Hse Approved Specification
Hse Approved Specification
Hse Approved Specification
Specification DOT-4BW(HSE)
ISSUE 1
December 1995.
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Contents
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
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4. Authorised Steel
4.1. Table I
Designation
Chemical
composition,
percent-ladle analysis
Grade 11
Grade 212
Grade 3245
Carbon
0.10/0.20
0.24 maximum
0.22 maximum
Manganese
1.10/1.60
0.50/1.00
1.25 maximum
Phosphorus,
maximum
0.04
0.04
0.046
Sulphur, maximum
0.05
0.05
0.05
0.15/0.30
0.30 maximum
Silicon
Copper, maximum
0.4
Niobium
0.01/0.04
Heat treatment
authorised
()
(3)
(3)
Maximum stress
(N/mm2)
240
240
240
Any suitable heat treatment in excess of 593oC (1100oF), except that liquid quenching is not
permitted.
For compositions with a maximum carbon content of 0.15 % of ladle analysis, the
maximum limit for manganese on ladle analysis may be 1.4%.
5
Rephosphorized Grade 3 steels containing no more than 0.15% phosphorus are permitted if
carbon content does not exceed 0.15% and manganese does not exceed 1%.
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Limit or maximum
specified (%)
Carbon
To 0.15 inclusive
Over 0.15 to 0.40
inclusive
0.02
0.03
0.03
0.04
Manganese
To 0.60 inclusive
Over 0.60 to 1.15
inclusive
Over 1.15 to 2.50
inclusive
0.03
0.03
0.04
0.04
0.05
0.05
Phosphorus7
All ranges
0.01
Sulphur
All ranges
0.01
Silicon
To 0.30 inclusive
Over 0.30 to 1.00
inclusive
0.02
0.03
0.05
0.05
To 1.0 inclusive
Over 1.00 to 2.00
inclusive
0.03
0.03
0.05
0.05
To 1.0 inclusive
Over 1.00 to 2.00
inclusive
0.03
0.03
0.05
0.05
To 0.90 inclusive
Over 0.90 to 2.10
inclusive
0.03
0.03
0.05
0.05
To 0.20 inclusive
Over 0.20 to 0.40
inclusive
0.01
0.01
0.02
0.02
Zirconium
All ranges
0.01
0.05
Niobium
To 0.04 inclusive
0.005
0.01
Aluminium
0.04
0.04
0.05
0.05
Copper
Nickel
Chromium
Molybdenum
4.3. Heads
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Material for heads shall be the same as 4.1. of this section or shall be open hearth, electric or
basic oxygen carbon steel of uniform quality. Content percent for the following not over:
Carbon 0.25, Manganese 0.60, Phosphorous 0.045, Sulphur 0.050.
Heads shall be hemispherical or ellipsoidal in shape with a maximum ratio of 2:1. If low
carbon steel is used thickness of such heads shall be determined by using a maximum wall
stress of 165 N/mm2 (24000 p.s.i.) in formula in 9.1.
5. Identification of material
The material of construction shall be identified by a suitable method.
6. Defects
Material with seams, cracks, laminations or other injurious defects, not authorised.
7. Manufacture
7.1. By suitable appliances and methods; dirt and scale to be removed as necessary to afford
proper inspection; no defect acceptable that is likely to weaken the finished cylinder
appreciably; reasonably smooth and uniform surface required. Exposed bottom welds on
cylinders over 460 mm (18 inches) long shall be protected by footrings. Minimum thickness
of heads shall be not less than 90 percent of the required thickness of the side wall. Heads
shall be concave to pressure.
7.2. Circumferential seams.
By electric-arc welding. Joints shall be butt with one member offset (joggle butt) or lap with
minimum overlap of at least four times nominal sheet thickness.
7.3. Longitudinal seams in shells.
7.3.1. Longitudinal electric-arc welded seams shall be of the butt welded type. Welds shall
be made by a machine process including automatic feed and welding guidance mechanisms.
Longitudinal seams shall have complete joint penetration, and shall be free from undercuts,
overlaps or abrupt ridges or valleys. Misalignment of mating butt edges shall not exceed 1/6
of nominal sheet thickness or 0.8 mm (0.0312 inch) whichever is less. All joints with
nominal sheet thickness up to and including 3.2 mm (0.125 inch) shall be tightly butted.
When nominal sheet thickness is greater than 3.2 mm (0.125 inch), the joint shall be gapped
with maximum distance equal to one-half the nominal sheet thickness of 0.8 mm (0.0312
inch) whichever is less. Joint design, preparation and fit-up shall be such that the
requirements of 7.3.3. are satisfied.
