Julabo FP 50 He User Manual
Julabo FP 50 He User Manual
Julabo FP 50 He User Manual
Operating Manual
Refrigerated and
Heating Circulators
air cooled
F25-HE
F32-HE
F34-HE
FP40-HE
FP50-HE
water cooled
FPW50-HE
19532460.doc
11.10.12
Congratulations!
You have made an excellent choice.
JULABO thanks you for the trust you have placed in us.
This operating manual has been designed to help you gain an understanding of the operation and
possible applications of our circulators. For optimal utilization of all functions, we recommend that you
thoroughly study this manual prior to beginning operation.
10/12
Printed in Germany
HE
TABLE OF CONTENTS
Operating manual.................................................................................................................. 5
1.
Intended use................................................................................................................... 5
5.
Preparations ................................................................................................................. 20
5.1. Installation................................................................................................................ 20
5.2. Bath fluids ................................................................................................................ 21
5.3. Temperature application to external systems .......................................................... 22
5.3.1. Tubing ................................................................................................................. 23
5.4. Filling / draining........................................................................................................ 24
6.
Operating procedures................................................................................................... 25
Setting of temperatures................................................................................... 27
menu............................................................. 27
HE
Operating manual
1.
Intended use
JULABO circulators have been designed to control the temperature of specific fluids in a bath tank.
The units feature pump connections for temperature control of external systems (loop circuit).
JULABO circulators are not suitable for direct temperature control of foods, semiluxury foods and tobacco, or pharmaceutical and medical products.
Direct temperature control means unprotected contact of the object with the bath
medium (bath fluid).
1.1.
Description
1x10
The circulators are operated via the splash-proof keypad. The implemented
microprocessor technology allows to set and to store different values that can be
indicated on the VFD COMFORT-DISPLAY. Three menu keys facilitate adjusting
setpoints, warning and safety functions and menu functions.
Temperature- and time-dependent processes can be stored and executed using the
integrated programmer.
The TCF - Temperature Control Features give the user access to all important
temperature control parameters. This means full control of the control behavior at all
times and the ability to manually adjust or adapt the controls to the specific
application.
Electrical connections:
The serial interface, switchable from RS232 to RS485, allows modern process
technology without additional interface.
Connection for Pt100 external sensor for external temperature measurement and
control.
Alarm output for external alarm message or control of JULABO refrigerating baths
or solenoid valve (cooling water).
The electronic module (option) provides 3 further analog connections (alarm input,
standby input, recorder output, programmer input).
The early warning system for low level signals that bath fluid needs to be refilled
before the low level protection conforming to IEC 61010-2-010 causes a complete
shutdown of the main functional elements.
Intelligent pump system: The pump capacity (electronically adjustable via the motor
speed) enables to adapt to varying conditions for internal and external temperature
applications.
ICC
TCF
ATC3
RS232
Pt100
SMART
PUMP
2.
The products of JULABO ensure safe operation when installed, operated, and maintained according to
common safety regulations. This section explains the potential dangers that may arise when operating
the circulator and also specifies the most important safety precautions to preclude these dangers as
far as possible.
The operator is responsible for the qualification of the personnel operating the units.
The personnel operating the units should be regularly instructed about the dangers involved with
their job activities as well as measures to avert these dangers.
Make sure all persons tasked with operating, installing, and maintaining the unit have read and
understand the safety information and operating instructions.
When using hazardous materials or materials that could become hazardous, the circulator may be
operated only by persons who are absolutely familiar with these materials and the circulator.
These persons must be fully aware of possible risks.
If you have any questions concerning the operation of your unit or the information in this manual,
please contact us!
Contact
HE
Use:
The bath can be filled with flammable materials. Fire hazard!
There might be chemical dangers depending on the bath medium used.
Observe all warnings for the used materials (bath fluids) and the respective instructions (safety data
sheets).
Insufficient ventilation may result in the formation of explosive mixtures. Only use the unit in well
ventilated areas.
Only use recommended materials (bath fluids). Only use non-acid and non corroding materials.
When using hazardous materials or materials that could become hazardous, the operator must affix
the enclosed safety labels to the front of the unit so they are highly visible:
If this unit is intended for use within the United States of America, all 3 warning labels must be affixed
to the housing of the unit prior to use.
Directions for the positioning of the individual warning labels are enclosed with the warning labels
included in the delivery. Warning labels must be easily visible to users.
1
or
2
Particular care and attention is necessary because of the wide operating range.
There are thermal dangers: Burn, scald, hot steam, hot parts and surfaces that can be touched.
Warning label W26: Colors: yellow, black
Hot surface warning.
(The label is put on by JULABO)
Observe the instructions in the manuals for instruments of a different make that you connect to the
circulator, particularly the respective safety recommendations. Also observe the pin assignment of
plugs and technical specifications of the products.
2.1.
Disposal
The circulator contains a back-up battery that supplies voltage to memory chips when the unit is
switched off. Do not dispose of the battery with household waste!
Depending on battery regulations in your country, you might be obliged to give back used or defect
batteries to gathering places.
The product may be used with oil as bath fluid. These oils fully or partially consist of mineral oil or
synthetic oil. For disposal, observe the instructions in the safety data sheets.
These units contains refrigerants at this time considered not to have any negative effects on the
ozone layer. However, during the long operating period of the unit, disposal prescriptions may change.
So only qualified personnel should take care of disposal.
Contact an authorized waste management company in your country.
Disposal with household waste (unsorted waste) or similar collections of municipal
waste is not permitted!
HE
2.2.
