3M ESPE Soft Monophase

3M ESPE Monophase
Polyether Impression Material

Technical Data Sheet

 Content

1. 3M ESPE (Soft) Monophase Material

from the inventor of polyether impression materials ......................................................................... 3 4

2. Polyether characteristics .......................................................................................................................... 5 7

2.1 Hydrophilicity of unset and set materials

2.2 Snap-set behaviour

2.3 Flow properties

2.4 Detail reproduction

2.5 Material properties

3. Clinical .......................................................................................................................................................... 8 11

3.1 Polyether impression materials from 3M ESPE the leaders in implant impressions.

3.2 Excellent impression results using any implant system you choose.

Open tray (direct)

Closed tray (indirect)

Closed tray (direct)

Passionate about
Precision
2
1
3M ESPE (Soft) Monophase Material
from the inventor of polyether impression materials

3M ESPE Soft Monophase and Monophase Polyether Impression Materials are the materials of choice for
all kinds of precision impressions and are especially well suited for implant and edentulous impressions.

The bright new colour guarantees enhanced readability and patients will enjoy a fresh
minty flavour and appreciate how easily the impression can be removed from the mouth.

Both materials are available for convenient automatic mixing in the Pentamix System from
3M ESPE, delivering high-quality mixing results and ultimate efficiency at the touch of button.

Features & Benefits:

Great readability thanks to bright new colour

Enhanced patient comfort thanks to fresh minty flavour and easy removal from the mouth of Soft version

Outstanding impression precision due to outstanding initial hydrophilicity

Excellent flow properties delivering great details

Unique snap-set behaviour to prevent setting while you are working

Secured implant coping position due to rigidity of polyether materials

Available for automatic mixing with the Pentamix 2 and Pentamix 3 Mixing Unit

Indications:

Implant impressions

Functional impressions

Crown and bridge impressions

Inlay and onlay impressions

Fixation impressions

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 Benefits of automatic mixing with the Pentamix System

Fast, time-saving procedure and push-button activation Hygienic direct filling of trays and syringes
Homogeneous, void-free mixtures of reproducible quality More efficient workflow and higher productivity
Economical, accurate dispensing of material

Automatic mixing of impression materials using the Pentamix system results in a mixing quality that is free from streaks and
voids. Figure 1 shows the difference between a common hand-mix material kneaded by hand (left) and automatically mixed
3M ESPE Soft Monophase Polyether Material (right).

3M ESPE Soft Monophase Polyether

A recent study at the University of Washington (Seattle, USA)* Impression material
mixed by hand
Impression Material automatically mixed
with the Pentamix System
investigated operators preference for different mixing techniques
and durations of mixing and tray loading. All users, from dental
students to experienced dentists, preferred automated mixing
with a Pentamix system to hand-mixing or automatic mixing
using a hand dispenser, regardless of the viscosity of the
impression material employed. Use of a Pentamix device also
made it easier to achieve equal mixing ratios between base
and catalyst, leading to a better-quality mix (Fig. 1).
Fig. 1: Mixing quality of automatically mixed 3M ESPE Soft Monophase Material (right)
compared to a common hand-mix material. Source: 3M ESPE internal data

Development of 3M ESPE automatically

mixed precision impression materials

3M ESPE (Soft)
Permadyne Penta H
Monophase Polyether
Impregum
Impregum Penta

Ramitec Impregum F Permadyne Garant 2:1 Penta Soft MB Soft Quick Impression Material

Impregum Soft
Impregum Permadyne Penta L Impregum Penta Polyether Tray
Impregum
Permadyne
Penta Ramitec Penta Soft HB/LB Impression Material

1965 1974 1980 1987 1993 1994 1995 2000 2001 2004 2009 2012

Penta

Soft

Fig. 2: Development of 3M ESPE automatically mixed precision impression materials. Source: 3M ESPE internal data

* J. NAM, A. J. RAIGRODSKI, J. TOWNSEND, X. LEPE, and L. A. MANCI; Assessment of preference of mixing techniques and duration of mixing and tray loading for two viscosities of vinyl polysiloxane material;
J Prosth Dent 2007:12-17

Since the introduction of the first polyether impression materials more than 45 years ago, 3M ESPE innovations have
continuously advanced impression technology.

