally in the hardware:
Press <F3: Data> when in the Main screen (Figure 4-3) to access the Filter Data screen
(Figure 8-1). From this screen, enter <F4: PwrDat> to view additional data for the
current record of interval data in the Power Outages screen (Figure 8-2). Press <F4:
FiltDat> when in the Power Outages screen to return to the Filter Data screen.
Press <F5: IntvDat> when in the Filter Data screen to view the Interval Data screen
(Figure 8-3), or press <F5: FiltDat> when in the Interval Data screen to return to the
Filter Data screen. With the exception of the Power Outages screen, the sampler
displays the last record of the respective database when the user enters the screens.
There are no editable fields in any of these displays.
Data for each filter used in the Partisol-FRM Sampler are stored as a separate record
of filter data. For readability, the sampler splits the display of filter data records
between two screens: the Filter Data screen (Figure 8-1) and the Power Outages screen
(Figure 8-2). Press <F4> to toggle between these two screens while remaining in the
same filter data record.
The sampler displays the following filter data fields in the Filter Data screen:
AveFlow The unit shows the average volumetric flow rate (l/
min) during the sampling period in the AveFlow
field.
The Power Outages screen (Figure 8-2) contains the following additional information
for each record of filter data:
ID1, ID2 The ID1 and ID2 fields display the user-defined
information entered prior to sampling in the Filter
Setup Screen (Section 5.2).
The soft keys of the Filter Data screen and Power Outages screen have the following
effects upon the location of the viewing pointer:
Pressing <F10: Output> when in the Filter Data screen allows the user to download
records from the current position of the viewing pointer to the last record of the
database through the RS232 port of the Partisol-FRM Sampler. Press <F10: Output>
again to interrupt the downloading of information before reaching the last record.
Refer to Section 8.3 for a detailed discussion of this downloading feature.
The sampler displays the following information in the Interval Data screen:
Amb Temp The Amb Temp field displays the five-minute aver-
age of the ambient temperature (°C).
Filt Temp The Filt Temp field displays the five-minute aver-
age of the filter temperature (°C).
Amb Pres The Amb Pres field displays the five-minute aver-
age of the ambient pressure (mm Hg).
The soft keys of the Interval Data screen have the following effects upon the location
of the viewing pointer (remember to use the shift key to access F6-F10):
Pressing (Shift ,F:5>) <F10: Output> when in the Interval Data screen allows the user
to download records from the current position of the viewing pointer to the last record
of the database through the RS232 port of the Partisol-FRM Sampler. Press <F10:
Output> again to interrupt the downloading of information before reaching the last
record. Refer to Section 8.3 for a detailed discussion of this downloading feature.
The Filter Data screen (Figure 8-1) and Interval Data screen (Figure 8-3) contain the
<F10: Output> key to download stored data through the sampler’s RS232 port to
another serial device.
R&P supplies the Partisol-FRM Sampler with AKCOMM software (41-004001) and
a 9-to-9 pin computer cable (07-000587) to enable the creation of data files containing
stored information on a personal computer. The AKCOMM software diskette
contains an instructional data file describing the program’s use. Alternately, other
commercially-available software may be used to receive and store transferred
information on a personal computer (PC).
Attach the ends of the 9-to-9 pin computer cable to the RS232 port of the Partisol-FRM
Sampler and the RS232 connector of a PC to link the two devices. Then ensure that
the Baud Rate, Config and XON/XOff Cont RS232 parameters displayed in the
RS232 Setup screen (Section 9.2) are appropriately defined for the software being
employed.
✔ Pressing <F10: Output> The <F10: Output> keystroke allows the user to download records from the current
while in the Filter Data or position of the viewing pointer to the last record when in the Filter Data screen (Figure
Interval Data Screen is a
convenient way to download 8-1) or Interval Data screen (Figure 8-3). Pressing <F10: Output> again prior to
stored information. completing the download cancels the data transfer.
The following text describes the format of the fields contained in each record of filter
and interval data downloaded by the sampler.
Each record of filter data contains the comma-delimited data fields shown below.
Records are separated from each other by the “carriage return” (ASCII 013) and “line
feed” (ASCII 010) characters.
ID1 (“ ” or “xx”)
ID2 (“ ” or “xx”)
Set Start Date ("yy/mm/dd")
Set Start Time (hh.mm)
Actual Start Date ("yy/mm/dd")
Actual Start Time (hh.mm)
Set Stop Date ("yy/mm/dd")
Set Stop Time (hh.mm)
Total Sample Time (hh.mm)
Average Flow Rate (l/min)
Flow Coefficient of Variation (%)
Sampled Volume (m³)
Minimum Ambient Temperature (°C)
Average Ambient Temperature (°C)
Maximum Ambient Temperature (°C)
Minimum Filter Temperature (°C)
Average Filter Temperature (°C)
Maximum Filter Temperature (°C)
Minimum Ambient Pressure (mm Hg)
Average Ambient Pressure (mm Hg)
Maximum Ambient Pressure (mm Hg)
Maximum Temperature Differential (°C)
Date of Maximum Temp Differential ("yy/mm/dd")
Time of Maximum Temp Differential (hh.mm)
Status Codes (“xxx”)
✔ The sampler includes the Beginning Time of Power Interruption 1 (hh.mm), see below
status codes field and/or Beginning Time of Power Interruption 2 (hh.mm), see below
power interruption fields
Beginning Time of Power Interruption 3 (hh.mm), see below
only for the number of
events that occurred. Beginning Time of Power Interruption 4 (hh.mm), see below
Beginning Time of Power Interruption 5 (hh.mm), see below
Beginning Time of Power Interruption 6 (hh.mm), see below
Beginning Time of Power Interruption 7 (hh.mm), see below
Beginning Time of Power Interruption 8 (hh.mm), see below
Beginning Time of Power Interruption 9 (hh.mm), see below
Beginning Time of Power Interruption 10 (hh.mm), see below
The number of fields in each record of filter data varies, depending upon the number
of status codes and/or power interruptions recorded. If the sampler did not experience
any status codes or power interruptions during sampling, the sampler omits all of the
status codes and power interruption fields. Otherwise, filter data records contain fields
for only the number of status codes and/or power interruptions encountered.