Technical specifications
F25-HE
F32-HE
0,01
0,01
Cooling capacity
Medium: ethanol
Refrigerant
C
kW
+20 0 -20
0.26 0.2 0.06
+20
Overall dimensions
(WxDxH)
cm
R134a
23x42x64
R134a
31x42x64
(WxL)
cm
12x14
18x12
Bath depth
cm
14
15
Filling volume
liters
3 ... 4,5
5,5 ... 8
Weight
kg
32
38
V/ Hz
A
V/ Hz
A
V/ Hz
A
V/ Hz
A
207-253 / 50
12
--------103-127 / 60
13
90-110 / 50-60
13
207-253 / 50
12
207-253 / 60
12
103-127 / 60
14
90-110 / 50-60
14
Bath opening
230 V/50 Hz
(at 230 V)
230 V/60 Hz
(at 230 V)
115 V/60 Hz
(at 115 V)
100 V/60 Hz
(at 100 V)
-20 -30
F34-HE
-30 ... 150
0.01
Cooling capacity
Medium: ethanol
Refrigerant
C
kW
Overall dimensions
(WxDxH)
cm
R134a
38x58x64
(WxL)
cm
24x30
Bath depth
cm
15
Filling volume
liters
14 ... 20
Weight
kg
44
V/Hz
A
V/ Hz
A
V/ Hz
A
207-253 / 50
12
207-253 / 60
12
103-127 / 60
14
Bath opening
230 V/50 Hz
(at 230 V)
230 V/60 Hz
(at 230 V)
115 V/60 Hz
(at 115 V)
FP40-HE
C
FP50-HE
FPW50-HE
-50 ... 200
0.01
0.01
Cooling capacity
Medium: ethanol
Refrigerant
C
kW
Overall dimensions
(WxDxH)
cm
R134a
36x46x71
R404A or R507
42x49x72
(WxL)
cm
23x14
18x12
Bath depth
cm
20
20
Filling volume
liters
9 ... 16
5.5 ... 8
Weight
kg
49
57
V/Hz
A
V/ Hz
A
207-253 / 50
13
207-253 / 60
13
207-253 / 50
14
207-253 / 60
14
Bath opening
230 V/50 Hz
(at 230 V)
230 V/60 Hz
(at 230 V)
HE
Temperature selection
digital
via keypad
indication on monitor
Temperature indication
Resolution
ATC3
INT/EXT
0.01
3 / 9
Temperature control
kW
2,0
kW
1,0
at 0 bar
stages
1 ... 4
l/min
22 ... 26
bar
0.7
bar
0.4
Electrical connections:
Ambient temperature
See page 11
C
5 40
10
HE
Electrical connections:
External alarm device 24-0 V DC / max. 25 mA
Computer interface RS232 or RS485
External Pt100 sensor
Optional for HE, SE
(Order No. 8900100 Electronic module with analog connections)
Programmer input -100 C to 400 C = 0 - 10 V or 0 - 20 mA or 4 - 20 mA
Input for the signal of a flow meter or external manipulated variable
Temperature recorder outputs
0 - 10 V (0 V = -100 C, 10 V = 400 C)
0 - 20 mA (0 mA = -100 C, 20 mA = 400 C)
4 - 20 mA (4 mA = -100 C, 20 mA = 400 C)
Standby input
for external emergency switch-off
Alarm output
for external alarm signal
Safety installations according to IEC 61010-2-010:
Excess temperature protection
adjustable from 0 C ... 320 C
Low liquid level protection
float switch
Classification according to DIN 12876-1
class III
Supplementary safety installations
Early warning system for low level
High temperature warning function
Low temperature warning function
Supervision of working sensor
Reciprocal sensor monitoring between
working and safety sensors
Alarm message
Warning message
float switch
optical + audible (in intervals)
optical + audible (in intervals)
plausibility control
difference >35 K
optical + audible (permanent)
optical + audible (in intervals)
11
2.3.
max.
6 bar
3.5 to 6 bar
<20 C
7,5 to 9,0
< 100 ppm
> 1 ppm
> 0,5 dH
60 ppm < [HCO3-] < 300 ppm
< 500 s / cm
< 50 ppm
< 2 ppm
< 0,5 ppm
< 0,5 ppm
< 0,5 ppm
< 0,05 ppm
< 10 ppm
< 50 ppm
< 0,1 ppm
impermissible
impermissible
Notice:
Danger of corrosion of heat exchanger due to unsuitable quality of cooling
water.
Due to its high content of lime hart water is not suitable for cooling and causes
calcination of the heat exchanger.
Ferrous water or water containing ferrous particles will cause formation of rust
even in heat exchangers made of stainless steel.
Chlorous water will cause pitting corrosion in heat exchangers made of stainless
steel.
Due to its corrosive characteristics distilled and deionized water is unsuitable
and will cause corrosion of the bath. .
Due to its corrosive characteristics sea water is not suitable.
Due to its microbiological (bacteria) components which settle in the heat
exchanger untreated and unpurified river water and water from cooling towers is
unsuitable.
Avoid particulate matter in cooling water.
Avoid putrid water.
Notice:
Cooling water circuit
Risk of oil leaking from the cooling circuit (compressor) of the recirculating cooler into
the cooling water in case of a fault in the circuit!
Observe the laws and regulations of the water distribution company valid in the
location where the unit is operated.
12
HE
Operating instructions
3.
3.1.
3.2.
13
3.3.
Safety recommendations
Follow the safety instructions to avoid personal injury and property damage. Also, the
valid safety instructions for workplaces must be followed.
Only connect the unit to a power socket with an earthing contact (PE protective
earth)!
The power supply plug serves as a safe disconnecting device from the line and
must always be easily accessible.
Place the unit on an even surface on a base made of nonflammable material.
Do not stay in the area below the unit.
Make sure you read and understand all instructions and safety precautions listed in
this manual before installing or operating your unit.
Set the excess temperature safety installation at least 25 C below the fire point of
the bath fluid.
Observe the limited working temperature range when using plastic bath tanks.
Never operate the unit without bath fluid in the bath.
Pay attention to the thermal expansion of bath oil during heating to avoid
overflowing of the fluid.
Prevent water from entering the hot bath oil.
Do not drain the bath fluid while it is hot!
Check the temperature of the bath fluid prior to draining (e.g., by switching the unit
on for a short moment).
Use suitable connecting tubing.
Avoid sharp bends in the tubing, and maintain a sufficient distance from
surrounding walls.
Make sure that the tubing is securely attached.
Regularly check the tubing for material defects (e.g., for cracks).
Never operate damaged or leaking units.
Always turn off the unit and disconnect the mains cable from the power source
before performing any service or maintenance procedures, or before moving the
unit.
Always turn off the unit and disconnect the mains cable from the power source
before cleaning the unit.
Always empty the bath before moving the unit.
Transport the unit with care.
Sudden jolts or drops may cause damage in the interior of the unit.
Observe all warning labels.
Never remove warning labels.
Never operate units with damaged mains power cables.
