Ordinary Portland Cement, 33 Grade - Specification: Indian Standard
Ordinary Portland Cement, 33 Grade - Specification: Indian Standard
Ordinary Portland Cement, 33 Grade - Specification: Indian Standard
(Reaffirmed 2004)
Edition 5.8
(2005-05)
Indian Standard
UDC
666.942
BIS 2007
BUREAU
OF INDIAN
STANDARDS
Price Group 4
FOREWORD
This Indian Standard (Fourth Revision) was adopted by the Bureau of Indian Standards on 20
June 1989, after the draft finalized by the Cement and Concrete Sectional Committee had been
approved by the Civil Engineering Division Council.
This standard was first published in 1951 and subsequently revised in 1958, 1967 and 1976. This
fourth revision incorporates the experience gained with the use of this specification and brings the
standard in line with the present practices followed in the production and testing of cement.
Since the third revision of this standard was published, a large number of amendments have been
issued from time to time in order to modify various requirements based on experience gained with
the use of the standard and the requirements of the users, and also keeping in view the raw
materials and fuels available in the country for the manufacture of cement. The important
amendments include increase in insoluble residue from 2 to 4 percent, incorporating 33 MPa as
the 28-day compressive strength, making autoclave soundness test compulsory irrespective of
magnesia content, incorporating a provision for retest in respect of autoclave soundness test after
aeration of the cement, incorporating a clause on false set and permitting packaging of cement in
25-kg bags. In view of these large number of amendments, the Sectional Committee decided to
bring out this fourth revision of the standard incorporating all these amendments so as to make it
more convenient for the users.
The Sectional Committee also decided that ordinary Portland cement should be designated by its
28-day compressive strength and, therefore, the title of this standard has been modified in this
revision, after taking out the provisions relating to low heat Portland cement for covering in a
separate standard.
Mass of cement packed in bags and the tolerance requirements for the mass of cement packed in
bags shall be in accordance with the relevant provisions of the Standards of Weights and Measures
( Packaged Commodities ) Rules, 1977 and B-1.2 ( see Annex B ). Any modification in these rules in
respect of tolerance on mass of cement would apply automatically to this standard.
This standard contains clause 11.4.1 which gives option to the purchaser and clauses 6.5 and 9.3
which call for agreement between the purchaser and the supplier.
In the formulation of this standard, considerable assistance has been rendered by the National
Council for Cement and Building Materials, New Delhi as many of the revisions are based on the
studies carried out by them.
The composition of the technical committee responsible for the formulation of this standard is
given in Annex C.
This edition 5.8 incorporates Amendment No. 1 (July 1990), Amendment No. 2 (November 1991),
Amendment No. 3 (June 1993), Amendment No. 4 (November 1998), Amendment No. 5 (October
1999), Amendment No. 6 (May 2000), Amendment No. 7 (December 2003) and Amendment No. 8
(May 2005). Side bar indicates modification of the text as the result of incorporation of the
amendments.
For the purpose of deciding whether a particular requirement of this standard is complied with,
the final value, observed or calculated, expressing the result of a test or analysis, shall be rounded
off in accordance with IS 2 : 1960 Rules for rounding off numerical values ( revised ). The number
of significant places retained in the rounded off value should be the same as that of the specified
value in this standard.
IS 269 : 1989
Indian Standard
1 SCOPE
1.1 This standard covers the manufacture and
chemical and physical requirements of 33 grade
ordinary Portland cement.
2 REFERENCES
2.1 The Indian Standards listed in Annex A are
necessary adjuncts to this standard.
3 TERMINOLOGY
3.1 For the purpose of this standard, the definitions given in IS 4845 : 1968 shall apply.
4 MANUFACTURE
4.1 33 grade ordinary Portland cement shall be
Performance
Improver
Percentage
Addition, Max
Requirement
Fly ash
Granulated slag
Silica fume
Limestone
5
5
5
5
Metakaoline
5 CHEMICAL REQUIREMENTS
5.1 When tested in accordance with the
methods given in IS 4032 : 1985, 33 grade
ordinary Portland cement shall comply with
the chemical requirements given in Table 1.
