Dbs Manual PDF
Dbs Manual PDF
Dbs Manual PDF
Operating instructions
Electronic Moisture Analyser
KERN DBS
Version 1.0
04/2011
GB
DBS-BA-e-1110
KERN DBS
GB Version 1.0 04/2011
Operating instructions
Electronic Moisture Analyser
Contents
1 Technical data ................................................................................................ 4
2 Appliance overview ....................................................................................... 6
2.1 Overview of display.................................................................................................................. 8
2.1.1 Display examples ..................................................................................................................... 12
2.2 Keyboard overview................................................................................................................. 13
3 Basic Information (General)........................................................................ 15
3.1 Proper use............................................................................................................................... 15
3.2 Improper Use .......................................................................................................................... 15
3.3 Warranty .................................................................................................................................. 15
3.4 Monitoring of Test Resources............................................................................................... 15
3.5 Danger Information ................................................................................................................ 16
3.5.1 “Hazard information” sticker ..................................................................................................... 20
4 Transport and storage................................................................................. 21
4.1 Testing upon acceptance ...................................................................................................... 21
4.2 Packaging / return transport ................................................................................................. 21
5 Unpacking, Setup and Commissioning ..................................................... 21
5.1 Installation Site, Location of Use.......................................................................................... 21
5.2 Unpacking and checking ....................................................................................................... 24
5.2.1 Scope of delivery / serial accessories ...................................................................................... 24
5.3 Placing ..................................................................................................................................... 25
5.4 Mains connection ................................................................................................................... 28
5.4.1 Turning On the Power .............................................................................................................. 29
5.5 Commissioning....................................................................................................................... 30
5.6 Connection of peripheral devices......................................................................................... 30
6 Adjustment ................................................................................................... 31
6.1 Adjust balance ........................................................................................................................ 31
6.2 Adjust temperature ................................................................................................................ 33
6.3 ISO/GLP log............................................................................................................................. 36
7 Menu ............................................................................................................. 37
7.1 Navigation in the menu .......................................................................................................... 38
7.1.1 Numeric entry ........................................................................................................................... 39
8 Moisture analysis......................................................................................... 40
8.1 Start drying ............................................................................................................................. 40
8.2 Abort drying ............................................................................................................................ 42
8.3 Finish drying ........................................................................................................................... 42
8.4 Turn off appliance .................................................................................................................. 42
2 DBS-BA-e-1110
9 Drying parameters ....................................................................................... 43
9.1 Save / access .......................................................................................................................... 44
9.2 Adjust ...................................................................................................................................... 45
9.2.1 Drying modes ........................................................................................................................... 45
9.2.1.1 Drying mode AUTO (Standard drying/switch-off criterion “∆M“)......................................... 45
9.2.1.2 Drying mode TIME (Standard drying/switch-off criterion “Time“) ....................................... 46
9.2.1.3 RAPID Drying mode (Rapid drying) ..................................................................................... 47
9.2.1.4 SLOW Drying mode (Slow drying) ....................................................................................... 49
9.2.1.5 STEP Drying mode (Step drying)......................................................................................... 51
9.2.2 Result display ........................................................................................................................... 54
9.2.3 Start criterion ............................................................................................................................ 56
10 Miscellaneous settings................................................................................ 57
10.1 Enter sample designation...................................................................................................... 57
10.2 Set date/time for measuring protocol .................................................................................. 58
10.3 Menu Lock............................................................................................................................... 59
10.4 Change password .................................................................................................................. 61
10.5 Enter identification number................................................................................................... 62
10.6 Resetting the menu ................................................................................................................ 63
11 Print, store and call-up measurement results ........................................... 64
11.1 Pin allocation RS232C interface ........................................................................................... 65
11.2 Interface parameters .............................................................................................................. 66
11.3 Output interval ........................................................................................................................ 68
11.4 Call up and print out measuring results .............................................................................. 69
11.5 Print out currently preset drying parameters...................................................................... 70
11.6 Delete measuring results from memory .............................................................................. 71
11.7 Printout examples .................................................................................................................. 72
12 General information concerning moisture analysis ................................. 75
12.1 Application .............................................................................................................................. 75
12.2 Basics ...................................................................................................................................... 75
12.3 Adjustment to existing measuring method ......................................................................... 75
12.4 Preparing a sample ................................................................................................................ 76
12.5 Sample material ...................................................................................................................... 77
12.6 Sample size / originally weighted in quantity...................................................................... 77
12.7 Drying temperature ................................................................................................................ 78
12.8 Recommendations / Guidelines............................................................................................ 78
13 Service, maintenance, disposal.................................................................. 83
13.1 Cleaning .................................................................................................................................. 83
13.2 Service, maintenance............................................................................................................. 84
13.2.1 Remove protective glass guard ........................................................................................... 84
13.2.2 Lamp change ....................................................................................................................... 86
13.2.3 Replacing fuses.................................................................................................................... 87
13.3 Disposal................................................................................................................................... 87
14 Instant help................................................................................................... 88
14.1 Error messages ...................................................................................................................... 89
15 Declaration of conformity ........................................................................... 91
DBS-BA-e-1110 3
1 Technical data
50°C - 200°C
Temperature range
1°C increments selectable
Warm-up time 2h
Reproducibility
0.001 g
„Weighing mode“
Recommended adjustment
50g (F1)
weight, not added (class)
• 5°C….+40°C ambient temperature
Environmental conditions
• max 85% air humidity non-condensing
4 DBS-BA-e-1110
• AUTO
Switch-off criterion
The drying is finished when the preset weight loss
(∆M ) remains constant for 30 seconds.