7.3.2. Maximum joint efficiency shall be 1.0 when each seam is radiographed completely.
Maximum joint efficiency shall be 0.90 when one cylinder from each lot of 50 consecutively
welded cylinders is spot radiographed. In addition, one out of the first five cylinders welded
following a shut down of welding operations exceeding four hours shall be spot radiographed.
Spot radiographs, when required, shall be made of a finished welded cylinder and shall
include the girth weld for 50 mm (2 inches) in both directions from the intersection of the
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longitudinal and girth welds and include at least 150 mm (6 inches) of the longitudinal weld.
Maximum joint efficiency of 0.75 shall be permissible without radiography,
7.3.3.
Welding procedures and operators shall be qualified in accordance with
CGA Pamphlet C-3.
8. Welding of attachments
The attachment to the tops and bottoms only of cylinders by welding of neckrings, footrings,
handles, bosses, pads and valve protection rings is authorised provided that such attachments
and the portion of the container to which they are attached are made of weldable steel, the
carbon content of which shall not exceed 0.25 percent.
9. Wall thickness
9.1. For outside diameters over 150 mm (6 inches) the minimum wall thickness shall be 2
mm (0.078 inch).
In any case the minimum wall thickness shall be such that the wall stress calculated by the
formula (see Note 1):
S = [2P (1.3D2 + 0.4d2)] / [E (D2 - d2)]
shall not exceed the lesser value of any of the following:
(1)
The value shown in Table I, for the particular material under consideration.
(2)
One-half of the minimum tensile strength of the material determined as required in
section 14.
(3)
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10.1. Each cylinder shall be uniformly and properly heat treated prior to test by the applicable
method shown in Table 1. Heat treatment shall be accomplished after all forming and
welding operations.
10.2. Heat treatment is not required after welding or brazing weldable low carbon parts to
attachments of similar material which have been previously welded to the top or bottom of
cylinders and properly heat treated, provided such subsequent welding or brazing does not
produce a temperature in excess of 205oC (400oF) in any part of the top or bottom material.
11. Openings in cylinders
11.1. All openings shall be in the heads or bases.
11.2. Openings in cylinders shall be provided with adequate fittings, bosses, or pads, integral
with or securely attached to the cylinder by welding.
11.3. Threads shall comply with the following:
(1)
(2)
Taper threads shall be of length not less than as specified for American
Standard Taper Pipe threads.
(3)
Straight threads, having at least 4 engaged threads, to have tight fit and
calculated shear strength at least 10 times the test pressure of the cylinder; gaskets
required, adequate to prevent leakage.
11.4. Closure of fittings, boss or pads shall be adequate to prevent leakage.
12. Safety relief devices and protection for valves, safety devices and other connections,
if applied
12.1. No person may offer a cylinder charged with a compressed gas for transportation unless
the cylinder is equipped with one or more pressure relief devices sized and selected as to type,
location, and quantity and tested in accordance with CGA Pamphlet S-1.1. The pressure
relief device system must be capable of preventing rupture of the normally charged cylinder
when subjected to a fire test conducted in accordance with CGA Pamphlet C-14. Cylinders
shall not be shipped with leaking safety devices. Safety relief devices shall be tested for leaks
before the charged cylinder is shipped from the cylinder filling plant; it is expressly forbidden
to repair leaking fuse plug devices, where leak is through the fusible metal or between the
fusible metal and the opening in the plug body, (except by removal of the device and
replacement of the fusible metal). Exceptions are as follows:
12.1.1. Except as provided in Notes 1, and 3, safety relief devices are not required on
cylinders 305 mm (12 inches) or less in length, exclusive of neck, and 114 mm (4.5 inches)
or less in outside diameter.
NOTE 1: Safety relief devices are required on cylinders charged with a liquefied gas for
which this part requires a service pressure of 125 bar (1800 p.s.i.) or higher.
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NOTE 2: Safety relief devices are required on cylinders charged with nonliquefied gases to a
pressure of 125 bar (1800 p.s.i.) or higher at 21oC (70oF).
12.1.2. Safety relief devices are not required on cylinders charged with non-liquefied gas
under pressure of 20.7 bar (300 p.s.i.) or less at 21oC (70oF).
12.1.3. Safety relief devices are prohibited on cylinders charged with DOT Division 2, 3 or
Division 6.1 materials in Hazard Zone A.
