CT Lab Manual
CT Lab Manual
CT Lab Manual
1. FINENESS OF CEMENT
2. NORMAL CONSISTENCY OF CEMENT
3. INITIAL AND FINAL SETTING TIMES OF CEMENT
4. SPECIFIC GRAVITY OF CEMENT
5. COMPRESSIVE STRENGTH OF CEMENT
6. SOUNDNESS OF CEMENT
7. FINENESS MODULUS OF FINE AND COARSE AGGREGATE
8. SPECIFIC GRAVITY, VOID RATIO, POROSITY AND BULK DENSITY OF
COARSE AND FINE AGGREGATES
9. BULKING OF SAND
10. WORKABILITY TESTS ON FRESH CONCRETE
11. COMPACTION FACTOR TEST
12. TEST FOR COMPRESSIVE STRENGTH OF CEMENT CONCRETE
.
FINENESS OF CEMENT
(IS: 269-1989 and IS: 4031-1988)
AIM: To determine the fineness of the given sample of cement by sieving.
APPARATUS: IS-90 micron sieve conforming to IS:460-1965, standard balance, weights,
brush.
INTRODUCTION: The fineness of cement has an important bearing on the rate of hydration
and hence on the rate of gain of strength and also on the rate of evolution of heat. Finer cement
offers a greater surface area for hydration and hence the faster and greater the development of
strength. Increase in fineness of cement is also found to increase the drying shrinkage of
concrete. Fineness of cement is tested either by sieving or by determination of specific surface by
air-permeability apparatus. Specific surface is the total surface area of all the particles in one
gram of cement.
FINENESS BY SIEVING:
PROCEDURE:
1. Weigh accurately 100 g of cement and place it on a standard 90 micron IS sieve.
2. Break down any air-set lumps in the cement sample with fingers.
3. Continuously sieve the sample giving circular and vertical motion for a period of 15
minutes.
4. Weigh the residue left on the sieve. As per IS code the percentage residue should not
exceed 10%.
PRECAUTIONS: Air set lumps in the cement sample are to be crushed using fingers and not to
be pressed with the sieve. Sieving shall be done holding the sieve in both hands and with gentle
wrist motion. More or less continuous rotation of the sieve shall be carried out throughout
sieving.
OBSERVATIONS:
S.No
weight
of
taken(g)
Fineness (%)
OBSERVATIONS:
Weight of cement Weight of water Plunger
S. No taken in gms
taken in gms
penetration
(a)
(b)
(mm)
Time
Taken
Consistency
of
cement in % by
weight b/a * 100
W1 g
Trial 1
W2 g
W3 g
W4 g
W5 g
Trial2
Trail3
PRECAUTION:
1. Only kerosene which is free of water shall be used.
2. At time of weighing the temperature of the apparatus will not be allowed to exceed the
specified temperature.
3. All air bubbles shall be eliminated in filling the apparatus and inserting the stopper.
4. Weighing shall be done quickly after filling the apparatus and shall be accurate to 0.1 mg.
5. Precautions shall be taken to prevent expansion and overflow of the contents resulting from
the heat of the hand when wiping the surface of the apparatus.
RESULT: Average specific gravity of given sample of cement =
COMMENTS:
33.33 percent
33.33 percent
33.33 percent.
2. Treat the interior faces of the mould with a thin coating of mould oil.
3. Place the assembled mould on the table of the vibration machine and firmly hold it is
position by means of suitable clamps.
4. Securely attach a hopper of suitable size and shape at the top of the mould to facilitate
filling and this hopper shall not be removed until completion of the vibration period.
5. Immediately after mixing the mortar, place the mortar in the cube mould and rod with a
rod.
6. The mortar shall be rodded 20 times in about 8 seconds to ensure elimination of entrained
air and honey combing.
7. Place the remaining quantity of mortar in the hopper of the cube mould and rod again as
specified for the first layer and then compact the mortar by vibrations.
8. The period of vibration shall be two minutes at the specified speed of 12,000 + 400
vibrations per minute.
9. At the end of vibration remove the mould together with the base plate from the machine
and finish the top surface of the cube in the mould by smoothing surface with the blade of
a trowel.