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2 Polyether characteristics
With its unique and proven material characteristics, 3M ESPE (Soft) Monophase Polyether Impression Material reliably delivers
exceptionally detailed impressions even under difficult clinical conditions and a very precisely fitting final restoration work.

2.1 Hydrophilicity of unset and set materials

The superb detail reproduction of polyether impression material is primarily a result of its initial hydrophilicity, which in turn is due
to polyethers chemical makeup. Hydrophilicity allows the material to precisely reproduce surfaces that are moist with saliva or
even blood.

The contact angle of a water droplet placed on the surface of an impression material indicates its hydrophilicity: the lower the
contact angle, the higher the hydrophilicity.

High hydrophilicity of an impression material right from the start of the working time is of the utmost clinical relevance. Figure 3
shows a comparison of the initial hydrophilicity before setting of 3M ESPE Monophase and Soft Monophase polyether impression
materials and four well-known competing VPS monophase materials. 3M ESPE materials exhibit the lowest contact angles and
therefore the highest hydrophilicity.

3M ESPE polyether materials are hydrophilic by nature and therefore show excellent flow properties throughout the entire working
time, whereas VPS materials have to be hydrophilized by surface-active additives that must first migrate to the surface before the
impression material fully develops its hydrophilic properties.

3M ESPE (Soft) Monophase Impression Material shows a significantly lower contact angle and therefore higher hydrophilicity.

Hydrophilicity of 3M ESPE (Soft) Monophase Polyether Impression Material in unset state

78.4 71.2 100.3 111.4 94.9 107.9

3M ESPE Monophase 3M ESPE Soft Monophase Aquasil Ultra Flexitime Monophase Honigum Mixstar Mono, Affinis Monobody System 360,
Polyether Impression Material Polyether Impression Material Monophase, Dentsply Dynamix, Heraeus DMG Coltne Whaledent

Fig. 3: Initial contact angles of water drops on different impression materials. The water drops were set on the pastes 45 seconds after the start of mixing. The contact angle was measured directly
at a drop age of 0 seconds. Source: 3M ESPE internal data

Hydrophilicity of 3M ESPE (Soft) Monophase Polyether Impression Material in set state

To ensure excellent results for disinfection and pouring, high hydrophilicity is needed to ensure a wettable surface.
Due to its hydrophilic behaviour, the impression can be poured without using an additional wetting agent.

78.2 85.3 100.5 110.3 111.5 107.1

3M ESPE Monophase 3M ESPE Soft Monophase Aquasil Ultra Flexitime Monophase Honigum Mixstar Mono, Affinis Monobody System 360,
Polyether Impression Material Polyether Impression Material Monophase, Dentsply Dynamix, Heraeus DMG Coltne Whaledent

Fig. 4: Initial contact angles of water drops on different impression materials. The water drops were placed on set material. The contact angle was measured directly at a drop age of 0 seconds.
Source: 3M ESPE internal data

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 2.2 Snap-set behaviour
3M ESPE Monophase and Soft Monophase Polyether Impression Materials both offer a very long working time. In contrast
to A-type silicones (VPS), 3M ESPE (Soft) Monophase material does not change its consistency during the working time.
Snap Set

A-type silicones 3M ESPE Soft Monophase

Working time Setting time
Viscosity

Time

Fig. 5: Schematic overview of setting in A-silicones and polyethers.

To show the materials behaviour during working time, the consistencies of different impression materials were measured according
to ISO 4823:2000 after 25 seconds and at the end of each materials working time (Method is described in Hader S., Kuppermann
B., Ranftl D., Klettke T.: Flow of Fast-Setting Light Bodied Impression Materials During Working Time, CED 2005, #607). Figure 6
shows that the flowability of 3M ESPE (Soft) Monophase material does not change until the end of the working time. This guarantees
reliable handling during the impression procedure even for complex cases.

