Foul Condensate8

Evaporators for Stillage Concentration
Evaporation for Stillage Concentration

The spent residues that result as by-products from sugar and starch processes, yeast production, fermentation processes and alcohol distilleries are generally called spent wash, vinasses or stillage. Depending on the raw materials being processed, the following stillages exist: Molasses (vinasses) Grain stillage: wheat, rye, maize, triticale, sorghum stillage Potato stillage Whisky stillage (barley, pot ale) Yeast stillage These thin liquor stillages contain all the nutrients of the raw materials except for their fermented starch and sugars: i.e. they contain proteins, fat, fibre, minerals etc. in greater concentrations than were present in the original raw material. These liquors can therefore be processed into added-value animal feeds by concentration and, if necessary, drying and crystallisation/precipitation of certain seals (e.g. potassium, sodium). GEA Wiegand has a global reputation as a specialist engineering company, with a reputation that goes back nearly 100 years. Furthermore, GEA Wiegand has extensive expertise in the range of upstream and downstream processes and unit operations required in the field of stillage concentration.

Fig. 1: Diagram of an alcohol plant with a thermally integrated stillage concentration system
Raw Material
Decanter
Thin Stillage Wet Cake
Milling / Disintegration
Raw Stillage
Live Steam
Animal Feeds wet
Evaporator
Fermentation
Distillation
Exhaust Vapour
Concentrate
Condensate
Mash
Dryer
Animal Feeds dry
Concentration and temperature

The thin stillages resulting from alcohol distilleries typically have a concentration range of between 5 and 10 % TS. The final concentration that can be achieved depends on the type of raw material being processed, the qualities achieved by mechanical separation (the amount of suspended versus dissolved solids), and the
Properties of Feed liquors and Concentrate following evaporation
fermentation process (table). Viscosity of the concentrated liquor is normally the measure that determines the upper concentration limit. The concentrate quality, dried stillage quality and fouling behaviour are largely influenced by the temperatures within the evaporator. Temperatures of between 50 and 105 C are used. .
Thin Stillage Feed
Raw Material Type of Stillage % TS Viscosity cP Density kg/m
Sugar Beet Sugar Cane 7 -10 <1 1030 60 - 100 50 - 65 20 - 150 1300 - 1400 50 - 60 5-8
Barley (Whisky) 5 -6 <1 1020 70 - 90 40 - 45 300 -800 1100 70 -105 2-4
Wheat Rye 7 -9 <1 1030 60 - 80 25 - 30 500 - 1000 1060 60 - 80 1-2
Maize 5 -7 <1 1020 50 - 70 30 - 50 200 1060 60 2 500 1150 80 4
Yeast 5 -10 <1 1030 30 - 50 50 - 65 100 - 150 1200 -1300 60 - 70 8 - 15
Temperature C % TS Stillage Viscosity cP Concentrate Density kg/m Discharge Temperature C s K
0000
40C Maize sd 60C Maize sd
1000
80C Maize sd
Fig. 2:Stillage viscosity versus concentration. Fig 3:Boiling point elevation (in degrees Celsius) versus
Viscosity
concentration.
100
10
1 0 10 20 30 40 50 Concentration 60
40C Whisky 60C Whisky 80C Whisky 40C Wheat 60C Wheat 80C Wheat 40C Maize 60C Maize 80C Maize 40C Maize sd 60C Maize sd 80C Maize sd
70
80
Fig. 2 Fig 3.
1000
100
Viscosity
10
40C Cane 60C Cane 80C Cane 40C Beet 60C Beet 80C Beet
The properties of stillage from the same raw material can differ significantly due to seasonal variations, and are affected by the method of pretreatment. Specialized analysis and evaporation tests are therefore required to verify the design conditions in each individual case. GEA Wiegand has its own established Research and Development Centre, where state-of-the-art laboratory equipment, fixed and mobile pilot plants are available for evaporation trials, testwork and specialized analysis.
3
0,1 0 10 20 30 40 Concentration 50 60 70
Evaporator selection
Falling film and forced circulation evaporators are used for the concentration of stillage. Evaporator selection is normally determined by the required concentration ratio, the evaporation rate, the type of heating or heat recovery system, and in particular, by the viscosity and fouling characteristics of the stillage. Falling film evaporators are used for low viscosities, of up to about 100 cP and large evaporation rates. For higher concentration ranges, forced circulation evaporators are used, handling viscosities of up to 1000 cP, for example.
A F 2 1 A D
D F E 2 1 C E C
Where the product has a tendency to scale or foul, e.g. in the case of a vinasses containing calcium sulphates, for forced circulation evaporators are commonly used.
A Product D Vapour
1 Falling film calandria 3 Separator
B Concentrate E Deaeration 2 Forced circulation calandria C Condensate F Steam
Plant arrangements
The arrangement of an evaporator is determined by the type and quantity of the liquor to be processed, the energy available and the operating period required for the plant. In most cases, the plant arrangement depicted in one of the following examples is selected: Arrangement A: Multiple-effect, combined falling film and forced circulation evaporator, heated with live steam or by thermal vapour recompressor Arrangement B:
Fig. 4: 5-effect falling film and forced circulation evaporator, heated by thermal vapour recompressor, concentrating 30 tonnes/hr vinasses, arrangement A
Falling film pre-evaporator heated by mechanical vapour recompressor (MVR) and forced circulation finisher, heated by steam or mechanical vapour recompressor, for medium to large evaporation capacities, 20 to 120 tonnes/hr. Arrangement C: Combined falling film and forced circulation evaporator, heated by dryer exhaus vapour, for medium to very large evaporation capacities, 50 to 150 tonnes/hr Arrangement D: Combination of two or more lines of typ B arrangement, for the treatment of extremely large stillage quantities exceeding 150 tonnes/hr evaporation
Fig. 5: 4-effect falling film and forced circulation evaporator, heated by mechanical vapour recompressor, concentrating 125 tonnes/hr of whisky stillage, as per arrangement B (flow sheet in fig. 6)
Fig.. 6 1 4 Falling film effects 5, 6 Forced circulation effects 7 - 9 Straight tube preheater
10 11 12 13, 14
Plate preheater Condenser Condensate vessel Mechanical vapour recompressors
A Product B Concentrate C Condensate
D Live steam: E Deaeration F Cooling water
7 1
8 2
9 3 4
11 5 6
12 14
13 10
Fig. 7: 5-effect falling film and forced circulation evaporator, heated by dryer exhaust vapour, concentrating 140 tonnes/hr of stillage from 6.6 % to 35 % TS, arrangement C
Fig.. 8: 1 3 Falling film effects 4 5 6, 7 8, 9 Forcedc circulation effect Separator Condensers Condensate feed tanks 10 Vapour scrubber 11 Vapour fans 12 Condensate flash vessel 13 Exhaust stack A, B C1, C6 C2 4 C5 D Product, concentrate Cleaned condensate Vapour condensate Foul condensate Dryer exhaust vapour E F G H I Deaeration Live steam Cooling water Service water Exhaust air and vapour mixture
Animals feeds plant

