Ammonia Design 2520of 2520equipments
Ammonia Design 2520of 2520equipments
Ammonia Design 2520of 2520equipments
L ρg
= 0.56
G ρ l
At the top
Hence choosing the larger value of 0.61
From Graph
G 2f Fpψµ l0.2
= 0.038
ρ g ρl g
Where
Gf = gas superficial velocity
Fp = packing factor = 53 m-1
ψ = correction factor for density = 1.029
µl = viscosity of liquid in cp = 0.299
ρg = density of gas = 0.487 kg/m3
ρl = density of liquid = 934.4 kg/m3
g = acceleration due to gravity
On substituting we obtain
Gf =2.085 kg/m2 s
Operating G = 0.85Gf
= 1.772kg/m2s
Ac = Gb/G
Ac = 20.85/1.772
A = 9.948 m2
Di = 3.20 m
Lmin
LW =
ρ l aAc
Where
Lmin = minimum flow rate of liquid = 555.00 kg/s
ρl = density of liquid = 934.4 kg/m3
a = surface area of packing per unit volume = 92 m2/m3
wetting rate is greater than 0.85 ft3/ft hr hence no weeping will occur
Evaluation of tower height
Z = H OG N OG
Gm
H OG = H g + m Hl
Lm
For ring type of packings
0.15
ϕC Z
Hl = Scl0.5
3.28 3.05
ϕ = correlation parameter for a given packing = 0.11
C = correlation parameter for high gas flow rates = 0.5
Scg = Schmidt no for liquid phase = 163.6
Z = tower height
On substitution
Hl = 0.181Z0.15
m = slope of the equilibrium curve =11.25
Lm = 100449.7 kmol/hr
Gm = 9643.0 kmol/hr
Overall number of transfer units in the gas phase
1 1 + Yb
Yb
dY
N OG = ∫Y Y − Y * 2 ln 1 + Yt
−
t
Y Y* 1/(Y-Y*)
0.005 0 200
0.015 0.005 100
0.025 0.010 66.67
0.035 0.015 50
0.045 0.020 40
0.055 0.025 33.33
0.065 0.032 30.30
0.075 0.039 27.78
0.085 0.047 26.32
0.095 0.057 26.32
0.105 0.065 25
0.115 0.075 25
0.125 0.083 23.81
0.135 0.095 25
0.145 0.100 22.22
0.155 0.107 20.83
0.165 0.116 20.41
0.175 0.128 21.17
0.185 0.138 21.17
0.195 0.151 22.73
0.205 0.164 24.49
0.210 0.171 25.64
0.215 0.180 28.57
0.215
dY
∫
0.005
Y −Y*
= 7.284 + 0.259 = 7.543
Z = 5.0 m
It is assumed that cooling water inlet temperature is 293 K and exit temperature
is 308 K.
Amount of cooling water mc = Q/Cp ∆T = 79.4 kg/s
Inlet temperature t1 = 293 K
Outlet temperature t2 = 308 K
LMTD =
(T1 − T2 ) − (t 2 − t1 )
T − T2
ln 1
t1 − t 2
= 50.38 K
T1 − T2
R= = 6.46
t 2 − t1
t 2 − t1
S= = 0.12
T1 − t1
Routing of Fluids
The gases are taken on shell side. Cooling water is taken on the tube side.
Q
A= = 242.83m 2
U d (LMTD )C
For the exchanger 1 inch 16 BWG tubes are chosen
do = 25.4 mm
di = 22.1 mm
area of tube per unit length = 0.2168 ft2/ft
Assumption is made that the tubes are of length 16 ft
Hence the area per tube a = 4.1888 ft2 = 0.3333 m2
No of tubes
A
Nt = = 730
a
From the tube count table we have for 1 inch o.d tubes on 1.25 inch square pitch
Nt =738 Np = 4 Ds = 1067 mm
Hence corrected area for heat transfer A =Nt x a = 245.97 m2
Thus corrected coefficient of heat transfer Uac = 341 W/m2 K
Velocity
Tube side
Tube cross sectional area for flow of fluid in one tube pass
π 2 Nt
aT = di = 0.0708m 2
4 Np
where
di is the tube inside diameter =22.1 mm
Nt is the number of tubes =738
Np is the number of tube passes =4
mC
vT = = 1.125 m
aT ρ T s
where
mc is the mass flow rate of cold water
ρt is the density of tube side fluid
The velocity of a liquid should lie between 1 and 2 m/s which is satisfied.
