Scribd Logo
Upload

Welcome to Scribd!

  • 38 views

    Expaiment:: Ppumognote Oohuten Witadandaxc Sodaum

    Uploaded by

    Nilotpaul Kundu Dhrubo
    This experiment aimed to standardize a potassium permanganate solution using sodium oxalate. When potassium permanganate is added to an acidic sodium oxalate solution, it undergoes an oxidation-reduction reaction. By titrating the sodium oxalate solution with potassium permanganate and calculating the molarity, the standardization is achieved. The determined molarity of potassium permanganate from this experiment was 0.021 M, with an error of 8.7% from the expected value of 0.023 M. Factors like impurities in reagents and improper acidity of solutions can impact the accuracy of the results.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd

    Expaiment:: Ppumognote Oohuten Witadandaxc Sodaum

    Uploaded by

    Nilotpaul Kundu Dhrubo
    38 views8 pages
    This experiment aimed to standardize a potassium permanganate solution using sodium oxalate. When potassium permanganate is added to an acidic sodium oxalate solution, it undergoes an oxidation-reduction reaction. By titrating the sodium oxalate solution with potassium permanganate and calculating the molarity, the standardization is achieved. The determined molarity of potassium permanganate from this experiment was 0.021 M, with an error of 8.7% from the expected value of 0.023 M. Factors like impurities in reagents and improper acidity of solutions can impact the accuracy of the results.

    Original Title

    chem 7

    Copyright

    © © All Rights Reserved

    Available Formats

    PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    This experiment aimed to standardize a potassium permanganate solution using sodium oxalate. When potassium permanganate is added to an acidic sodium oxalate solution, it undergoes an oxidation-reduction reaction. By titrating the sodium oxalate solution with potassium permanganate and calculating the molarity, the standardization is achieved. The determined molarity of potassium permanganate from this experiment was 0.021 M, with an error of 8.7% from the expected value of 0.023 M. Factors like impurities in reagents and improper acidity of solutions can impact the accuracy of the results.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    38 views8 pages

    Expaiment:: Ppumognote Oohuten Witadandaxc Sodaum

    Uploaded by

    Nilotpaul Kundu Dhrubo
    This experiment aimed to standardize a potassium permanganate solution using sodium oxalate. When potassium permanganate is added to an acidic sodium oxalate solution, it undergoes an oxidation-reduction reaction. By titrating the sodium oxalate solution with potassium permanganate and calculating the molarity, the standardization is achieved. The determined molarity of potassium permanganate from this experiment was 0.021 M, with an error of 8.7% from the expected value of 0.023 M. Factors like impurities in reagents and improper acidity of solutions can impact the accuracy of the results.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    You are on page 1of 8

    Experiment Numbern 07

    Name ok tRe expaiment:


    SBandardizatien o Potwoaium

    Ppumognote oohuten witadandaxc Sodaum


    Oxolote Soluion
    CowVe CHEM 114
    Name Soumyo Dip Baneryee
    Roll 1903016
    Depontment IPE

    Dede o expeiment 23 November, 2020

    Dode oh oubmunien 6 Decembet, 2020


    Obiective
    TRe
    The obectihve a Ris experiment
    sandond
    patasium poumonganade witk
    stundndtze
    Teaction helps to
    Aodium oralate oluten.

    albout
    abou Oidoien and reduthien theoy. No
    Reo No

    n Re expeument
    ndicaton is ed
    wti
    end point aa e colon o
    to detvmine

    ehumges wk tRe neaohen


    potavium peunanganet

    Tnbroduchen'
    potaium peumanyunaie
    In ths experiment

    autionia tundaroized utR Re help


    odim oxalate aolution, t io a eelox-
    dandand.

