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    Ca-Channel From d8 Endeavor Serviceman Doc-M88-Exx264 v1

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    agoo
    This document provides instructions for adjusting the proportional counter on a D8 ENDEAVOR diffractometer. It describes performing an HV scan to determine the optimal high voltage value, then a pulse height analysis to set the discriminator lower level and width. The HV is set at the maximum value from the scan. A pulse height analyze is then done to evaluate the peak maximum, left limit, and window width which are entered into the configuration and saved.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd

    Ca-Channel From d8 Endeavor Serviceman Doc-M88-Exx264 v1

    Uploaded by

    agoo
    148 views4 pages
    This document provides instructions for adjusting the proportional counter on a D8 ENDEAVOR diffractometer. It describes performing an HV scan to determine the optimal high voltage value, then a pulse height analysis to set the discriminator lower level and width. The HV is set at the maximum value from the scan. A pulse height analyze is then done to evaluate the peak maximum, left limit, and window width which are entered into the configuration and saved.

    Original Description:

    Bruker D8 endeavor Ca-Channel

    Original Title

    Ca-channel from d8 endeavor serviceman doc-m88-exx264 v1

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    This document provides instructions for adjusting the proportional counter on a D8 ENDEAVOR diffractometer. It describes performing an HV scan to determine the optimal high voltage value, then a pulse height analysis to set the discriminator lower level and width. The HV is set at the maximum value from the scan. A pulse height analyze is then done to evaluate the peak maximum, left limit, and window width which are entered into the configuration and saved.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    148 views4 pages

    Ca-Channel From d8 Endeavor Serviceman Doc-M88-Exx264 v1

    Uploaded by

    agoo
    This document provides instructions for adjusting the proportional counter on a D8 ENDEAVOR diffractometer. It describes performing an HV scan to determine the optimal high voltage value, then a pulse height analysis to set the discriminator lower level and width. The HV is set at the maximum value from the scan. A pulse height analyze is then done to evaluate the peak maximum, left limit, and window width which are entered into the configuration and saved.

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    © All Rights Reserved
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    Adjusting the D8 ENDEAVOR

    4.7 Proportional counter (Ca-Channel)

    4.7.1 HV scan
    • Select DIFFRAC.SUITE.COMMANDER as application calibration.

    Detector High Voltage 1530 V


    Discriminator Lower Level 1,4 V
    Discriminator Width 0,2 V
    Amplification 50
    Shape 2

    Primary divergence slit 1 mm / 0,5°


    Soller (prim./sek.) 2,5° axial Soller
    Sample Sample with Ca
    Anti-Scatter Screen Fixed Distance Mode 20 mm
    Sample rotation none
    Theta/2Theta 20°/40°
    Kβ Filter none
    Absorber none
    Detector opening 1D-Modus ca. 3,9°
    Generator Anode kV/mA
    Cu 40 kV/40 mA
    Co 35 kV/40 mA
    Scan range 1200-1800 V
    Scan type HV scan
    Increment 5 V
    Scan Speed 0,5 s

    DOC-M88-EXX264_ V1 - 11.2015_ 61
    Adjusting the D8 ENDEAVOR

    • High-voltage value determined at the maximum value.


    • Enter it as DetectorHighVoltage in the configuration and write changed configuration on
    the system.

    62 DOC-M88-EXX264_ V1 - 11.2015_
    Adjusting the D8 ENDEAVOR

    4.7.2 Pulse Height Analyze

    Detector High Voltage Value determined above


    Amplification 50
    Shape 2

    Primary divergence slit 1 mm / 0,5°


    Soller (prim./sek.) 2,5° axial Soller
    Probe Sample with Ca
    Anti-Scatter Screen Fixed Distance Mode 20 mm
    Sample rotation none
    Theta/2Theta 20°/40°
    Kβ Filter none
    Absorber none
    Detector opening 1D-Modus ca. 3,9°
    Generator Anode kV/mA
    Cu 20 kV/5 mA
    Co 20 kV/5 mA
    Range 0,5-5 V
    Scantype discriminator scan
    Scan Speed 0,5 s

    • Measurement evaluation
    1. Test: peak maximum should be about 1.5 V

    DOC-M88-EXX264_ V1 - 11.2015_ 63
    Adjusting the D8 ENDEAVOR

    2. Check the left limit and window width at about 5-10% peak height: Move the cursor to this
    height and double click.
    ´ A line marks the window position. The software transfers left boundary and window
    width in detector settings.
    3. Read and check values.
    4. Enter values in configuration.
    5. Write configuration in database and activate on your system.

    64 DOC-M88-EXX264_ V1 - 11.2015_

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