Ruben
Ruben
Ruben
Benchtop Spectrophotometer
Operation Manual
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OPERATION
MANUAL
CE Declaration
Manufacturer's Name: X-Rite, Incorporated Authorized Representative: X-Rite, Incorporated Siemensstrae 12b 63263 Neu-Isenburg Germany Phone: +49 (0) 61 02-79 57-0 Fax: +49 (0) 61 02 -79 57-57 Model Name: Model No.: Directive(s) Conformance: Color i5 CI5 EMC 89/336/EEC LVD 73/23/EEC
Note: This is a class A product. In a domestic environment this product may cause interference in which case the user may be required to take adequate measures.
Equipment Information
Use of this equipment in a manner other than that specified by X-Rite, Incorporated may compromise design integrity and become unsafe. WARNING: This instrument is not for use in explosive environments.
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Proprietary Notice
The information contained in this manual is derived from patent and proprietary data of X-Rite, Incorporated. The contents of this manual are the property of X-Rite, Incorporated and are copyrighted. Any reproduction in whole or part is strictly prohibited. Publication of this information does not imply any rights to reproduce or use this manual for any purpose other than installing, operating, or maintaining this instrument. No part of this manual may be reproduced, transcribed, transmitted, stored in a retrieval system, or translated into any language or computer language, in any form or by any means, electronic, magnetic, mechanical, optical, manual, or otherwise, without the prior written permission of an officer of X-Rite, Incorporated. This product may be covered by one or more patents. Refer to the instrument for actual patent numbers. Copyright 2011 by X-Rite, Incorporated ALL RIGHTS RESERVED
X-Rite is a registered trademark of X-Rite, Incorporated. All other logos, brand names, and product names mentioned are the properties of their respective holders.
Warranty Information
X-Rite, Incorporated (X-Rite) warrants each instrument manufactured to be free of defects in material and workmanship for a period of 12 months, unless different local regulations apply. This warranty shall be fulfilled by the repair or replacement, at the option of X-Rite, of any part or parts, free of charge including labor, F.O.B. its factory or authorized service center. This warranty shall be voided by any repair, alteration, or modification, by persons other than employees of X-Rite, or those expressly authorized by X-Rite to perform repairs, and by any abuse, misuse, or neglect of the product, or by use not in accordance with X-Rites published instructions. X-Rite reserves the right to make changes in design and /or improvements to its products without any obligation to include these changes in any products previously manufactured. Correction of defects by repair or replacement shall constitute fulfillment of all warranty obligations on the part of X-Rite. THIS WARRANTY IS EXPLICITLY IN LIEU OF ANY OTHER EXPRESSED OR IMPLIED WARRANTIES, INCLUDING ANY IMPLIED WARRANTY OF MERCHANTABILITY OR FITNESS FOR ANY PARTICULAR PURPOSE. THIS WARRANTY OBLIGATION IS LIMITED TO REPAIR OR REPLACEMENT OF THE UNIT RETURNED TO X-RITE OR AN AUTHORIZED SERVICE CENTER FOR THAT PURPOSE. This agreement shall be interpreted in accordance with the laws of the State of Michigan and jurisdiction and venue shall lie with the courts of Michigan as selected by X-Rite, Incorporated.
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Table of Contents
Before using your spectrophotometer Safety first! Performance and Environmental Specifications Whats in the box? Optional Accessories Installation Sample Preview Methods Sample Door Computer Monitor Used for Sample Preview Installing the Computer Monitor and Cabling for Sample Preview Instructions for Category A: RS-232 Instrument Control Setup Instructions for Category B: USB Instrument Control Setup Optional LCD Sample Preview Monitor 4 4 5 6 6 7 7 8 9 9 9 10 10
Operation
Status Panel Programmable Status Panel Buttons Calibration Reflectance Calibration Procedure Transmission Calibration Procedure Taking Reflectance Measurements Taking Transmission Measurements Transmission Measurement Setup Film Measurements Liquid Measurements Initiating Measurements Instrument Modeling UV Control Aperture Control Specular Control
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WELCOME
The Color i5 laboratory spectrophotometer is a mid-range spectrophotometer with an array of advanced product features to accurately measure a variety of samples. Your Color i5 Spectrophotometer offers these features: Tri-Beam technology that measures Specular component included and excluded for gloss assessment. Multiple areas of view in both reflectance and transmittance. Self-adjusting, dual zoom lens that eliminates configuration errors between aperture plates and lens position. Video preview for measurement accuracy and targeting purposes. Automated ultra violet adjustment when measuring fluorescent or optically brightened samples. USB and RS-232 interfaces that eliminate connectivity issues. Clear status panel display with dual remote read buttons for standard and sample measurements and warning indicators for calibration interval. Dampened sample arm holder that prevents sample damage. Supports Embedded NetProfiler.