• TIME
The drying is finished after the preset time, 1 minute –
4 hours (1 minute increments)
or 12 hours can be selected
DBS-BA-e-1110 5
2 Appliance overview
Front view:
Pos. Description
1 Viewing panel
2 Sample dish
3 Display
4 Bubble level
5 Keyboard
6 Adjustable foot
7 Heated cover
8 Halogen lamp
9 Temperature sensor
6 DBS-BA-e-1110
Rear view:
Pos. Description
10 Anti-theft protection device connection
11 Not documented
12 RS232
13 USB, not documented
14 Mains connection socket
15 Fuse box
DBS-BA-e-1110 7
2.1 Overview of display
AUTO
Heating-up period
TIME
Heating-up period
8 DBS-BA-e-1110
RAPID
Heating-up period “pre-heating
step”
SLOW
Heating-up period
STEP
Heating-up period step 1
Drying step 1
+ see chap. 9.2.1.5
Drying step 2
Drying step 3
DBS-BA-e-1110 9
6
Previous drying time
7
Current temperature
Weight display
Display % moisture
10 DBS-BA-e-1110
a Status display „Equipment“
DBS-BA-e-1110 11
2.1.1 Display examples
During drying:
After drying:
2 Previous time
3 Current temperature
9 Measuring value (unit in the preset result display) + see chap. 9.2.2
12 DBS-BA-e-1110
2.2 Keyboard overview
Turn on/off
• Call up menu
• Scroll back
• Taring
• Zeroing
DBS-BA-e-1110 13
• Exit menu
• Back to moisture analysis mode
• Quit
Start drying
Complete drying
14 DBS-BA-e-1110
3 Basic Information (General)
3.3 Warranty
Loss of warranty due to
DBS-BA-e-1110 15
3.5 Danger Information
WARNING
! The moisture analyser is used to analyse the moisture content of materials.
This instrument must be used exclusively for this purpose. Any other usage
may cause a risk to personnel, damage to the equipment or other material
damage.
! The moisture analyser should be used mainly for the drying of aqueous
substances.
! Carefully read this operation manual before setup and commissioning, even if
you are already familiar with KERN appliances.
16 DBS-BA-e-1110
! Make sure that liquids do not get in contact with the interior of the device or
the connections at the rear of the device.
If you spill liquid on the device, disconnect it immediately.
Afterwards do not operate the moisture analyzer and have it checked by a
competent KERN stockist before any further use.
! Never place combustible materials on, under or next to the equipment, as the
environment of the instrument heats up to a high temperature.
DBS-BA-e-1110 17
! Explosive, easily flammable samples and samples that go into a chemical
reaction when subjected to heat, may not be analysed with the moisture
analyser.
! Careful when removing the sample. The sample itself, the sample dish and the
heating unit may be very hot.
18 DBS-BA-e-1110
Hazards during and after measuring
! Careful when removing the sample. The sample itself, the sample dish and the
heating unit may be very hot.
! Use the sample retainer at all times as it allows safe working and prevents
burns.
! Individual parts of the case (e. g. the ventilation grids) may heat up
considerably during operation. Therefore, only take hold of the equipment by
the marked handles.
DBS-BA-e-1110 19
3.5.1 “Hazard information” sticker
! Ventilation grilles and inspection windows may become very hot during
operation
! Disconnect the equipment from the power supply prior to changing a lamp,
see chap. 13.2.2.
20 DBS-BA-e-1110
4 Transport and storage
DBS-BA-e-1110 21
On the installation site observe the following:
! Protect the device against direct draughts due to open windows and doors.
! Avoid extreme heat and temperature fluctuations e.g. due to installation next
to radiators.
22 DBS-BA-e-1110
! Never store materials on the equipment.
! Do not expose the device to extreme dampness for longer periods of time.
Non-permitted condensation (condensation of air humidity on the appliance)
may occur if a cold appliance is taken to a considerably warmer environment.
In this case, acclimatize the disconnected appliance for ca. 2 hours at room
temperature.
DBS-BA-e-1110 23
5.2 Unpacking and checking
Open package, take out the appliance and accessories. Verify that there has been no
damage and that all packing items are present.
1. Instrument
2. 50 disposable sample dishes
3. Dish holder
4. Wind protection ring
5. Heat shield
6. Spare fuse
7. Removal aid
8. Power cable
9. Protective cover
10. Operating instructions
11. Menu overview
12. Hexagonal socket wrench
24 DBS-BA-e-1110
5.3 Placing
The moisture analyser is delivered in pieces. Check immediately after unpacking all the
parts that the delivery is complete and assemble the individual components as described
below.
