FSW of Aluminium Alloys
FSW of Aluminium Alloys
FSW of Aluminium Alloys
Introduction
Historical background and principles
Radically new joining processes do not come along very
often: friction stir welding (FSW) was one such event,
being invented by the TWI in 1991.1,2 Since then
research and development in FSW and associated
technologies has mushroomed, with many companies,
research institutes and universities investing heavily in
the process and international conference series dedicated
to its study. By the end of 2007, TWI had issued 200
licences for use of the process, and 1900 patent
applications had been filed relating to FSW.3 The
number of research papers has also grown exponentially.
In essence, FSW is very simple, although a brief
consideration of the process reveals many subtleties. The
principal features are shown in Fig. 1. A rotating tool is
pressed against the surface of two abutting or overlapping plates. The side of the weld for which the
rotating tool moves in the same direction as the
traversing direction, is commonly known as the advancing side; the other side, where tool rotation opposes the
traversing direction, is known as the retreating side{.
An important feature of the tool is a probe (pin) which
protrudes from the base of the tool (the shoulder), and is
of a length only marginally less than the thickness of the
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Table 1 AWS designations for wrought Al alloy groups and basic temper designations applicable to heat-treatable Al
alloys
50
F As fabricated
O Annealed: there may be a suffix to indicate the specific
heat treatment.
H Strain hardened (cold worked): it is always followed by
two or more digits to signify the amount of cold work
and any heat treatments that have been carried out
W Solution heat treated: applied to alloys that precipitation
harden at room temperature (natural aging) after a solution
heat treatment. The designation is followed by a time
indicating the natural aging period, e.g. W 1 h
T Thermally aged:
T1: cooled and naturally aged
T2: cooled, cold worked and naturally aged
T3: solution heat treated, cold worked and naturally aged
T4: solution heat treated and naturally aged
T5: cooled and artificially aged
T6: solution heat treated and artificially aged
T7: solution heat treated and overaged or stabilised
T8: solution heat treated, cold worked and artificially aged
T9: solution heat treated, artificially aged and cold worked
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and provides physical insight into all of these relationships. Since FSW modelling has been reviewed elsewhere,77,78 this aspect is not explicitly covered in the
present review, except where modelling helps to interpret
and complement the experimental observations, or to
clarify issues debated in the literature.
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Applications
Commercial applications have been reported across
many industries, and some selected examples are shown
below which illustrate the widening appeal of the
process. This list is representative rather than exhaustive, and it should be emphasised that new applications
are appearing all the time. It should be noted that FSW
does not restrict the operating temperature range of
aluminium alloys, with applications ranging from
cryogenic temperatures (e.g. liquid oxygen and liquid
hydrogen rocket fuel tanks) to mildly elevated temperatures (e.g. heat exchangers in heating systems). Most
FSWs used in production are butt welds, although lap
welds and friction stir spot welds are also being applied
with increasing frequency.
