Bla Bla
Bla Bla
Bla Bla
1985
Incorporating
Amendment No. 1
Concrete admixtures —
Part 3: Specification for
superplasticizing admixtures
Contents
Page
Committees responsible Inside front cover
Foreword ii
1 Scope 1
2 Definitions 1
3 Sampling 1
4 Performance requirements 1
5 Uniformity tests and requirements 2
6 Provision of information 2
7 Marking 3
Appendix A Preparation of concrete for acceptance tests 4
Appendix B Tests on control mix and test mix concretes 6
Table 1 — Performance tests and requirements for high
workability test mix concrete A 1
Table 2 — Performance tests and requirements for water
reduced test mix concrete B 2
Table 3 — Uniformity tests and requirements 2
Table 4 — Fine aggregate grading limits 4
Bibliography 8
© BSI 10-2000 i
BS 5075-3:1985
Foreword
This Part of BS 5075 has been prepared under the direction of the Cement,
Gypsum, Aggregates and Quarry Products Standards Committee and is based on
an initial draft provided by the Cement Admixtures Association. This Part of this
standard incorporates such recommendations of other organizations as the
Technical Committee felt were appropriate, and is based on the results of
cooperative tests carried out in accordance with earlier drafts of this Part.
This Part of this standard is concerned only with retarding superplasticizing
admixtures.
The requirements for non-retarding superplasticizers which were previously
covered by this part of BS 5075 have been superseded by the issue of BS EN 934-2
and BS EN 934-6.
Where existing British Standards and specifications call up non-retarding
superplasticizers meeting the requirements of BS 5075-3, products with an
existing certificate showing compliance with that standard can still be accepted.
Products which have been tested to the requirements of BS EN 934-2 should also
be accepted as showing technically equivalent performance.
Where standards and specifications call up BS EN 934, it is recommended that
for an interim period, BS 5075 certification should be continued to be accepted as
technically equivalent.
Accelerating and retarding water-reducing admixtures are covered by BS 5075-1
and admixtures for mortar are covered by BS 4887. All other types of admixture
for concrete are now covered by BS EN 934-2.
Admixtures for mortars are covered by BS 4887. Major changes are made to this
part of this British Standard by Amendment No. 1 subsequent to the publication
of BS EN 934-2.
This Part of BS 5075 specifies acceptance tests which demonstrate the ability of
a particular formulation to meet stipulated performance requirements, and
admixture uniformity tests which demonstrate that a particular consignment is
similar to material which has previously been submitted to the acceptance tests.
Either may be carried out by the vendor or at an independent laboratory at the
request of the purchaser.
In the acceptance tests, provision has been made for the diverse applications of
retarding superplasticizing admixtures in practice and the differing chemical
nature of those available. Some of the tests are therefore relevant to the use of
retarding superplasticizing admixtures to produce very high workability, whilst
the remainder are relevant to obtaining very large reductions in water content.
In the first of these applications, it is usually the intention to produce flowing
concrete without drastic alteration of the mix designs employed for normal
concrete. Excessive bleeding, segregation, retardation or air-entrainment are
undesirable, however, and should not be promoted by the use of superplasticizing
admixtures in this type of concrete.
In the second application, a large reduction in water content is required without
loss of workability. An extension of initial stiffening time is required within limits
and the requirement for early but not later age strength development is relaxed.
The principle has been followed of having one test mix concrete at the same
water/cement ratio as a control mix to establish the effect of the admixture on
workability and strength. In a second test mix, a fixed water reduction is made
and the concrete is tested against specified requirements for workability,
stiffening time and strength. An upper limit is placed on the air content of the
concrete in both test mixes.
ii © BSI 10-2000
BS 5075-3:1985
Workability can change rapidly immediately after mixing. However, tests have
shown that a relatively stable state is attained within 10 min to 15 min from the
completion of mixing and this time has been selected for establishing initial
workability. In the case of flowing concrete, there is usually a tendency for the
effect of the superplasticizing admixture on workability to diminish steadily with
time and, in order to ensure adequate retention of the initial high workability, a
requirement for loss of workability on standing has been introduced.
The stiffening time test, which is carried out on mortar sieved from the concrete,
is used to determine the times required for a standard needle to indicate a
resistance to penetration of 0.5 N/mm2 and 3.5 N/mm2. Work has shown that the
time to reach a resistance of 0.5 N/mm2 corresponds approximately to the
extreme limit for placing and compacting concrete, and the time to reach a
resistance of 3.5 N/mm2 gives a guide to the time available for the avoidance of
cold joints.