Each record of interval data contains the comma-delimited data fields shown below.
Records are separated from each other by the “carriage return” (ASCII 013) and “line
feed” (ASCII 010) characters.
This section describes the continuous analog voltage signal generated by the Partisol-
FRM Sampler to indicate flow rate and the existence of any status conditions, as well
as the setup of the hardware’s RS232 interface. The bidirectional AK communication
protocol (Appendix D) implemented in the sampler’s RS232 port allows users to
retrieve the current values of system variables, set new values for operating param-
eters, as well as retrieve stored filter and interval data (Section 8).
✔ The sampler’s analog The four-pin connector on the back panel of the Partisol-FRM Sampler labeled “User
voltage output provides a Output” transmits a continuous 0-5 VDC analog voltage signal whose level reflects
continuous feedback of the
unit's current sample flow
the current sample flow rate and the existence of any status conditions. The voltage
rate and status condition. output is determined in the following manner:
Appendix C details the pin assignments of the four-pin User Output connector, as well
as the assembly diagram for the mating connector (06-002453) supplied with each
sampler.
The settings in the RS232 Setup screen (Figure 9-1) define the hardware and software
configuration of the system’s RS232 port. When in the Main screen, press <F5:
Setup> and then <F4: RS232> to display the RS232 Setup screen. The fields of this
screen are editable in any of the unit’s operating modes.
Appendix C contains a listing of the pin assignments of the sampler’s 9-pin RS232
port.
The RS232 Setup screen (Figure 9-1) contains the following user-definable fields.
Baud Rate This is the data transmission rate (baud, bits per second).
Use the <F2: -> and <F3: +> keys to select the appropriate
✔ The Baud Rate, Config baud rate when in the Edit Mode. The default setting of this
and XOn/XOff Cont param-
parameter is 9600.
eters must match the
settings of the personal
computer or other serial Config This parameter represents the data transfer format (data
device connected to the bits-parity-stop bits). Use the <F2: -> and <F3: +> keys to
sampler. select between “8-N-1” and “7-E-1”when in the Edit
Mode. The default setting of this parameter is “8-N-1” (8
stop bits, no parity, 1 stop bit).
XOn/XOff Cont The user may turn software data flow control on or off by
pressing the <F2: -> and <F3: +> keys when in the Edit
Mode. The default setting of this parameter is “OFF.”
AK Station This is the ASCII code for the one-digit Station Number
✔ The sampler only uses used by the AK Protocol (Appendix D). The default value
the AK Station, AK Channel of this parameter in the sampler and AKCOMM software
and AK Append parameters
when using the AK Protocol
is 52, which is the ASCII representation for “4.” This
described in Appendix D. parameter is not used when performing the data down-
loading described in Section 7.3.
The Baud Rate, Config, and XOn/XOff Cont parameters above not only define data
transmission when using the AK Protocol, but are also used by the Partisol-FRM
Sampler when downloading data directly from the Filter Data screen and Interval Data
screen (Section 8.3).
This section describes the routine maintenance and performance verification proce-
dures required to maintain the consistent operation of the Partisol-FRM Sampler.
Upper and lower cassette Inspect the seals that rest against the filter cassette
seals every time a filter is exchanged. Wipe the seals with
a clean dry cloth as required. Inspect the seals once
a year for drying and cracking, and replace them if
necessary (22-002182).
External leak check Perform an external leak check after every 5 days of
inlet usage (Section 10.2.4).
Internal leak check Perform an internal leak check after every 4 weeks
or every month of inlet usage (Section 10.2.6).
WINS PM-2.5 impactor Clean the greased impactor section of the WINS
PM-2.5 impactor after every 5 days of inlet usage
(Appendix H.2). The impactor must be cleaned
when the unit is not sampling.
PM-10 inlet Clean the PM-10 inlet after every 14 days of inlet
usage (Appendix H.1). The inlet must be cleaned
when the unit is not sampling.
Large in-line filter Exchange the large in-line filter in the sampler every
six months of operation (32-002643). Turn off the
sampler (Section 5.4) to replace the large in-line
filter.
Air screens Clean the air screens located under the sampler’s
rain hoods every 6 months of operation.
Battery voltage Check the voltage level of the batteries on the main
computer board in the electronics compartment
every six months (Appendix F.1).
R&P recommends that the user perform the routine maintenance procedures de-
scribed in Section 10.1 at the same time as the audits explained below.
NOTE: The user can access the Audit screen (Figure 10-1)
only when the sampler is in the Stop Operating Mode. Refer
to Section 5.3 for an explanation of the sampler’s operating
modes.
NOTE: Refer to Section 6 of the U.S. EPA 2.12 Quality Assurance Handbook for
further information on the ambient temperature sensor audit.
1) When in the Setup screen, press <F5: Audit> to display the Audit
screen (Figure 10-1).
NOTE: Refer to Section 6 of the U.S. EPA 2.12 Quality Assurance Handbook for
further information on the filter temperature audit.
1) When in the Setup screen, press <F5:Audit> to display the Audit
screen (Figure 10-1)
2) Determine the current temperature (°C) at the location of the
sample filter in the Partisol-FRM Sampler using an external
thermometer (°C = 5/9 x (°F - 32)).