Marine
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3 a typical generic ow path of plate material round clockwise rotating pin in FSW, taken from two-dimensional CFD
model with cylindrical tool moving from left to right (after Seidel and Reynolds),111 b,c effect of interfacial boundary
conditions (b stick; c slip) on predicted ow from two-dimensional CFD model with proled tool (after Colegrove and
Shercliff):112 change in thickness of streamlines indicates nal location of points initially forming straight line transverse to weld line (analagous to Cu foil in d) and d metallographic marker experiment using transverse copper foil,
illustrating ow induced by pin (after Reynolds)113
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a AA6082 on retreating side (left side lighter); b 6082 on advancing side (right side lighter)
9 Macrographs showing stir zone/TMAZ of 6082/5083 dissimilar welds with a 6082 on retreating side (left side lighter); b
6082 on advancing side (right side lighter) for welds made at traverse speed of 200 mm min21 and various rotation
speeds (dotted lines on 560 rev min21 welds show approximate size and position of 6 mm dia. pin)53
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a volumetric flaw in 2014;140 b tunnel (wormhole) defect at base of Trivex tool when welding 7449 at 120 rev min21/
60 mm min21;130 c surface defect located under shoulder in 2014A (Ref. 140)
11 Characteristic void aws in friction stir welds:
Location
Cause
Plate interface
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12 a oxide defect in 5083 alloy which can in severe cases lead to kissing bond at the base,161 b magnied view showing increased oxide inclusion level in 2014 along prior joint line140 and c schematic of joint line remnant161
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17 Evidence of partial melting on retreating side of nugget in FSW of 6 mm thick AA7050T7451 alloy164
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18 Lap weld defects showing hooking on advancing side and plate thinning on retreating side in lap welds between
7075 (upper) and 2024 (lower) alloys
19 a aws in cross-section from 6061 FSW tailor welded blank specimen (cylindrical threaded pin, welding speed
1200 mm min21, spindle speed 1500 rev min21, shoulder penetration 0 mm) and b corresponding synthetic aperture
focusing technique ultrasonic image169
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a nugget; b nugget/TMAZ boundary; c HAZ region177 (scale bar corresponds to 50 mm in each case)
20 Microstructure of 2199 alloy FSW displayed using inverse pole gure map obtained by EBSD, showing renement of
microstructure in nugget
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21 Microstructure in 6 mm thick 2195 alloy a before and b after post-weld heat treatment202
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formation eliminates the prior deformation microstructure in cold worked material, the hardness of the nugget
region is independent of the original condition, as seen
for alloy 5083 in Fig. 22.
Since few finely dispersed second phase particles exist
to pin grain boundaries, the effects of recovery and
recrystallisation are, unsurprisingly, different from those
in precipitation hardened alloys. Thus the extremely
elongated and deformed grains found in the nonrecrystallised TMAZ in precipitation hardened alloys
are not generally seen in precipitate free alloys. The
transition from non-recrystallised to recrystallised is far
less distinct, implying that recrystallisation is much
easier in the absence of precipitates. Experiments by
Genevois et al.222 have shown that at 350uC, heavily
strained 5251 will recrystallise in 15 s, whereas identically treated 2024 required 1800 s to recrystallise.
Microstructural modelling in non-heat-treatable alloy
FSW has been limited to predicting the loss of hardness
across the weld in initially cold worked tempers.52 The
minimum hardness corresponds to complete recrystallisation, while the base metal hardness corresponds to no
recrystallisation. The problem is therefore to predict the
positions between which the volume fraction recrystallised varies from 0 to 100%. The resulting hardness is
then estimated using a linear rule of mixtures of the
limiting hardness values. The extent of recrystallisation
is primarily determined by the peak temperature reached
in the weld thermal cycle, together with the duration of
the time at temperature. A common approach to
modelling microstructural change in a thermal cycle is
to replace the cycle with an isothermal hold of duration
teq at the peak temperature Tp of the cycle. The duration
of the hold is defined to be that which provides the same
kinetic strength, I, as the thermal cycle, defined as
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a 7050 parent material: well characterised intragranular precipitates are g9 [Mg(Zn,Cu,Al)2] and intergranular precipitates
are g (MgZn2) and/or Mg3Zn3Al2; b area in HAZ, where same precipitates are found but thermal cycle has led to 56
increase in size; c area from recrystallised nugget, where some grains had significant dislocation densities: dislocations
are pinned by Al3Zr dispersoids or Al7Cu2Fe inclusions
26 Comparison of microstructures in 7050 FSW191 (TEM bright eld images: welds made at 396 rev min21,
102 mm min21)
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does not form easily, as the weld will cool very rapidly
through the temperature range where such precipitation
can occur. Figure 28 shows typical examples of HAZ
and nugget microstructures.
Fonda et al.196 have studied the precipitation
sequence in an underaged 2195 alloy of 25 mm
thickness. Figure 29 shows examples of the precipitate
structure in the HAZ, TMAZ and nugget for 2195, and
clearly exemplifies the significant changes which occur.