    LacUEn .

    o a 7acien in whieh
    A edor Tea etien

    betueen pecie a in
    electron ave tnanakovred
    which
    which
    otomvo thange oxidotion numbeu). Reactm
    nobved in tte eachem

    Mn+4H0
    MnO +3H 5e

    KMnOu4 +5 Na,e2O+6A;So4 kz90 +2Mnsa,t


    5Na, SD4+ 10co2+
    8 HO

    is Tedueed o M and
    In vachen
    MnO
    Mn 0

    2
    oxidized to Co The olkouling
    equetien wed to ealeulate Re stmertk
    eb potuum peunanganade

    V x Sox = Sna
    Vred X Szed

    Indicatoo and why wed

    he dineet 7eactien is alow

    Ma tbuatien . The in
    0D ene ean oee

    pemanganade added to he acidkaed


    drop o
    ozalote oluhen ane not deealorized immediade.
    M jo podueed n the neachion acta a a
    gitR pezmainganate do torm
    Coctaulbyat, They TIeAct

    immecliore oxilodion atates o angnese. hee

    Twact nopid witk onalade to


    in
    in tw,

    give the oducto o KMnOy act an


    gfve .

    eaction. The pink eolo


    auto catakyat n Hius

    even he aohehiom
    kMna diasinguishable.

    veryolilude.

    Appon.cctuo
    t) Analygticol Balanee
    i)Voumebuc lask
    ) Conieal tlonk
    Buwrete

    v) Pipete
    v) Menuring cylnor (5oml)
    vi) Pipete illor
    vil) Fiunmel

    xWine Gauge
    Tnipod
    X) Buween Bwren
    Name a the chemicals wed

    )Na C204 134a/mol)


    )2N HSO4
    in) kMnO4 Souien
    DL woder

    Dat
    pecmangonote bouhen
    Stondardize o potwsoium
    CuitR sanclanud aodium 0Xalode souhon

    No Valume Burette neading DRtoenee Aege


    Fina
    ok buette Volume
    oberscahione NoC204 nidial
    h iial
    acding oho kMn
    m) Readig Rasding
    (ml) (nL)
    10 0,10 9.9 96

    02 10 9.9 19.6 97

    05 196 29.3 9.7


    Calculecho
    = 10 mL
    Na,CgO
    0.05 M
    SNOCaa4
    NagC a
    VMnO 91mL

    zom
    V.XSon Vut X Sul
    Sju

    2X 0.05 X 10
    MnOy
    5 X 9.3

    0.021 M

    Reauld
    M
    Phe deleroninedl atmerth e kMnO4 0.021

    Porcentue
    Knoun value - Oboenved vauue
    Xloo
    Foreertoge oevw
    Known Value

    0.023 O.0U
    Jpo).
    0,02

    8:7

    fercendoge UTON i 8.7


    Dipcusaion tandord
    A kMnOy ia mot a pimany

    ot ke
    Subetance So dedocmmokion
    Some oh the gacto kat might hanper=
    se eNneoW).

    Re potcoee% v
    ciwold
    mwst be atrngy acidie oo
    e ooluhen
    noTunauly wed.
    Ade 70actions. Sulphurue acid io

    Ainee nitrote
    on o
    Ntie acid Uwouitabl
    whuch may
    modewde oton oxidiaing ogent
    Hel Wedl, m a y
    inderhere wth KMn k
    C ion is eent,
    be onidzed to

    rosutta core obtuuned becowe deme pet-


    Aigh
    wed. oxidizing the Hel to
    manganoote i p n

    eliminate TRe intrference o ehloride on. The

    naur renAon
    w acid in the acid sduthen
    owoimg
    esduees tRe MnO
    2+
    MyO+1616H*+ lo e > 2M +5 ++8H20
    amy a ubble entery Re bwette while

    pouung acid Jubbe ohould be emevedb

    dzopping 6ut e solution until tRe ain


    oveibly
    buluble i buwrctte

    3 l n Rhe KMnOu souten, here CN ome impuutie

    maunly MnO, Seme M ve poduced Tem Mnb


    vhich 7eacts wtr MnO4
    kMnOq and oa mare
    MnO
    Mna
    2 MnO +2H20 +3Mm. 5 Min+ 4H*

    Pounangenade aolution should e added moderrodely


    and. at e same time ihas 7o be atixed To

    elem obien eorstavrly

    You might also like