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    Chm260 Tutorial 2

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    adlina asnawi
    The document provides the FTIR spectra and analysis of various compounds. It asks the student to: 1) Analyze spectra 1-3 to identify bonds in compounds X and Y (alcohol and ketone) and justify spectrum 3 is propanal. 2) Identify three peaks in heptanoic acid spectrum and their bonds. 3) Compare butanol and butanone based on characteristic wavenumbers. 4) Justify a strong absorption in methylbenzene spectrum. 5) Estimate C=O stretching order in three compounds. 6) Select three important peaks in 3-hydroxy benzaldehyde spectrum and identify functional groups.

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    Chm260 Tutorial 2

    Uploaded by

    adlina asnawi
    580 views4 pages
    The document provides the FTIR spectra and analysis of various compounds. It asks the student to: 1) Analyze spectra 1-3 to identify bonds in compounds X and Y (alcohol and ketone) and justify spectrum 3 is propanal. 2) Identify three peaks in heptanoic acid spectrum and their bonds. 3) Compare butanol and butanone based on characteristic wavenumbers. 4) Justify a strong absorption in methylbenzene spectrum. 5) Estimate C=O stretching order in three compounds. 6) Select three important peaks in 3-hydroxy benzaldehyde spectrum and identify functional groups.

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    FTIR

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    The document provides the FTIR spectra and analysis of various compounds. It asks the student to: 1) Analyze spectra 1-3 to identify bonds in compounds X and Y (alcohol and ketone) and justify spectrum 3 is propanal. 2) Identify three peaks in heptanoic acid spectrum and their bonds. 3) Compare butanol and butanone based on characteristic wavenumbers. 4) Justify a strong absorption in methylbenzene spectrum. 5) Estimate C=O stretching order in three compounds. 6) Select three important peaks in 3-hydroxy benzaldehyde spectrum and identify functional groups.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    580 views4 pages

    Chm260 Tutorial 2

    Uploaded by

    adlina asnawi
    The document provides the FTIR spectra and analysis of various compounds. It asks the student to: 1) Analyze spectra 1-3 to identify bonds in compounds X and Y (alcohol and ketone) and justify spectrum 3 is propanal. 2) Identify three peaks in heptanoic acid spectrum and their bonds. 3) Compare butanol and butanone based on characteristic wavenumbers. 4) Justify a strong absorption in methylbenzene spectrum. 5) Estimate C=O stretching order in three compounds. 6) Select three important peaks in 3-hydroxy benzaldehyde spectrum and identify functional groups.

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    CHM260 (TUTORIAL FTIR)

    Name: Nur Adlina bt Asnawi Matric ID: 2017433934

    Answer the following questions.

    1) Answer the following questions based on the given Spectrum 1, 2 and 3.


    CHM260 (TUTORIAL FTIR)

    a) Predict the bonds associated with the two (2) labeled absorption peaks shown in Spectrum 1 and
    2, respectively.
    Spectrum 1
    2998: C-H
    1712: C=O
    Spectrum 2
    3345: O-H
    1162: C-O

    b) Decide which compound (X or Y) corresponds to each Spectrum 1 and 2, respectively.


    OH O

    H3CCH3 H3COH
    Compound X Compound Y

    Compound X: spectrum 2
    Compound Y: spectrum 1

    c) Spectrum 3 belongs to propanal (C3H6O). Justify this statement based on the labeled absorption
    bands on Spectrum 3 and give the corresponding functional groups.
    1703: Carboxylic acid
    2820: Aldehydes
    2738: Aldehydes
    2) The following diagram is the IR spectrum of heptanoic acid, CH 3(CH2)5COOH. Identify three (3)
    important peaks and their corresponding bonds associated with each peak.

    2971: C-H
    1721: C=O
    1296: C-O
    CHM260 (TUTORIAL FTIR)

    3) Compare butanol and butanone based on the characteristic wavenumbers of their IR spectra.
    Butanol is in an alcohol group with wavenumbers (3400-3300)
    Butanone is in ketone group with wavenumbers (1720-1708)

    4) Justify the strong absorption at 1450-1600 cm-1 in the IR spectrum of methylbenzene.


    Aromatic ring and alkane
    5) Estimate the C=O stretching of the following compounds in the order of increasing wavenumber.
    O O

    CH3 H H3C C H3
    H3C OH

    H3C
    CH3 CH3 O
    2-methylbutanal 2-methylbutanoic acid 3-pentanone

    2-methylbutanal, 3-pentanone, 2-methylbutanoic

    6) Given below is the FTIR spectrum of 3-hydroxy benzaldehyde. Select three (3) important peaks and
    determine the functional groups and wavenumbers associated with the peaks.

    Phenol: O-H (3600-3200)


    Aromatic rings: C-H (3100-3000)
    Aldehyde: C-H (2760-2700, 2860-2800)
    CHM260 (TUTORIAL FTIR)

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