3) Verify that the value for temperature displayed as “Filter Temp”
in the Audit screen is within ±2° C of the measured temperature.
If this is not the case, perform the filter temperature calibration
procedure (Section 11).
1) When in the Setup screen, press <F5: Audit> to display the Audit
screen (Figure 10-1).
2) Determine the current ambient station pressure in mm Hg (abso-
lute pressure, not corrected to sea level).
• To convert from Atmospheres @ 0 °C to mm Hg, multiply by 760.
• To convert from millibars to mm Hg, multiply by 0.75012.
• To convert from inches Hg @ 32 °F to mm Hg, multiply by 25.4.
3) Verify that the value for “Ambient Pres” in the Audit screen is
within ±10 mm Hg of the measured ambient pressure. If this is
not the case, perform the ambient pressure calibration procedure
(Section 11).
Although the Audit screen (Figure 10-1) contains a <F5: LeakCk> soft function key,
your Partisol-FRM Sampler may not support the automatic leak check function.
Follow the instructions in Section 10.2.4.1 to determine whether your unit supports
this function.
1) When in the Setup screen, press <F5: Audit> to display the Audit
screen (Figure 10-1).
2) Remove the PM-10 inlet from the sampler.
3) Install a filter cassette containing a new 47 mm filter into the unit.
4) Install the flow audit adapter (Figure 10-2) (57-000618) onto the end
of the sample tube of the sampler. Ensure that the valve on the flow
audit adapter is in the open position. .
.
Figure 10-2. Flow audit
adapter installed onto the
end of the sample tube.
5) Press the <F5: LeakCk> soft function key. If the sampler does not
support the automatic external leak check function, it will display a
“System does not support auto leak check” message (Figure 10-3).
If your sampler displays this message, go to Section 10.2.4.2. If the
sampler does support an automatic external leak check function, go
to step 6.
10) Press the <ENTER> key. The system will now pull a vacuum and
begin a 30 second leak check cycle. At the end of the cycle, a “Leak
Check Pass” or “Leak Check Fail” message will display on the
screen. If the leak check fails, the unit will display the actual measure
of vacuum loss. The pass criteria is a loss of 15 inches (381 mm Hg)
or less. If the leak check fails, go to step 11. If the leak check passes,
go to step 12.
11) Replace the filter cassette with a new filter cassette and repeat the
leak check procedure. If the leak check fails a second time, refer to
Section 11.
12) Open the flow controller manual valve that you closed in step 9.
13) Slowly open the valve of the flow audit adapter.
14) If you will be performing a flow audit (Section 10.2.5) immediately,
go to Section 10.2.5. If you will not be performing a flow audit, go to
step 15.
15) Remove the flow audit adapter from the end of the sample tube.
16) Install the PM-10 inlet onto the end of the sample tube.
17) Remove the filter cassette from the sampler and discard the
47mm filter used during the external leak check.
1) When in the Setup screen, press <F5: Audit> to display the Audit
screen (Figure 10-1).
2) Remove the PM-10 inlet from the sampler.
3) Install a filter cassette containing a new 47 mm filter into the unit.
4) Install the flow audit adapter (Figure 10-2) (57-000618) onto the end
of the sample tube of the sampler. Ensure that the valve on the flow
audit adapter is in the open position.
5) Press <F2: Valve>.
6) Press <F3: Pump>.
7) Turn the valve on the flow audit adapter to its closed position (Figure
10-2).
8) Shut off the flow to the flow controller assembly by turning the
manual shut-off valve (flow control manual valve) that is attached to
the large air filter on the left-hand side of the manifold in the hub.
This corresponds to location “A” in Figure 10-4.
9) Watch the vacuum gauge and record the reading on the vacuum
gauge when it becomes stable. The gauge should read at least 15
inches H2O (381 mm Hg).
10) Shut off the flow to the pump by turning the other manual shut-off
valve (pump manual valve) located on the bottom of the manifold in
the hub.
11) Press <F3: Pump>.
12) Record the reading on the vacuum gauge. This reading should not
drop by more than 8.5 inches Hg during this 30 second period. This
corresponds to a leak of 80 ml/min. If the reading does drop by more
than 8.5 inches Hg during this 30 second period, trace the internal
(and external) flow paths to identify problems in tubing or connec-
tions.
13) Open the flow controller manual valve and pump manual valve that
you closed in steps 8 and 10.
14) Slowly open the valve of the flow audit adapter.
15) Press <F2: Valve>.
Perform the ambient temperature audit (Section 10.2.1), filter temperature audit
(Section 10.2.2), pressure audit (Section 10.2.3) and external leak check (Section
10.2.4) before executing the flow audit procedure.
1) When in the Setup screen, press <F5: Audit> to display the Audit
screen (Figure 10-1).
2) Install a filter cassette containing a 47 mm filter into the hard-
ware. This filter will be thrown away at the end of this flow audit.
3) Remove the PM-10 inlet from the end of the sample tube.
4) If you are using the Streamline Flow Transfer Standard (FTS) to
audit the flow of the Partisol-FRM Sampler, go to step 5. If you
are not using the Streamline FTS to audit the flow of the Partisol-
FRM Sampler, go to step 13.
5) Press the <ESC> key to display the Setup screen.
6) When in the Setup screen, press <F1:EDIT>.
7) Press the down (<↓>) arrow to display the “FTS CONST m” field.
(<↓
8) Locate the “m” constant on the FTS Calibration sheet, and enter
it into the “FTS CONST m” field.
9) Press the down (<↓>) arrow to display the “FTS CONST b” field.
(<↓
10) Locate the “b” constant on the FTS Calibration sheet, and enter it
into the “FTS CONST b” field.
11) Press the <ENTER> key.