12.1.4. Safety relief devices are prohibited on cylinders charged with fluorine.
12.1.5. Safety relief devices are not required on cylinders charged with methyl mercaptan;
with mono-, di-, or trimethylamine, anhydrous; with not over 4.5 kg (10 pounds) of nitrosyl
chloride; or with less than 75 kg (165 pounds) of anhydrous ammonia
12.1.6. Safety relief devices, if used, must be in the vapour space of cylinders containing
pyrophoric liquids.
12.2. Container valve protection.
Containers charged with flammable, corrosive, or noxious gases, shall have their valves
protected by one of the following methods.
12.2.1. By equipping the containers with securely attached metal caps of sufficient strength
to protect the valves from damage during transit.
12.2.2. By boxing or crating the containers so as to give proper protection to the valves.
12.2.3. By so constructing the containers that the valve is recessed into the container or
otherwise protected so that it will not be subjected to a blow when the container is dropped on
a flat surface.
12.2.4. By loading the containers compactly in an upright position and securely bracing in
cars or motor vehicles, when loaded by the consignor and to be unloaded by the consignee.
12.2.6. By equipping with valves strong enough to avoid damage during transit for containers
containing non liquefied gas under pressure not exceeding 20.7 bar (300 p.s.i.) at 21oC (70oF).
13. Hydrostatic test
13.1. By water jacket, or other suitable method, operated so as to obtain accurate data.
Pressure gauge must permit readings to accuracy of 1 percent. Expansion gauge shall permit
readings of total volumetric expansion to accuracy either of 1 percent or 0.1 cubic centimetre.
13.2. Pressure must be maintained for 30 seconds and sufficiently longer to insure complete
expansion. Any internal pressure applied after heat treatment and previous to the official test
shall not exceed 90 percent of the test pressure.
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13.3. Permanent volumetric expansion shall not exceed 10 percent of the total volumetric
expansion at test pressure.
13.4. Cylinders shall be tested as follows:
13.4.1. At least 1 cylinder selected at random out of each lot of 200 or less shall be tested as
outlined in paragraphs 13.1., 13.2., and 13.3. of this section to at least two times
service pressure.
13.4.2. All cylinders not tested as outlined in paragraph 13.4.1. of this section shall be
examined under pressure of at least two times service pressure and show no defect.
13.5.
One finished cylinder selected at random out of each lot of 500 or less successively
produced shall be hydrostatically tested to 4 times service pressure without bursting.
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14.3.1.
The yield strength shall be determined by either the "off-set" method or the
"extension under load" method as prescribed in ASTM Standard E8-78.
14.3.2. In using the "extension under load" method, the total strain (or "ex-tension under
load"), corresponding to the stress at which the 0.2 % permanent strain occurs may be
determined with sufficient accuracy by calculating the elastic extension of the gauge
length under appropriate load and adding thereto 0.2 percent of the gauge length.
Elastic extension calculations shall be based on an elastic modulus of 206.8 x 109
N/m2 (30 x 106 p.s.i.). In the event of controversy, the entire stress-strain diagram shall
be plotted and the yield strength determined from the 0.2% offset.
14.3.3. For the purpose of strain measurement, the initial strain reference shall be set while
the specimen is under a stress of 83 N/mm2 (12000 p.s.i.), the strain indicator reading
being set at the calculated corresponding strain.
14.3.4. Cross-head speed of the testing machine shall not exceed 3.2 mm (0.125 inch) per
minute during yield strength determination.
15. Elongation
Physical test specimens shall show at least 40 percent for 50 mm gauge (2 inch) length or at
least 20 percent in other cases, except that these elongation percentages may be reduced
numerically by 2 for 50 mm (2 inch) specimens and by 1 in other cases for each 52 N/mm2
(7500 p.s.i.) increment of tensile strength above 345 N/mm2 (50000 p.s.i.) to a maximum of
four increments.
16. Test of welds
16.1. Tensile test. A specimen shall be cut from one cylinder of each lot of 200 or less. The
specimen shall be taken across the longitudinal seam and shall be prepared and tested in
accordance with and shall meet the requirements of CGA Pamphlet C-3.
16.2. Guided bend test. A "root" test specimen shall be cut from the cylinder used for the
tensile test specified in section 16.1. Specimens shall be taken across the longitudinal seam
and shall be prepared and tested in accordance with and shall meet the requirements of CGA
Pamphlet C-3.
