Westfalia Separator - Separators For The Diary Industry
Westfalia Separator - Separators For The Diary Industry
Westfalia Separator - Separators For The Diary Industry
Food Tec
Mechanical Separation
Division
Separators
for the
Dairy Industry
Contents
4
2.1
2.1.1
2.1.2
2.2
2.2.1
2.2.2
10
2.2.3
11
2.2.4
15
15
18
2.2.7
18
20
20
21
22
22
23
2.2.10.2 Pumps
23
23
24
25
2.2.10.6 Installation of
cold milk separators
27
Separation temperature
28 3.
Milk Separators
28
3.1
Type of Construction
28
3.1.1
29
3.1.2
29
3.2
29
3.2.1
General
30
3.2.2
30
3.3
1
3
3.4
33 3.5
34 4.
34
4.1
Buttermilk Separation
34
4.1.1
34
4.1.2
Process parameters
35
4.1.3
Separation efficiency
36
4.2
Whey Separation
36
4.2.1
36
4.3
36
4.4
Retentate Separation
37
4.5
Cream Concentration
37
4.5.1
37 4.5.2
38 5.
Special Processes
Food Tec
Westfalia Separator
Food Tec
Westfalia Separator
1000 tonnes
Nutritive value
Variables: breed of cow, lactation time,
climate and feeding
Physical properties
Variables: mechanical and
heat treatment
Chemical properties
Variables: enzyme reactions,
bacterial influence
Economic importance
Variables: efficiency of mechanical
separation processes
260
234
208
182
156
130
104
78
52
26
0
0
10 15 20 25 30 35 40 45 50
Calendar week
Fig. 3
values:
in an annual cycle
Fat:
3.75.3%
Protein: 3.34.3%
Westfalia Separator
Food Tec
12,000
8000
2
3.0
3.25
3.5
3.75
4.0
4.25
4.5
2.5
2.75
2.0
2.25
1.75
1.5
1.25
1.0
0.5
0.75
4000
Fig. 4
Size distribution of the fat
globules in an annual cycle
These include:
Preserving extraction of the milk
Transport of the milk through the
milking plant. Care must be taken
to separate the air necessary for
transport of the milk as much
as possible from the milk itself
Fig. 5
Diagram of different milk line
diameters for the same milk
28/30
1
38/40
2
50/52
3
Food Tec
66/70
4
Westfalia Separator
flow
Fig. 6
Diagram of the
permissible vacuum
Not permissible
permissible
permissible
42
40
70/66
50/44
52/50
40/34
40/38
1 1/2 in
1 in
Pipeline diameter
Pipeline plant
Centrifugable or extractable
free fat content
Free fatty
acids
Fig. 7
Quality curve of the free
0
10
20
30
40
50
60
Temperature in C
Westfalia Separator
Food Tec
Fig. 8
Cooling the milk
on the farm
30
Critical area
25
20
1st milking
P
0.6 0.7
15
max 12C
~2h
up to 10 h ~ 1 h
10
max 1 h bis 10 h
~1h
max 1 h
Time (h)
The motion of tank vehicles only partially filled causes turbulence in the liquid, and this can damage the
milk. Correct cleaning of the tank (CIP) is essential.
As shown in Fig. 9, it should not be possible to influence the operation of the pumps.
Food Tec
Westfalia Separator
1)
PI
PI
Bad:
Tank filled from above
Hose line to pump
Better:
Tank filled from below
Gravity feed by fixed pipeline
Pipeline diameter adequate
2)
Bad:
Tank filled and emptied
via a single pipeline
Better:
One tank being filled
One tank being emptied
3)
Bad:
Parallel switching of pumps
Better:
Each pump has its own
suction line
Fig. 9
Different pump operations
2.5
Refrigerated and
stored milk
1.5
Fresh milk
20
30
40
Fig. 10
Residual fat content in the skim
milk after processing of cold-stored
and fresh whole milk
10
Westfalia Separator
50
60
Food Tec
This process is to some extent reversible. By increasing the separation temperature the fat globule membranes can be returned almost to their original state.