12) Press <F5: Audit> to display the Audit screen. Go to step 13.
13) If you are using the Streamline FTS to audit the flow of the
Partisol-FRM Sampler, install the Streamline FTS onto the end of
the sample tube (Figure 10-5). If you are not using the Streamline
FTS to audit the flow of the Partisol-FRM Sampler, you may need
to install the flow audit adapter (57-000618) onto the end of the
sample tube (Figure 10-2). If you will be using the flow audit
adapter, ensure that you install it onto the end of the sample tube
with its valve in the open position.
21 Verify that the flow rate measured on the flow meter matches the
sampler’s original flow design value (16.7 l/min) to within ±5%. If
the flow rate measured on the flow meter matches the sampler’s
original flow design value (16.7 l/min) to within ±5%, go to step
22. If the flow rate measured on the flow meter does not match
the sampler’s original flow design value (16.7 l/min) to within
±5%, calibrate the external flow meter.
22) Return to the Main screen by pressing the <ESC> key twice.
23) Remove the flow metering hardware.
24) Install the PM-10 inlet onto the end of the sample tube.
25) Remove the filter cassette from the sampler and discard the 47
mm filter.
1) Clean the filter cassette with a clean cloth and alcohol to remove
any oil or other material.
2) Insert a leak check disk (36-004768) into the filter cassette.
3) Install the filter cassette into the sampler and push on the handle
to move the filter cassette into the sampling position.
4) When in the Setup screen, press <F5: Audit> to display the Audit
screen (Figure 10-1).
5) Press <F2: Valve>.
6) Press <F3: Pump>.
7) Shut off the flow to the flow controller assembly by turning the
manual shut-off valve (flow control manual valve) that is attached to
the large air filter on the left-hand side of the manifold in the hub.
This corresponds to location “A” in Figure 10-4.
8) Record the reading on the vacuum gauge.
9) Shut off the flow to the pump by turning the other manual shut-off
valve (pump manual valve) located on the bottom of the manifold in
the hub.
10) Press <F3: Pump>.
11) Record the reading on the vacuum gauge. This reading should not
drop by more than 8.5 inches Hg during this 30 second period. This
corresponds to a leak of 80 ml/min. If the reading does drop by more
than 8.5 inches Hg during this 30 second period, trace the internal
flow paths to identify problems in tubing or connections.
12) Press <F2: Valve>.
13) Open the flow controller manual valve and pump manual valve that
you closed in steps 7 and 9.
14) Slowly open the valve of the flow audit adapter.
15) Remove the flow audit adapter from the end of the sample tube.
16) Install the PM-10 inlet onto the end of the sample tube.
17
17)) Remove the filter cassette from the sampler.
18
18)) Remove the leak check disk from the filter cassette.
This section contains instructions for performing an interface board, ambient tem-
perature, filter temperature, ambient pressure, and flow calibration of the Partisol-FRM
Sampler. The temperature and pressure calibrations must be done before the flow
calibration.
2) Locate the test point labeled “+6V” in the front section of the
interface board (Figure 11-2), and the “+2.5V” and “+10V” test
point in the back part. All three test points are red.
3) Locate the black ground test point labeled “GND” in the front
portion of the interface board.
4) Ensure that the sampler is turned on and that the display back-
light is on. The backlight must be on during the +6 V calibration.
If the backlight is off, press any key on the keypad to turn it on.
5) Place the positive lead of a multimeter on the +6 V test point.
6) Place the ground lead on the ground test point.
7) Locate R21 on the rear section of the interface board. R21 is a
horizontal pot, and its designation “R21” is silk-screened on the
board.
8) Adjust R21 until the multimeter reads 6.00 VDC ± 0.05 V.
9) Place the positive lead on the +2.5V test point.
10
10)) Locate R53 on the rear section of the interface board. R53 is a
blue vertical pot, and its R53 designation is silkscreened on the
board.
11) Adjust R53 until the multimeter reads 2.500 VDC ± 0.002 V
12) Place the positive lead of the multimeter on the +10 V test point.
13) Locate R44 on the rear section of the interface board. R44 is a
blue vertical pot, and its designation “R44” is silk-screened on
the board.
14) Adjust R44 until the multimeter reads 10.000 VDC ± 0.002 V.
Please note that the following procedure must be performed after the interface board
calibration and before the temperature, pressure and flow calibrations.
Placement of positive
lead for analog input
calibration test point
PWM1.
8) Press <F1: Edit> to enter the Edit Mode. Enter a number between
“0.050” and “0.150” volts and press the <ENTER> key.
9) Watch the value displayed in the row labeled “A/I,” under the
column labeled “Calc.” Ensure that this value does not vary by
more than ±0.005 volts after watching it for 5 seconds. If this
number is not stable, choose a new number for “A/O” between
“0.050” and “0.150” volts.
10) Read the voltage displayed on the multimeter.
11) Using the arrow keys, position the cursor so that it is in the row
labeled “A/I” under the column labeled “Act.”
12) Press <F1: Edit> to enter the Edit Mode. Enter the voltage reading
from the multimeter (to three digit accuracy, i.e., 0.xxx) in this
position and press the <ENTER> key. The unit will now calculate
the “Offset” value.
13) Ensure that the value now displayed in the row labeled “A/I”
under the column labeled “Calc” matches the value displayed on
the multimeter, within ±0.005 volts.
14) Using the arrow key, position the cursor so that it is in the “A/O”
field.
15) Press <F1: Edit> to enter the Edit Mode. Enter a number between
“4.800” and “4.900” volts and press the <ENTER> key.
16) Observe the value displayed in the row labeled “A/I” under the
column labeled “Calc.” Ensure that this value does not vary by
more than ±0.005 volts after watching it for 5 seconds. If this
number is not stable, choose a new number for “A/O” between
“4.800” and “4.900” volts.
