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    Dynamic Mechanical Analysis

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    Ihlasul Amal
    This document discusses dynamic mechanical analysis (DMA), a technique used to study and characterize materials. It examines how DMA can be used to measure the glass transition temperature (Tg) and other thermal/mechanical properties of polymers by applying an oscillating stress or strain and measuring the material's response over a range of temperatures. The document outlines various test configurations and behaviors observed, such as the rubbery plateau, and how properties like Tg, impact resistance, and crosslinking can be evaluated through DMA. It recommends additional reading on thermomechanical techniques and their applications.

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    Dynamic Mechanical Analysis

    Uploaded by

    Ihlasul Amal
    16 views22 pages
    This document discusses dynamic mechanical analysis (DMA), a technique used to study and characterize materials. It examines how DMA can be used to measure the glass transition temperature (Tg) and other thermal/mechanical properties of polymers by applying an oscillating stress or strain and measuring the material's response over a range of temperatures. The document outlines various test configurations and behaviors observed, such as the rubbery plateau, and how properties like Tg, impact resistance, and crosslinking can be evaluated through DMA. It recommends additional reading on thermomechanical techniques and their applications.

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    karakterisasi material

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    DMA

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    This document discusses dynamic mechanical analysis (DMA), a technique used to study and characterize materials. It examines how DMA can be used to measure the glass transition temperature (Tg) and other thermal/mechanical properties of polymers by applying an oscillating stress or strain and measuring the material's response over a range of temperatures. The document outlines various test configurations and behaviors observed, such as the rubbery plateau, and how properties like Tg, impact resistance, and crosslinking can be evaluated through DMA. It recommends additional reading on thermomechanical techniques and their applications.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    16 views22 pages

    Dynamic Mechanical Analysis

    Uploaded by

    Ihlasul Amal
    This document discusses dynamic mechanical analysis (DMA), a technique used to study and characterize materials. It examines how DMA can be used to measure the glass transition temperature (Tg) and other thermal/mechanical properties of polymers by applying an oscillating stress or strain and measuring the material's response over a range of temperatures. The document outlines various test configurations and behaviors observed, such as the rubbery plateau, and how properties like Tg, impact resistance, and crosslinking can be evaluated through DMA. It recommends additional reading on thermomechanical techniques and their applications.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
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    Dynamic Mechanical Analysis

    mechanical testing
    dynamic mechanical analysis
    relationships
    test configurations
    typical behaviour

    For purely crystalline


    materials, Tg occurs

    Tg is related to molecular mass


    up to a limiting value
    b transitions are often In semicrystalline polymers,
    related to the toughness a crystal-crystal slip, Ta* occurs

    Rubbery plateau (2)

    For thermosets,
    Rubbery plateau is related no Tm occurs
    to Me between cross-links Tll in some
    or entanglements amorphous Tm = melting (1)
    polymers
    polycaprolactone
    impact resistance in nylon
    material specification
    thermoset cure
    determination of Tg
    effect of plasticiser
    stress relief
    PET
    effect of frequency
    frequency domain
    frequency master curve
    effect of molecular weight
    gellation of polymer solution
    thermoset curing
    Gillham-Enns or TTT diagram
    recommended reading

    M. Reading and P.J. Haines; “Thermomechanical, dynamic mechanical and associated


    methods” in; P. J. Haines; “Thermal methods of analysis: Principles, Applications and
    Problems” Blackie, London (1995) pp.123-160.

    K.P. Menard; “Dynamic Mechanical Analysis: A Practical Introduction to Techniques


    and Applications”, CRC Press, Boca Raton (1999)

    D. M. Price, “Thermomechanical and Thermoelectrical Methods”, in P.J. Haines (ed.)


    Principles of Thermal Analysis & Calorimetry, ch. 4, Royal Society of Chemistry,
    Cambridge (2002) pp. 94-128.

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