For this reason, higher separation temperatures are
used today than were customary in the past. Fig. 10
illustrates the behaviour of separation efficiency as a
function of the holding time at low temperature.
pH level
Free fat values (FF)
Free fatty acids (FFA)
Size distribution of the fat globules
1.3
1.2
LF
1.1
1.0
0.9
0.8
FFS
0.7
0.6
Jan.
Feb.
March
Apr.
May
June
July
Aug.
Sept.
Oct.
Nov.
Dec.
Fig. 11
Content of free fatty acids and
lipolysable fat in whole milk
on delivery to the dairy during
the year (Zurich)
Food Tec
11
Westfalia Separator
FFA
milliquiv./l
Fig. 12
FFA value as a function of
the shelf life and the initial
FFA value
1.5
1.4
+35.2%
1.3
1.2
+31.5%
1.1
1.0
+19.3%
0.9
0.8
0.7
0.6
0.5
x
x
0.4
0
x
x
x
x
+13.3%
12
h
12
Westfalia Separator
Free fat
Methods for measuring the level of free fat (FF)
which provide reliable and reproducible results have
been available for some time. Two methods, the
centrifugal and extraction methods can be used,
however, only the extraction method gives reliable
information. The difference is that the centrifugal
method measures only the fat outside the fat globule membrane. With the extraction method the
fat enveloped by a porous, i.e. partially damaged
membrane, is also measured. The latter damage
has a noticeable effect, particularly with long storage times, as the fat turns to oil with time. If active
lipase is present, there is also the risk of lipolytic
attack in the event of damaged membranes.
Food Tec
Fig. 13
FFA1
FFA2
]
1.4
1.3
1.2
1.5
F measured
Residual fat contet, FMM SK
FSK min
[ ]
FFA2
Free fatty acids, FF
FFA1
1.5
1.4
1.3
1.2
FSK
1.1
1.1
1.0
1.0
measured by
gravimetric analysis
9
Samples
Hand milked
Every 2 days from farmers i.e. 4 milkings
Whole milk from balance tank in dairy
fresh tested
24 h 56C storage temp.
36 h 56C storage temp.
AGF [%]
FFA [milliquiv./l]
Inspection of test series (2) and (3) shows an identical tendency in the slope of the curve. This allows
the following conclusions to be drawn with respect
to the FF values:
Fig. 14
Effect of cold
clarification
16
1.6
1.4
1.2
14
1.0
12
0.8
10
0.6
0.4
0.2
4
2
1
1'
1''
2'
2''
3'
3''
Food Tec
13
Westfalia Separator
1572864
1048576
II
50
Volume units in l
75
524288
25
1.03
1.09
1.10
1.23
1.30
1.38
1.47
1.56
1.65
1.75
1.86
1.97
2.10
2.22
2.36
2.50
2.66
2.82
2.99
3.18
3.37
3.58
3.80
4.03
4.27
4.54
4.81
5.11
5.42
5.75
6.10
6.48
6.57
7.30
7.74
8.22
8.72
9.25
9.82
10.42
11.06
11.73
8192
75
4096
50
II
25
Volume units in l
12288
7.52
6.67
5.93
5.26
4.67
4.15
3.68
3.27
2.90
2.58
2.29
2.03
1.81
1.60
1.42
1.26
1.12
1.00
0.89
0.79
0.70
Fig. 16
Size distribution of the fat
globules in the skim milk
14
Westfalia Separator
Food Tec
96 100
II
64
50
25
32
EI = 98.875 %
EII = 98.65 %
Product temperature 53 C
Cream fat content 42 %
Period tested: 2/'87
7.52
6.67
5.93
5.26
4.67
4.15
3.68
3.27
2.90
2.58
2.29
2.03
1.81
1.60
1.42
1.26
1.12
1.00
0.89
0.79
0.70
Fig. 17
Separation curves (whole
milk to skim milk)
Food Tec
15
Westfalia Separator
Separation in %
75
is measured as an
increase in free air
content
20
x
x
x
10
< 20 10-3 dm3
Vair < 20 cm3 (first approximation)
20 cm3/Liter = 2%
15
10
5 mg O2 = ca. 25 mg air
25 10-6 kg air
10
20
30
40
50
kg
= 1.293 3
m
temperature
Fig. 18
Saturation point of gas
in liquids as a function of
temperature
16
Westfalia Separator
Food Tec
1 Special design
2 Standard design
Westfalia Separator
xx
xxx
xxx