17) Read the voltage displayed on the multimeter.
18) Using the arrow keys, position the cursor so that it is in the row
labeled “A/I” under the column labeled “Act.”
19) Press <F1: Edit> to enter the Edit Mode. Enter the voltage reading
from the multimeter (to three digit accuracy, i.e., 0.xxx) in this
position and press the <ENTER> key. The unit will now calculate
the “Span” value.
20) Ensure that the value now displayed in the row labeled “A/I”
under the column labeled “Calc” matches the value displayed on
the multimeter within ±0.005 volts.
21) Remove the multimeter leads from the interface board, and the
analog input calibration cable from the back of the electronics
compartment.
22) After the user has performed the analog input calibration, they
must now perform the temperature, pressure and flow calibra-
tions.
NOTE: If the instrument has been reset and you have recorded the “Offset” and
“Span” values for the flow, you may enter these numbers directly when in the
Edit Mode.
NOTE: Refer to the U.S. EPA 2.12 Quality Assurance Handbook, Section 6.
1) Return the sampler to the Main screen (Section 4.3).
2) The device must be in the Stop Operating Mode (Section 5.3) to
perform an ambient temperature calibration.
3) When in the Main screen, press <F5: Setup> and <F2: Calib> to
display the Calibration screen (Figure 11-3).
4) Determine the current temperature (°C) at the ambient tempera-
ture sensor using an external thermometer, [°C = 5/9 x (°F - 32)].
5) Press <F1: Edit> to enter the Edit Mode, and move the cursor to
the row labeled “AmbT” under the “Act” (actual) column.
6) Enter the current ambient temperature (°C) and press the <EN-
TER> key. If necessary, use the <F6: +/-> key (Shift F1>) to enter
negative temperatures when in the Edit Mode.
7) Upon receiving the actual temperature, the system’s microproces-
sor automatically computes the “Span” value for the ambient
temperature. Record this value for future reference.
NOTE: If the instrument has been reset and you have recorded the “Span” value
for the ambient temperature, you may enter it directly in the “Span” column when
in the Edit Mode.
NOTE: Refer to the U.S. EPA 2.12 Quality Assurance Handbook, Section 6.
1) Return the sampler to the Main screen (Section 4.3).
2) The device must be in the Stop Operating Mode (Section 5.3) to
perform a filter temperature calibration.
3) When in the Main screen, press <F5: Setup> and <F2: Calib> to
display the Calibration screen (Figure 11-3).
4) Determine the current temperature (°C) at the location of the
sample filter in the Partisol-FRM Sampler using an external
thermometer, [°C = 5/9 x (°F - 32)].
5) Press <F1: Edit> to enter the Edit Mode, and move the cursor to
the row labeled “FltT” under the “Act” (actual) column.
6) Enter the current filter temperature (°C) and press the <ENTER>
key. If necessary, use the <F6: +/-> key to enter negative tempera-
tures when in the Edit Mode.
7) Upon receiving the actual temperature, the system’s microproces-
sor automatically computes the “Span” value for the filter
temperature. Record this value for future reference.
NOTE: If the instrument has been reset and you have recorded the “Span” value
for the filter temperature, you may enter it directly in the “Span” column when
in the Edit Mode.
NOTE: Refer to the U.S. EPA 2.12 Quality Assurance Handbook, Section 6.
1) Return the sampler to the Main screen (Section 4.3).
2) The device must be in the Stop Operating Mode (Section 5.3) to
perform an ambient pressure calibration.
3) When in the Main screen, press <F5: Setup> and <F2: Calib> to
display the Calibration screen (Figure 11-3).
4) Determine the current ambient station pressure in mm Hg (abso-
lute pressure, not corrected to sea level).
• To convert from Atmospheres @ 0 °C to mm Hg, multiply by 760.
• To convert from millibars to mm Hg, multiply by 0.75012.
• To convert from inches Hg @ 32 °F to mm Hg, multiply by 25.4.
5) Press <F1: Edit> to enter the Edit Mode, and move the cursor to
the row labeled “Pres” under the “Act” (actual) column.
6) Enter the current ambient pressure (mm Hg) and press the <EN-
TER> key.
7) Upon receiving the actual pressure, the system’s microprocessor
automatically computes the “Span” value for the ambient pres-
sure. Record this value for future reference.
NOTE: If the instrument has been reset and you have recorded the “Span” value
for the ambient pressure, you may enter it directly in the “Span” column when
in the Edit Mode.
The temperature and pressure calibrations described above must be performed before
performing the flow calibration. In addition, the leak check discussed in Section 9.2.4
must also be undertaken before executing the following instructions.
The Partisol-FRM Sampler supports both a single-point and five-point flow calibra-
tion routine (refer to the U.S. EPA 2.12 Quality Assurance Handbook, Section 6).
R&P recommends that the user perform the flow calibration whenever the sampler has
been transported, any electromechanical maintenance has been done, or the sampler
flow deviates from the set flow by ±5%. The sampler should be calibrated at least once
per calendar year.
NOTE: If the instrument has been reset and you have recorded the “Offset” and
“Span” values for the flow, you may enter these numbers directly when in the Edit
Mode.
22) When in the Flow Calibration screen, wait for the “Current Flow”
value to stabilize at each of these levels (16.7, 17.5, 15.8, 18.3 and
15.0 l/min). When “Current Flow” value stabilizes at each of these
levels, press <F1: Edit>, move the cursor to the “Actual Flow”
field, and enter the flow rate displayed by the external flow meter.
Then press the <ENTER> key. The sampler uses this information
to compute the proper flow span value. Go to step 23.