Repairs are to be carried out only by qualified service personnel.
Some parts of the bath tank and the pump connections may become extremely hot
during continuous operation. Therefore, exercise particular caution when touching
these parts.
14
HE
Caution:
The temperature controlling i.e. of fluids in a reactor constitutes normal circulator
practice.
We do not know which substances are contained within these vessels.
Many substances are:
inflammable, easily ignited or explosive
hazardous to health
environmentally unsafe
i.e.: dangerous
The user alone is responsible for the handling of these substances!
The following questions shall help to recognize possible dangers and to reduce the
risks to a minimum.
Are all tubes and electrical cables connected and installed?
Note:
sharp edges, hot surfaces in operation, moving machine parts, etc.
Do dangerous steams or gases arise when heating?
Is an exhaust needed when working?
What to do when a dangerous substance was spilled on or in the unit?
Before starting to work, obtain information concerning the substance and
determine the method of decontamination.
Notice:
Check the safety installations at least twice a year!
Excess temperature protection according to IEC 61010-2-010.
With a screwdriver turn back the adjustable excess temperature protection until the
shut-down point (actual temperature).
Low level protection according to IEC 61010-2-010.
To check the function of the float, it can be manually lowered with a screwdriver for
example.
WARNING
This product contains chemicals known to the state of California to cause cancer, birth
defects or other reproductive harm.
15
4.
Front view
Rear view
FPW50
16
HE
1a
for circulator
1b
VFD COMFORT-DISPLAY
Header: Control indicators
Line 1: Actual value
internal or external
The display is depending on the selected control mode in the
menu > Control < (internal or external).
Line 2: Working temp. setpoint, constantly S xxx.xx
Line 3: Actual value (E = external or I = internal)
Alternating with the display in line 1
Use the keys
to indicate further values in line 3
PI Capacity in % - with manipulated variable set to >control<*
PS Capacity in % - with manipulated variable set to >serial<* or
>eprog<*
H Heater capacity in Watts
U Mains voltage Volts
F Flow rate in liters/minute
(providing EPROG input set to >Flowrate<)
*refer to >MENU/CONFIG< >CONFIG / ACTVAR>
2.1
Remote control
2.2
2.3
Navigation keys
4.1
1. Key: >OK<
Start / Stop (pump / heater )
2. >OK< in the menu Menu item / select submenu for setting
Save set value
Save selected parameter
A beep signals the end of setting
After the actions Start, Stop and change from VFD Display to standard
display the key
is locked for a short time.
The above graph front side shows an example for standard display.
17
1. Key:
4.3
Menu keys
4.4
4.5
4.6
ext Pt100
8
SERIAL
9
12
18
HE
16a
16b
17a
17b
18
19
20
21
22
Pump connectors
23
suction pump
pressure pump
24
"
19
Preparations
5.
5.1.
Preparations
Installation
Set selector dial for cooling machine in position "1" for operation
with HE circulator.
20
HE
5.2.
Bath fluids
Caution:
Carefully read the safety data sheet of the bath fluid used, particularly with regard to
the fire point!
If a bath fluid with a fire point of 65 C is used, only supervised operation is possible.
Water: The quality of water depends on local conditions.
Due to the high concentration of lime, hard water is not suitable for temperature
control because it leads to calcification in the bath.
Ferrous water can cause corrosion - even on stainless steel.
Chloric water can cause pitting corrosion.
Distilled and deionized water is unsuitable. Their special properties cause
corrosion in the bath, even in stainless steel.
Temperature range
5 C to 80 C
-20C to 50C
21
Preparations
5.3.
If the circulator is operated without external system, close the pump connector (22)
with the cap nut.
Temperature application to external, closed systems
The circulator is used for temperature application to external,
closed systems (loop circuit) with simultaneous temperature
application in the circulator bath.
ext
Pt100
SERIAL
T16A
T16A
21
22
Important:
22
the external bath, turn the circulator off with the Start/Stop key.
HE
Return flow safety device
If the liquid levels in the circulator bath and the external system are at
different heights, overflowing must be prevented after the power has
been turned off.
Flood hazard!
For this reason, shut-off valves can be integrated in the loop circuit.
Order No.
8 970 456
8 970 457
5.3.1.
Description
Shut-off valve (suitable up to +90 C)
Shut-off valve (suitable up to +200 C)
Tubing
Recommended tubing:
Order No.
Length
8930008
1m
8930012
1m
8930108
1m
8930112
1m
8930410
1m
8930412
1m
8 930 209
8 930 210
8 930 211
8 930 214
8 930 220
8 930 221
8 930 222
8 930 223
0.5 m
1.0 m
1.5 m
3.0 m
0.5 m
1.0 m
1.5 m
3.0 m
CR tubing
CR tubing
Viton tubing
Viton tubing
Insulation for tubing
Insulation for tubing
8 mm inner dia.
12 mm inner dia.
8 mm inner dia.
12 mm inner dia.
8 mm inner dia.
12 mm inner dia.
Temperature range
-20 C to 120 C
-20 C to 120 C
-50 C to 200 C
-50 C to 200 C
-50 C to 100 C
-50 C to 100 C
-100 C to +350 C
-50 C to +200 C
Warning:
Tubing:
At high working temperatures the tubing used for temperature application and cooling
water supply represents a danger source.
A damaged tubing line may cause hot bath fluid to be pumped out within a short time.
This may result in:
Burning of skin
Difficulties in breathing due to hot atmosphere
Safety recommendations
Employ suitable connecting tubing.
Make sure that the tubing is securely attached.
Avoid sharp bends in the tubing, and maintain a sufficient distance from
surrounding walls.
Regularly check the tubing for material defects (e.g. for cracks).
Preventive maintenance: Replace the tubing from time to time.
23
Preparations
5.4.
Filling / draining
Notice:
Pay attention to the thermal expansion of bath oil during heating to avoid
overflowing of the liquid.
Do not drain the bath fluid while it is hot!
Recommendation: Temperature range 5 C to 40 C
Check the temperature of the bath fluid prior to draining (by switching the unit on
for a short moment, for example).
Store and dispose the used bath fluid according to the laws for environmental
protection.
Filling
Take care that no liquid enters the interior of the circulator.