Safety first!
Your Color i5 spectrophotometer is very safe to use. However, like all electronic equipment you must follow these common sense safety guidelines to ensure your personal safety and the future integrity of the unit. PLEASE READ AND FOLLOW INSTRUCTIONS It will be helpful to you if you review this document completely before you attempt to install and use your Color i5. RETAIN THIS MANUAL FOR FUTURE REFERENCEKeep this manual handy for others to read or refer to when they need to operate the unit. OBEY WARNINGSPlease follow all of the precautions described in this operation manual. If you use your spectrophotometer in a manner not intended, the built in safety protection may be impaired. PROTECT FROM WATER AND MOISTUREDo not use your spectrophotometer in an area where there is a possible hazard of electric shock from spilled water or other liquids or uncontrolled moisture. NOT FOR USE IN AN EXPLOSIVE ENVIRONMENT!- Do not use your spectrophotometer in an area where there is the possibility of explosions.
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Performance Specifications Repeatability Inter-Instrument Agreement Geometry Illumination Measurement time Duty cycle Spectral Range Wavelength Interval Photometric range Photometric resolution 0.03 RMS E CIELAB White tile 0.15 Avg. 13 BCRA Series II tiles SCI D\8 Tri-beam simultaneous SCE\SCI Pulsed Xenon, D65 Calibrated 2.5 seconds (flash & data acquisition) 480 measurements per hour max 360 to 750 nm 10 nm 0.0% to 200% 0.01% reflectance
Environmental Specifications Electrical Requirements Operating Temperature Storage Temperature Altitude Pollution Operating Humidity Storage Humidity Dimensions Weight Interface 100-240 VAC/50-60 Hz, UL Category II AC line input is 1.5 amps. 10 C to 35 C -20 C to 55 C Maximum 2000M UL Category 2 20% to 80% relative, non-condensing 05% to 90% relative, non-condensing 23 cm W x 25 cm H x 47 cm D 12 kgs USB/RS-232/38400 baud
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Optional Accessories The following are optional items you may purchase for your Color i5. You may have already purchased some of these optional accessories. Please refer to Spare Parts and Accessories on for ordering information. LCD preview monitor Application software kit NetProfiler standards and subscription Stand for Horizontal Measurement Plane Toggle Pad Subassembly with White Ceramic Backing: User-installable replacement toggle pad that includes an embedded white ceramic backing Transmission kit (Accessory/transmission box)
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Installation
To install your spectrophotometer you need to follow these steps. 1. Locate the 12-volt Power Supply in the shipping carton. Connect the single-pin end to the spectrophotometer and connect the three-prong end to a power receptacle.
Back of i5 Connections 2. Install the PC-based software driver using the Driver/Documentation CD. Always install the driver before connecting the spectrophotometer to the PC. 3. Connect your computer to the spectrophotometer using either USB or RS232, but not both. Note: Under the standard configuration of the spectrophotometer, you can use the USB connection or your RS-232 cable to send and receive measurement data. If the RS-232 connection is used the COM port should be set to 38.4k baud, 8 bit no parity. Do not simultaneously use the USB and the RS-232 cable 4. Locate the on/off switch at the rear. The Status LED will flash for 5 seconds to indicate the power up sequence. 5. The spectrophotometer will then test the UV and zoom mechanisms. The appropriate LEDS will flash during the test. The LEDs will stop flashing to indicate successful power on diagnostics.
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Sample Door
The Color i5 sample door is capable of opening for a completely unobstructed view of the sample presented at the view port. When completely open, the sample door allows you to adjust the sample at the view port for optimal placement. To use the Sample Door, proceed as follows: 1. Open the sample arm by grasping it and pulling it towards you. Place your sample at the view port and close the sample arm. 2. Using your fingertips, open the door at the pry notches and gently lower the door to the complete open position. See the figure below.
Pry notch
Pry notch
Sample door
Figure 1. Opening the hinged sample door 3. With the Sample Door completely open, view the sample at the view port and make sure the sample is in an optimal position for measuring.
Figure 2. Observing the sample through the viewport opening 4. Close the Sample Door. Prepare for measurement.