CURING SPECIMEN:
1. Keep the filled moulds at a temperature of 27 + 2 0 C in an atmosphere of at least 90 %
relative humidity for about 24 hours after completion of vibration.
2. At the end of that period remove them from the moulds.
3. Immediately submerge in clean fresh water and keep them under water until testing.
4. The water in which the cubes are submerged shall be renewed every 7 days and shall be
maintained at a temperature of 27 0C + 20C.
5. After they have been taken out and until they are tested the cubes shall not be allowed to
become dry.
TESTING:
1. Test three cubes for compressive strength at the periods mentioned under the relevant
specification for different hydraulic cements, the periods being reckoned from the
completion of vibration.
2. The compressive strength shall be the average of the strengths of three cubes for each
period of curing.
3. The cubes shall be tested on their sides without any packing between the cube and the
steel platens of the testing machine.
4. One of the platens shall be carried base and shall be self adjusting and the load shall be
steadily and uniformly applied starting from zero at a rate of 350 Kgs/Cm2/ min.
The cubes are tested at the following periods
Ordinary portland cement
3, 7 and 28 days.
Rapid hardening portland cement 1 and 3 days.
Low heat portland cement
3 and 7 days.
CALCULATION:
Calculate the compressive strength from the crushing load and the average area over which the
load is applied. Express the results in N/mm2 to the nearest 0.05 mm2.
Compressive strength in N/mm2 = P/A =
10
11
SOUNDNESS OF CEMENT
(IS 269-1989 AND IS 4031-1988 PART 3)
AIM: To determine the soundness of the given sample of cement by "Le Chatelier" Method.
APPARATUS: Le Chatelier apparatus conforming to IS 5514-1969, Balance, Weights, Water
bath.
INTRODUCTION: It is essential that the cement concrete shall not undergo appreciable change
in volume after setting. This is ensured by limiting the quantities of free lime, magnesia and
sulphates in cement which are the causes of the change in volume known as unsoundness.
Unsoundness in cement does not come to surface for a considerable period of time. This test is
designed to accelerate the slaking process by the application of heat and discovering the defects
in a short time. Unsoundness produces cracks, distortion and disintegration there by giving
passage to water and atmospheric gases which may have injurious effects on concrete and
reinforcement.
The apparatus for conducting the test consists of small split cylinder of spring brass or other
suitable metal of 0.5mm thickness forming a mould 30 mm internal diameter and 30mm high.
On either side of the split mould are attached to indicators with pointed ends, the distance from
these ends to the center of the cylinder being 165 mm. The mould shall be kept in good condition
with the jaws not more than 50mm apart.
PROCEDURE:
1. Place the lightly oiled mould on a lightly oiled glass sheet and fill it with cement paste
formed by gauging cement with 0.78 times the water required to give a paste of standard
consistency.
2. The paste shall be gauged in the manner and under the conditions prescribed in
determination of consistency of standard cement paste, taking care to keep the edges of
the mould gently together
3. While this operation is being performed cover the mould with another piece of glass
sheet, place a small weight on this covering glass sheet and immediately submerge the
whole assembly in water at a temperature of 27 0 - 20 C and keep there for 24 hours.
4. Measure the distance separating the indicator points.
5. Submerge the moulds again in water at the temperature prescribed above.
6. Bring the water to boiling, with the mould kept submerged for 25 to 30 minutes, and keep
it boiling for three hours.
7. Remove the mould from the water allow it to cool and measure the distance between the
indicator points.
8. The difference between these two measurements represents the expansion of the cement.
9. For good quality cement this expansion should not be more than 10mm.
OBSERVATIONS:
Initial distance between the indicator points in mm =
Final distance between the indicator points in mm =
Expansion in mm = final length - initial length =
RESULT: Expansion in mm
12
Sieve size
Weight
retained
Kgs.
% Weight
retained
75 mm
40 mm
20 mm
13
% weight
passing
Cumulative
% Weights
retained
4.
5.
6.
7.
8.
9.
10.