40

38 25 s
End of Working Time
36

34

32

30

28

26
3M ESPE 3M ESPE Aquasil Ultra Flexitime Affinis Honigum
Monophase Soft Monophase Monophase Monophase Monobody Mixstar Mono

Fig. 6: Diameter of discs for different materials according to ISO 4823:2000 consistency test. The discs were produced 25 seconds after start of
mixing and at the end of the respective working time. Source: 3M ESPE internal data

Moreover, studies* show that polyether impression materials are less temperature sensitive than
A-silicones. These results support the clinically proven reliability of 3M ESPE polyether impression
materials.

* Source: Berg et al.: Temperature effects on the rheological properties of current polyether and polysiloxane impression materials during setting,
J Prosth Dent. 90.2 (2003):150-161; Klettke et al.: Temperature effect on the setting of dental impression materials, IADR 2007 #914

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2.3 Flow properties
As well as being hydrophilic, 3M ESPE polyethers structural background also makes it thixotropic. The result is a unique polyether,
well suited for the monophase technique. 3M ESPE (Soft) Monophase Material offers a balanced flow stable in the tray but flowa-
ble for syringing the preparation.

A study analysing the insertion forces of different tray impression materials confirms the suitability of 3M ESPE polyether as a tray
material. (Klettke et al.: Insertion force of tray impression materials, IADR 2008 #3194). Moreover, both 3M ESPE Monophase and
Soft Monophase fulfil even the ISO criterion for detail reproduction applied for wash materials. Thanks to their thixotropy, all 3M ESPE
polyether impression materials are ideal for the monophase technique.

2.4 Detail reproduction

3M ESPE (Soft) Monophase impression material shows out-
standing detail reproduction and is able to capture the finest
details of surfaces even in moist environments.

Especially for the monophase technique, it is important to

have a suitable colour for good margin readability and detail
examination. The fresh green colour of both materials allows
for easy checking of all details captured by the impression.

2.5 Material properties

Properties 3M ESPE Monophase 3M ESPE Soft Monophase

Polyether Impression Material Polyether Impression Material

Consistency of mixture [mm] 35 36

Hardness [Shore A/24h] 56 47

Tear strength [MPa] 2.42 1.94

Elongation at rupture [%] 396 351

Toughness [J] 1.26 0.86

Linear dimensional change [%] -0.43 -0.29

Recovery from deformation [%] 97.5 98.3

Strain in compression [%] 3.2 5.4

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 3 Clinical
Polyether impression materials from 3M ESPE tried and tested for many years and practically synonymous with top-notch
impression precision offer all clinically relevant properties for optimum implant-supported prosthetic restorations.

3.1 Polyether impression materials from 3M ESPE

the leaders in implant impressions.
Among dental professionals, 3M ESPE polyether impression material represents the ultimate
in impression precision and is also a preferred choice for challenging implant impressions.

The results of a survey* carried out in Europe (Germany, Italy) and the U.S. show that
3M ESPE polyether material is the impression material most often used for implant-supported
prosthetic restorations.

Of the dentists who participated in the survey, 75% of those in Germany, close to 50%
in Italy, and 36% in the U.S. preferred 3M ESPE polyether materials to restore implants
making these materials leaders in the field of implant impressions.

* GfK Globus 2005

The implant treatment plan can only be as accurate as the impression. The performance and detail reproduction of 3M ESPE
Monophase and Soft Monophase Polyether Impression Material help you:

Achieve a detailed impression on the first take. Whether using an open or closed tray technique, or making implant
or abutment-level impressions, a detailed impression reduces the chance of costly retakes.

Capture impressions of transfer copings with confidence. Ensure the precise orientation and position of the implant
in the mouth. Using various impression materials, Perry et al. showed significantly higher torque strength for 3M ESPE
polyethers. Higher torque strength means less implant rotation, which is beneficial for maintaining secure implant positions
(Perry et al.: Effects of various impression materials on implant coping torque strength, IADR 2007 #1477).