Evidence is shown for the coarsening of the T1 and h9
precipitates. In the TMAZ, these precipitates are
gradually replaced by a d9 phase (Al3Li), with none of
the initial phases being present in the hottest part of the
unrecrystallised TMAZ. GuinierPreston zones were
also detected at this point. Rod shaped precipitates,
identified as TB phase (Al7Cu4Li), were detected in the
nugget region. These often nucleate on b9 (Al3Zr) which
is difficult to distinguish from the d9 phase.
Generally, the trends in precipitation observed in 2xxx
and 7xxx series alloys have been matched in 6xxx
series alloys. Coarsening of b9 precipitates and solution
of needle precipitates was observed in the HAZ of
welds in alloy 6063.142,192,204,228 However, studies of
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29 Transmission electron diffraction patterns and micrographs from HAZ, TMAZ and nugget region of friction stir weld
in 2195 alloy196
The evolution of microstructure and hardness in heattreatable alloy FSW has been modelled in most detail,
adapting methods developed for arc welding.238244 For
the HAZ, the problem is purely thermal; for the TMAZ
and nugget there is the potential added complexity of
coupling between the deformation microstructure and
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30 Semi-empirical model predictions and measured hardness proles in 20 mm thick friction stir weld in 7449TAF, at
six different depths through thickness (after Colegrove et al.)248
31 Predicted evolution of a precipitate volume fraction and b equivalent radius in AA7449T7 friction stir weld, for three
positions typical of nugget, TMAZ and HAZ (after Colegrove et al.)248
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a Mg trace for joining 5083H321 (light) to 6061T6 (dark); b Cu trace for joining 2219T87 (light) to 7075T6 (dark)
32 X-ray maps from nugget regions in dissimilar welds (100 mm markers)
Dissimilar welds
In agreement with the distinct macroscale separation
discussed in the section on Mixing across dissimilar
welds, close examination of weld cross-sections commonly shows alternating bands of each alloy, often only
micrometres wide. Larsson et al.49 have described EDS
scans of Mg across two boundaries between 5083 and
6082 regions. The transition between the two Mg levels
is located to within a few micrometres, suggesting only
limited diffusion occurs. No evidence of regions with an
intermediate composition can be seen. Many other
examples exist which show the sharp transition, for
example that shown in Fig. 32, which shows X-ray maps
from 2219T87/7075T6 and 5083H321/6082T6 dissimilar welds. In both cases the sharp boundaries
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Mechanical properties
There is an ever increasing volume of data in the
literature on mechanical properties of friction stir
welds.255 It is thus beyond the scope of the present
review to summarise all aspects. An ISO standard (ISO
25239: Friction stir welding aluminium) on FSW will
be published in 2009; this uses other ISO standards to
define standard mechanical tests. When considering
specimen design, as for all welding processes, the
dimension of the initial test specimens should have some
relationship to the final structure, in particular to ensure
that the heat sink is representative, and that a steady
state is reached (at least approximately) and that the
residual stresses are comparable. Finally it should be
noted that hardness was discussed above as a useful
means of delineating microstructural changes across
friction stir welds.
Tensile properties
It is often stated that the tensile properties of friction stir
welds generally equal or exceed those reported for fusion
welds. Although this is often the case, some qualification
of this statement is in order:
(i) tensile properties of fusion welds made with a
filler are often determined as much by the filler
as by the welding process: in general when fusion
welding aluminium alloys, the filler wire is not
the same composition as the parent material, and
therefore may not have the same mechanical
properties
(ii) alloys such as 2xxx and 7xxx are designed to
have high strength, and therefore the strength of
welds is of particular importance. Unfortunately,
these alloys are generally difficult, and sometimes impossible, to weld by fusion processes;
thus, comparative data from high quality fusion
welds is scarce, or non-existent, and comparisons
with FSW are not always straightforward
(iii) when comparing tensile data on different types
of weld, care should be taken to establish how
the measurements have been made, e.g. removing
the overfill in fusion welds may affect the
properties, and not all authors state whether or
not this has been done; determination of yield
stress is dependent on the technique and equipment used (again not always stated).