Recommended maximum filling level with water as bath fluid:
30 mm below the tank rim
Recommended maximum filling level with bath oils:
40 mm below the tank rim
After filling, immerse the samples in the bath or place the lid on
the bath, in case the opening is not to be used.
The circulator provides an early warning system for low level that
may be triggered when changing samples in the bath.
Draining
23
24
HE
6.
6.1.
Operating procedures
Power connection
Caution:
Only connect the unit to a power socket with earthing contact (PE protective
earth)!
The power supply plug serves as safe disconnecting device from the line and must
be always easily accessible.
Never operate equipment with damaged mains power cables.
Regularly check the mains power cables for material defects (e.g. for cracks).
We disclaim all liability for damage caused by incorrect line voltages!
Check to make sure that the line voltage matches the supply voltage
specified on the identification plate. Deviations of 10 % are permissible.
Connect the circulator with mains power cable (17a) to the mains
outlet (18).
Connect the control cable (9) between the connectors (9a, 9b).
6.2.
6.2.1.
Start:
key.
Press
The actual bath temperature is displayed on the VFD COMFORTDISPLAY. The circulating pump starts with a slight delay.
Stop:
Press
key.
or
key pressed.
Keep
The VFD COMFORT-DISPLAY indicates the message "OFF".
25
Operating procedures
6.2.2.
To save energy, turn off the cooling machine with the mains switch
(1b) whenever cooling is not required.
26
HE
7.
7.1.
Setting of temperatures
Using the pre-settings in the
menu
key to call up the menu for temperature selection.
Press the
Press
menu
or
key.
The circulator uses the new working temperature value for temperature
control.
key.
key.
key to 85.00 C
key.
27
Setting of temperatures
7.2.
28
The circulator uses the new working temperature value for temperature
control.
HE
8.
SECVAL
(Security Values)
SAFETMP
AL-TYPE
OVERTMP
SUBTEMP
8.1.
Exact setting:
1. Press the key
2. Press the
Recommendation:
Set the excess temperature protection at 5 C to 10 C above the working
temperature setpoint.
29
8.1.1.
Turn off the unit with the mains switch, refill bath fluid and turn
the unit on again!
3. Float
4. Circulating pump
5. Heater
Warning:
When adding bath fluid, always us the type of fluid which is identical with the fluid in
the bath.
Bath oils must not contain any water and should be pre-heated approximately to the
current bath temperature! Explosion hazard at high temperatures!
30
HE
8.2.
Factory setting:
>WARNING<
key.
.
key.
key if the parameter is to retained.
Setting >WARNING<
A mere warning function with optical and audible warning signal (interval
tone) A message appears on the VFD COMFORT-DISPLAY:
or
OVERTMP
SUBTEMP
Setting >ALARM<
Temperature limit with shutdown of heater and circulating pump.
An audible alarm sounds (continuous tone) and a message appears on
the VFD COMFORT-DISPLAY:
or
OVERTMP
SUBTEMP
31
8.3.
Over temperature
Sub temperature
1. Press the
.
or
and
The warning functions are only activated if the actual bath temperature
remains within the set limit values for 3 seconds after switch-on.
Recommendation:
Set the over temperature warning value >OVERTMP< 5 C to 10 C above
the working temperature setpoint.
Set the sub temperature warning value >SUBTMP< 5 C to 10 C below the
working temperature setpoint.
32
HE
9.
Menu functions
1. Open the menu by pressing the
2. Use the
3. Press the
Press the
key.
Menu level 1
Start program
Page 34
Page 37
Page 39
Page 40
Page 44
DYNAMICS - internal
Control parameter - XP-, TN-, TV- INTERNAL
Control parameter - XP-, TN-, TV- XPU-, EXTERNAL
Adjustable interface parameters
BAUD RATE, PARITY, HANDSHAKE
Page 50
Page 51
33
Menu functions
Menu level 1
Analog inputs/outputs
Recorder output CHANNEL 1, 2, 3
EPROG External programmer input
EX-STBY - STAND-BY input
ALARM - output
9.1.
Page 60
Requirements:
1. Create a program. (refer to next chapter)
2. Return to the Start-MENU and confirm the desired setting of each
Start-Menu
Menu level 1
> GO <
Level 2
Press the
key if a parameter is to be retained.
Correction function for parameters or values (prior to OK)
Parameter level
and
example: STEP 1
or
34
(STDBY / SETPNT)
Parameter STanDBY: the circulator switches to
OFF-.
Parameter SETPoiNT: the circulator constantly
keeps the temperature at the value of the last step.
HE
Level 2
Parameter level
oer
or
start at the set time under parameter (TIMER ).
Set time in the example below:
09. August 2009, 11:15 hrs
Parameter level
Submenu TIMER
>YEAR< year
Check the correct setting of the internal real time clock if required
(see MENU CONFIG)
35
Menu functions
The started program
After the start the program will indicate the currently calculated setpoint in line
2
S XX.XX. The value increases within the time period >TSLICE< until the
target temperature >SETPNT< of the section is reached.
If the time period in a section is set to 0, the next section will not begin until
the target temperature has been reached.
A
B
C1
C2
D1
D2
36
HE
9.2.
Menu level 1
1 program
10 sections
(Nr.)
(C)
(hh.mm)
C
200
1
100
00:20
Step 1
2
180
00.10
4
4
180
00:20
6
6
75
00:50
8
75
00:20
150
100
75
50
25
Graph1
10 20 30 40 50 60 10 20 30 40 50 60 10 [min]
Sections without set value and time are skipped. They can be defined
retroactively and the integrated into the program.
37
Menu functions
Menu level 1
>EDIT<
> DELETE<
Level 2
Press
key, if a parameter is to be retained.
Correction function for parameters or values (prior to OK)
Level 3
Parameter level
(STEP 1 10)
(time slice)
38
Delete program
Program steps can be deleted individually or
entirely. (STEP 01, 02, 10, ALL).
and
and
HE
9.3.
Examples:
Soll
Illuminated display:
Ist
stage 1 ... 4
For protecting the pump motor, the rotation speed (i.e. the pump pressure
stage) changes with the load applied.
Example: The viscosity of the bath fluid (i.e. the load applied to the pump
motor) changes with the working temperature in the bath.