The following diagram depicts the most common process for the processing of wheat stillage, the DDGS (dried distillers grains with solubles) animal feeds plant. The raw stillage is first transferred through a highperformance centrifuge, where the wet cake containing about 30 % TS is decanted. The remaining thin stillage, from which suspended solids have been separated to the largest possible extent, is conveyed through buffer tanks to the evaporation plant, where it is concentrated to about 28 42 % Ts. The stillage concentrate from wet cake from the decanter drying system, where they are material and finally dried to about 5 10 %. the evaporator and the are transferred to the mixed with recycled dry a residual moisture of
Ring dryers or steam tube dryers are generally used for the drying of DDGS.
Fig.. 9: A, B E F G H Raw stillage Concentrate Wet cake Dryer vapours Dried stillage/DDGS 1 2 3 4 5 6 Raw stillage tank Decanter Thin stillage tank Evaporation plant DDGS dryer DDGS-silo C, D Thin stillage
Our Range of Products in Summary

Evaporation Plants
for the concentration of all kinds of liquid food, organic and inorganic solutions, effluents, and other liquid products by means of thermal or mechanical vapour recompression, single or multiple effects with additional components for heating, cooling, degassing, crystallization, rectification, etc.
Plants for Distillation/Rectification for the separation of multicomponent mixtures, for instance for the recovery of organic solvents, for the production, purification and dehydration of bioalcohol of different qualities. Lines for the Production of Alcohol from the treatment of raw material, fermentation, distillation and processing of stillage right through to steam drying. Plants for Crystallization of effluents containing salt and other aqueous solutions. Project Studies, Engineering for plants in the supply programme.
Membrane Filtration for the concentration of liquid food, process water, organic and inorganic solutions and waste water; for the separation of impurities for upgrading and recycling of recyclable material; based on technology and references of GEA Filtration, Hudson/USA.
GEA Wiegand GmbH Einsteinstrae 9 - 15 D-76275 Ettlingen Tel.: +49 (0) 72 43 / 7 05-0 . Fax: +49 (0) 72 43 / 7 05-3 30 E-Mail: info@gea-wiegand.de Internet: www.gea-wiegand.de P14E 0305

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Evaporators for Stillage Concentration

Evaporation for Stillage Concentration

Animal Feeds wet

Animal Feeds dry

Concentration and temperature

Thin Stillage Feed

Raw Material Type of Stillage % TS Viscosity cP Density kg/m

Barley (Whisky) 5 -6 <1 1020 70 - 90 40 - 45 300 -800 1100 70 -105 2-4

Wheat Rye 7 -9 <1 1030 60 - 80 25 - 30 500 - 1000 1060 60 - 80 1-2

Maize 5 -7 <1 1020 50 - 70 30 - 50 200 1060 60 2 500 1150 80 4

Yeast 5 -10 <1 1030 30 - 50 50 - 65 100 - 150 1200 -1300 60 - 70 8 - 15

Temperature C % TS Stillage Viscosity cP Concentrate Density kg/m Discharge Temperature C s K

1 Falling film calandria 3 Separator

B Concentrate E Deaeration 2 Forced circulation calandria C Condensate F Steam

Plate preheater Condenser Condensate vessel Mechanical vapour recompressors

A Product B Concentrate C Condensate

D Live steam: E Deaeration F Cooling water

Animals feeds plant

Our Range of Products in Summary

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