No requirements for tests on hardened concrete have been introduced, apart from
those relating to compressive strength. Drying shrinkage, creep, and long term
durability are still under investigation, and the effect of superplasticizing
admixtures on these properties should be the subject of advice from the
admixture manufacturer.
The admixture uniformity tests include determination of dry material content,
ash content and chloride ion content. The standard requires that the chloride
content of the admixture shall be declared so that the user will be fully aware of
the amount of chloride that will be introduced into the concrete, and if necessary
will be able to take appropriate precautions.
When a purchaser requires a certificate stating that an admixture complies with
this Part of BS 5075, the manufacturer should provide the information given
in 6.1. Additional information relating to the correct use of the admixture as
given in 6.2 should also be made available on request.
The performance of retarding superplasticizing admixtures should be assessed in
the particular concrete to be used because the performance may be affected by
changes in concrete composition.
Certification. Attention is drawn to the certification facilities described on the
inside back cover of this standard.
A British Standard does not purport to include all the necessary provisions of a
contract. Users of British Standards are responsible for their correct application.
Compliance with a British Standard does not of itself confer immunity
from legal obligations.
Summary of pages
This document comprises a front cover, an inside front cover, pages i to iv,
pages 1 to 8, an inside back cover and a back cover.
The BSI copyright notice displayed in this document indicates when the
document was last issued.
Sidelining in this document indicates the most recent changes by amendment.
1)
The term “manufacturer” throughout this standard includes the supplier where appropriate.
© BSI 10-2000 1
BS 5075-3:1985
Table 2 — Performance tests and requirements for water reduced test mix concrete B
Property Test reference Type of admixture
2 © BSI 10-2000
BS 5075-3:1985
e) the sources of the cement and aggregates used d) the packaging, recommended storage
in the tests; conditions, maximum storage time before use,
f) the dosages of admixture used in each of the and special precautions at extremes of
test mixes; temperature, including instructions regarding
liquids which have become frozen. Where any
g) the values, where applicable, for each control
special requirements on storage life apply, they
and test mix, of slump, flow, air content and
shall be stated, e.g.:
water/cement ratio as well as the cement content
of the control mix; “This admixture shall not be taken to comply
with BS 5075-3:1985 after (date)”
h) the loss of workability for test mix A, as
measured by slump, after standing for specified e) instructions for use and any necessary safety
periods; precautions, e.g. if caustic, toxic or corrosive;
i) the percentage water reduction for test mix B; f) any known incompatibility with other
admixtures or with certain types of cement, etc.;
j) the stiffening times for the control mix and for
test mix B; g) the manufacturer’s recommended dosage or
dosages;
k) the ratio of the mean compressive strength of
the cubes at the appropriate ages from each of h) the effects of underdosage and overdosage.
test mixes A and B to the mean compressive
strength of the control mix cubes; 7 Marking
l) the composition as follows: When admixtures are supplied in containers they
1) the dry material content; shall be clearly marked with the following
information. When the material is supplied into a
2) the ash content; bulk container at the point of delivery, the same
3) the relative density of liquid admixtures; information shall be provided in writing at the time
4) the chloride ion content, expressed as a of delivery as follows:
percentage by mass of total admixture. a) the name, trade mark or other means of
6.2 General information identification of the manufacturer;
The following information shall be available2) in b) the trade designation of the product, i.e. brand
writing: name, reference number and/or letter;
a) the physical state (i.e. liquid or solid) and c) the description of the material, i.e. retarding
colour; superplasticizing admixture;
b) the generic type of main active constituents, d) the chloride ion content, expressed as a
e.g. sulfonated melamine formaldehyde percentage by mass of total admixture;
condensate, sulfonated naphthalene e) a summary of storage requirements including
formaldehyde condensate or lignosulfonate; any special requirements on storage life, as
c) the chloride content relative to the cement indicated in 6.2 d), which shall be clearly
mass contributed by the recommended dosage or marked, e.g.:
dosages, expressed as a percentage by mass of “This admixture shall not be taken to comply
chloride ion; with BS 5075-3:1985 after (date)”
f) instructions for use and any necessary safety
precautions, e.g. if caustic, toxic or corrosive;
g) the manufacturer’s recommended dosage or
dosages;
h) the number and date of this Part of this British
Standard, i.e. BS 5075-3:19853).
2) Informationis normally provided by the manufacturer in a data sheet but may be made available by a supplier after
re-packaging bulk material.