10 mm
4800 microns
2400 microns
1200 microns
600 microns
300 microns
150 microns
Sieve size
1
2
3
4
5
6
4800 microns
2400 microns
1200 microns
600 microns
300 microns
150 microns
Kgs
Weight
retained
% Weight
retained
% weight
passing
Minimum retained
2
Maximum retained
3.5
6
6.9
7.5
8.0
6.9
7.5
8.0
8.5
14
Cumulative
% Weights
retained
Trail 1
Weight of empty container
Weight of container with material
Weight of container + material + water
Weight of container + water
W1
W2
W3
W4
Trail 2
W3 - W1 / ((W4 - W1)-(W3-W2))
ii) Porosity = Vol. of Voids / Total Vol. of aggregate *100
W3 - W2 / (W4 - W1) * 100
iii) Specific gravity = W2 - W1 / ((W4 - W1) - (W3 - W2))
iv) Bulk density = W2 - W1 / (W4 - W1)
Fine aggregate: Void Ratio and porosity
1. Take 150 ml of dry sand (v1 ml) in clean measuring jar of 1000 ml capacity.
2. Add a measured quantity of 100 ml clean water to the above sample (v2 ml) i.e. v2=100 ml
3. Shake the jar thoroughly till all air bubbles are expelled.
4. Now note the readings against the top surface of water in the jar (V3 ml)
Void ratio = v1 + v2 - v3 / v3 - v2
Porosity = v1 + v2 - v3 / v1
Specific gravity of fine aggregates:
1. Weigh the empty measuring jar of 1000 ml capacity = W1
2. Take the weight of empty measuring jar with 150 ml of sand
Empty jar + sand
=W2
3. Take the weight of empty measuring jar with 150 ml of sand and 100 ml of water
Empty jar + sand + water
= W3
4. Remove the mix of sand and water from bottle and fill it with water up to volume V3 then
weigh it.
Empty jar + water
= W4
Specific gravity = Weight of solids / Volume of Solids
W2 - W1 / ((W4 - W1) - (W3 - W2))
PRECAUTIONS: While filling the container with water in determining void ratio and porosity
of coarse aggregate care should be taken that water should not be in excess of the level of course
aggregate.
RESULT:
1) Specific gravity of course aggregate.
2) Void ratio of course aggregate.
3) Porosity of coarse aggregate.
4) Bulk density of course aggregate.
5) Specific gravity of fine aggregate.
6) Void ratio of the given fine aggregate.
7) Porosity of the given time aggregate.
COMMENTS:
.
16
BULKING OF SAND
AIM: To ascertain the bulking phenomena of given sample of sand.
APPARATUS: 1000ml measuring jar, brush.
INTRODUCTION: Increase in volume of sand due to presence of moisture is known as bulking
of sand. Bulking is due to the formation of thin film of water around the sand grains and the
interlocking of air in between the sand grains and the film of water. When more water is added
sand particles get submerged and volume again becomes equal to dry volume of sand. To
compensate the bulking effect extra sand is added in the concrete so that the ratio of coarse to
fine aggregate will not change from the specified value. Maximum increase in volume may be 20
% to 40 % when moisture content is 5 % to 10 % by weight. Fine sands show greater percentage
of bulking than coarse sands with equal percentage of moisture.
PROCEDURE:
1) Take 1000ml measuring jar.
2) Fill it with loose dry sand upto 500ml without tamping at any stage of filling.
3) Then pour that sand on a pan and mix it thoroughly with water whose volume is equal to 2%
of that of dry loose sand.
4) Fill the wet loose sand in the container and find the volume of the sand which is in excess of
the dry volume of the sand.
5) Repeat the procedure for moisture content of 4%, 6%, 8%, etc. and note down the readings.
6) Continue the procedure till the sand gets completely saturated i.e till it reaches the original
volume of 500ml.
OBSERVATIONS:
S.No
Volume of dry
loose sand V1
1.
500 ml
2.
3.
4.
5.
6.
% moisture
content added
2%
4%
6%
8%
GRAPH: Draw a graph between percentage moisture content on X-axis and percentage bulking
on Y-axis. The points on the graph should be added as a smooth curve. Then from the graph,
determine maximum percentage of bulking and the corresponding moisture content.