1. Fit heat shield.
DBS-BA-e-1110 25
3. Install dish holder, ensuring correct positioning, on .
5. Level the equipment with foot screws [1] until the air bubble of the water balance is
in the prescribed circle.
26 DBS-BA-e-1110
Fig. 1
Fig. 2
If the air bubble is at the lefthand edge, level the equipment with the righthand foot
screw, see Fig.1.
If the air bubble is at the righthand edge, level the equipment with the lefthand foot
screw, see Fig.2.
Fig. 3
Fig. 4
If both foot screws are turned simultaneously in clockwise direction, the air bubble will
move forwards (see Fig.3).
If both foot screws are turned simultaneously in anticlockwise direction, the air bubble will
move backwards (see Fig.4).
DBS-BA-e-1110 27
5.4 Mains connection
Power supply is provided via the supplied mains cable.
Check, whether the voltage acceptance on the scales is set correctly. Do not connect
the appliance to the power grid unless the information on the appliance (sticker)
matches the local mains voltage.
Important:
Does the labelling (115 VAC ± 10% or 230 VAC ± 10%) match the local mains
voltage?
- Do not connect if mains voltages are different!
- If matching, connect the scales.
The moisture analyzer must be connected to a standard socket with earth terminal.
Do not eliminate the protective effect by using an extension lead without earth
terminal. For power supplies from power grids without earth terminals call a specialist
to establish equivalent protection according to the relevant installation regulations.
28 DBS-BA-e-1110
5.4.1 Turning On the Power
Supply balance with power via the mains power cable. The display lights up and
the equipment conducts a self-test.
To switch on press the ON/OFF button. The equipment conducts a segment test.
As soon as the weight display appears, the instrument will be ready to weigh.
DBS-BA-e-1110 29
5.5 Commissioning
In order to obtain exact results, the appliance must have reached its operating
temperature (see warm-up time chap. 1).
For this warm-up time the appliance must be connected to the power supply.
The accuracy of the appliance depends on the local acceleration of gravity.
Strictly observe hints in chapter Adjustment.
30 DBS-BA-e-1110
6 Adjustment
DBS-BA-e-1110 31
• If the value of the adjustment weight needs to be changed, use the
navigation buttons to make the required setting (see chap. 7.1.1.
“Numerical input”).
• The adjustment protocol output is started upon connection to an
optional printer and activated GLP function (see chap. 6.3).
When the adjustment weight display flashes, e.g.
50g, place it carefully in the centre of the sample
dish.
Adjustment starts.
32 DBS-BA-e-1110
6.2 Adjust temperature
We recommend sometimes to check the temperature value of the device using the
optional temperature calibrating set DBS-A01. The temperature is measured at two
points (100°C and 180°C) and can be adjusted at these two points.
The equipment should cool down first to room temperature after the last heating
period.
Preparation:
Fix the temperature sensor on the
temperature calibration set in
accordance with the illustration.
DBS-BA-e-1110 33
Call up menu:
Press the Menu button to access the menu and
the first menu item “PRoGRM” will be
displayed.
Use navigation buttons to select menu
item “CAL”.
• Do not leave the heated cover open for more than 1 minute during the
heating-up period, otherwise the error message “ERR.100” will appear.
In this case press ESC and restart menu item “TEMP”.
• Attention: some parts e.g. ventilation grilles and inspection windows
may become very hot during operation.
• The adjustment must be made within 15 minutes when the temperature
display flashes, otherwise the temperature adjustment will be aborted
(ABORT will be displayed).
Temperature calibration for the first point takes
15 min. Compare the displayed temperature
value on the thermometer with that of the
moisture analyser whilst the temperature
display is flashing. If the two values do not
match, correct them using the navigation
buttons and confirm with the ENTER
button Numerical input, see chap. 7.1.1.
34 DBS-BA-e-1110
The second temperature point to be tested will
be displayed.
Confirm with the ENTER button, the second
heat-up phase is started.
Temperature calibration for the second point
takes 15 min. Compare the displayed
temperature value on the thermometer with that
of the moisture analyser whilst the temperature
display is flashing. If the two values do not
match, correct them using the navigation
buttons and confirm with the ENTER
button Numerical input, see chap. 7.1.1.
The adjustment is completed when “END” is
displayed. The device returns to the menu
automatically.
The adjustment protocol output is started upon
connection to an optional printer and activated
GLP function (see chap. 6.3).
DBS-BA-e-1110 35
6.3 ISO/GLP log
Quality assurance systems require printouts of measuring results as well as of
correct adjustment stating date and time and equipment identification. The easiest
way is to have a printer connected.
36 DBS-BA-e-1110
7 Menu
DBS-BA-e-1110 37
7.1 Navigation in the menu
• Call up menu
• Exit menu
38 DBS-BA-e-1110
7.1.1 Numeric entry
DBS-BA-e-1110 39
8 Moisture analysis
First set the drying parameters as described in chap. 9 during initial start-up.
40 DBS-BA-e-1110
Close heated cover and measuring will start
automatically.
DBS-BA-e-1110 41
8.2 Abort drying
The measuring can be aborted at any time by
pressing the STOP button. A long signal will sound,
and “ABORT” will be displayed.