IS 269 : 1989
IS 12423 may be referred.
(2)
Ratio of percentage of lime to percentages of silica,
alumina and iron oxide, when calculated by the
formula
Requirement
(3)
Not greater than 1.02 and not less than 0.66
CaO 0.7 SO 3
----------------------------------------------------------------------------------------------2.8 SiO 2 + 1.2 Al 2 O 3 + 0.65 Fe 2 O 3
ii)
iii)
iv)
v)
6 PHYSICAL REQUIREMENTS
6.1 Fineness
When tested for fineness by Blaines air
permeability method as described in IS 4031
(Part 2) : 1988, the specific surface of cement
shall not be less than 225 m2/kg.
6.2 Soundness
6.2.1 When tested by Le Chatelier method and
autoclave test described in IS 4031 (Part 3) :
1988, unaerated cement shall not have an
expansion of more than 10 mm and 0.8 percent,
respectively.
6.2.1.1 In the event of cements failing to comply
with any one or both the requirements specified
in 6.2.1, further tests in respect of each failure
shall be made as described in IS 4031 (Part 3) :
1988 from another portion of the same sample
after aeration. The aeration shall be done by
spreading out the sample to a depth of 75 mm
at a relative humidity of 50 to 80 percent for a
total period of 7 days. The expansion of cements
so aerated shall be not more than 5 mm and 0.6
percent when tested by Le Chatelier method
and autoclave test respectively.
6.3 Setting Time
The setting time of the cements, when tested by
the Vicat apparatus method described in
IS 269 : 1989
9.1.1 Similar information shall be provided in
the delivery advices accompanying the shipment
of packed or bulk cement ( see 9.3 ).
9.2 The net mass of cement per bag shall be 50
kg ( see Annex B ).
9.2.1 The net mass of cement per bag may also be
25 kg, 10 kg, 5 kg, 2 kg or 1 kg subject to
tolerances as given in 9.2.1.1 and packed in
suitable bag as agreed to between the purchaser
and the manufacturer.
9.2.1.1 The number of bags in a sample taken
for weighment showing a minus error greater
than 2 percent of the specified net mass shall
not be more than 5 percent of the bags in the
sample. Also the minus error in none of such
bags in the sample shall exceed 4 percent of the
specified net mass of cement in the bag.
However, the net mass of the cement in a
sample shall be equal to or more than 25 kg, 10
kg, 5 kg, 2 kg or 1 kg, as the case may be.
9.2.2 When cement is intended for export and if
the purchaser so requires, packing of cement may
be done in bags or in drums with an net mass of
cement per bag or drum as agreed to between the
purchaser and the manufacturer.
9.2.2.1 For this purpose the permission of the
certifying authority shall be obtained in advance
for each export order.
9.2.2.2 The words FOR EXPORT and the net
mass of cement per bag/drum shall be clearly
marked in indelible ink on each bag/drum.
9.2.2.3 The packing material shall be as agreed
to between the manufacturer and the purchaser.
9.2.2.4 The tolerance requirements for the
mass of cement packed in bags/drum shall be as
given in 9.2.1.1 except the net mass which shall
be equal to or more than the quantity in 9.2.2.
9.3 Supplies of cement in bulk may be made by
arrangement between the purchaser and the
supplier (manufacturer or stockist).
9 DELIVERY
9.1 The cement shall be packed in bags [jute
sacking bag conforming to IS 2580 : 1982,
double hessian bituminized (CRI type),
multi-wall paper conforming to IS 11761 : 1986,
polyethylene lined (CRI type) jute, light weight
jute conforming to IS 12154 : 1987, woven
HDPE conforming to IS 11652 : 1986, woven
polypropylene conforming to IS 11653 : 1986,
jute synthetic union conforming to IS 12174 :
1987 or any other approved composite bag]
bearing the manufacturers name or his
registered trade-mark, if any. The words 33
grade ordinary Portland cement, and the
number of bags (net mass) to the tonne or the
net mass of the cement shall be legibly and
indelibly marked on each bag. In case
performance improvers are added, the bags
shall also be marked Permitted performance
improvers are added. Bags shall be in good
condition at the time of inspection.