NOTE: If the instrument has been reset and you have recorded the “Offset” and
“Span” values for the flow, you may enter these numbers directly when in the Edit
Mode.
23) Return to the Main screen by pressing the <ESC> key three times.
24) Restore the sampling hardware to its original state by removing
the flow metering hardware and reinstalling the PM-10 inlet on
the sample tube. Remove the filter cassette from the sampler,
and discard the installed filter.
✔ Use great care when The Title screen (Figure 12-1) provides the user access to the unit’s reset functions
performing the reset (Section 4.2). With this screen displayed on the instrument, the user can initiate reset
commands described in this
section.
functions by making use of the function keys in the manner described below. The user
should exercise these capabilities with care, as information can be lost inadvertently
if making an improper choice.
Pressing <F1: RDefs> with the Title screen displayed (Figure 12-1) causes the
sampler to reset its operating parameters to their default settings. The system
generates a single beep after the Title screen disappears to confirm that it has executed
this command.
Pressing <F3: HReset> twice with the Title screen displayed (Figure 12-1) performs
the function of both the <F1: RDefs> and <F2: RData> keys above, and additionally
resets the system’s EPROM. The sampler generates three beeps after the Title screen
disappears to confirm that it has executed this command. As a safeguard, the <F3:
HReset> key must be pressed twice with the Title screen displayed to reset the
hardware.
Pressing <F4> twice with the Title screen displayed sets the current password
protection to “off.” This can be useful if the user has misplaced the code used to turn
on password protection, or if the user encounters any difficulties in turning password
protection off. The sampler beeps four times upon successful deactivation of pass-
word protection.
This appendix contains all the instrument software screens displayed by the Partisol-
FRM Sampler, along with the hierarchy of screens.
Title Screen
Main Screen
Power Outages
Screen
Interval Data
Screen
Flow Calibration
Screen
This appendix contains a listing of the most important program register codes (PRCs)
used in the software of the Partisol-FRM Sampler. The user would use these codes
when using the hardware’s two-way serial communication capability (Appendix D)
to request the current value of variables, to change the value of certain system
parameters, and to download data from the sampler’s internal data logger.
13 Ambient Pressure (5-min average) mmHg N/A N/A N/A not editable
16 Current Flow Rate (5-min average) l/min N/A N/A N/A not editable
Program register codes (PRCs) whose values are defined by codes are detailed below.
The Partisol-FRM Air Sampler contains two connectors for communicating analog
and serial information with external devices:
Figure C-1. Pin assign-
ments of user output User Output This 4-pin connector, located on the back panel of
connector. the sampler, transmits an analog voltage level in
accordance with the current flow rate and the exist-
ence of any status conditions (Section 8). The pin
layout, as viewed from the end of the connecting
cable, is shown in Figure C-1 and is defined below:
The connection between the RS232 connector and a personal computer is accom-
plished using a straight 9-to-9 pin cable that R&P supplies as part of the sampler’s
basic configuration.
Appendix D: Two-W
Two-Way Serial Communication
wo-Way
D.1. AK PROTOCOL
The AK Protocol for serial communication not only allows the user to query the
present value of system variables remotely, but also permits the user to change the
values of system variables and download information from the sampler’s internal data
logger. The AKCOMM software provided with the sampler uses this protocol for two-
way communication directly to a computer or through a modem. The following
commands of the AK Protocol are presented in detail in the following pages:
The following pages detail the format of the transmission and response messages of
the commands listed above.
AK Protocol
Ask Register Command (AREG)
AK Station 52 ASCII code for the 1-digit Station Number (for example "4": 052). The Station Number is always 1 digit in
length.
AK Chan 75048 ASCII code representation of the 2-digit Channel Number (for example: "K0": 075, 048). The Channel
Number is always 2 digits in length.
AK Append 13010 Optional: Up to 3 ASCII codes can be added to response from instrument. In this case, <CR> and <LF>
(ASCII codes 013 and 010) are appended to the response. Enter 0 if nothing is to be appended.
3 A 3 A A
Ask Register command. Enter the
4 R 4 R R
Program Register Code of the
4-digit Ask Register command.
desired variable in bytes 21 to 23
5 E 5 E E
below.
6 G 6 G G
AK Protocol
Enter Register Command (EREG)
AK Station 52 ASCII code for the 1-digit Station Number (for example "4": 052). The Station Number is always 1 digit in
length.
AK Chan 75048 ASCII code representation of the 2-digit Channel Number (for example: "K0": 075, 048). The Channel
Number is always 2 digits in length.
AK Append 13010 Optional: Up to 3 ASCII codes can be added to response from instrument. In this case, <CR> and <LF>
(ASCII codes 013 and 010) are appended to the response. Enter 0 if nothing is to be appended.
3 E 3 E E
Enter Register command. Enter the
4 R Program Register Code in bytes 21 4 R R
to 23 below, and the new value of 4-digit Enter Register command.
5 E the variable in bytes 15 and 5 E E
following.
6 G 6 G G
AK Protocol
Ask Storage Command (ASTO)
AK Station 52 ASCII code for the 1-digit Station Number (for example "4": 052). The Station Number is always 1 digit in
length.
AK Chan 75048 ASCII code representation of the 2-digit Channel Number (for example: "K0": 075, 048). The Channel
Number is always 2 digits in length.
AK Append 13010 Optional: Up to 3 ASCII codes can be added to response from instrument. In this case, <CR> and <LF>
(ASCII codes 013 and 010) are appended to the response. Enter 0 if nothing is to be appended.
3 A 3 A A
Ask Storage command. Enter the
4 S 4 S S
number of records to be
4-digit Ask Storage command.
downloaded from storage in bytes
5 T 5 T T
11 to 13 below.
