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    Agilent 355 SCD and 255 NCD: Detector Startup

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    venkata.krishnan
    Detector Startup Complete Startup (from total shut down) 1 Turn the instrument from Standby to On, and allow the system to evacuate for approximately 1 minute. Detector Shutdown Daily Shutdown (Standby Mode) 1 Turn off the ozone generator with the button on the front of the Detector.

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    Attribution Non-Commercial (BY-NC)
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    Agilent 355 SCD and 255 NCD: Detector Startup

    Uploaded by

    venkata.krishnan
    60 views4 pages
    Detector Startup Complete Startup (from total shut down) 1 Turn the instrument from Standby to On, and allow the system to evacuate for approximately 1 minute. Detector Shutdown Daily Shutdown (Standby Mode) 1 Turn off the ozone generator with the button on the front of the Detector.

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    G6600-90031

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    Detector Startup Complete Startup (from total shut down) 1 Turn the instrument from Standby to On, and allow the system to evacuate for approximately 1 minute. Detector Shutdown Daily Shutdown (Standby Mode) 1 Turn off the ozone generator with the button on the front of the Detector.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    60 views4 pages

    Agilent 355 SCD and 255 NCD: Detector Startup

    Uploaded by

    venkata.krishnan
    Detector Startup Complete Startup (from total shut down) 1 Turn the instrument from Standby to On, and allow the system to evacuate for approximately 1 minute. Detector Shutdown Daily Shutdown (Standby Mode) 1 Turn off the ozone generator with the button on the front of the Detector.

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    Agilent 355 SCD and 255 NCD

    Quick Reference Guide

    Detector Startup

    Complete Startup (from total shut down)


    1 Turn on the detector and establish carrier gas flow.
    2 Turn on the vacuum pump with the toggle button located on the front panel
    of the Detector.
    3 Turn the instrument from Standby to On, and allow the system to evacuate
    for approximately 1 minute.
    4 Turn on the air to the ozone generator and set the regulator inside the front
    door of the Detector to between 3 and 6 psig.
    5 Turn on the ozone generator.
    6 Turn on the Interface Controller with the toggle on the back panel of the
    box.

    Daily Startup (from daily shutdown)


    1 Turn the instrument from Standby to On, and allow the system to evacuate
    for approximately 1 minute.
    2 Turn on the air to the ozone generator and set the regulator inside the front
    door of the Detector to between 3 and 6 psig.
    3 Turn on the ozone generator.

    Detector Shutdown

    Daily Shutdown (Standby Mode)


    1 Turn off the ozone generator with the button on the front of the Detector.
    2 Turn down the oxidant flow to 0 with the regulator located in the front door
    of the Detector.
    3 Turn the Detector power to Standby.

    It is recommended to leave the vacuum pump and Dual Plasma Controller


    operating at all times.

    Agilent Technologies
    Agilent 355 SCD and 255 NCD

    Complete Shutdown (long periods of time)


    1 Turn off the ozone generator with the button on the front of the Detector.
    2 Turn down the air flow to 0 with the regulator located in the front door of
    the Detector.
    3 Turn the Detector power to Standby.
    4 Turn off the power switch on the Controller and allow at least 15 minutes
    for the burner to cool.
    5 Turn off the vacuum pump.
    6 Turn off the Detector gases.

    Table 1 Typical Operating Conditions

    Condition SCD NCD

    Detector Pressure (Torr) 4-8 (6-12*) 4-10

    Dual Plasma Controller Pressure (Torr) 300-400 100-250

    Burner Temperature (°C) 800 900-950

    Hydrogen Flow Rate (sccm) 40-50 4-6

    Oxidant Flow Rate (sccm) 60-65 (air) 8-12 (oxygen)

    Background Noise (mV) 0.3-2.0 0.3-1.0

    *Oil-free pump

    Table 2 Maintenance Schedule

    Component/Material Operating Life*


    Pump Oil ~3 month

    Oil Coalescing Filter ~3 months

    Chemical Trap ~3 months

    *Operating life is based on the total time logged during operation of the 355 SCD with the burner and ozone
    generator on.

    2 Quick Reference Guide


    Agilent 355 SCD and 255 NCD

    Quick Reference Guide 3


    Agilent Technologies

    © Agilent Technologies, Inc. 2007


    Printed in USA
    First edition, March 2007
    Agilent Technologies, Inc.
    2850 Centerville Road
    Wilmington, DE 19808-1610 USA

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