Either
Press ESC key. The equipment reverts to Moisture
analysis mode and the measuring result is
discarded.
or
Press STOP key again.
The measuring result, marked by the indicator [ ]],
will be displayed and saved.
42 DBS-BA-e-1110
9 Drying parameters
The equipment can be used to store complete drying programs with drying
parameters individually adapted to the sample.
Four drying modes (Standard drying, Step drying, Slow drying and Rapid drying) and
two switch-off criteria (Time-controlled and Automatic) can be selected.
Further parameters such as drying time, drying temperature and ∆M (constant weight
loss per 30 seconds) should be set depending on the modes, see table below.
Select memory location for the drying program prior to selecting the drying
parameters, see chap. 9.1.
DBS-BA-e-1110 43
9.1 Save / access
10 memory locations, which can be simply called up and started as necessary under
the saved Program number, are available for complete drying processes.
44 DBS-BA-e-1110
9.2 Adjust
• ∆M
Press the Menu button to access the menu and
the first menu item “PRoGRM” will be displayed.
DBS-BA-e-1110 45
9.2.1.2 Drying mode TIME
(Standard drying/switch-off criterion “Time“)
The drying will be carried out at the drying temperature preset by the user and will
end automatically when the preset time has expired.
SETTINGS:
• Drying mode TIME
• Drying temperature
• Drying time
46 DBS-BA-e-1110
9.2.1.3 RAPID Drying mode (Rapid drying)
A preheating step is switched on for Rapid drying, i.e. the temperature will increase
very quickly and will exceed the preset drying temperature until it falls below the
preset reference value (weight loss/30 sec).
After that the temperature will be adjusted down to the set value. The drying will end
depending on the setting, when the preset time has expired or the preset weight loss
(∆M) remains constant for 30 seconds.
Rapid drying is suitable for samples with high moisture content (e.g. liquids).
Settings:
• RAPID Drying mode
• ∆M “pre-heating step”
• Drying temperature
DBS-BA-e-1110 47
Press ENTER to confirm selection. The currently
present switch-off criterion will be displayed.
Use navigation buttons to select the
required setting,
TIME = time-controlled
∆M = automatic
TIME setting
Press ENTER to confirm selection. The currently
set drying time is displayed.
Use navigation buttons to select the
required setting, 1 minute – 4 hours (1 minute
increments) or 12 hours can be selected
Press ENTER to save.
48 DBS-BA-e-1110
9.2.1.4 SLOW Drying mode (Slow drying)
The Slow drying temperature is increased more slowly to the preset value than for
Standard drying.
The drying will end depending on the setting, when the preset time has expired or the
preset weight loss (∆M) remains constant for 30 seconds.
Slow drying is suitable for samples that cannot tolerate rapid heating by the heaters.
The same applies to samples that form a skin during rapid heating. This skin will then
affect the evaporation of the trapped moisture.
Settings:
• Drying temperature
DBS-BA-e-1110 49
Press ENTER to confirm selection. The currently
present switch-off criterion will be displayed.
Use navigation buttons to select the
required setting,
TIME = time-controlled
∆M = automatic
TIME setting
Press ENTER to confirm selection. The currently
set drying time is displayed.
Use navigation buttons to select the
required setting, 1 minute – 4 hours (1 minute
increments) or 12 hours can be selected
Press ENTER to save.
50 DBS-BA-e-1110
9.2.1.5 STEP Drying mode (Step drying)
Step-by-step drying is suitable for substances that display special behaviour during
warming. 2 or 3 steps can be selected.
The individual steps are freely selectable regards duration and temperature rising
step.
The drying will end depending on the setting for step 2 or 3, when the preset time has
expired or the preset weight loss (∆M) remains constant for 30 seconds.
Settings:
or or
-
∆M ∆M
DBS-BA-e-1110 51
4. Preset drying time for step 1
Press ENTER to confirm. The currently preset
drying time for step 1 will be displayed.
Use navigation buttons to select the
required setting, 1 minute – 4 hours (1 minute
increments) can be selected
5. Set drying temperature for step 2
Press ENTER to confirm and the currently
preset drying temperature for step 2 will flash
in the display.
Use navigation buttons to select the
required setting,
50°C – 200°C (1°C increments) can be
selected.
6. Set drying time or ∆M for step 2
Acknowledge using ENTER key, the current
setting is displayed.
Use navigation buttons to select switch-
off criterion (TIME or ∆M) for step 2.
Setting ∆M
Press ENTER to confirm selection. The
currently preset value for ∆M will be
displayed.
Use navigation buttons to select the
required setting, 0.01% – 0.1% (0.01%
increments) can be selected.
or
TIME setting
Press ENTER to confirm selection. The
currently set drying time is displayed.
Use navigation buttons to select the
required setting, 0 minutes – 240 hours (1
minute increments) can be selected
If 0 minutes are entered, the next step will be
cancelled.
Press ENTER to confirm.
Continue from step 8 for 2-step drying.
Continue from step 7 for 3-step drying.