PRECAUTIONS:
1) While mixing water with sand grains, mixing should be thorough and uniform.
2) The sample should not be compressed while being filled in jar.
3) The sample must be slowly and gradually poured into measuring jar from its top.
4) Increase in volume of sand due to bulking should be measured accurately.
17
RESULT: The maximum bulking of the given sand is -----------at -----------% of moisture
content.
COMMENTS:
18
Place the mixed concrete in the cleaned slump cone in 4 layers each approximately 1/4 in
height of the mould. Tamp each layer 25 times with tamping rod.
4) Remove the cone immediately, rising it slowly and carefully in the vertical direction.
5) As soon as the concrete settlement comes to a stop, measure the subsistence of the concrete
in cms, which gives the slump.
Note: Slump test is adopted in the Laboratory or during the progress of the work in the field for
determining consistency of concrete where nominal max., size of aggregates does not exceed 40
mm. Any slump specimen which collapses or shears off laterally gives incorrect results and at
this juncture the test is repeated only true slump should be measured.
OBSERVATIONS:
S.No
1
2
3
4
W/c Ratio
0.5
0.6
0.7
|0.8
Slump in mm
19
PRECAUTIONS:
1) The strokes are to be uniformly applied through the entire area of the concrete section.
2) The cone should be removed very slowly by lifting it upwards without disturbing the
concrete.
3) During filling the mould must be firmly pressed against the base.
4)
Vibrations from nearly machinery might also increase subsidence; hence test should be
made beyond the range of ground vibrations.
COMMENTS: This test is not a true guide to workability. For example, a harsh coarse mix
cannot be said to have same workability as one with a large portion of sand even though they
have the same slump.
Recommended slumps of concrete mix of various works
S.No
1
2
3
4
Description of work
Road work
Ordinary beams to slabs|
Columns thin vertical section & retaining Walls etc
Mass concrete(Runway, |Pavements)
20
10. Find the weight of cylinder i.e cylinder filled with partially compacted concrete (W2 kgs)
11. Refill the cylinder with same sample of concrete in approx. 4 layers, tamping each layer
with tamping for 25 times in order to obtain full compaction of concrete.
12. Level the mix and weigh the cylinder filled with fully compacted concrete (W3 Kg)
13. Repeat the procedure for different for different a trowel.
OBSERVATIONS AND CALCULATIONS:
Weight of cylinder = W1 Kgs.
S.No
W/c ration
1
2
3
4
0.5
0.6
0.7
0.8
Wt.
With
partially
compaction
W2
(Kgs)
Compaction
factor
(W1- W2)/
(W3- W1)
PRECAUTIONS:
1. The top hopper must be filled gently.
2. The mix should not be pressed or compacted in the hopper.
3. If the concrete in the hopper does not fall through when the trap door is released, it should
be freed by passing a metal rod. A single steady penetration will usually affect release.
COMMENTS: It is more sensitive, precise than slump test and is particularly useful to
concrete mixes of low workability.
22
Concreting
Degree of
Values of
workability
workability
0.75 to 0.80
vibration
2
Low
0.8 to 0.85
Medium
0.85 to 0.92
with
vibration
3
Concreting
of heavily
reinforce
High
d
23
0.92 to above
24
In case of cylinders, a correction factor according to the height to diameter ratio of specimen
after capping shall be obtained from the curve shown in fig. 1 of IS: 516-1959. The product of
this correction factor and the measured compressive strength shall be known as the corrected
compressive strength, this being the equivalent strength of a cylinder having a height/diameter
ratio of two. The equivalent cube strength of the concrete shall be determined by multiplying the
corrected cylinder strength by 5/4.
REPORTING OF RESULTS:
The following information shall be included in the report on each test specimen:
a) Identification mark
b) Date of test
c) Age of specimen
d) Curing conditions including date of manufacture of specimen in the field
e) Weight of specimen
f) Dimensions of specimen
g) Compressive strength
h) Maximum load and
i) Appearance of fractured faces of concrete and type of fractures if these are unusual
RESULT: Compressive strength of Concrete --------------.
COMMENTS:
25
26