Shell Side
Shell side cross sectional area for fluid flow
aS =
(P0 − d o )l s Ds = 0.1423m 2
Po
Where
Po = pitch = 31.75 mm
do = outside diameter = 25.4 mm
Ds = shell inside diameter = 1067 mm
ls = baffle spacing assumed to be 0.5 Ds = 534mm
Shell side velocity is given by
ms
vs = = 10.325 m
as ρ s s
Where
ms = shell side mass flow rate
ρs = shell side fluid density
The velocity of flow for gases must lie between 10 and 40 m/s which is satisfied
Tube side
Reynolds number
ρvd i
Re = = 27524.8
µ
Where
µ is the viscosity of fluid
ρ is the density of fluid
dI is the inside diameter of tube
Prandtl number
µC p
Pr = = 10.75
k
Where
Cp is the specific heat capacity
k is the thermal conductivity
Nusselts equation is given as
ρv s d o
Re = = 53759
µ
Prandtl number
µC p
Pr = = 0.94
k
By Deitus Bolter equation Nusselts number
1 1 1 d 1 1 ln (d o d i )
= + + i + + d i
U ht htd d o hs hsd k
Where
hd represents the dirt coefficient. It is assumed to be 2839 W/m2 K for both shell
and tube side
On substitution we obtain
U = 366.4 W/m2 s
The design value is larger than the assumed value. Hence design is safe.
Pressure Drop
Tube side
Re = 27524.8
ρv 2
∆Pc = 2.5 t = 1576.25 N m 2
2
∆Pt = N p (∆PL + ∆Pc ) = 19.842kPa
Where
Np is the no of tube passes =4
The pressure drop for liquids must lie between 14 and 70 kPa. Hence the design
is safe from view of pressure drop on the tube side.
Shell Side
Pressure drop in the cross flow section
0.14
f W 2N µw
∆Pbk = b k 2 c
ρS m µl
fk is the ideal tube bank friction factor =0.104
W is the mass flow rate = 23.8 kg/s
D s [1 − 2(l c Ds )]
Nc = = 16.8
Pp
Nc is no of tube rows crossed in one cross flow section
lc is the baffle cut =0.25 Ds
Pp is pitch parallel to flow = 31.75 mm
Ds is the shell inside diameter =1067 mm
ρ is the fluid density = 20.3 kg/m3
Sm is cross flow near centerline for one cross flow section = 0.1423 m2
∆Pbk = 0.4555 kPa
Pressure drop for an ideal window section
W 2 (2 + 0.6 N cw )
∆Pwk = b
SmSw ρ
b =2 x 10-3
Sw is for flow through window =0.1598 m2
∆Pwk = 0.3657 kPa
N
∆P = [(N b − 1)∆Pbk + N b ∆Pwk ]+ 2∆Pbk 1 + cw
Nc
L
Nb = −1 = 8
ls
∆P = 7.845 kPa
The pressure drop for gases should be between 2 and 20 kPa. Hence the design is
safe on shell side also
MECHANICAL DESIGN OF ABSORBER
Material for shell is Carbon Steel
THICKNESS OF SHELL
Thickness of shell = ts
pD
ts = +c
2 fJ + p
Where,
Di = Inner Diameter of vessel = 3.2m
Working Pressure = 1 atm = 1.054kgf/cm2
p = Design Pressure = 1.1 x 1.054 = 1.137 kgf/cm2
f =Permissible Stress = 950 kgf/cm2
J= Joint Efficiency = 0.85
c= Corrosion allowance =2mm
ts = 6mm
thickness of shell is 6mm
th= 6mm
Axial Stress Due to Pressure
Axial stress due to pressure =fap
pDi
f ap =
4(t s − c )
= 355.4 kgf/cm2
Stress due to Dead Load
a) Compressive Stress due to weight of shell up to a distance X
Do = Di + 2 ts =3.212m
Density of Shell material = ρs = 7700 kg /m3
π 2
(Do − Di2 )ρ s X
f ds = 4
π 2
(Do − Di2 )
4
=.77X kgf/cm2
b) Compressive stress due to weight of insulation at height X
Insulator used is asbestos
Thickness of insulation = tins =100mm
Diameter of insulation = Dins
Density of insulation =2300 kg / m3
Mean diameter of vessel = Dm
For large diameter column
Dins = Dm
πDins t ins ρ ins X
f ins =
πDm (t s − c) )
= 1.925 kgf/cm2
c) Compressive stress due to liquid in column up to height X
Density of liquid =ρl = 934.4 kg/m3
π 2
Di ρ l ε
f liq = 4
πDm (t s − c )
= 23.29 kgf/cm2
d) Compressive stress due to attachment
i. Packing weight
ii. Head weight
iii. Ladder
Density of packing (pall ring) = 270 kg /m3
π 2
Di ρ p X
Packing Weight = 4
πDm (t s − c )
Where,
Pressure due to wind = Pw = 125 kgf/m2
=0.2778 X2 kgf/cm2
Downwind side
Jftmax = -fwx - fap -fdx
807.5 = -365.4-3.1792-39.645 X +0.2778 X2
Solving for X for compressive stresses
X=167 m
Hence the column will support a height of 5m as the calculated height is much
higher than 5 m in both cases
FLANGE THICKNESS
Thickness of flange = tf
tf= [G√(p/K f) ] + c
Where,
K=1/[ 0.3 + ( 1.5 Wm hG)/H x G]
Hydrostatic end force = H = (π /4) G2 p
=2.003 x10 6 N
hG is radial distance from gasket load reaction to bolt circle,
hG = ( B – G )/ 2
= 0.0155
B = outside diameter of gasket + 2 x diameter of bolt + 12mm
= 4.927 m
Wm = 2.039 x 10 6 N
K= 3.28
Hence the thickness of flange = 90.47 mm
NOZZLE THICKNESS
Material Carbon steel
Considering diameter of nozzle = Dn =150 mm
Thickness of nozzle =tn
Material is Stainless steel ( 0.5 cr 18 Ni 11 Mo 3)
Permissible stress =130 x 10 6 N/m2
J=0.85
pD
tn =
2 fJ − p
tn = 1.24mm
No corrosion allowance , since the material is stainless steel.