When assessing tensile data, it should be remembered
that, as shown above, the microstructure across a
friction stir weld is typically highly non-uniform. As a
result yield strength, tensile strength and ductility may
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change considerably over very short distances. Consequently very different results can be obtained according to whether the welds have been tested longitudinal or
transverse to the weld. The stressstrain response will
vary even for cross-weld tests according to the width of
sample, since this will determine the retained residual
stresses (see below), and the length of the testpieces since
this will determine the average ductility/overall elongation, 0?2% yield stress, etc. There are many reports of
low elongation in cross-weld tensile tests of welds;
however, in many cases this is not due to low ductility,
as confirmed by the significant reduction in area.
Instead, the strain will have been concentrated in a very
small part of the gauge length where a locally softer
microstructure may have formed. Studies of deformation by Mahoney et al.6 on 6?35 mm 7075T7541 and
Liu et al.256 on 5 mm 1050H24, 6061T6 and 2017
T351 have demonstrated the variability in strain across
transverse tensile samples. Consequently, overall elongation measurements made on cross-weld samples tend to
be unrepresentative of any region of the weld and serve
only to identify the likely failure location under static
loading.
Two strategies have been developed for extracting
more representative data to map the properties across
friction stir welds, the former more suited to extracting
longitudinal properties, the latter capable of extracting
transverse properties:
(i) the excision of matchstick style microtensile test
samples: in this manner samples can be removed
parallel to the welding direction x that are
representative of parent, TMAZ, HAZ or weld
nugget
(ii) the cutting out of thin cross-weld testpieces: here,
the microstructure varies along the length y of the
testpiece, but not through the thickness z or
width x, provided the testpiece is sufficiently thin.
In such a case deformation behaviour will vary as
a function of y position. This can be monitored
by full field strain mapping using laser speckle
interferometry or digital image correlation, for
example.
Microtensile testing has provided the bulk of the data
delineating the variation in mechanical properties across
the various microstructural zones of friction stir welds
(Fig. 34a and b). Such studies include those by von
Strombeck and co-workers,257259 Allehaux et al.260
using 10 mm thick 7349T6 alloy and Denquin et al.261
using 6 mm thick 6056 alloy. In the last case, minimum
ductility was reported in the centre of the nugget region;
the stressstrain response parallel to the welding
direction was measured as a function of lateral distance
from the weld, e.g. Fig. 34b.
Cross-weld testing can provide useful insights if the
strain is measured as a function of position through the
microstructural zones. Initially, this was carried out by
monitoring closely spaced parallel lines6 or Vickers
indents,204 laser extensometry262 or a small number of
strain gauges.263 Mahoney et al.6 recorded the distribution of strain at failure for 7075T651 alloy FSW which
showed very close agreement with the hardness variation
characteristic of FSW for the alloy. The peak elongation
(,15%) corresponded to the HAZ with the strain in the
weld nugget close to that of the parent in accord with
their similar hardness. A more sophisticated approach is
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34 a hardness proles for Al2024 friction stir weld at three depths,259 b corresponding longitudinal tensile performance
as determined by microtensile specimens,259 c variation in hardness (bold circles) and 0?2% proof stress (open circles) as determined from cross-weld tensile test180 monitored by electronic speckle pattern interferometry for FSW
AA5083 welded at 200 mm min21 and d corresponding evolution of tensile strain with position across weld as crossweld load is raised180 (HAZ boundaries marked by dashed lines)
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Residual stresses
As welded residual stresses
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FSW
Plate
358
Extrusion 323
310
200
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of residual stresses is a complex area, and an authoritative summary of the methods which can be used is
beyond the scope of this review. Readers are referred to
other texts for more detailed information on the origins
of weld residual stresses,271,272 as well as the measurement of residual stresses by destructive (e.g. hole
drilling,273 contour method)274,275 and non-destructive
(e.g. neutron diffraction,273,276,277 synchrotron X-ray
diffraction277,278 and magnetic)275,279 techniques.