Flow rate:
22 ... 26 l/min
Factory setting:
stage 2
Pump pressure
[bar]
0.4
0.5
0.6
0.7
Suction pump
[bar]
0.2
0.26
0.33
0.4
Total capacity
in a loop circuit
[bar]
0.6
0.76
0.93
1. Press the
key.
1.1
key
pressing the
The set parameter flashes (example: >LEVEL 2<)
3. Change the parameter by pressing
key.
or
Press the
39
Menu functions
9.4.
Menu level 1
Level 2
Parameter level
or
or
or
or
and
AUTOSTART on = on
AUTOSTART off = off
See WARNING page 42
or
PUMP ON
PUMP OFF
or
or
40
HE
Level 2
Level 3
Parameter level
+
+
+
+
9.4.1.
for remote
41
Menu functions
9.4.2.
In addition to the serial interface via remote control the circulator offers
the possibility to adjust the setpoint via analog interface >ext. Pt100< or
>REG+E-PROG<.
OFF - Setpoint setting with the navigation keys
or the integrated programmer.
PT100 - Setpoint setting via the analog socket ext. Pt100 using an
external temperature sensor or an appropriate voltage/current
source.
PT100
EPROG
>
The E-Prog input can only be used either under menu item >SP
EXT < or under menu item >ACTVAR<
(see page 43).
>
9.4.3.
AUTOSTART
Warning:
For supervised or unsupervised operation with the AUTOSTART function avoid any
hazardous situation to persons or property
Take care to fully observe the safety and warning functions of the circulator.
42
Notice:
The circulator has been configured and delivered by JULABO in
accordance with the NAMUR recommendations. This means for the start
mode that the unit must enter a safe operating status after a power
failure. This safe operating status is indicated by the message OFF or
R OFF on the VFD COMFORT-DISPLAY.
A complete, all-pole shutdown of the main functional elements such as
heater and pump motor is effected.
The values set on the circulator remain saved and the unit is restarted by
pressing the start/stop key in manual control.
In remote control mode the values need to be resent by the PC via the
interface.
If such a safety standard is not required, the NAMUR recommendations
can be bypassed with the AUTOSTART function thus allowing a direct
start of the circulator by pressing the mains switch or using a timer.
HE
9.4.4.
OFF-MODE
Factory setting:
PMP OFF
Factory setting:
CONTROL
Possible parameters:
CONTROL The internal control electronics of the circulator controls
the heater und the connected cooling unit. Self-tuning is possible.
SERIAL The heater or the connected cooling unit receives the control
signal via the serial interface. Self-tuning is not possible.
EPROG - The heater or the connected cooling unit receives the control
signal via the E-Prog input. Self-tuning is not possible.
Important:
Under
to
Warning:
The working temperature range of the circulator is determined during configuration. If
set to >CONTROL<, this range cannot be exceeded.
If set to > SERIAL < and > EPROG <, heat or cold is applied to the bath without
control. The permissible maximum temperature can be exceeded. The user has to take
adequate precautions for temperature control.
Materials, such as gaskets or insulations for example, may be damaged or destroyed, if
the permissible maximum temperature is exceeded.
The safety and warning functions >
their fullest capacity.
43
Menu functions
9.4.6.
9.4.7.
9.5.
Menu level 1
Press the
key if a parameter is to be retained. Correction function
for parameters or values (prior to OK)
Level 2
Parameter level
or
or
or
44
OFF - no selftuning.
ONCE - single selftuning (factory setting)
ALWAYS - continual selftuning.
HE
Level 2
Parameter level
C-TYPE INTERNAL
and
or
0.1 99.9
3 9999
0 999
C-TYPE EXTERNAL
+
0.1 99.9
3 9999
The parameter flashes, set by pressing
+
0 999
0.1 99.9
45
Menu functions
9.5.1.
Pt100
Attention:
Place the external sensor into the temperature-controlled medium and securely fix the
sensor.
Pt100
46
M+R
Description Material
200x6 mm , stainless steel
200x6 mm , glass
20x2 mm , stainless steel
300x6 mm , stainless steel
300x6 mm , stainless steel / PTFE coated
600x6 mm , stainless steel / PTFE coated
900x6 mm , stainless steel / PTFE coated
1200x6 mm , stainless steel / PTFE coated
Extension cable for Pt100 sensor
M+R in-line Pt100 sensor
Cable
1.5 m
1.5 m
1.5 m
1.5 m
3m
3m
3m
3m
3.5 m
The M+R in-line Pt100 sensor is a flow sensor and can be installed loop
circuit
HE
9.5.2.
SELFTUNING
Selftuning:
When performing a selftuning for the controlled system (temperature
application system), the control parameters Xp, Tn and Tv are
automatically determined and stored.
Possible parameters:
OFF - no selftuning
The control parameters ascertained during the last identification are
used for control purposes.
ONCE - single selftuning (factory setting)
The instrument performs a single selftuning of the controlled system
key or after receiving a start
after each start with the
command via the interface.
ALWAYS - continual selftuning
The instrument performs a selftuning of the controlled system
whenever a new setpoint is to be reached.
Use this setting only when the temperature application system
changes permanently.
9.5.3.
Dynamic internal
Factory setting:
NORM
temp. stability
Possible parameters:
APER
NORM
APER
Setpoint
t
C
APER (aperiodic)
NORM
temp. stability
APER
temperature ramp
47
Menu functions
9.5.4.
In most cases the control parameters preset in the factory are adequate
for achieving an optimum temperature sequence.
The control parameters allow adjustment to special control processes..
Proportional range >Xp<
The proportional range is the range below the setpoint in which the
control circuit reduces the heating capacity from 100% to 0 %
Reset time >Tn< (Integral component)
48
HE
9.5.5.
COSPEED - external
Int. temperature
Ext. temperature
5
3
0
Setpoint
9.5.6.
In most cases the control parameters preset in the factors are adequate
for achieving an optimum temperature sequence.
The control parameters allow adjustment to special control processes.
The proportional range Xpu of the cascaded controller is only needed for
external control.
49
Menu functions
9.6.
Menu level 1
Factory settings:
4800 Baud
even
hardware handshake
Level 2
Parameter level
Press the
retained.
even:
odd:
no:
key if a parameter is to be
50
(Software handshake)
(Hardware handshake)
HE
9.7.