52 DBS-BA-e-1110
7. Set drying parameters for step 3.
For drying temperature input, see step 5.
DBS-BA-e-1110 53
9.2.2 Result display
The result display enables the selection of a display in % moisture, % dry mass,
ATRO* dry mass, ATRO* moisture and residual weight in grams.
Calculation:
Explanation of symbols
W: Starting weight (weight at start of measuring)
D: Residual weight (weight value at the end of measurement)
M: Weight loss = starting weight – residual weight
[%] moisture
0 – 100%
ATRO* moisture:
0 – 999%
Menu settings:
Press the Menu button to access the menu and
the first menu item “PRoGRM” will be displayed.
54 DBS-BA-e-1110
Use the navigation key to select menu item
„UNIT“.
Acknowledge using ENTER key, the current
setting is displayed.
Select the desired unit using the navigation keys
( ).
Display Description
DBS-BA-e-1110 55
9.2.3 Start criterion
The menu item “START” enables the selection of Manual and Automatic start of a
measurement.
56 DBS-BA-e-1110
10 Miscellaneous settings
Options:
1st and 2nd digit: „0 – 9“ or „A –Z“ or „_“
3th and 4th digit: “0-9” (the value is automatically increased by “1” for each
measurement, it reverts to “00” upon reaching “99”)
DBS-BA-e-1110 57
10.2 Set date/time for measuring protocol
Display Description
[YYMMDD] Year/Month/Day
[MMDDYY] Month/Day/Year
[DDMMYY] Day/Month/Year
58 DBS-BA-e-1110
10.3 Menu Lock
The menu setting operations can be locked so that the settings cannot be changed.
The following menu blocks are available despite menu lock.
DBS-BA-e-1110 59
Remove the menu lock
60 DBS-BA-e-1110
10.4 Change password
Standard password (factory setting): „9999“
DBS-BA-e-1110 61
10.5 Enter identification number
Options:
Four characters, to select from „0 – 9“ or „A –Z“ or „_“
62 DBS-BA-e-1110
10.6 Resetting the menu
A menu reset will return all the settings to factory setting.
DBS-BA-e-1110 63
11 Print, store and call-up measurement results
The data exchange between moisture analyser and printer occurs via the RS 232C
interface.
In addition to the measurement result, for the finished drying process all drying
parameters are automatically stored with the printout (100 positions). The memory
location designation is automatically allocated with a consecutive number (XX00 –
XX99) as well as a selectable designation “XX” (see chap. 10.1).
+ Call up and print out measuring results, see chap. 11.4
RS232
• Communication parameters (baud rate, bits and parity) for moisture analyser
and printer must concur, see chap. 11.2.
64 DBS-BA-e-1110
11.1 Pin allocation RS232C interface
DBS-BA-e-1110 65
11.2 Interface parameters
Baud rate 1200bps 2400bps 4800bps 9600bps 19.2k bps 38.4k bps
• Parity
Selectable settings:
Display P.NoNE* P.oDD P.EVEN
Parity Small parity, 8 bit Odd parity, 7 bit Straight parity, 7 bit
• Stop bit
Selectable settings:
Display SToP. 1* SToP. 2
66 DBS-BA-e-1110
• Handshake
Selectable settings:
Display HS.HW* HS.SW HS.TiM HS.oFF
Hand- Hardware
Software handshake Timer handshake No handshake
shake handshake
• Delimiter (terminator)
Selectable settings:
Display CR* LF CR+LF
Terminat
CR LF CR+LF
or
Press ESC to return to Moisture analysis mode.
DBS-BA-e-1110 67
11.3 Output interval
68 DBS-BA-e-1110
11.4 Call up and print out measuring results
DBS-BA-e-1110 69
11.5 Print out currently preset drying parameters
70 DBS-BA-e-1110
11.6 Delete measuring results from memory
DBS-BA-e-1110 71
11.7 Printout examples
72 DBS-BA-e-1110
2. Adjustment log „Balance“
-COMPLETE
-SIGNATURE-
Signature Processor
DBS-BA-e-1110 73
3. Adjustment log „Temperature“
-COMPLETE
-SIGNATURE-
Signature Processor
74 DBS-BA-e-1110
12 General information concerning moisture analysis
12.1 Application
In all cases where moisture is added to or removed from products, a fast
determination of the moisture content is of enormous importance. For countless
products the moisture content is not only a quality feature but also an important cost
factor. Very often fixed limits for moisture content apply to the trade in industrial or
agricultural goods as well as chemical or food products which are defined by terms of
delivery and general standards.
12.2 Basics
Moisture does not only mean water but includes all substances that evaporate when
heated up. In addition to water this includes,
- Fats
- Oils
- Alcohol
- Solvent
- etc...
There are various methods to analyse moisture in a product.
KERN DBS uses a method called thermogravimetrics. In accord with this method, the
sample is weighed before and after heating, determining the material moisture by
looking at the difference.