Several authors have determined residual stresses
non-destructively using synchrotron X-ray diffraction.180,280284 Although different materials were examined, there is broad agreement in the results, in that the
longitudinal stresses tend to show the largest variation,
being most tensile in the HAZ, lower in the nugget and
compressive in the parent plate (Fig. 35).
Similar trends have been recorded by Staron et al.285
using neutron diffraction. Destructive methods such as
the contour method,286,287 the crack compliance
method288 and incremental centre hole drilling289 have
also been applied.
The characteristic magnitude and profile of the
longitudinal stresses across a friction stir weld are
shown in Fig. 35 for a range of alloys. The longitudinal
stresses are typically much greater than the transverse.
As is clear from the figure, the stresses tend to be tensile
over a region extending just beyond the diameter of the
tool shoulder. The tensile region tends to encompass the
nugget and TMAZ and reflects the extent of the hot
region beneath the shoulder. The peak stresses are often
found just inside or just beyond the shoulder radius.
Often the peak stress lies within the HAZ despite the
lower hardness often found there. Lower level compressive residual stresses are typically found in the parent
plate beyond the HAZ. The depth of the tensile plateau
below the tensile peaks and the presence of a subsidiary
peak on the weld centreline appear to be alloys specific.
It should also be noted that the breadth of the tensile
region and the magnitude of the stresses vary greatly
according to the processing conditions. For example,
Threadgill et al.
36 Longitudinal and transverse residual stress variation: above, plate cross-section in 20 mm thick AA7449/7449 friction
stir weld (tool diameter 34 mm);326 below, at midthickness for dissimilar 6082/5083 weld (tool diameter 18 mm) in
3 mm thick plate54 (weld started at white spot and nished at black spot). In both cases advancing side is on right
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37 Measured and predicted effect of traverse speed and rotation speed: experimental data are for 2199,301 predictions
for 7050297
thermal models, these are capable of predicting differences in stress between the advancing and retreating
sides of the weld. Typically very little difference is either
predicted or observed in practice; however, Fig. 37 does
show slightly high measured and predicted stresses on
the advancing side and this observation is supported by
the work of others.299
The evolution of longitudinal stress as the tool passes
is depicted in Fig. 38. It demonstrates that ahead of the
tool the compressive stress caused by the expanding hot
material impinges on the compressive yield stress locus,
causing local plastic straining. Just behind the tool
longitudinal tensile stresses begin to generate as the weld
material cools. Initially stress development near to the
weld line is limited by the low tensile yield stress
(Fig. 38c). This local tensile plastic straining at the weld
line results in the characteristic M shape typically
observed in the welded plate (Fig. 38d), as the hot region
plastically deformed in compression, to a greater width,
ahead of the tool becomes stressed in tension as it cools
behind the tool. As the tool travels forwards and the
temperature falls, the tensile stress level builds up at a
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a as heat source approaches and compressive stresses form; b directly through tool centre, showing resultant reduction
in thermal strain by compressive yielding; c 8 mm behind centre of pin and at edge of shoulder, as heat source
retreats, material begins to cool and tensile yielding occurs; d final stress state after removal of tensioning loads
38 Effect of external mechanical tensioning (given as percentage of parent plate yield stress) on predicted longitudinal
residual stress proles for AA2024T6 plate friction stir welded at 770 rev min21 and 195 mm min21 (tensile and compressive yield loci are shown as dashed lines)296
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39 a comparison of measured (left)266 and predicted (right) longitudinal stress proles for AA7449W51 welded plates as
function of tensioning level (0, 5, 10, 20, 30% of parent alloy yield stress): dotted prole represents predicted untensioned (0%) case for which there were no measured results; b residual stress at midthickness near weld line as function of applied global tensioning level for various alloys290,326
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the FSW tool shoulder can be rolled along the weld line
once the weld has cooled. Recent stress measurements
suggest that this approach is much more effective than
when applied during welding (Fig. 40) with loads in
excess of 15 kN leading to compressive weld stresses for
2199.324 This compares with little effect during welding
using two rollers and a combined down force of 75 kN.