We can use thickness of 3mm
SUPPORT FOR ABSORBER
Material used is structural steel ( IS 800)
Skirt support is used.
Inner Diameter of the vessel = Di =3.2m
Outer Diameter of the vessel = Do =3.212m
Height of the vessel = H = 5.0m
Density of carbon steel= ρs = 7700 kg /m3
Density of liquid = ρl = 934.4 kg /m3
Total weight = Weight of vessel+ Weight of Attachments (liquid+ packing + head
+ ladder)
=59430 kg
total stress due to dead loads
∑ w 59.00
f ds = = kgf/cm2
πDm t t
p1 = 128.5 kgf/m2
h1=8m
1.4 p1 H 2 0.054
f wb = = kgf/cm2
πDm t t
Stress due to Seismic Load
Load F= CW
W is total Weight of vessel
C is Seismic Coefficient =0.08
8CWH 0.2246
f sb = = kgf/cm2
3πDo t t
tB= 63mm
Anchor Bolt,
Wmin=45000 kg (assumed)
fc = (Wmin/ A ) – (Mw /Z)
= 1.115 kgf/cm2
Fc is positive ,hence anchor bolts are not required if the safety factor is above 1.5
Wmin R
j=
Ms
= 7.45
The safety factor is above 1.5. Hence anchor bolts are not required.
MECHANICAL DESIGN OF SHELL AND TUBE HEAT
EXCHANGER
NOZZLE THICKNESS
Material used is carbon steel
Considering diameter of nozzle to be 150mm
Permissible stress = f = 950 kgf/cm2
Corrosion allowance = 3mm
pDi
th = +c
2 fJ − p
=5mm
HEAD THICKNESS
pRiW
Thickness of head = t h = +c
2 fJ
1
W = 3 + Ri =1.77
4 ri
Hence th = 60 mm thickness
TRANSVERSE BAFFLE
Spacing between baffles as = 534 mm
Flange Thickness
Inner diameter of flange =Dfi = 1143 mm
Outer diameter of flange = 1167mm
Gasket Size G=1155 mm
Material is Steel Jacketed asbestos
Width of gasket =N = 24 mm
Gasket factor = m = 3.75
Minimum design seating stress = ya= 5.34 kgf/cm2
Basic gasket seating width bo = N/2
bo = 24 mm / 2 = 12 mm
Effective gasket seating width
b = 2.5 ( bo )0.5 = 9 mm
under atmospheric conditions, the bolt load due to gasket reaction is given by
Wm1 = πbGYa = 100500 kg
Design pressure = p = 50.9 kgf/cm2
After the internal pressure is applied, the gasket which is compressed
earlier, is released to some extent and the bolt load is given by
π 2
Wm 2 = 2πbGmp + G p = 667719 kg
4
Thickness of flange = tf
p
tf = G +c
kf
Where,
1
k=
1.5wm hg
0.3 +
HG
π 2
Hydrostatic end force = H = G p
4
hG is radial distance from gasket load reaction to bolt circle,
hG = (B – G )/2
=37.5 mm
B = bolt circle diameter
wm is the greater of the two loads in this case Wm2
Hence the thickness of flange = 138.8 mm
TUBE SIDE
Stainless steel ( IS- grade 10)
Tube thickness
pD
tt =
2 fJ + p
Where,
Working pressure = 1atm = 1.054 kgf/cm2
Design pressure = p =1.1 times 1.054 = 1.136 kgf/cm2
Permissible Stress =f = 950 kgf/cm2
J=1 for seamless tubes
Thickness of tube =0.2 mm
The thickness of tubes is taken as 2 mm with no corrosion allowance as the
material is made of stainless steel.