xxx
xxx
xxx
xxx
xxx
Fig. 19
Flat bottom flask
for gas tests
If tests for gas are to be carried out in existing installations, the following should be borne in mind:
Food Tec
17
Westfalia Separator
2
= centrifugation coefficient = r
g
= radius [m]
1
= angular velocity
s
1.035
1
0.98
1.03
0.96
1.025
0.94
1.02
0.92
1.015
0.90
1.01
0.88
1.005
0.86
10
[ ]
2
= d g
18
= settling speed in centrifugal field [m/s]
= diameter of fat globule [m]
= 1 2
= density of the skim milk [kg/m3]
= density of the fat globules [kg/m3]
= dynamic viscosity [kg/ms]
= acceleration due to gravity [9,81 m/s2]
vZ
v z
d
1
2
g
7
6
5
4
3
2
1
0
70
1
20
30
40
50
60
Skim milk
Skim milk
Cream 40%
50
40
30
60 70 80
Temperature C
20
10
5
3
Temperature C
Whole milk
Milk fat
Fig. 20
Density and dynamic
viscosity as a function of
the temperature
18
Westfalia Separator
Food Tec
FSK min
FSK measured
Feed,
whole milk
2.0
I
1.9
II
1.8
Cream
1.7
II
1.6
1.5
1.4
III
1.3
r1
IV
1.2
Sediment
1.1
1.0
a
20
25
Fig. 21
Residual fat content in the
skim milk at different
cold-storage times of the
whole milk and separator
types as a function of the
separation temperature
30
40
50
60
Separation temperature C
Food Tec
Skim milk
r2
Fig. 22
Single separation
space in a milk separator
19
Westfalia Separator
0.25
0.3
Q = 100%
0.2
Q = 75%
0.15
0.1
Q = 50%
0.05
1.75
1.50
Grenzbereich
1.25
1.00
5 C
8 C
12 C
40
15 C
Fig. 23
Fig. 24
to Rse-Gottlieb as a function
50
60
70
Cream fat content [%]
A basic mode of operation of the cold milk separator is to control the cream flow by adjusting the
pressure of the product feed. By means of this pressure, the cold, 40 percent cream can be made to
discharge from the centre of the separator bowl
under pressure, in spite of its extremely high viscosity. However this can only be achieved with the
aid of hermetically-sealed product feed and cream
discharge lines. When we consider the sedimentation speed in cold milk separation, we find that it is
influenced by the increased dynamic viscosity. Flow
characteristics of the cream are also affected, so that
separability is considerably less than with warm milk
separation. The relatively low residual fat content in
the skim milk shown in Fig. 23 can only be achieved,
however, when the period of dwell of a particle in
the disc stack is increased by reduction of the feed
throughput. At product temperatures < 4C there
is the disadvantage that the flow paths in the disc
stack become blocked in a very short time.
The adjustments of the discharge pressures necessary to control the fat content in the cream have
no effect on separation efficiency up to the limiting
range (see Fig. 24). If this limiting range is exceeded, a slightly higher residual fat content can be
expected in the skim milk. Fig. 24 shows the residual
fat content in the skim milk as a function of the fat
content in the cream. Within the limiting range, the
residual fat content in the skim milk can be maintained at almost a constant level. This is achieved as
follows: the level of fat in the cream must be kept
stable. Any volume increase in the fat content of
the feed results automatically in approximately a 10fold increase in its concentration in the cream. If the
fat content in the whole milk were to change from
4.0 to 4.5 percent, then, with the same settings on
the separator, the fat content in the cream would
increase, for example, from 45 to 50 percent.
