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    FT-IR Chemical Analysis

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    Afrah M
    The FT-IR analysis identified the biomolecules responsible for reducing silver ions and capping the resulting silver nanoparticles synthesized using Curcuma longa tuber extract. Spectra of the extract containing nanoparticles showed absorption peaks corresponding to functional groups like amines, C-O-C and C-O bonds indicating these groups helped reduce silver ions and bind to the nanoparticles. Spectra of the extract without nanoparticles did not show these peaks, suggesting the components responsible for bioreduction and capping.

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    FT-IR Chemical Analysis

    Uploaded by

    Afrah M
    25 views1 page
    The FT-IR analysis identified the biomolecules responsible for reducing silver ions and capping the resulting silver nanoparticles synthesized using Curcuma longa tuber extract. Spectra of the extract containing nanoparticles showed absorption peaks corresponding to functional groups like amines, C-O-C and C-O bonds indicating these groups helped reduce silver ions and bind to the nanoparticles. Spectra of the extract without nanoparticles did not show these peaks, suggesting the components responsible for bioreduction and capping.

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    3Physical approaches

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    The FT-IR analysis identified the biomolecules responsible for reducing silver ions and capping the resulting silver nanoparticles synthesized using Curcuma longa tuber extract. Spectra of the extract containing nanoparticles showed absorption peaks corresponding to functional groups like amines, C-O-C and C-O bonds indicating these groups helped reduce silver ions and bind to the nanoparticles. Spectra of the extract without nanoparticles did not show these peaks, suggesting the components responsible for bioreduction and capping.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    25 views1 page

    FT-IR Chemical Analysis

    Uploaded by

    Afrah M
    The FT-IR analysis identified the biomolecules responsible for reducing silver ions and capping the resulting silver nanoparticles synthesized using Curcuma longa tuber extract. Spectra of the extract containing nanoparticles showed absorption peaks corresponding to functional groups like amines, C-O-C and C-O bonds indicating these groups helped reduce silver ions and bind to the nanoparticles. Spectra of the extract without nanoparticles did not show these peaks, suggesting the components responsible for bioreduction and capping.

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    FT-IR chemical analysis Ag-NPs after extract bioreduction with AgNO 3.

    The spec-
    The FT-IR spectra were recorded to identify the possible
    trum in Figure 7A shows transmission peaks at 3295,
    biomolecules responsible for the reduction of the Ag  ions
    2923, 1638, 1375, 1134, 1004, 851, 514, and 393 cm1.
    and capping of the bioreduced Ag-NPs synthesized by the
    Similarly,

    [cps/uA]
    C. longa extract. After complete bioreduction of Ag, the
    transmission peaks for the tuber-powder extract contain-
    C. longa tuber-powder extract was centrifuged at 15,000
    ing Ag-NPs were at 3329, 2920, 1952, 1643, 1420, 1147,
    rpm for 20 minutes to isolate the Ag-NPs from proteins
    1011, 867, 689, 510, and 299 cm 1. Three absorption peaks
    and other compounds present in the solution. Figure 7A
    located around 867, 1011 and 1147 cm1 can be assigned
    shows the FT-IR spectrum of C. longa tuber powder that
    as the absorption peaks of –C–N stretching vibrations of
    did not contain AgNO3, whereas Figure 7B shows the
    the amine, –C–O–C or –C–O groups, respectively. 24,30 The
    spectrum containing bonds or functional groups such as –C–O–C–, –C–O, and

    –C–N, –C–O–C or –C–O


    C–O
    B C–H
    Transmittance (au)

    O–H 1147 Ag...O


    Ag...O
    A 1952 1420 867
    2920 1643

    3329 689
    851
    1011 510
    1375
    299
    2923 1638 1134
    3295

    514 393
    1004

    4000 3500 3000 2500 2000 1500 1000 500

    Wavelength
    (cm−1)
    Figure 7 Fourier-transform infrared spectra for the Curcuma longa tuber-powder extract
    (A) and Ag/C. longa (B) after 24 ho

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