By contrast post-weld mechanical tensioning is much
less effective than that applied during welding.296
Distortion
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a initial residual stress before crack (solid line) and contribution of crack to stress intensity factor (dashed line) as function of crack growth for transverse crack; b corresponding residual stress redistribution ahead of crack tip
41 Residual stresses in 3?2 mm thick 2024 friction stir weld testpiece, measured by crack compliance technique (horizontal dashed line indicates compressive yield strength of material)299
Fatigue
As with other mechanical property data, care needs to be
taken to ensure that full information on the test
procedure is available. In particular, in some fatigue
tests, the surface of friction stir welds is dressed to remove
flash and the surface markings. Occasionally even more
material is removed, and this is acceptable if the weld in
question is machined in the same way in service. When
comparing data, R values should be checked to ensure
they are the same especially in cases where residual
stresses may exist in the testpiece, but these are not always
reported. Examination of the literature has shown that
the following generalisations can be made:
(i) in simple SN tests on cross-weld samples, the
fatigue performance of friction stir butt welds is
typically less good than that of the parent
material tested under the same conditions.327,328
Many studies have found that after milling the
top surface, the fatigue performance of 2014,
6013 and 7475 FSW joints approached that of
the parent alloys,329331 yet in other studies332
the properties remain significantly below parent
material benchmarks
(ii) the fatigue performance of friction stir butt
welds generally comfortably exceeds that of
comparable fusion welds,93,226,330,331,333,334 a
trend reported for many alloy grades
(iii) failure is normally (but not always) associated
with an initiation event at the geometric stress
concentration at the side of the weld on the
upper surface;335 where this has been machined
away, failure normally initiates in the region of
lowest strength. For many alloy groups, these
two locations are very close together
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a in as-welded condition; b after 2% stretching (filled and open symbols correspond to different samples)
42 Crack growth data for FSW in 2024T351 for cracks growing parallel to weld in CT samples:341 plots are for cracks
located at various distances from weld line propagating parallel to weld
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43 Comparison of fatigue crack growth rates in laboratory air between weld nugget and HAZ for friction stir
welds in 7050T7451 plate at load ratios R50?33 and
0?7: specimens were in as FSWzT6 condition191
Fracture toughness
Fracture toughness is not normally a problem in
aluminium alloys, but there are nevertheless areas where
it is important, in particular at very low temperatures
such as those encountered in cryogenic structures, or in
exterior surfaces of airframes. Fracture toughness has
been studied using a number of testing configurations
for alloys including 2014,374,375 2024,257,376 2139,116,377
2195,378 5083,374,379 6061,257,258 7075,374 and 7449.254,380
Mochizuki et al.379 found that for 5083O, in contrast
to hardness and static strength, the Charpy impact
energy and critical crack tip opening displacement
(CTOD) in the friction stir weld are much higher than
those corresponding to the parent metal or the HAZ.
This was ascribed to the fact that the fine grained
microstructure in the stir zone helps to increase ductile
crack initiation and propagation resistance.
Dawes et al.374 investigated the R curve behaviour of
2014A, 5083 and 7075; typical data are shown in Fig. 44.