10 SAMPLING
10.1 A sample or samples for testing may be
taken by the purchaser or his representative, or
by any person appointed to superintend the
work for purpose of which the cement is
required or by the latters representative.
10.1.1 The samples shall be taken within three
weeks of the delivery and all the tests shall be
commenced within one week of sampling.
10.1.2 When it is not possible to test the
samples within one week, the samples shall be
packed and stored in air-tight containers till
such time that they are tested.
10.2 In addition to the requirements of 10.1,
the methods and procedure of sampling shall be
in accordance with IS 3535 : 1986.
3
IS 269 : 1989
option of the purchaser or his representative and
the tests shall be carried out in accordance with
this standard on the written instructions of the
purchaser or his representative.
11.4.2 Cost of Testing
The manufacturer shall supply, free of charge,
the cement required for testing. Unless
otherwise specified in the enquiry and order,
the cost of the tests shall be borne as follows:
a) By the manufacturer if the results show
that the cement does not comply with the
requirements of this standard, and
b) By the purchaser if the results show that
the cement complies with the requirement
of this standard.
11.4.3 After a representative sample has been
drawn, tests on the sample shall be carried out
as expeditiously as possible.
12 REJECTION
12.1 Cement may be rejected if it does not
comply with any of the requirements of this
specification.
12.2 Cement remaining in bulk storage at the
mill, prior to shipment, for more than six
months, or cement in bags, in local storage in
the hands of a vendor for more than 3 months
after completion of tests, may be retested before
use and may be rejected if it fails to conform to
any of the requirements of this specification.
ANNEX A
( Clause 2.1 )
LIST OF REFERRED INDIAN STANDARDS
IS No.
IS No.
Title
IS 4032 : 1985 Method of chemical analysis of
hydraulic cement ( first revision )
IS 4845 : 1968 Definitions and terminology
relating to hydraulic cement
IS 4905 : 1968 Methods for random sampling
IS 11652 : 1986 High
density
polyethylene
(HDPE) woven sacks for
packing cement
IS 11653 : 1986 Polypropylene
(PP)
woven
sacks for packing cement
IS 11761 : 1986 Multi wall paper sacks for
cement, valved-sewn-gussetted
type
IS 12089 : 1987 Granulated
slag
for
the
manufacture of Portland slag
cement Specification
IS 12154 : 1987 Light weight jute bags for
packing cement
IS 12174 : 1987 Jute synthetic union bags for
packing cement
IS 12423 : 1988 Method for colorimetric analysis
of hydraulic cement
IS 15388 : 2003 Silica fume Specification
Title
IS 650 : 1966
IS 1727 : 1967
IS 1760
Methods of chemical analysis
(Part 3) : 1992 of limestone, dolomite and
allied
materials : Part 3
Determination of iron oxide,
alumina, calcium oxide and
magnesia ( first revision )
IS 2580 : 1982
IS 3535 : 1986
IS 3812
Pulverized
fuel
ash
(Part 1) : 2003 Specification : Part 1 For use as
pozzolana in cement, cement
mortar and concrete ( second
revision )
IS 4031
Methods of physical tests for
(Parts 1 to 13) hydraulic cement
4
IS 269 : 1989
ANNEX B
( Clause 9.2 and Foreword )
TOLERANCE REQUIREMENTS FOR THE MASS OF CEMENT PACKED IN BAGS
than 5 percent of the bags in the sample. Also
the minus error in none of such bags in the
sample shall exceed 4 percent of the specified
net mass of cement in the bag.