Tube Sheet
The tube sheet is held between shell flange and the channel. The joint on the shell
flange side is of male and female facing and on the channel side of ring facing,
since the pressure on the channel
Thickness of Tube Sheet
kp
t ts = FG
f
Where F = 1
K=0.25
Thickness of tube sheet = 18 mm
Channel and Channel Cover
Carbon Steel
Thickness of channel
Permissible stress = f = 95 kgf/cm2
K=0.3
Thickness of channel
kp
th = G
f
Substituting the values the thickness of the channel and channel cover is
obtained as 19mm
Flange Joint
Gasket material is steel jacketed asbestos
Gasket width (N) = 22 mm
Gasket factor = m = 5.5
Minimum design seating stress = Ya= 12.66 kgf/cm2
Basic gasket seating width bo = N / 8
bo = 2.75 mm
Effective gasket seating width
b = bo
Mean diameter = G = 1000mm
Design pressure = p = 1.136 kgf/cm2
Wm1 = πGby a
Under atmospheric conditions, the bolt load due to gasket reaction is given by
= 10002 kgf
After the internal pressure is applied, the gasket which is compressed
πG 2 p
Wm 2 = 2bπGmp +
4
earlier, is released to some extent and the bolt load is given by
= 109374 kgf
Bolt used is hot rolled carbon steel
fa is permissible tensile stress in bolts under atmospheric condition
fb is permissible tensile stress in bolts under operating condition
For Cr Ni Steel,
fa= 1406 kgf/cm2
fb = 66 kgf/cm2
Wm1
Am1 =
fb
=7.114 cm2
Wm 2
Am 2 =
fa
= 16.572 cm2
Am is larger area of Am1 and Am2 =16.572 cm2
Number of bolts = mean diameter / bo x 2 = 40 bolts
To determine the size of bolts , the larger of above two areas should be
considered
Am
db =
4π
= 36 mm
Using M 48 bolts
Pitch diameter = 44.68 mm
Minor diameter = 41.795 mm
π
Ab = (4.4681 + 4.1795)2
8
Actual bolt area is given by
= 19.66 cm2
Minimum pitch diameter = G +N+2db = 1118mm
Hence Bolt diameter is chosen as B= 1150 mm
p
tf = G +c
kf
1
k=
1.5Wm hG
0.3 +
HG
Flange Thickness
=2.91
Hence tf = 25 mm
THICKNESS OF NOZZLE
Considering inlet and outlet diameter to be 200mm
pD
tn =
2 fJ + p
Thickness of nozzle
= 1 mm
Thickness of nozzles is taken as 6mm
SUPPORT FOR SHELL AND TUBE HEAT EXCHANGER
Length of the heat exchanger = 4.88m
InnerdiameterofShell=1067 mm
Outer diameter of Shell = 1137 mm
Inner diameter of tube = 22.1 mm
Outer diameter of tube = 25.4 mm
Number of tubes =738
Density of Steel =ρs =7850 kg /m3
Density of Liquid =ρl = 995.3 kg/m3
Volume of Shell body = V = (π / 4) ( Do2 – Di2 ) x L
= 0.591m3
Weight of Shell body = Ws = V x ρs
= 4479 kg
Volume of Tubes = Vt = ( π / 4 ) ( do2 – di2 ) x L x N
= 0.44 m3
Total Weight of Tubes = Wt = Vt x ρs
= 3360 kg
Volume of Head = Vh = 0.087 Di3
= 0.106m3
Weight of Head = Wh = Vh x ρs
= 801 kg
Weight of Liquid = Wl = ( π / 4) (di2) x L x N x ρl
= 10845 kg
Total Weight = W = Ws+ Wt + Wh + Wl
= 19485 kgf
Q =W/2 =9742.5 kgf
Distance of saddle center line from shell end =A= 0.6 x Ri
=320 mm
Longitudinal Bending Moments
Radius = R =1.067m
Height of head =H = 0.136 m
The bending moment at the supports is
M1 = QA [ 1 – {(A/L)+ (R2 - H2) / 2 AL}/{1 + 4H/3L}]
= 1842.6 kgf m
The bending moment at the center of the span is given by
M2 = ( Q L / 4)[{1+ 2 ( R2 - H2 ) / L2 }/{1+ 4H / 3L} - ( 4A / L) ]
= 2131kgf m