6 O 6 O O
14 <ETX> ASCII code 003. 14 <CR> <LF> Up to 3 digits appended to the end
of the response transmission,
SET CURRENT DATA STORAGE BUFFER 15 <LF>
according to the entry for RS-Para
1 in PRC 38 Filter Data 16 3.
2 in PRC 38 Interval Data
The instrument then transmits the number of storage
records shown in response bytes 10 to 12 above. Each
record is followed by <CR><LF>. Refer to Section 7 for the
format of the downloaded data records.
AK Protocol
Set Storage Marker Command (SSTO)
AK Station 52 ASCII code for the 1-digit Station Number (for example "4": 052). The Station Number is always 1 digit in
length.
AK Chan 75048 ASCII code representation of the 2-digit Channel Number (for example: "K0": 075, 048). The Channel
Number is always 2 digits in length.
AK Append 13010 Optional: Up to 3 ASCII codes can be added to response from instrument. In this case, <CR> and <LF>
(ASCII codes 013 and 010) are appended to the response. Enter 0 if nothing is to be appended.
3 S 3 S S
4 S 4 S S
4-digit Set Storage Marker 4-digit Set Storage Marker
command. command.
5 T 5 T T
6 O 6 O O
17 17
18 18
19 19
AK Protocol
Response if Command Addressed to Instrument is Unrecognizable
AK Station 52 ASCII code for the 1-digit Station Number (for example "4": 052). The Station Number is always 1 digit in
length.
AK Chan 75048 ASCII code representation of the 2-digit Channel Number (for example: "K0": 075, 048). The Channel
Number is always 2 digits in length.
AK Append 13010 Optional: Up to 3 ASCII codes can be added to response from instrument. In this case, <CR> and <LF>
(ASCII codes 013 and 010) are appended to the response. Enter 0 if nothing is to be appended.
3 3 ?
4 4 ?
Question marks inserted in place of
unrecognized command.
5 5 ?
6 6 ?
7 7 <space> Space.
9 9 <space> Space.
10 10 S
Syntax error.
11 11 E
12 12 <ETX> ASCII code 003.
16 16
17 17
18 18
19 19
Other equipment required to install the EPROM include a ground strap (R&P part #
13-002601) and EPROM extraction tool (R&P part #12-002579), which also can be
ordered from R&P.
This section contains the parts and accessories for the Partisol-FRM Sampler.
F.1. CONSUMABLES
Aside from the 47 mm collection filters and 37 mm WINS impactor filters used in the
Partisol-FRM Sampler, the only regular consumable item in the hardware is the large
in-line filter located in the pump compartment. This item should be exchanged every
six months.
The batteries on the computer board at the back of the electronics compartment must
be exchanged as needed. The computer board uses a 25 mm diameter round battery
(Panasonic CR2330) and a socket battery at location U4 (Dallas Semiconductor
DS1213C).
1. Measure the voltage across the ground (“GND”) test point in the center of
the interface board and the top surface of the round battery on the
computer board. This voltage should be at least 2.5 VDC.
2. Measure the voltage across pins 14 and 28 on U4 for part number 06-
002565. This voltage should be at least 2.5 VDC.
F.2. PARTS
Basic Hardware
Dome connector for sample tube 13-004300
Viton upper cassette seal 22-002680
Lower cassette seal 22-004276
Power switch 04-002649
Cooling fan 10-002251
Foam fan covers 10-003092
Liquid Crystal Display (LCD) 10-002254
Rubber foot 33-002262
Sample tube 36-004293
Power line filter 02-002400
Transformer 03-002402
Interface board 50-003709
Computer board 50-002407
Standard Partisol pump, 120 VAC 10-002418
Standard Partisol pump, 240 VAC 10-002452
Partisol pump rebuild kit (2 required) 59-002642
Solenoid valve 59-002456
Flow control assembly 55-002663
Streamline FTS 57-004506
Streamline FTS with manometer 57-004506-001
Flow audit adapter 57-000618
Accumulator assembly 55-002555
Ambient temperature sensor package 59-002640
Latch for filter exchange mechanism 33-004221
Large rain hood 38-004011
Gasket for large rain hood 33-004201
Small rain hood 36-003817
Gasket for small rain hood 33-002371
AKCOMM software diskette 41-004001
Manuals
Partisol-FRM Operating Manual 42-004298
Partisol-FRM Service Manual 42-004278
Partisol-FRM Quick Start Guide 42-004299
Other Products
Support stand 57-004644
Partisol-FRM EPROM software revision kit 59-004302
Insulating jacket 10-004359
This appendix contains a filter log to keep track of all important readings associated
with each exposed filter. R&P encourages users to make photocopies of the form or
to use a similar format.
PAGE G-2
Revision B.001
This appendix contains the maintenance procedures for the PM-10 inlet and the PM-
2.5 WINS impactor used in the Partisol-FRM Sampler.
Maintenance Frequency
R&P recommends that the user remove and clean the PM-10 inlet, and check its O-
ring after every 14 days of inlet usage.
Follow these steps to remove the PM-10 inlet from the sampler:
1) Lift the PM-10 inlet upward off the aluminum sample inlet tube.
2) Disassemble the upper and lower inlet halves by unscrewing
counterclockwise the top acceleration assembly from the lower
collector assembly (Figure H-1).
1) Mark the top plate deflector cone and lower plate with a pencil
scribe to indicate proper orientation for easier reassembly after
cleaning and maintenance.
2) Using a Philips-blade screwdriver, remove the four pan head
screws from the top of the top plate, and lift the top plate off the
four threaded spacer standoffs and set aside.
3) Inspect the insect screen for contamination and clean by lifting
the screen off the lower plate rain deflector and brush or rinse
with water until clean. Dry and reinstall.