Example:
1-point calibration
C
TT1
B (INT)
C
3-point calibration
C
TT
B (EXT)
TT1
C
TT 1 = Original curve
Pt100
ext
C
TT
M
M = Temperature measuring instrument with temperature sensor
B = Bath tank (INTernal or EXTernal)
T = circulator
CT = Temperature on measuring point
TT = Temperature on circulator
51
Menu functions
Menu level 1
Level 2
Parameter level
Press the
key if parameter is to be retained.
Correction function for parameters or values (prior
to OK).
or
or
calibration.
Level 2
If only a 1-point calibration is carried out, the following menu items are not
indicated anymore
Parameter level
The value is only indicated
52
HE
Level 2
Parameter level
If only a 2-point calibration is carried out, the following menu items are not
indicated anymore
The value is only indicated
9.7.1.
In the first submenu the ATC function is set for the >INTERN< internal or the
>EXTERN< external temperature sensor.
Calibration can be carried out for the internal temperature sensor and for the
external temperature sensor connected to the socket ext. Pt100.
The circulator is able to save both parameter sets. However only the one
which has been set under menu item >ATC SENSOR < is displayed.
9.7.2.
In the second submenu the ATC function for the temperature sensor selected
above is activated >YES< or deactivated >NO<.
>YES< (factory setting) The controller of the circulator uses the original
curve of the temperature sensor or the new curve measured during the
ATC calibration.
Important: Set to >NO< during the calibration process
>NO< An ATC calibration is to be carried out.
Important: Set to >YES< after calibration.
In the > ATC STATUS < >YES< the ATC calibration always affects the
current working temperature; also the one set via interface.
53
Menu functions
9.7.3.
Pairs of values:
TMPVAL X: Circulator temperature 1 or 2 or 3 (actual value TT )
The actual temperature of the bath is simultaneously saved with the
calibration value >CALVAL< and can be indicated for control purposes
(value does not flash).
CALVAL X: Calibration temperature 1 or 2 or 3 (actual value CT )
The calibration value is determined with a temperature measuring
device and saved under menu item >CALVAL<.
(value flashes
54
HE
9.7.4.
Menu level 1
(Example: <25>).
80.00 C
120.00 C
160.00 C
and
and
.
Confirm once more by pressing the key
The bath is heated up.
Wait for approx. 5 minutes until the temperature is constant.
Read the value of measuring point CT on the device and enter under menu
item >CALVAL X< by using the keypad.
>CALVAL 1< (79.70 C)
>CALVAL 2< (119.50 C)
>CALVAL 3< (159.30 C)
4. Calibration
Menu level 1
Level 2
Press the
key if parameter is to be retained. Correction function for
parameters or values (prior to OK).
Setting is required only for the first calibration point.
Parameter level
Menu functions
(50) +
The second of 3 points is calibrated.
Return to 2. set working temperature value SETPNT: 160.00 C
The value is only indicated.
(159) +
Decimal digits flash, set by pressing
(30) +
The 3-point calibration is completed
5. Return to standard operation
56
HE
9.8.
MENU LIMITS
Menu level 1
Level 2
Parameter level
+
Decimal digits flash, set by pressing
+
0 100 %
0 100 %
In case of external control these menu items are additionally indicated.
+
Decimal digits flash, set by pressing
+
57
Menu functions
9.8.1.
The heating and cooling capacity of the unit are adjustable. 100 %
corresponds to the technical specification of the equipment.
Setting range:
HEAT MAX
0 to 100 % in 1 % steps
COOLING MAX 0 to 100 % in 1 % steps
9.8.2.
58
Protects the pump motor from high viscosity of the bath fluid at low
temperatures.
HE
BAND HIGH / LOW Band limitation
The band limitation is active during external control. Varied, practiceoriented setting are feasible for heat-up and cool-down phases.
Setting range: 0 C ... 200 C
BAND HIGH and BAND LOW allow for the limitation of the difference
between the temperatures in the internal bath and the external system to
any maximum value for the heat-up and cool-down phase.
During the heat-up phase this difference value is always added to the
actual external temperature. During the cool-down phase the difference
value is subtracted.
C
200
150
Internal bath
external system
100
75
BAND HIGH
BAND LOW
50
25
10 20 30 40 50 60 10 20 30 40 50 60 10 [min]
59
Menu functions
9.9.
In order to use the analog inputs and outputs, the circulator must be
equipped with the electronic module available as option.
Order No. 8 900 100 Electronic module
ALARM STAND-BY
REG+
E-PROG
This submenu enables setting of the input and output values for the
programmer input and the temperature recorder outputs of socket REG+EPROG.
The >STAND-BY< input and the >ALARM< output are configurable.
Menu level 1
Press the
key if parameter is to be retained. Correction function for
parameters or values (prior to OK).
Level 2
Level 3
Parameter level
ACTINT
[C]
internal actual temperature value
(bath temperature)
ACTEXT
[C]
external actual temperature
value (external sensor)
S-POINT
[C]
active setpoint temperature
POWER
[%]
60
HE
Level 2
Level 3
Parameter level
or
61
Menu functions
Level 2
Level 3
Parameter level
Lower VALue
Upper VALue
or
and
62
HE
9.9.1.
CHANNEL 3
EPROG
CHANNEL 2
REG+E-PROG :
1. Select CHANNEL 1, 2 or 3
2. First define the desired output value for CHANNELs 1 to 3:
CHANNEL 1
REG+E-PROG
1.
3.
or
0V
Example 1:
10 C
210 C
200 K
197 C
202 C
5 K
0 mA
4 mA
20 mA
10 C
63
Menu functions
9.9.2.
CHANNEL 3
EPROG
CHANNEL 2
CHANNEL 1
REG+E-PROG
>
>
>
>FLOWRAT<
Indication on display
FLOWRAT
The E-Prog input can only be used either under menu item >CONFIG
-SP EXT< < or under menu item >CONFIG ACTVAR<
If the input is neither occupied by > SP EXT < or > ACTVAR <, the
signal of a flow meter can be connected.
CONFIG<
>
then >MENU IN/OUT<
>
>
>
64
HE
Examples:
4.
and
5.
and
Example:
Set the external voltage or current source output for the equivalent of
50 C temperature setpoint.
- to standard display.