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Instructions for Category B: USB Instrument Control Setup Note: Make sure you have installed the Color i5 Driver software before proceeding. Following the order of the setup steps is very important. 1. Insert the USB PC connector to the USB port on your computer. 2. Insert the USB PC connector to the USB- B port on the Ci5. 3. You should now have the USB Cable connected to your PC and instrument. Install the USB Video Adapter Driver Software. To do this, load the Adapter CD into your CDROM drive. The installation will automatically begin. Follow the prompts on your computer screen to complete the installation. Do not proceed to the next step until you complete the Adapter Driver Installation. 4. Insert the USB connector on the Adapter (at the end of the single cord) to the USB-A port on the Ci5. 5. Insert the RCA connector on the Adapter to the top Sample Preview Monitor port on the Ci5.
Monitor stem
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5. Connect the DIN-8 connector from the Preview Monitor to the DIN-8 connector on the supplied cable. 6. Connect the yellow connector on the cable to the video out connection at the rear of the instrument. 7. Connect the black connector on the cable to the monitor power connection at the rear of the instrument. NOTE: The white and red connectors on the cable are not required for this installation.
8. Press the power button on the side of the monitor to turn it on. When powered on, whatever sample is currently on the view port is seen on the display.
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OPERATION
Status Panel
Trial button Preview button Standard button
Aperture Setting: Possible choices are LAV (Large Area of View) MAV (Medium Area of View) SAV (Small Area of View) * This LED will blink if the zoom lens setting and the installed aperture plate do not match.
NetProfiled: Green (enabled) Yellow (not enabled) Blank (not NetProfiled) Blinking (run NetProfiled again) UV Setting: Possible choices are D65 Excluded Adjusted Position 1 Adjusted Position 2 Calibrated: Red (Uncalibrated) Green (Calibrated)
Measurement Type: Possible choices are Transmission (LED will blink if the instrument is configured for Direct Transmission, steady for Total Transmission Reflection
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Calibration
Calibration is recommended every 8 hours of spectrophotometer operation. Each spectrophotometer configuration that is used should be calibrated. A configuration consists of four components: Measurement Mode: Transmission or Reflectance Aperture size (SAV, MAV, LAV) Specular included or excluded condition (SCI or SCE) UV included or excluded condition. Different UV calibrator positions do not constitute a required calibration configuration. The spectrophotometer automatically measures Specular included and excluded for every reflectance configuration.
Reflectance Calibration Procedure To calibrate your spectrophotometer in Reflectance Measurement Mode you need to use your application software. Follow these steps: 1. Launch the calibration process from the software interface. 2. You will be prompted to present and then remove the calibration tile and to prepare for the black trap. 3. Once the calibration process is complete, the Calibrated LED becomes lit. Any change to the spectrophotometer configuration may result in the calibration LED turning from green (calibrated) to red (not calibrated). Remember that each configuration needs to be calibrated. Transmission Calibration Procedure To calibrate your spectrophotometer in Transmission Measurement Mode you need to first locate the following items in your transmission kit box: Spectralon Plaque Transmission Sample Holder Black Plastic Blocking Panel
Caution: Care should be taken with the Spectralon plaque as the surface is very fragile. 1. Using your application software launch the calibration process from the software interface. 2. Mount the Spectralon Plaque to the measurement port at the front of the instrument. Follow any prompts from the software regarding the white calibration. 3. When you are prompted for the Black Calibration, place the Sample Transmission Holder inside the Transmission compartment and load the Black Plastic Blocking Panel in the Transmission sample holder. For more information on loading the Sample Transmission Holder in the Ci5, refer to Taking Transmission Measurements. 4. Click OK to any message for black trap calibration. 5. Once the calibration process is complete, the Calibrated LED becomes lit. Any change to the spectrophotometer configuration may result in the calibration LED turning from green (calibrated) to red (not calibrated). Remember that each configuration needs to be calibrated.
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Front of instrument
Front of instrument
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3. Align the sample holder base plate pins to the base plate mounting channel holes inside the transmission area. There are mounting holes in the channel at both the sphere and the lens. For total transmission measurements, position the base plate with the clamp mounting holes on the sphere side. For direct transmission measurements (LAV only), position the base plate with the clamp mounting holes on the lens side.
Sphere Side
Front of instrument Clamp mounting holes
Lens Side
Sphere Side
Lens Side
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Film Measurements 1. Attach the appropriate stop to the base plate and clamp to the carriage base with the thumb screws. For total measurements, make sure the stop is position against the sphere before tightening the thumb screws. For LAV, sample contacts the sphere. No stop is recommended.
Sample clamp Sample stop for SAV and MAV. Stop not recommended for LAV.
