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    Dynamic Mechanical Analysis: Duncan Price IPTME, Loughborough University

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    Dynamic Mechanical Analysis: Duncan Price IPTME, Loughborough University

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    Dynamic

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    Dynamic

    Copyright:

    Attribution Non-Commercial (BY-NC)
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    Download as ppt, pdf, or txt
    84 views22 pages

    Dynamic Mechanical Analysis: Duncan Price IPTME, Loughborough University

    Uploaded by

    Sujay Dsouza
    Dynamic

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PPT, PDF, TXT or read online from Scribd
    Download as ppt, pdf, or txt
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    Dynamic Mechanical Analysis

    Duncan Price IPTME, Loughborough University


    Copyright: D.M.Price@lboro.ac.uk (2006)

    mechanical testing

    dynamic mechanical analysis

    relationships

    test configurations

    typical behaviour
    For purely crystalline materials, Tg occurs

    b transitions are often related to the toughness

    Tg is related to molecular mass up to a limiting value In semicrystalline polymers, a crystal-crystal slip, Ta* occurs Rubbery plateau (2)

    Rubbery plateau is related to Me between cross-links or entanglements

    Tll in some amorphous polymers

    For thermosets, no Tm occurs Tm = melting (1)

    polycaprolactone

    impact resistance in nylon

    material specification

    thermoset cure

    determination of Tg

    effect of plasticiser

    stress relief

    PET

    effect of frequency

    frequency domain

    frequency master curve

    effect of molecular weight

    gellation of polymer solution

    thermoset curing

    Gillham-Enns or TTT diagram

    recommended reading

    M. Reading and P.J. Haines; Thermomechanical, dynamic mechanical and associated methods in; P. J. Haines; Thermal methods of analysis: Principles, Applications and Problems Blackie, London (1995) pp.123-160.
    K.P. Menard; Dynamic Mechanical Analysis: A Practical Introduction to Techniques and Applications, CRC Press, Boca Raton (1999) D. M. Price, Thermomechanical and Thermoelectrical Methods, in P.J. Haines (ed.) Principles of Thermal Analysis & Calorimetry, ch. 4, Royal Society of Chemistry, Cambridge (2002) pp. 94-128.

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