Press
The temperature value adjusted and set on the external voltage or
current source is displayed in line 2 of the VFD COMFORT-DISPLAY for
control purposes. (Example: SP 50.00 C).
This EPROG input enables the use of different voltage and current
values as program parameters.
C
300
250
B
200
150
100
80
60
40
20
1 2 3 4 5 6 7 8 9 10
2 4 6 8 10
14
18 20 mA
65
Menu functions
Example out of diagram A:
Adjusting the voltage source for an output of 7.6 V!
The instrument calculates this value from the rise angle of the two
predecided end points (in example A: 7.6 V correspond to an external
setpoint temperature of 152.0 C ).
After returning the VFD display to standard display, this value is
displayed in line 2 (Example: SP 152.00 C).
Notice:
If this adjustment is not correctly performed at two different points, the setpoint setting
will be incorrect.
9.9.3.
Important:
The usable temperature range between > LVAL < and > UVAL < is limited to the
configured working temperature range of the circulator resp. of the unit combination
(working temperature range see technical specifications)
ALARM-output / Stand-by-input
Alarm output (10)
(for external alarm signal)
Possible parameters:
(STANDBY or ALARM or AL-STBY)
ALARM
Alarm-TYPE
Possible parameters:
( NORMAL or INVERS )
For >TYPE- NORMAL< pins 2 and 3 are connected in any case
according to the selected > AL-OUT Function<
For >TYPE- INVERS < pins 2 and 1 are connected in any case according
to the selected > AL-OUT Function<
Switching capacity
Switching voltage
Switching current
66
max.
max.
max.
30 W / 40 VA
125 V/
1A
HE
EX-STBY: External Stand-by input
(for external switch-off)
AK
Possible parameters:
STAND-BY
to start.
STAND-BY
67
The code for the cause of alarm is indicated on the VFD COMFORTDISPLAY.
Alarm without shutdown:
The code for the cause of alarm is indicated on the VFD COMFORTDISPLAY. The warning signal sounds in regular intervals. The messages
appear every 10 seconds.
68
HE
Error message with ticker:
>SENSOR DIFFERENCE ALARM-CHECK VISCOSITY AND PUMP STAGE<
Defect of working or excess temperature protector.
Working temperature sensor and excess temperature protector report a
temperature difference of more than 35 K.
Error message with ticker:
> INTERNAL HARDWARE ERROR-CALL SERVICE <
Other errors
Error in A/D converter
Error message with ticker:
> EXCESS TEMPERATURE PROTECTOR ALARM-CHECK ADJUSTMENT <
Excess temperature protector defect.
The protection temperature is below the set working temperature setpoint.
Set the protection temperature to a higher value.
Error message with ticker:
> EXTERNAL SENSOR ALARM-CHECK EXTERNAL SENSOR <
External control was set but the Pt100 external senor was not connected or is
defect.
Error message with ticker:
> CLEAN CONDENSER OR CHECK COOLING WATER <
Insufficient cooling of condenser. Clean the air-cooled condenser. Check the
flow and the temperature of the cooling water of a water-cooled condenser.
Error message with ticker:
> COMPRESSOR FAILURE-CHECK REFRIGERATOR <
Stage 1 of the compressors does not work.
Automatic restart after short cool-down, message E 21 goes off.
Stage 2 of the compressor does not work.
Cooling machine overload protection
The driving motor of the cooling compressor is equipped with an overload
protection which is triggered by increased internal temperatures or excessive
current consumption.
Shutdown can be caused by
- insufficient ventilation,
- insufficient wall distance,
- soiled condenser,
- high room temperature
- switching off and on in short sequence
Excess temperature in stage 1 of the compressor.
Excess temperature in stage 2 of the compressor.
Short circuit of control line to cooling machine during self-test.
69
4s
15
By quickly switching off and restarting the unit the alarm is cancelled.
If the error occurs once more after the restart, a remote diagnosis is required.
30
Warning:
Before exchanging the fuses, turn off the mains power switch and disconnect the
power plug from the mains socket!
Only use fine fuses with a nominal value as specified.
Fuses:
The mains fuses on the rear of the unit may easily be exchanged as
shown on the left.
Circulator: Fine fuses T 16 A , dia.5 x 20 mm
Cooling machine: Fuse T 10.0 A, dia.5 x 20 mm
Example:
70
Manufacturer
Schurter
Supplier
Schurter
Wickmann
Wickmann
Type
G-fuse insert SPT
T16A 5x20mm
G- fuse insert
T10,0A 5x20 mm
Order No.
No. 0001.2516
No. 19195
HE
ext. Pt100
Shield
Pt100
Plug
Look on
soldering side.
RS232C
PC (9-pol)
Pin 3 TxD
Pin 2 RxD
Pin 5 GND
Pin 8 CTS
Pin 7 RTS
Order No.
Description
8 980 073
8 900 110
71
Electrical connections
/ Control output
The connector may only be used for control of a JULABO refrigerated
circulator or JULABO MVS Solenoid valve controller for cooling water.
Pin assignment:
Pin
Signal (only with attached JULABO equipment)
1
+24 V (I max. current 25 mA)
2
0V
3
Alarm relay
4
Reserved - do not use!
5
Cooling pulse
Alarm output
(for external alarm signal)
This potential-free change-over contact is activated in case of an alarm
when pins 2 and 3 are connected.
Switching capacity
Switching voltage
Switching current
max.
max.
max.
30 W / 40 VA
125 V/
1A
ALARM
STAND-BY input
(for external emergency switch-off)
AK
Pin assignment:
2
3
STAND-BY
Pin
1
2
3
Signal
not connected
5 V / DC
0V
3
2
5
6
REG+E-PROG
Pin
1 Voltage output
2 Voltage output
3 GND for outputs
4 Programmer input
5 Current output
6 GND for Progammer
Channel 1
Channel 2
EPROG
Channel 3
72
Signal
0 ... 10 V
0 ... 10 V
0V
0 to 10 V / 0 to 20 mA
0 to 20 mA / 4 to 20 mA
0V
HE
5
9
1
6
RS232C
1. Check the interface parameters for both interfaces (on circulator and PC)
and make sure they match.
(Serial interface refer to page 50)
2. In the menu > MENU CONFIG < set
the menu item
to
12.2.