The conventional drying chamber method follows the same principle, with the
exception that this method requires a considerably longer measuring period. . In
accord with the drying chamber method, the sample is heated from the outside to the
inside by a hot air current, so as to remove the moisture. The radiation applied in the
KERN DBS penetrates mainly the sample in order to be transformed inside it into
heat energy that is, warming from the inside to the outside. A minor amount of
radiation is reflected by the sample, a reflection that is less in dark samples than in
light-coloured ones. The depth of penetration of the radiation depends on the
permeability of the sample. In samples of low permeability the radiation only
penetrates the outer layers of the sample, possibly resulting in imperfect drying,
incrustation or burning. For that reason the preparation of a sample is of great
importance.
DBS-BA-e-1110 75
12.4 Preparing a sample
Prepare one sample at a time for measuring. This prevents the sample from
exchanging moisture with its surroundings. If several samples have to be taken at the
same time, they should be packed in airtight boxes so that they do not undergo
changes during storage.
To receive reproducible results, spread the sample thinly and evenly on a sample
dish.
Patchy spreads will produce inhomogeneous heat distribution in the sample to be
dried resulting in incomplete drying and increased measuring time. Sample clusters
generate increased heating of the upper layers resulting in combustion or
incrustation. The high layer thickness or possibly arising incrustation makes it
impossible for the moisture to escape from the sample. Due to this residual moisture,
measured results calculated in this way will not be comprehensible or reproducible.
For liquids, pastes or melting samples we recommend to use a glass fiber filter. The glass
fiber filter has the following advantages:
• Even distribution thanks to capillary attraction
• no formation of droplets
• fast evaporation due to a greater surface
76 DBS-BA-e-1110
12.5 Sample material
Easy to determine are usually samples with the following characteristics:
- Grainy to powdery, pourable solids
- Thermally stable materials, emitting the moisture to be determined easily
without other substances evaporating at the same time
- Liquids that vaporize to leave a dry substance without developing a film
DBS-BA-e-1110 77
12.7 Drying temperature
Bear in mind the following factors when setting the drying temperature:
Colour of sample:
Light-coloured samples reflect more heat radiation than dark ones and therefore
require a higher drying temperature.
78 DBS-BA-e-1110
Table of applications:
Drying Solid
Weight Drying Moisture
period body
Material Sample temperature %
(approx.) %
(g) ( °C) (approx.)
(min) (approx.)
ABS (Novodur P2H-AT) 10 60 10 0.11
Accumulator lead 10 110 2,6 0.19
Acryl granulate 10-15 80 12 0.18
Activated carbon 10 80 9,8 13.33
Activated carbon 7.6 80 4.1 6.12
Sliced pineapple 5 110 14.4 6.71
Sliced apple (dry) 5-8 100 10-15 76.5
Sliced apple (humid) 5-8 100 5-10 7.5
Artesan powder 0.5 80 3.5 98.44
Aspartame granulate 0.5 105 3.4 96.84
Bath milk 3 80 27.4 83.87
Cotton seed 3-4 110 6.3 6.8
Blue-veined cheese 2 160 13.3 53.06
Body lotion 3 80 31.6 87.76
Beans 4.5 150 9.7 11.85
Butter 1.7 140 4.3 84.95
Acetyl cellulose 5.5-6 50 1.3 0.81
Chinese Virility powder 2.5-3 110 5.5 6.24
CN photographic paper 2 150 6.4 5.81
Cornflakes 2-4 120 5-7 9.7
Roof tile mass 2.5 160 10 81.74
Roof tile mass 7 160 20 81.74
Dialysis membrane
0.5 80 2.2 7.85
(Polyethes – polycarbonate)
Dialysis membrane
0.5-0.7 80 2.0 7.86
(Polyethes – polycarbonate)
Indoor sealing compound 3 160 7 64.04
Dispersion adhesive 1.5 140 9.5 55.69
Dispersion adhesive (watery) 2.5 155 7.2 43.77
Dolomite 10-12 160 6.1 0.06
Printer ink fluid 1.5 120 10 19.15
E-filter dust of waste
7-10 135 7 26.23
incineration
Peas, „danish yellow“ 3.5 135 7.9 15.19
Peanut cores 2.8 100 4 1.97
Peanut cores 3 100 6 3.2
Refreshment candies 3-3.4 90 2.9 0.29
Dye powder 1.5 120 3.5 99.07
Fine ceramic mass 2.5 160 9 86.89
Film waste 8-9 60 1.2 0.4
River water 4 160 20 99.2
Fudge/sugar mass 5 130 20 8
Formaldehyde urea dispersion 2 155 7.6 34.07
Cottage cheese 1.4 70 15 41.03
Forage pellets 3-4 150 5.7 6.35
Dried beans 3-4 105 5 7.3
Dried peas 5-7 110 9.6 5.89
Dried carrots 5.5-6 120 3 4.92
Dried chicken dung 4 140 8 14.81
Dried corn 5-7 110 10 6.21
Glass powder 8-10 160 5 0.26
DBS-BA-e-1110 79
Drying Solid
Weight Drying Moisture
period body
Material Sample temperature %
(approx.) %
(g) ( °C) (approx.)
(min) (approx.)