20
Westfalia Separator
Food Tec
% FQ
% FQN
1.5
1.2
1.0
0.9
0.75 QN
QN
1.25 QN
1.5 QN
FQN = Fat content at nominal capacity
Fig. 25
Feed throughput of the
separator as a function
of the residual fat content
in the skim milk
On the other hand, the upper range of the appropriate separation temperature (5560C) should be
chosen if the fat content in the cream is high. Thus,
if the cream fat content is above the limiting range,
i.e. between 60 and 80 percent, a product temperature between about 60 and max. 75C must be
chosen with an increasing fat content. The production of such high-percentage creams from an initial
product of (3040 percent) cream or whole milk
naturally has a particular effect on the residual fat
content in the respective skim milk. However, this
will not be further discussed in this document.
Fig. 26
System for control of the
separator feed throughput
System
Flexibility
Price
Product influence
Influence on
feed pump
Flow constrictor
limited
OPTIMAL
acceptable
acceptable
acceptable
acceptable
Frequency controlled
acceptable
OPTIMAL
depending kW
OPTIMAL
rating of motor
working range
Food Tec
21
Westfalia Separator
18
17
15
14
13
FI
PI
FC
2
3
FC
5
Fig. 27
Flow diagram of a milk
processing line
10
12
4 6
11
16
7 Milk skimming
separator
8 Flow meter
9 Adjustable flow
constrictor
10 Cream heater/cooler
11 Line to cream tank
1 Storage tank
2 Pump
3 Balance tank
4 Feed pump
5 Flow constrictor
6 Plate heat exchanger
22
Westfalia Separator
12 Solid tank
13 Pressure gauge
14 Constant pressure valve
15 Heat holding section
16 Booster pump
17 Pressure holding valve
18 Flow divertion valve
Food Tec
2.2.10.2 Pumps
Much has already been said on this subject. However, it should also be mentioned that in our opinion
a great deal more attention should be paid to the
design and operation of pumps than is generally the
case today.
Fig. 28
Pressure curve in the
pasteuriser for a given
throughput capacity
(Representation based on the
p (bar)
Pressure diff. 2
Pressure diff. 1
6
5
KDV
4
Pressure diff. 2
Pressure diff. 1
Exchanger 2
Exchanger 1
2
Separator
1
0
Exchanger 2
Heater
Exchanger 1
0
Booster pump
Heat holding
6
Separator with
low feed pressure
Separator with
high feed pressure
Food Tec
Cooler
23
Westfalia Separator
10
11
Fig. 29
Control and measuring
1
P1
P4
P3
PI
P5
FI
24
Westfalia Separator
Food Tec
11
12
13
14
PI
PI
FIC
PIC
Viac
FIC
1
Fig. 30
Installation diagram for
cold milk separation
10
1 Storage tank
(whole milk)
2 Pump
3 Balance tank
4 Feed pump
5 Inductive
flowmeter
9
6 Automatic valve
7 Pressure gauge
8 Rinse line
9 Cold milk separator
10 Control valve (skim milk)
11 Line to tank (skim milk)
Food Tec
15
12 Pressure gauge
3 Mass flow meter
1
14 Control valve
15 Cream storage tank
16 Pump
25
Westfalia Separator
16
Displacement
with water
Overflow
Total ejection
Filling of bowl
Overflow
Total ejection
After attainment
of temperature
30 60 min.
Lye
Overflow
Total ejection
Intermediate flushing
with water
Overflow
Total ejection
After attainment
of temperature,
15 30 min.
Acid
Overflow
Depending on the
installation ~ 5 mins
Total ejection
Bowl flushing
with water
Fig. 31
5 60 min.
Automatic overflow
milk separators
26
Westfalia Separator
Food Tec
Lye:
Temperature 7080C
Concentration 1.52.0 percent
The bacteria-removing separator HyVOL CSE 500 stands for highest capacities in the bacterial clarification of milk. The model from the innovative E-generation reliably separates even the smallest spore
formers. With a top capacity of up to 50,000 l/h, this separator is moving into a new dimension. An
essential feature of the CSE series is the Westfalia Separator HydroSoft system. It operates with a comparatively small feed pressure and minimises the shear forces. The gentle treatment guarantees premium product quality. Thanks to the total ejection option, the E-generation also improves the efficiency
of CIP.
Food Tec
27
Westfalia Separator
3. Milk Separators
3.1 Type of construction
Two basic types of construction are used for milk
separators. Separators with solid-wall bowl are used
for discontinuous processing and separators with
self-cleaning bowl for continuous processing.