73
Remote control
12.3.
List of commands
Command
Parameter
Response of circulator
out_mode_01
out_mode_01
out_mode_01
out_mode_02
out_mode_02
out_mode_02
out_mode_03
out_mode_03
Selftuning off.
Temperature control by using the stored parameters.
Selftuning once
Single selftuning of controlled system after the next start.
Selftuning always
Continual selftuning of controlled system whenever a new
setpoint is to be reached.
Set external programmer input to voltage.
Voltage
0 V ... 10 V
Set external programmer input to current.
Current
0 mA ... 20 mA
out_mode_04
out_mode_04
out_mode_05
out_mode_05
out_mode_08
out_mode_08
out_sp_00
xxx.xx
out_sp_01
xxx.xx
out_sp_02
xxx.xx
out_sp_03
xxx.xx
out_sp_04
xxx.xx
out_sp_06
xxx.xx
out_sp_07
out_par_04
x.x
out_par_06
xxx
out_par_07
xxx
3 ... 9999
out_par_08
xxx
0 ... 999
out_par_09
xxx
out_par_10
xxx
1 ... 99.9
out_par_11
xxx
3 ... 9999
74
SubTemp
HE
Command
Parameter
Response of circulator
out_par_12
xxx
out_par_13
xxx
out_par_14
xxx
out_par_15
xxx
0 ... 200 C
out_par_16
xxx
0 ... 200 C
out_hil_00
-xxx
out_hil_01
xxx
0 ... 999
Command
Parameter
Response of circulator
version
none
status
none
in_pv_00
none
in_pv_01
none
in_pv_02
none
in_pv_03
none
in_pv_04
none
in_sp_00
none
in_sp_01
none
in_sp_02
none
in_sp_03
none
OverTemp
in_sp_04
none
SubTemp
in_sp_05
none
in_sp_07
none
in_sp_08
none
in_par_00
none
in_par_01
none
in_par_02
none
Si - Internal slope
in_par_03
none
Remote control
Command
Parameter
Response of circulator
in_par_04
none
in_par_05
none
in_par_06
none
in_par_07
none
in_par_08
none
in_par_09
none
in_par_10
none
in_par_11
none
in_par_12
none
in_par_13
none
in_par_14
none
in_par_15
none
in_par_16
none
in_mode_01
none
in_mode_02
none
in_mode_03
none
in_mode_04
none
in_mode_05
none
in_mode_08
none
in_hil_00
none
Selected setpoint:
0 = SETP 1
1 = SETP 2
2 = SETP 3
3 = Last setpoint setting was carried out
through an external programmer
Selftuning type:
0 = Selftuning off
1 = Selftuning once
2 = Selftuning alwayS
Type of the external programmer input:
0 = Voltage 0 V to 10 V
1 = Current 0 mA to 20 mA
Internal/external temperature control:
0 = Temperature control with internal sensor.
1 = Temperature control with external Pt100 sensor.
Circulator in Stop/Start condition:
0 = Stop
1 = Start
Adjusted control dynamics
0 = aperiodic
1 = standard
Max. cooling power (%).
in_hil_01
none
76
HE
12.4.
Status messages
Status messages
Description
00 MANUAL STOP
01 MANUAL START
02 REMOTE STOP
03 REMOTE START
12.5.
Error messages
Error messages
Description
Invalid command.
Value lies outside the adjusted range for the high and low
temperature warning limits. But value is stored.
77
Description
78
Turn off the unit with the mains switch and disconnect the
power plug.
Open the screws (A) and remove the dummy plate.
Carefully insert the upper edge (B) into the rear panel from
below, align the electronic module at top and bottom and
applying light pressure connect the 15-pole connector.
Attach the electronic module using the screws (A).
The circulator is ready for use. It automatically recognizes the
installed electronic module.
HE
79
To maintain the full cooling performance, clean the condenser from time to
time.
Switch off the unit, disconnect mains power cable.
Hold the venting grid, pull out and remove.
Clean the ribbed condenser with a vacuum cleaner.
Replace the venting grid.
Switch on the unit.
Cleaning:
For cleaning the bath tank and the immersed parts of the circulator, use
low surface tension water (e.g., soap suds).
Clean the outside of the unit using a wet cloth and low surface tension
water.
The circulator is designed for continuous operation under normal
conditions. Periodic maintenance is not required.
The tank should be filled only with a bath fluid recommended by JULABO.
To avoid contamination, it is essential to change the bath fluid from time to
time.
Repairs
Before asking for a service technician or returning a JULABO
instrument for repair, please contact an authorized JULABO service
station.
80
HE
WARRANTY PROVISIONS
INCIDENTAL OR CONSEQUENTIAL DAMAGES TO BUYER OR ANY THIRD PARTY AND ALL SUCH
DAMAGES ARE HEREBY DISCLAIMED.
6.
Assignment. Buyer shall not assign any of its rights or obligations hereunder without the prior
written approval of Seller; provided, however, that if Buyer is a distributor of Seller, the rights and obligations of Buyer
under these Warranty Provisions shall inure to the benefit of and be binding upon Buyers customers who provide the
products proof of purchase to Seller pursuant to the terms set forth herein. Seller may assign any or all of its rights or
obligations hereunder without Buyers prior consent.
7.
Governing Law. The Warranty Provisions and all questions relating to their validity, interpretation,
performance, and enforcement shall be construed in accordance with, and shall be governed by, the substantive laws
of the Commonwealth of Pennsylvania without regard to its principles of conflicts of law.
8.
Waiver. Any failure of the part of Seller to insist on strict compliance with the Warranty Provisions
shall no way constitute a waiver of such right. No claim or rights arising out of a breach of the Warranty Provisions by
Buyer may be discharged in whole or in part by a waiver of the claim or right, unless the waiver is in writing signed by
an authorized representative of Seller. Sellers waiver or acceptance of any breach by Buyer of any provisions of the
Warranty Provisions shall not constitute a waiver of or an excuse for nonperformance as to any other provision of the
Warranty Provisions nor as to any prior or subsequent breach of the same provision.
9.
Freight. Buyer will arrange and pay for shipping and handling charges for the unit to be returned to
the Seller.Seller will arrange and pay for shipping and handling for the return of the unit to the Buyer.
82