Carriage base Stop thumb screw (2) Carriage base thumb screw Base plate
2. Pull the clamp back and position the sample between the clamp and stop (refer to figures 7 and 8). You may want to temporarily tighten the carriage base thumb screw to hold the clap in place while positioning the sample. Slowly release the sample clamp/carriage base to secure the sample. Liquid Measurements 1. Loosely attached the flow cell stand assembly to the carriage base with two thumb screws. A clamp is not required for this measurement. 2. Slide the flow cell stand forward and tighten the thumb screws. 3. Insert the cuvette into the flow cell stand.
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Initiating Measurements 1. Trigger the measurement using one of the following methods: a. Select "Measure Standard" or "Measure Trial" from your application software interface. Follow the software instructions for loading the sample at the view port. OR b. Press the Standard or Trial button on the Color i5 Status Panel. 2. The measurement is taken. The data are presented to you in your application software. Follow the instructions for saving the data in the software.
Instrument Modeling
The Color i5 is already configured to model CE7000 measurements. However, the spectrophotometer can be configured to model CE3100 measurements. If you require backward data compatibility with the older CE3100 this mode should be selected in your application software. To use this feature, simply connect your spectrophotometer to your computer and choose CE3100 as the instrument selection in your application software interface. Take measurements as you normally would. The data provided by the Color i5 will simulate those that would have been taken by the CE3100.
UV Control
Your spectrophotometer is equipped with an automated 400nm UV filter. This can be set to fully Exclude the UV portion of the light source in the spectrophotometer or can be used to calibrate and adjust the UV level, for instance to match the UV component of D65 daylight. The Color i5 supports 3 pre-selected UV calibration positions for the filter you may wish to calibrate to D65 or other levels of UV. A UV illuminant checker is provided that has been calibrated with a CIE whiteness value for true D65. Your application software will drive the UV calibrator making successive measurements until it finds the correct calibrator position to give this value (Adjusted Position 1 and Adjusted Position 2).
Aperture Control
To change the aperture setting on the spectrophotometer you need to use your application software and the Aperture Plates. Select an aperture setting of SAV, MAV, or LAV.
Note: If you select the auto zoom lens option from your application software the spectrophotometer automatically moves the zoom lens whenever you change the aperture plate. In the Control Panel dialog box of your application software verify the "Auto" box is checked under the Area of View information on the Configuration tab. If you prefer to not have matching Area of View and Zoom Lens setting (to have a different illumination setup), do not check this box. If the zoom position and the installed aperture plate do not match, the Aperture LED will blink to indicate this discrepancy.
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Aperture rim
Aperture plate
Sample arm
Figure 13. Mounting the Aperture Plate on the Spectrophotometer 1. Prepare the aperture plate to be installed and make sure it is nearby. 2. Open the sample arm to the fully open position. 3. Open the sample preview door. Apply pressure at the back of the plate if necessary to remove it. 4. Locate the plate to be installed and fit the aperture over the rim on the spectrophotometer. Press the new plate firmly into place. The plate is magnetized to prevent it from falling out. 5. Gently close the sample arm.
Specular Control
To change the Specular Component setting on the spectrophotometer you need to use your application software. Select the desired Specular Component Setting- Included (SCI) or Excluded (SCE). Be sure to save the setting. You will notice the LED for either setting becomes lit based on your selection. The Color i5 simultaneously measures Specular included and Specular excluded for all reflectance measurements. Your application software should decide which measurement data to request from the spectrophotometer according to the user requirements.
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TECHNICAL SERVICE
In the event that you are unable to solve a problem, you may contact our Technical Service Department. Corporate Headquarters - USA 4300 44th Street SE Grand Rapids, Michigan 49512 Phone 1 800 248 9748 or 1 616 803 2100 Fax 1 800 292 4437 or 1 616 803 2705 Corporate Headquarters - Europe Althardstrasse 70 8105 Regensdorf Switzerland Phone (+41) 44 842 24 00 Fax (+41) 44 842 22 22 Corporate Headquarters - Asia 36th Floor, No. 169 Electric Road Hong Kong, China Phone (852) 2568 6283 Fax (852) 2885 8610 Please visit www.xrite.com for a local office near you.
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A-VPM/I57LCD GM29021020
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Corporate Headquarters - USA 4300 44th Street SE Grand Rapids, Michigan 49512 Phone 1 800 248 9748 or 1 616 803 2100 Fax 1 800 292 4437 or 1 616 803 2705 Corporate Headquarters - Europe Althardstrasse 70 8105 Regensdorf Switzerland Phone (+41) 44 842 24 00 Fax (+41) 44 842 22 22 Corporate Headquarters - Asia 36th Floor, No. 169 Electric Road Hong Kong, China Phone (852) 2568 6283 Fax (852) 2885 8610