4) Using a general-purpose cleaner and paper towel, clean the top
plate deflector cone and internal wall surface of the acceleration
assembly.
NOTE: Be sure that after cleaning the acceleration nozzle is clean. If not, use a
cotton swab and cleaner to remove contamination.
5) Inspect the large diameter impactor nozzle O-ring for wear. Re-
place, if necessary, or using a light coating of silicone grease,
apply a thin film on the O-ring itself, and likewise a light coating
on the aluminum threads of the acceleration assembly.
6) After reinstalling the insect screen, align the top plate markings
with the lower plate markings. The four holes in the top plate
should align with the four spacer standoffs. Insert and securely
tighten the four pan-head screws.
NOTE: Most of the contamination in the inlet generally will be found on the
collector plate.
1) Using a general-purpose cleaner with a paper towel, clean the
collector assembly walls and three vent tubes. You may need to
use a cotton swab to clean the vent tubes.
2) Clean the bottom side of the collector assembly.
3) Using a cotton swab, clean the weep hole in the collector plate
where the moisture runs into the moisture trap.
4) Remove the rain jar and clean it.
5) Inspect the brass nipple fitting on the rain jar to ensure tightness
and non-blockage.
6) Place a light coating of silicone grease on the cork gasket inside
the cap of the rain jar.
7) Reinstall the rain jar onto the lower collector assembly.
8) Inspect the two inlet-to-inlet tube sealing O-rings for wear. Re-
place, if necessary.
9) Plase a light coating of silicone grease on the two inlet-to-inlet
tube sealing O-rings to ensure that a proper seal is made when
the PM-10 inlet is reinstalled on the sample inlet tube.
10
10)) Clean the threads on the top and bottom inlet assemblies.
11) Reassemble the top and bottom inlet assemblies until the threads
tighten. Hand-tighten only.
12
12)) Place the PM-10 inlet back on top of the sample inlet tube. Take
care not to damage the internal O-rings.
NOTE: For further information or parts, please contact R&P, its distributors or
representatives.
The procedures below describe the removal, cleaning, and reinstallation of the PM-
2.5 WINS impactor.
Follow these steps to remove the WINS impactor from the sampler:
5) Push the filter exchange mechanism toward the back slightly, and
lift the rollers through the slots in the left-hand and right-hand
guides (Figure H-5).
6) Allow the filter platform to settle downward, and remove the WINS
impactor and adapter.
7) Separate the adapter from the WINS impactor (Figure H-6).
3) Using a dry paper towel, wipe off the inside surfaces of the WINS
impactor. You may use a general purpose cleaner, if necessary.
4) Inspect all O-rings in the top and bottom sections of the WINS
impactor for damage and replace, if necessary.
5) Place a thin coating of O-ring lubricant onto the O-rings, if neces-
sary.
6) Remove the top of the impactor assembly by lifting it upward.
7) Remove any filter that was previously installed.
8) Clean the top and bottom of the impactor assembly using a dry
paper towel. You may use a general purpose cleaner, if neces-
sary.
9) Inspect the O-ring in the top section of the impactor assembly for
damage and replace, if necessary.
10) Place a thin coating of O-ring lubricant onto the O-ring, if neces-
sary.
11
11)) Place a new 37 mm borosilicate glass fiber filter onto the bottom
of the impactor assembly (Figure H-8).
12
12)) Place 42 to 44 drops of impactor oil onto the filter.
13) Place the top of the impactor assembly onto the bottom of the
assembly.
14) Place the impactor assembly into the bottom section of the WINS
impactor.
15) Screw the top of the WINS impactor onto the bottom section.
Ensure that the WINS impactor remains in the upright orientation
so that the oil in the impactor assembly does not spill.
16) Multiple WINS impactors can be prepared in this manner at one
time and kept for later use.
The Partisol-FRM Sampler can be configured with a variety of inlet systems. This
appendix describes the components of the PM-2.5 WINS impactor sampler configu-
ration and the PM-10 sampler configuration, and the procedures for converting the
Partisol-FRM from a PM-2.5 to a PM-10 sampler.
This following components comprise the PM-2.5 WINS inlet configuration as shown
in Figure I-1.
PM-10 inlet
Sample tube
WINS impactor
WINS adapter
B C
PM-10 inlet
Sample tube
Straight tube
Straight tube adapter
D
B C
4) Allow the filter platform to settle downward, and remove the WINS
impactor and adapter by pulling them straight downward.
5) Remove the PM-10 inlet from the sample downtube by pulling it
straight upward.
6) Remove the WINS adapter (Figure I-6) from the WINS impactor
and attach it to the straight tube.
7) Install the straight tube with the adapter into the Partisol-FRM
enclosure by pushing them straight upward until they hit a stop
(Figure I-7).
8) Install a filter carrier (with filter cassette) into the filter exchange
mechanism and close the mechanism by pushing the handle
toward the back of the enclosure (Figure I-7).
1) Remove the PM-10 inlet and straight tube from the sampler.
2) Separate the adapter from the straight tube.
3) Install the adapter onto the WINS impactor.
4) Install the WINS impactor with the adapter into the enclosure by
pushing them straight upward until they hit a stop.
5) Install a filter carrier (with filter cassette) into the filter exchange
mechanism and close the mechanism by pushing the handle
toward the back of the enclosure.
6) Install the sample tube by pushing it down until it hits a stop.
7) Tighten the bulkhead fitting.
8) Install the PM-10 inlet onto the sample tube by pressing it down-
ward until it hits a stop.
9) The Partisol-FRM is now configured as a PM-2.5 sampler (Figure I-
10). There is no difference in sampler programming or operation
with the PM-2.5 inlet installed on the unit.