3.2 Excellent impression results using any implant system you choose.
Several implant companies offer excellent implant options to choose from. No matter which system is preferred, using 3M ESPE
(Soft) Monophase impression material can help dentists to achieve the desired outcome, using the technique the clinician decides
is best for the indication. There are numerous techniques for making implant impressions. The three most common ones are
the open tray (direct) pick-up technique, closed tray (indirect) transfer impression technique and closed tray (direct)
snap-on technique.

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 pick-up technique

Open tray (direct)

In this technique, the direct transfer coping gets picked up and remains in the set impression upon removal from the mouth.
Once the impression has set, the screw holding the coping on the implant is accessed through the hole above/below the implant in
the open tray and unscrewed to allow removal of the impression from the mouth. Once outside of the mouth, the implant analogue
is connected to the transfer coping prior to pouring the stone model.

Removal of healing abutment Placement of transfer coping Tray selection open tray try-in Load tray

Remove healing abutment Verify correct seating of the coping Try-in the tray and create access window Load the tray material after using proper bleeding
Conrm prosthetic platform is free of bone debris with a radiograph Ensure there is appropriate clearance for entire technique
or soft tissue arch with no contact between tray and tissue Keep the mixing tip submerged in the tray material
Seat the coping and secure it using the method Evaluate tray-coping t, ensuring there is enough to prevent voids
recommended by the implant manufacturer clearance for coping to t easily through window Do not under-ll the tray
in tray

Evaluate final impression

Syringe around coping Tray seating and immobilisation Tray and coping removal with coping inserted (indexed)

While loading the tray, syringe the wash material Insert the loaded tray straight and evenly into Once impression material has set, remove Rinse impression before inspection
around the coping, and ensure continuous flow mouth avoid rotation screw holding coping in place, following implant Evaluate the impression for correct transfer and
around the entire coping Dont let patient bite down on tray manufacturers instructions common impression errors (see side bar on
Keep the mixing tip submerged in the wash mate- Immobilize the tray using passive pressure Remove tray from mouth carefully, with coping this page)
rial at all times to avoid trapping air bubbles embedded in the set impression Attach the implant analogue to coping embedded
Follow the recommended setting time in the
mouth using a timer Replace healing abutment immediately to prevent in the impression
soft tissue collapse Dry and disinfect impression before shipping

Bite registration

RECOMMENDED
Tips MATERIAL
Common causes for retakes: 3M ESPE (Soft)
Monophase
Distorted impression:
To prevent distortion, stabilize the tray while material is setting
Voids and bubbles:
Apply a layer of 3M ESPE Imprint Bite Material

Use enough material and keep tip submerged in extruded material
with a thickness of approximately 5 mm occlusal-
incisally to the entire lower arch Pick-up technique:
Have patient bite into proper occlusion
Tray-abutment contact: Widen implant windows in tray
Disinfect prior to shipping
Make an impression of the opposing arch and
submit it with case

9
 transfer impression technique

Closed tray (indirect)

In this technique, the indirect transfer coping remains on the implant during removal of the set impression from the mouth. Once the
impression has been removed, the coping is removed from the implant and connected with the implant analogue. The coping/analogue
assembly is then indexed (transferred) back into its corresponding position in the impression.

Removal of healing abutment Placement of transfer coping Tray selection open tray try-in Load tray

Remove healing abutment Verify correct seating of the coping Try-in the tray Load the tray material after using proper bleeding
Conrm prosthetic platform is free of bone debris with a radiograph Ensure there is appropriate clearance for entire technique
or soft tissue Block out hex-hole with material or components arch Keep the mixing tip submerged in the tray material
Seat the coping and secure it using the method recommended by the manufacturer Evaluate tray-coping t, ensuring there is no to prevent voids
recommended by the implant manufacturer impingement/interference Do not under-ll the tray

Evaluate final impression

Syringe around coping Tray seating and immobilisation Tray and coping removal with coping inserted (indexed)