28
Westfalia Separator
Food Tec
K1
w
r 2
r 1
a
Q M
QM
= 3
(r23 r13) . tana
= Angular velocity of bowl [1/s]
= Effective outside radius of disc [cm]
= Mean radius relative to position
of rising channels [cm]
= Angle of discs to horizontal
= Flow of feed milk per sec. [cm3/s]
and disc interspace
Food Tec
29
Westfalia Separator
2
5
3
4
Fig. 32
Schematic of the
separator
1 Feed tube
2 Bore
3 Distributor
4 Bore
5 Rising channel
6 Cream centripetal pump
30
Westfalia Separator
Food Tec
Fig. 33
Cold milk separator
5 Sediment holding space
6 Solids ejection ports
7 Sliding piston
Food Tec
31
Westfalia Separator
0,18
0,16
0,20
System with
1 piston valve
I
System with
2 piston valves
II
70
System mit
metering piston
and
1 piston valve
III
System with
differential
metering piston
and
2 piston valves
IV
60
50
40
0,14
0,12
30
0,10
0,08
20
0,06
0,04
10
0,02
Fig. 34
Development stages of the
hydraulic system for automatic
bowl ejection
32
Westfalia Separator
Food Tec
Fig. 36
Milk processing line
Fig. 35
Operation diagram of the
hydraulic system for opening
and closing the bowl
1 Control unit
2 Pilot valve
3 Closing water valve
4 Filling water valve
5 Non-return valve
6 Metering unit
Food Tec
33
Westfalia Separator
4. Special Processes
4.1 Buttermilk separation
Buttermilk
Buttermilk
Buttermilk
Buttermilk
from
from
from
from
sweet cream
sour cream
neutralised cream
the cask churning process
Self-cleaning separators and separators with solidwall bowl (not self-cleaning) can be used for the
separation of sweet cream buttermilk. This is owing
to the relatively small amount of coagulated protein which is separated out. This also applies to the
separation of buttermilk produced from churning
neutralised cream or buttermilk recovered from the
cask churning process.
34
Westfalia Separator
The process diagram is shown in Fig. 37. The buttermilk is pumped from the buttermaking machine
(1) to the silo (5). The buttermilk should be stored
at a temperature of 68C. In plate heat exchanger
(7), sweet cream buttermilk is heated to 3040C
and sour cream buttermilk to 3235C. The buttermilk from the neutralised cream churning and cask
churning processes can be treated in the same way
as sweet cream buttermilk. The separator throughput capacity should be approx. 50 percent of the
rated capacity for sour cream buttermilk and up to
100 percent of the rated capacity for sweet cream
buttermilk. The cream flows from the separator into
a cream collecting tank (10). The butterfat content
in the cream must be adjusted with the aid of a fine
adjustment valve to approx. 25 percent. The construction of the disc stack depends on the type of
buttermilk to be processed.
Food Tec
2
3
5
9
10
11
Fig. 37
1 Buttermaking machine
2 Buttermilk collecting vat
3 Pump
4 Cooler
5 Storage tank
6 Pump
The residual butterfat content in the separated buttermilk can only be estimated as lying somewhere
between 50 and 70 percent of the initial butterfat
content unless extensive tests are carried out. This
is due to important parameters in the buttermaking process such as cream treatment, type of buttermaking machine and butter production process.
These technical and technological parameters affect
the separability and hence the residual fat content
in the buttermilk. However, if the initial butterfat
content is known, the residual fat content in the
separated buttermilk can be estimated with a fairly
high degree of accuracy.
100 %
80 %
Limit of economic
efficiency
60 %
Range of results
40 %
Yield
20 %
0.5 %
Fig. 38
The butterfat yield as
a function of the initial
butterfat content
Food Tec
1%
35
Westfalia Separator
Fig. 39
Concentration of
protein in an
ultrafiltration plant
Westfalia Separator supplies whey skimming separators with a large capacity range. Details of the models and their specifications are available on request.
To improve the quality of the whey protein concentrates (WPCs), part of the concentrated fat can be
removed by re-separation. This can be employed, for
example to bring the final fat content of an 80 percent WPC to approx. 5 percent. Without re-separation the final fat content would be 7 percent under
optimum conditions.