This shows that the fracture toughness in the nugget and
the HAZ/TMAZ region exceeded that of the parent
material, presumably because of the very fine grain
structures. This effect was found for all alloys tested,
although the magnitude of the difference varied between
alloy types. von Strombeck et al.259 obtained similar
results on 2024T351, 5005H14 and 6061T6 alloys
using a CTOD parameter to measure toughness rather
than the J parameter used by Dawes. Only 2024 joints
exhibited similar or slightly lower fracture toughness
than the parent alloy. This behaviour was attributed to
changes in the characteristics of the inclusion and
precipitates population. Supporting these observations,
Brinkmann et al.258 have reported that the fracture
toughness of the nugget in 3 mm 6061T6 friction stir
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Corrosion
It is well established that microstructure is an important
factor in determining the corrosion behaviour of
aluminium alloys.384 A great deal of attention has been
focused on the Cu containing 2xxx and 7xxx series
(e.g. 2024,48,385390 7010, 7050, 7075),385,388,391393 which
show that the nugget becomes sensitised (Table 4). The
severe themomechanical processing refines the grain
structure and alters the precipitation distribution and
chemistry, particularly near the grain boundaries
(Tables 4 and 5). The relationship between microstructure and corrosion for 2024 is summarised in the form
of a timetemperaturecorrosion map384,410 in Fig. 47.
From this it is clear that the maximum thermal
excursion in the FSW weld region is above the knee in
the timetemperaturecorrosion curve and the cooling
rate sufficiently slow for pitting and intergranular
corrosion to occur.
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Localised corrosion
Mechanism
Test
Ref.
2024 TMAZ
Nugget
Nugget
HAZ/parent
HAZ
Nugget and HAZ
Exfoliation
Pitting/blistering
Intergranular/pitting (150 mm)
Pitting to 150 mm
Intergranular
Intergranular attack (low rotation spends
in nugget/high speeds predominantly HAZ))
Passive Pitting
ASTM G34
48
Immersion (NaClzH2O2)
48
Immersion (NaCl)
Gel visualisation and Immersion
(NaCLzH2O2)
Poarisation curves and ellectrochemical
impedance spectroscopy in NaCl
Immersion (NaCl)
385, 394
395, 396
Immersion (NaClzH2O2)
Immersion (NaCl)
116
386, 398
400
395
401
402
385
213, 392, 403,
404, 405
391
392, 404, 406
407
408
409
401
Nugget/HAZ Parent
2219 Parent
2139 Parent
2195 No preference
5083
5456
6082
6013
7010
7050
Parent
Nugget
Parent
HAZ
Nugget, TMAZ/HAZ
7075 HAZ
Intergranular
HAZ
HAZ
TMAZ/HAZ boundary
7108 TMAZ
Localised intergranular corrosion
7150 TMAZ
Immersion (NaClKNO3HNO3)
Immersion
Pitting potential cell
Salt spray
ASTM G34 EXCO
Immersion
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49 Macrographs (left) and corresponding gel visualisations (right) of corrosion attack on cross-sections of 2024 friction
stir welds after immersion in 0?1M NaCl for 24 h: welds were produced at different speeds and are arranged from top
to bottom in order of decreasing heat input396
Table 5 Typical relationship between microstructure, signicant localised corrosion mechanisms and main investigation
techniques for high strength aluminium alloy friction stir welds414
Zone
Microstructure
Parent
Strengthening ppts
Pitting
HAZ
Intergranular corrosion
Other corrosion phenomena
Intergranular corrosion
Intersubgranular corrosion
Pitting
TMAZ
Intergranular corrosion
Intersubgranular corrosion
Pitting
Nugget General absence of intragranular ppts Pitting
and ppt free zones
Intergranular corrosion
For some alloys, presence of
intragranular ppts and ppt free zones
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a general view following corrosion testing in Exco solution for 8 h; b network of CuMgAl2; c close-up of intergranular
corrosion
50 Scanning electron micrographs of intergranular attack on 2024 friction stir weld394
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Concluding remarks
Friction stir welding of aluminium is now a mature and
robust process, which is becoming increasingly well
established in the fabrication of critical components. It is
true to say that FSW has extended the use of welding in
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Acknowledgements
The authors are deeply indebted to many colleagues
within the global FSW community for numerous direct
and indirect contributions to this work, for making
available micrographs and figures and for many useful
discussions over the past few years. PLT and AJL were
afforded time by TWI to write this review. PJW is
grateful to Dr Altenkirch and Dr Steuwer for assistance
in providing some of the data presented.
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