Setting lotion 0.01 145 9 98.76
Setting lotion (extra strong) 1 130 8 97.85
Hair styling gel 5 105 37.0 94.71
Oat flakes 2 105 5.6 9.35
Hazelnut cores 2.2 100 3.8 4
Hazelnut cores (peeled) 2.6 100 4.5 3.74
Hydranal sodium tatrate – 2
1.6 160 12 15.67
– hydrate
Yoghurt 2-3 110 4.5-6.5 86.5
Coffee 2 150 8 4.99
Coffee cream 2-3 130 6-8 78.5
Coffee seed 3.5-4 120 8 8.53
Cocoa 2.5 105 4 3.45
Cocoa seed 4-5 130 7.8 6.23
Limestone 12-14 160 5 0.05
Potato powder 2.5-3.0 130 5.8 12.46
Potato chips 3-4 106 7.5 6.9
Ketchup 2 120 18 74.44
Silica gel 9.5 115 4.5 0.63
Adhesive 2-5 136 6-8 54.3
Garlic, powder 2 100 7.3 5.36
Coal powder 4 160 3.4 2.11
Chalk (natural) 8 160 1.7 0.06
Crystal sugar 3 90 2.8 0.05
Synthetic resin dispersion
2 160 5.9 60.21
(diluted)
Latex 1-2 160 5.2 38.64
Latex LE1 3-5 125 10.8 46.58
Latex LE2 3-5 125 9.4 50.37
Latex O44 3-5 125 9.4 50.65
Lentils 4 135 5.4 12.49
Loam soil 10-15 160 5.5 9.89
Loam clay 2.5 160 14.5 80.75
Skim milk powder 4 90 5.5 3.67
Low fat curd cheese 1.2 130 8 18.5
Corn starch 2 160 5.2 89.1
Almonds (caramelised) 3.5 80 4.8 1.81
Almonds (natural) 2.5 100 5.3 4.19
Almonds „californian“ 3 100 5.3 4.34
Margarine 2.2 160 4 19.15
Brick mass 7 160 20 80.13
Mayonnaise 1-2 138 10 56.5
Flour 8-10 130 4.5 12.5
Micronyle 7-8 60 8 0.4
Milk 2-3 120 6-8 88
Milk powder (MMP) 4.5 100 6.3 2.46
Milk powder (VMP) 4.5 100 5.5 2.56
Mozzarella 1.5 160 11.1 45.78
Multivitamin candies 3-3.4 115 3.3 0.4
Natural latex 1.4 160 5.3 42.56
Nougat mass 2.5 103 10 0.6
Noodle dough 0.55 160 5 12
Concentrated orange juice 2-3 115 13 52.1
80 DBS-BA-e-1110
Drying Solid
Weight Drying Moisture
period body
Material Sample temperature %
(approx.) %
(g) ( °C) (approx.)
(min) (approx.)
Paper 2-4 106 10 6.4
PA 6 (Ultramide B3WG5) 10 60 10 0.05
PA 6.6 (Ultramide B3WG5) 10 80 10 0.15
PBTP (Crastin SK645FR) 10 80 10 0.05
PC (Macrolon 2805) 10-12 80 15 0.08
PC/ABS (Babyblend T65MN) 9-11 80 10 0.12
Pepper, black, powder 2 85 8.8 7.97
PMMA (Plexiglass 6N) 10 70 10 0.12
Polypropylene 13 130 9 0.23
Polypropylene 3.3 120 2.2 0.09
Polystyrene sulfonic acid
2-2.5 120 8.7 19.01
Sodium salt solution
POM (Hostaform C9021)) 10 80 10 0.13
PS (Polystyrene 168 N) 10 80 10 0.05
Purine 2 105 3.8 8.64
Curd 1 140 7 18
Curd cheese, „Fat curd cheese“ 1.2 130 8 23
Silica sand 10-14 160 1.9 0.24
Raclette cheese 1.5 160 14.4 56.9
Canola seed 3-4 90 7.4 6.18
Rice (US parboiled) 3.5 105 12.5 10.98
Rye 4.5 150 11.5 10.72
Red wine 3-5 100 15-20 97.4
Sugar beet pulp pellets 4.5 150 8.6 11.77
Salt 2 100 3 4.9
Pretzel sticks 3-4 75 4.5 1.67
Sludge 11-12 130 90 80
Melted cheese 1.5 70 15 35.65
Chocolate 2.5 103 10 0.5
Chocolate powder 2-4 100 4 1.9
Chocolate water 2-3 90 10 6
Hogwash of kitchen waste 4-5 160 21 17.67
Lard 0.70 160 3.5 1.2
Shampoo 2 100 14.1 75.89
Soap 3 120 6 7.86
Mustard 2.5-3 80 19 34.69
Sesame seed 3 130 8 5.48
Soya bean flour 4.6 95 4.9 4.8
Soya beans, granulate 5 110 22.6 12.16
Bruised sunflower seed 3-3.5 100 4 5.92
Sunflower oil 10-14 138 2 0.1
Spaghetti 3 105 15.1 10.63
Rinsing agent 2 80 13.7 59.64
Dust 5-10 104 8-15 7.3
Starch derivative 2.5 150 12.3 30.29
Starch glue 1.5 100 8.9 17.96
Spread cheese 2.5-2.8 160 4.5 36.81
Soup
2-3 80 4.5-7 3
(instant product)
DBS-BA-e-1110 81
Drying Solid
Weight Drying Moisture
period body
Material Sample temperature %
(approx.) %
(g) ( °C) (approx.)