While loading the tray, syringe the wash material Insert the loaded tray straight and evenly into Remove tray from mouth carefully after end of Rinse impression before inspection
around the coping, and ensure continuous flow mouth avoid rotation setting time Evaluate the impression for correct transfer and
around the entire coping Dont let patient bite down on tray Remove coping post or assembly from implant common impression errors (see side bar on
Keep the mixing tip submerged in the wash Immobilize the tray using passive pressure after tray has been removed, following implant this page)
material at all times to avoid trapping air bubbles manufacturers instructions Insert coping assembly into impression
Follow the recommended setting time in the
mouth using a timer Replace healing abutment immediately to prevent Ensure the coping is properly aligned (indexed)
soft tissue collapse within the impression
Assemble coping with implant analogue Dry and disinfect impression before shipping

Bite registration

RECOMMENDED
Tips MATERIAL
Common causes for retakes: 3M ESPE (Soft)
Monophase
Distorted impression:
To prevent distortion, stabilize the tray while material is setting
Voids and bubbles:
Apply a layer of 3M ESPE Imprint Bite Material

Use enough material and keep tip submerged in extruded material
with a thickness of approximately 5 mm occlusal-
incisally to the entire lower arch Insufficient capture of detail around coping:
Have patient bite into proper occlusion
Syringe material without creating air bubbles around copings by
Disinfect prior to shipping
Make an impression of the opposing arch and keeping mixing tip submerged
submit it with case

10
 snap-on technique

Closed tray (direct)

The snap-on procedure is best described as a hybrid between the two techniques shown previously. In this closed tray procedure,
the direct transfer coping snaps-on to the top of the implant abutment in the mouth. Once the impression has set, the coping
becomes embedded in the impression and is pulled off of the implant abutment when the set impression is removed from the mouth.
Once outside of the mouth, the implant analogue is connected to the transfer coping prior to pouring the stone model.

Removal of healing abutment Placement of transfer coping Tray selection open tray try-in Load tray

Remove healing abutment Seat the abutment and secure it using the me- Try-in the tray Load the tray material after using proper bleeding
Conrm prosthetic platform is free of bone debris thod recommended by the implant manufacturer Ensure there is appropriate clearance for entire technique
or soft tissue Attach the snap-on transfer coping assembly arch Keep the mixing tip submerged in the tray
(see completed assembly in step 5) Evaluate tray-coping t, ensuring there is no material to prevent voids
impingement/interference Do not under-ll the tray

Evaluate final impression

Syringe around coping Tray seating and immobilisation Tray and coping removal with coping inserted (indexed)

While loading the tray, syringe the wash material Insert the loaded tray straight and evenly into Once impression material has set, remove tray Rinse impression before inspection
around the coping, and ensure continuous flow mouth avoid rotation from mouth carefully, with snap-on coping Evaluate the impression for correct transfer and
around the entire coping Dont let patient bite down on tray embedded in the set impression common impression errors (see side bar on
Keep the mixing tip submerged in the wash mate- Immobilize the tray using passive pressure Depending on the implant system used, either this page)
rial at all times to avoid trapping air bubbles A) Replace healing abutment immediately to Dry and disinfect impression before shipping
Follow the recommended setting time in the
mouth using a timer prevent soft tissue collapse, OR
B) Create the appropriate temporary restoration
to protect the abutment
Assemble coping with implant analogue
Bite registration

RECOMMENDED
Tips MATERIAL
Common causes for retakes: 3M ESPE (Soft)
Monophase
Distorted impression:
To prevent distortion, stabilize the tray while material is setting
Voids and bubbles:
Apply a layer of 3M ESPE Imprint Bite Material

Use enough material and keep tip submerged in extruded material
with a thickness of approximately 5 mm occlusal-
incisally to the entire lower arch Snap-on technique:
Have patient bite into proper occlusion
Coping-tray contact: Try-in the tray prior to making impressions
Disinfect prior to shipping
Make an impression of the opposing arch and and ensure proper size
submit it with case

11
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Ramitec are trademarks of 3M Company or
3M Deutschland GmbH. Used under license
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