Sample Size
20
32
50
80
125
200
IS 269 : 1989
ANNEX C
COMPOSITION OF THE TECHNICAL COMMITTEE
Cement and Concrete Sectional Committee, CED 2
Chairman
DR H. C. VISVESVARAYA
Representing
National Council for Cement and Building Materials, New Delhi
Members
SHRI K. P. BANERJEE
SHRI H ARISH N. MALANI ( Alternate )
SHRI S. K. BANERJEE
CHIEF ENGINEER (BD)
SHRI J. C. BASUR ( Alternate )
CHIEF ENGINEER (DESIGNS)
SUPERINTENDING ENGINEER (S & S)
( Alternate )
CHIEF ENGINEER (RESEARCH-CUMDIRECTOR)
RESEARCH OFFICER (CONCRETE
TECHNOLOGY) ( Alternate )
DIRECTOR
JOINT DIRECTOR ( Alternate )
DIRECTOR
CHIEF RESEARCH OFFICER ( Alternate )
DIRECTOR (C & MDD-II)
DEPUTY DIRECTOR (C & MDD-II)
( Alternate )
SHRI V. K. GHANEKAR
SHRI S. GOPINATH
SHRI A. K. GUPTA
SHRI J. SEN GUPTA
SHRI P. J. JAGUS
DR A. K. CHATTERJEE ( Alternate )
JOINT DIRECTOR STANDARDS (B & S)/CB-I
JOINT DIRECTOR STANDARDS (B & S)/CB-II
( Alternate )
SHRI N. G. JOSHI
SHRI R. L. KAPOOR
SHRI R. K. SAXENA ( Alternate )
DR A. K. MULLICK
SHRI G. K. MAJUMDAR
SHRI P. N. MEHTA
SHRI S. K. MATHUR ( Alternate )
SHRI NIRMAL SINGH
SHRI S. S. MIGLANI ( Alternate )
SHRI S. N. PAL
SHRI BIMAN DASGUPTA ( Alternate )
SHRI R. C. PARATE
LT-COL R. K. SINGH ( Alternate )
SHRI H. S. PASRICHA
SHRI Y. R. PHULL
SHRI S. SEEHRA ( Alternate )
DR MOHAN RAI
DR S. S. REHSI ( Alternate )
SHRI A. V. RAMANA
DR K. C. NARANG ( Alternate )
SHRI G. RAMDAS
SHRI T. N. SUBBA RAO
SHRI S. A. REDDI ( Alternate )
for
Cement
Industry
(Ministry
of
IS 269 : 1989
Members
Representing
DR M. RAMAIAH
Structural Engineering Research Centre (CSIR), Madras
DR A. G. MADHAVA RAO ( Alternate )
Cement Corporation of India, New Delhi
SHRI A. U. RIJHSINGHANI
SHRI C. S. SHARMA ( Alternate )
Central Board of Irrigation and Power, New Delhi
SECRETARY
SHRI K. R. SAXENA ( Alternate )
SUPERINTENDING ENGINEER (DESIGNS) Public Works Department, Government of Tamil Nadu
EXECUTIVE ENGINEER (SMD
DIVISION) ( Alternate )
Orissa Cement Limited, New Delhi
SHRI L. SWAROOP
SHRI H. BHATTACHARYYA
( Alternate )
Gannon Dunkerly & Co Ltd, Bombay
SHRI S. K. GUHA THAKURTA
SHRI S. P. SANKARNARAYANAN
( Alternate )
The Institution of Engineers (India), Calcutta
DR H. C. VISVESVARAYA
SHRI D. C. CHATURVEDI ( Alternate )
Director General, BIS ( Ex-officio Member )
SHRI G. RAMAN,
Director (Civ Engg)
Secretary
SHRI N. C. BANDYOPADHYAY
Joint Director (Civ Engg), BIS
Members
DR A. K. MULLICK
( Alternates to Dr H. C. Visvesvaraya)
DR (SMT) S. LAXMI
SHRI S. K. BANERJEE
National Test House, Calcutta
Directorate General of Technical Development, New Delhi
SHRI N. G. BASAK
SHRI T. MADHESHWAR ( Alternate )
Cement Manufacturers Association, Bombay
SHRI SOMNATH BANERJEE
Irrigation Department, Government of Punjab
CHIEF ENGINEER (RESEARCH-CUMDIRECTOR)
RESEARCH OFFICER (CT) ( Alternate )
Gujarat Engineering Research Institute, Vadodara
SHRI N. B. DESAI
SHRI J. K. PATEL ( Alternate )