16.3. Alternate guided bend test. This test may be used and shall be as required by CGA
Pamphlet C-3. The specimen shall be bent until the elongation at the outer surface, adjacent
to the root of the weld, between the lightly scribed gauge lines a. to b., shall be at least
20 percent, except that this percentage may be reduced for steels having a tensile strength in
excess of 345 N/mm2 (50000 p.s.i.), as provided in 15.
17. Radiographic examination
17.1. Radiographic inspection shall conform to the techniques and acceptability criteria set
forth in CGA Pamphlet C-3. When fluoroscopic inspection is used, permanent film records
need not be retained.
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17.2. Should spot radiographic examination fail to meet the requirements of paragraph (a) of
this section, two additional welds from the same lot of 50 cylinders or less shall be examined,
and if either of these fail to meet the requirements, each cylinder shall be examined as
previously outlined; only those passing are acceptable.
18 Rejected cylinders
18.1. Unless otherwise stated, if a sample cylinder or specimen taken from a lot of cylinders
fails the prescribed test, then two additional specimens shall be selected from the same lot and
subjected to the prescribed test. If either of these fail the test then the entire lot shall be
rejected.
18.2. Reheat treatment authorised; subsequent thereto, acceptable cylinders shall pass all
prescribed tests. Repair of welded seams by welding is authorised provided that all defective
metal be cut away and joint be rewelded as prescribed for original welded joints.
19 Marking
19.1. Marking on each cylinder stamped as follows:
19.1.1. DOT-4BW(HSE) followed by the service pressure (for example, DOT-4BW(HSE)
20.7 bar [300 p.s.i.] etc.).
19.1.2. A serial number.
19.1.3. An Authorised Inspecton Body's official mark.
19.1.4. Date of test (for example, 12-94 for December 1994).
19.1.5. Additional markings are permitted.
19.2. Sequence of marks.
Serial number shall be just below or immediately following the DOT(HSE) marks; inspector's
official mark shall be near the serial number. Date of test shall be so placed that dates of
subsequent test can easily be added. Symbol in front of or following the serial number, with
space between, or symbol and serial number stamped into welded or brazed-on valve spud
directly above the DOT(HSE) mark located on head of cylinder are also authorised. Other
variations in sequence of marks authorised only when necessitated by lack of space.
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19.3.2. On a metal plate attached to the top of the cylinder or permanent part thereof:
sufficient space shall be left on the plate to provide for stamping at least six retest
dates; the plate must be at least 1.6 mm (0.0625 inch) thick and shall be attached by
welding, or by brazing. The brazing rod is to melt at a temperature of 590oC (1100oF).
Welding or brazing shall be along all the edges of the plate.
19.3.3. On the neck, valve boss, valve protection sleeve, or similar part permanently attached
to the top of the cylinder.
19.3.4. On the footring permanently attached to the cylinder, provided the water capacity of
the cylinder does not exceed 11 kg (25 pounds).
19.4. Size of marks.
Space permitting, at least 6 mm (0.25 inch) high.
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APPENDIX 1.
Inspector's report
(a)
(Manufacturer's name)
(Signed) _______________________
The material used was type ________
(Inspector)
authorised in Table I of Spec. No. 4BW(HSE)
By: __________________
(Place) ......................................
(Date) .......................................
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Check
analysis
No.
Cylinders
represented C
(serial No.s)
Chemical analysis
P
Si Mn Ni
Cr
Mo
Cu
Al
Zr
(Place) ......................................
(Date) ......................................
Cylinders
represented
by test (serial
No.s)
Yield
strength
(N/mm2)
[p.s.i.]
Tensile
strength
(N/mm2)
[p.s.i.]
Elongation
(percent)
Reduction
of area
(percent)
Weld
Weld
tensile test bend test
(Signed) .....................................
(Place) .......................................
(Date) .........................................
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NOTE 1: When specifications require test for only one out of each lot of 200 or less cylinders, the check on the
others must be indicated by a notation hereon reading, "Each cylinder was subjected to a pressure of ## bar
(p.s.i.) and showed no defect".
1
If the tests are made by a method involving the measurement of the amount of liquid forced into the cylinder by
the test pressure, then the basic data, on which the calculations are made, such as the pump factors, temperature
of liquid, coefficient of compressibility of liquid, etc., must also be given.
2
Do not include removable cap but state whether with or without valve. These weights must be accurate to a
tolerance of 1 percent.
3
Report approximate maximum and minimum volumetric capacity for the lot.
Signed) .......................................
20. Report retention
The makers of cylinders under this specification must retain the test reports required by this
specification for fifteen years from the original test date of the cylinder.
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