(min) (approx.)
Tobacco 1.5 100 16 10.18
Tea, black 2 105 4 7.67
Pasta 1.5 120 8 10.64
Textile fibre 0.8-1.2 85 3.6 14.03
Theophylline 1.5 130 1.9 7.33
Thermoplastic PUR –
15-18 80 18 0.08
granulate
Walnut 2.8 100 5.6 3.5
Washing powder 2 160 12 7.32
Wheat spring water 2-3 90 10 6
Sausage casing 0.2 150 3.5 78.56
Toothpaste 2 100 7.7 34.28
Pulp 2.5 130 4.5 7.32
Cement 8-12 138 4-5 0.8
Sugar 4-5 138 10 11.9
Sugar beets 2 130 13.4 30.94
82 DBS-BA-e-1110
13 Service, maintenance, disposal
13.1 Cleaning
+ Before any maintenance, cleaning and repair work disconnect the
appliance from the operating voltage.
+ Only carry out cleaning tasks when the equipment has cooled down.
DBS-BA-e-1110 83
13.2 Service, maintenance
The appliance may only be opened by trained service technicians who are
authorized by KERN.
Ensure that the balance is regularly calibrated, see chap. Testing instruments
control.
84 DBS-BA-e-1110
3. Remove protective glass guard and clean with a
commercially available glass cleaner.
DBS-BA-e-1110 85
13.2.2 Lamp change
+ Disconnect equipment from power supply.
+ Only change the lamp when the equipment has cooled down.
1. Light
2. terminal
3. Plug connector
2. Remove plug connector [3]. Remove cable from
terminals [2] with care.
3. Loosen lamp [1] from the clips [4] on both sides.
4. Clips
4. Install new lamp in reverse order.
86 DBS-BA-e-1110
13.2.3 Replacing fuses
+ Disconnect equipment from power supply.
13.3 Disposal
Disposal of packaging and appliance must be carried out by operator according
to valid national or regional law of the location where the appliance is used.
DBS-BA-e-1110 87
14 Instant help
Display is not lit up. • The display unit is not switched on.
The weight display changes • Sample dish has contact with wind protection
constantly / the stability display device or heated cover.
does not appear.
• Draught/air movement
• Table/floor vibrations
88 DBS-BA-e-1110
14.1 Error messages
DBS-BA-e-1110 89
High zero point shift during
ERR.C01
adjustment
ERR.C02
ERR.C04 Press ESC to abort and repeat
There are objects in the sample
adjustment procedure.
Adjustment dish
error
Missing sample dish
ERR.oL
Overload Check sample dish
ERR.-oL
Should other error messages occur, switch balance off and then on again. If the error
message remains inform manufacturer.
90 DBS-BA-e-1110
15 Declaration of conformity
KERN & Sohn GmbH
D-72322 Balingen-Frommern Phone: 0049-[0]7433- 9933-0
Postbox 4052 Fax: 0049-[0]7433-9933-149
E-Mail: info@kern-sohn.de Internet: www.kern-sohn.de
Declaration of conformity
EC-Konformitätserklärung EC-Declaration of -Conformity
EC- Déclaration de conformité EC-Declaración de Conformidad
EC-Dichiarazione di conformità EC-Conformiteitverklaring
EC- Declaração de conformidade EC- Prohlášení o shode
EC-Deklaracja zgodności EC-Заявление о соответствии
D Konformitäts- Wir erklären hiermit, dass das Produkt, auf das sich diese Erklärung bezieht,
erklärung mit den nachstehenden Normen übereinstimmt.
EN Declaration of We hereby declare that the product to which this declaration refers conforms
conformity to the following standards.
CZ Prohlášení o Tímto prohlašujeme, že výrobek, kterého se toto prohlášení týká, je v souladu
shode s níže uvedenými normami.
E Declaración de Manifestamos en la presente que el producto al que se refiere esta
conformidad declaración está de acuerdo con las normas siguientes
F Déclaration de Nous déclarons avec cela responsabilité que le produit, auquel se rapporte la
conformité présente déclaration, est conforme aux normes citées ci-après.
I Dichiarazione di Dichiariamo con ciò che il prodotto al quale la presente dichiarazione si
conformitá riferisce è conforme alle norme di seguito citate.
NL Conformiteit- Wij verklaren hiermede dat het product, waarop deze verklaring betrekking
verklaring heeft, met de hierna vermelde normen overeenstemt.
P Declaração de Declaramos por meio da presente que o produto no qual se refere esta
conformidade declaração, corresponde às normas seguintes.
PL Deklaracja Niniejszym oświadczamy, że produkt, którego niniejsze oświadczenie
zgodności dotyczy, jest zgodny z poniższymi normami.
RUS Заявление о Мы заявляем, что продукт, к которому относится данная декларация,
соответствии соответствует перечисленным ниже нормам.
DBS-BA-e-1110 91