Maharashtra Engineering Research Institute, Nasik
DIRECTOR
RESEARCH OFFICER ( Alternate )
Central Water Commission, New Delhi
DIRECTOR (C & MDD II)
DEPUTY DIRECTOR (C & MDD II)
( Alternate )
Shree Digvijay Cement Co Ltd, Bombay
SHRI R. K. GATTANI
SHRI R. K. VAISHNAVI ( Alternate )
National Buildings Organization, New Delhi
SHRI J. SEN GUPTA
The Associated Cement Companies Ltd, Bombay
SHRI P. J. JAGUS
DR A. K. CHATTERJEE ( Alternate )
Research, Designs and Standards Organization, Lucknow
JOINT DIRECTOR, STANDARDS
(B & S) CB-I
JOINT DIRECTOR STANDARDS
(B & S)/CB-II ( Alternate )
Roads Wing (Ministry of Transport) (Department of Surface Transport), New Delhi
SHRI R. L. KAPOOR
SHRI R. K. DATTA ( Alternate )
The Hindustan Construction Co Ltd, Bombay
SHRI W. N. KARODE
Chettinad Cement Corporation Ltd, Poliyur, Tamil Nadu
SHRI R. KUNJITHAPATTAM
Hospital Services Consultancy Corporation (India) Ltd, New Delhi
SHRI G. K. MAJUMDAR
IS 269 : 1989
Members
SHRI K. P. MOHIDEEN
SHRI NIRMAL SINGH
SHRI S. S. MIGLANI ( Alternate )
SHRI Y. R. PHULL
SHRI S. S. SEEHRA ( Alternate )
SHRI A. V. RAMANA
DR K. C. NARANG ( Alternate )
COL V. K. RAO
SHRI N. S. GALANDE ( Alternate )
SHRI S. A. REDDI
DR S. S. REHSI
DR IRSHAD MASOOD ( Alternate )
SHRI A. U. RIJHSINGHANI
SHRI M. P. SINGH
SUPERINTENDING ENGINEER (D)
SENIOR DEPUTY CHIEF ENGINEER
(GENERAL) ( Alternate )
SHRI L. SWAROOP
SHRI H. BHATTACHARYYA ( Alternate )
SHRI V. M. WAD
Representing
Central Warehousing Corporation, New Delhi
Development Commissioner for Cement Industry (Ministry of Industry)
Central Road Research Institute (CSIR), New Delhi
Dalmia Cement (Bharat) Ltd, New Delhi
Engineer-in-Chiefs Branch, Army Headquarters
Gammon India Ltd, Bombay
Central Building Research Institute (CSIR), Roorkee
Cement Corporation of India Ltd, New Delhi
Federation of Mini Cement Plants, New Delhi
Public Works Department, Government of Tamil Nadu
Standard Mark
The use of the Standard Mark is governed by the provisions of the Bureau of Indian
Standards Act, 1986 and the Rules and Regulations made thereunder. The Standard Mark on
products covered by an Indian Standard conveys the assurance that they have been produced
to comply with the requirements of that standard under a well defined system of inspection,
testing and quality control which is devised and supervised by BIS and operated by the
producer. Standard marked products are also continuously checked by BIS for conformity to
that standard as a further safeguard. Details of conditions under which a licence for the use of
the Standard Mark may be granted to manufacturers or producers may be obtained from the
Bureau of Indian Standards.
Date of Issue
Amd. No. 1
July 1990
Amd. No. 2
November 1991
Amd. No. 3
June 1993
Amd. No. 4
November 1998
Amd. No. 5
October 1999
Amd. No. 6
May 2000
Amd. No. 7
December 2003
Amd. No. 8
May 2005
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