Optimum values can only be attained when the following conditions are met:
The degree of concentration in the evaporator
is m 1:4, corresponding to a max. dry
matter content of 25 percent DM
36
Westfalia Separator
Food Tec
With destabilisation
Destabilisation of the cream is carried out when a
cream concentration > 80 percent is to be obtained.
Before the cream is concentrated the fat globules
are reduced in size by homogenizing, whereby a
higher dispersion of the fat is obtained at the same
density. More detailed information is contained in
the documentation on production of butteroil.
Food Tec
37
Westfalia Separator
Adjust to this
height with
distilled water
Fig. 42
Mojonnier-measuring flask
38
Westfalia Separator
Food Tec
0.07
0.06
0.05
0.04
0.03
0.02
Traces
0.01
Fig. 40
Comparison of measuring
0.12
Modified
Bobcock
0.10
Original
Bobcock
1.6
0.08
1.3
1.0
0.06
0.7
0.04
0.4
0.02
Rse-Gottlieb
0.02
0.04
0.06
0.08
0.10
0.12
% fat in the skim milk by different methods of analysis
Fig. 41
Comparison of
different fat testing
methods
Food Tec
39
Westfalia Separator
% fat in powder
Example: separated whey concentrated 16 times
methods
6. Automatic Fat
Standardising Installations
Milk and cream standardisation is a process for
adjusting the butterfat content of the milk or cream
to a predetermined value. Exceeding the maximum
butterfat content means a financial loss for the
dairy.
Separator STANDOMAT base unit. For all milk applications a control signal is supplied for the feed flow
to the separator.
Models
The tendency today is for consumers to prefer milk
with a low fat content. Consequently, it is necessary
to market a wide range of products, e.g. milk with a
fat content of 0.5 percent, 1.5 percent, 2.6 percent,
3.0 percent and 3.5 percent.
Since the end of the 1980s Westfalia Separator has
been supplying solutions incorporating automatic
standardising systems to meet all market requirements.
Control system
With all models the cream fat content is determined
via density measurement in a mass flow meter. The
cream fat control is effected by variation of the
cream flow. Control procedures adapted to the different operating conditions (start up, production,
bowl discharge, shut down) take into account the
specific requirements of the separator. For standardising, a part of the cream flow is controlled via
an inductive flow meter and dosed back into the
skim milk. The control components for the skim
milk backpressure are integrated on the Westfalia
40
Westfalia Separator
Food Tec
Fig. 43
Westfalia Separator
STANDOMAT
Food Tec
41
Westfalia Separator
42
Westfalia Separator
Food Tec
Act proactively
With Westfalia Separator CapitalCare, our customers not only benefit from traditional services such
as inspection, maintenance, original spare part procurement and repairs, they also benefit from proactive risk-avoiding solutions, e.g. the online and
offline monitoring facility with Westfalia Separator
WEWATCH. Modernisation, supporting a companys work, or upgrading to reflect state-of-the-art
technology, also helps boost performance.
Food Tec
Programmed quality
There are, of course, even more areas of application for separators and decanters apart from beverage technology, dairy technology and vegetable
oil processing. As one of the leading companies
in the field of mechanical separating technology
in the world, Westfalia Separator also operates in
many other areas. Please contact us as required for
processing systems, for applications in the chemical
and pharmaceutical industries, biotechnology, oil and
fat recovery, the starch industry, industrial biotechnology, marine, energy, oil field, industry and environmental technology.
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Westfalia Separator
Beverage Technology
Dairy Technology
Oils and Fats Processing
Chemicals, Pharmaceuticals
and Biotechnology
Oils and Fats Recovery
Starch Technology and
Industrial Biotechnology
Environmental Technology
Marine
Energy
Oilfield
Industry
Engineering
Second Hand Machinery
Service
Westfalia Separator
Food Tec GmbH
Werner-Habig-Strae 1
59302 Oelde (Germany)
9997-8239-040/0206 EN
Printed in Germany
Subject to modification
Westfalia Separator
Food Tec
Take the Best Separate the Rest
A company of GEA Group