3)
Marking BS 5075-3:1985 on or in relation to a product is a claim by the manufacturer that the product has been manufactured
in accordance with the requirements of the standard. The accuracy of such a claim is therefore solely the manufacturer’s
responsibility. Enquiries as to the availability of third party certification to support such claims should be addressed to the
Director, Quality Assurance Division, BSI, Linford Wood, Milton Keynes MK14 6LO in the case of certification marks
administered by BSI or to the appropriate authority for other certification marks.
© BSI 10-2000 3
BS 5075-3:1985
4)
Information on the supply of the reference cement can be obtained from the Cement Admixtures Association, 38A Tilehouse
Green Lane, Knowle, West Midlands B93 9EY.
4 © BSI 10-2000
BS 5075-3:1985
© BSI 10-2000 5
BS 5075-3:1985
Appendix B Tests on control mix and After mixing, cover the concrete for the test to
test mix concretes prevent loss of water by evaporation and keep it at
a temperature of 20 ± 2 ºC. At 45 min after
B.1 General completion of mixing, re-mix the concrete by hand
using a shovel just enough to counteract any
Use the appropriate test procedure for each of the bleeding or segregation, and make duplicate
concrete mixes produced. Where compaction of the determinations of the slump. Discard this concrete
concrete is required it shall be accomplished by and keep the remaining concrete covered and then,
mechanical vibration using an identical method and at 4 h after completion of mixing, repeat the
procedure each time on concretes of similar re-mixing by hand and make duplicate
workability. The operator should be aware that, in determinations of the slump. Calculate and report
the case of test mix A, only a short period of the mean slumps to the nearest 5 mm.
vibration will be necessary due to the very high
workability of the concrete. Take samples of B.6 Air content
concrete for testing by the method given in
Determine the air content of each batch of the
BS 1881-1:19705). Carry out duplicate tests as
control and test concretes A and B to the
indicated in clause 4 of this standard.
nearest 0.1 %, in accordance with the procedure
B.2 Slump described in BS 1881-106 with the following
modification. Compact each layer of concrete in the
Determine the slump of the control mix and test mix air meter by mechanical vibration of minimum
concrete B by the method given in BS 1881-102. duration to give a relatively smooth concrete surface
Make duplicate determinations between 10 min with a glazed appearance (e.g. 5 s per layer on a
and 15 min after the completion of mixing. Vebe table). Carry out the tests between 30 min
Calculate and report the mean slumps to the and 45 min after the completion of mixing for each
nearest 5 mm. of the mixes. Cover the concrete to prevent
evaporation of water between the completion of
B.3 Flow mixing and start of the test. Discard the concrete
Determine the flow of duplicate samples of test mix used for this test.
concrete A between 10 min and 15 min after the
completion of mixing by the method given in B.7 Compressive strength
BS 1881-105. Calculate and report the mean flow in Cast sufficient 100 mm test cubes, within 60 min of
millimetres to the nearest 5 mm. completion of mixing for the control and test mix
concretes A and B, to provide three test cubes for
B.4 Stiffening times each of the ages specified in Table 1 and Table 2.
Determine the times from completion of mixing for Cast, cure and test the cubes in accordance with
the control mix and test mix concrete B to reach BS 1881-108, BS 1881-111 and BS 1881-116, but
resistances to penetration of 0.5 N/mm2 take care to avoid excessive vibration of test mix
and 3.5 N/mm2 according to the method given concrete A that may still be in a flowing condition. If
in C.4 of BS 5075-1:1982. one result within the set of three obtained on
specimens tested at the same age varies by more
B.5 Loss of workability on standing than ± 5 % from the mean, discard the result and
Determine the slump of test mix concrete A at 4 h, recalculate the mean of the two remaining results. If
when testing retarding superplasticizing more than one result varies by more than ± 5 % from
admixtures, using the method given in BS 1881-102 the mean, discard the set of results and repeat the
after the following operations. tests on the concrete. Calculate the ratio of the mean
compressive strength of the test mix
concretes A and B to that of the control mix
concretes as a percentage, to the nearest 1 %, at the
appropriate ages.
5)
BS 1881-1:1970 is under revision and will be superseded by BS 1881-125 “Methods of mixing and sampling fresh concrete in
the laboratory”.
6 © BSI 10-2000
blank 7
BS 5075-3:1985
Bibliography
6)
BS 1881-1:1970 is under revision and will be superseded by BS 1881-125 “Methods of mixing and sampling fresh concrete in
the laboratory”.
7)
Referred to in the foreword only.
8 © BSI 10-2000
BS 5075-3:1985
© BSI 10-2000
BS 5075-3:
1985
BSI — British Standards Institution
BSI
389 Chiswick High Road
London
W4 4AL