ExPERIMENT-I

To prepare 20M soluâon of Oxafc acd and uth îhs

help determîne the molotby aod atrength of te
queo _solution e KMnDu (pokossurn pexrnagoate)
APEASATyS: Soodard rneanuñoa fiasr io0.rmd, beakex,funnel,burette,
iperte,corical fiOSK,etc.

lCHEMCAsSoftd OxoIe actd,g'uen KMO Soluton,dislled i

oiNPICATOg KNODu îs a selt Indfcator

ED eoT:ColoYiess t permO0ent pink olouY (KMoDy în burete)

to prepare M aclution oxaliC acd usiog s0Oo

coe0Auia Alosk iae the pette §th M
sdluân and pipette aut 10rod of î îno oshed

)Re and il He burette, uh tte uen KMnDi anluTOn.

a)Add the test kibe l e d. HS04 n the anluon

4)Note he friÊnl regdhg the hirette.

ldrooufoe All a permanent ght nk cnlour a fnpated to

the soluion îb the fixaÀn osk on the l0st. single np.
5r. No. Burette Readng ConstoNt 8urette
Inta Reoding Anal Reacng Readîng
1)
2) 15 ml 16 m
3)
 6) NCte the pioal readig of the burette.
) Repecat. the obove steps 4-5 Enes unil y ger a
three conatat reacigs

2KMODy t3H,8Dut 5H,CaOy 2H,0 Kz60yt 2MOSDut18H,0+ID0,

Velune el oxoc odd prepared =100rnd

Molarih el oxafC aâd solufontaken0-05M
Neune e Oxalo acrd sclutionpex Rhation=0ml

ResALT: MOlanty e iven KMoDu aoluâon- O. 0264 M

2) Sxengoth e qven KMno aolufcn= 4.12L4 q
 CaJculotore
)Molañty
Moloriy XmnOu solufon:
MKNOOu VemnoSfichìometnc colent e NnDy
Moxoc oloRomerñe odent oKOTe Ad

MKMnD4 2
O.05 20

M Knu O.0264M

2) Strenath = Molaâty
MKMDOu x 158
0.0261 x 138 = 4134
:. Srengrh
 Date:

422

ExPERIMENT -IL
To prepare 0.05M solution A Ferous Atnoiuim aulphate
(Mohr's salt).usiog Hi eoluâpn Rod Out MOOmty and

ageoeeTYG St0ndard measufoaeOsK 00mbeakexfunne,burettea

pipette, corical flosk

dHEMICALS scid Mohra saltag'ven KMGls sclucn,dslled nter

oNDICATOR: KMOO is a sete hdfcotor

froCEDURE: )epare 100m e o.081 Mohr's salt scufon by cssnng

19609 A Mchr's solt n ciaâled mater. gise the fpette.
th the D.05M Mohrs salt sclutîn andd pipette out
20n4 o ît îo a 0Oshed corical fask.
)inse and RRIL the burette uâth t e aven KMO anlueiD.
)Add one test Hube qull e câl. A,S0, o the acluâo în
ne coial qask.
WNotethe îfaal readfig of the b
5)NO)add KMOly solu§on from burette All a permanent

e)Note the ioal readng e the, hurctte.

E)Repeot the above stepa A-5 nes to qet, a set of
| three ConcOKdant reccnga.
Teacher's Signature:.
 Burette Readfn9 Gonstant Burete
InfERau Readng Rnal eeadng Reodîng
1)
2) 10. m

3) 0.4 m
 M W F

NAME Page No.:

EXPT. YOUVA
NO. Dote:

ocAuATmoNS:

+l3H,0 )x5
KMOD4 8H,S0+10FesOu (NHL), SOL, 6H,0 jSO2Mns0t6

oOgEeuenoNS: Legbt Mohr ' salA =1.960-g

NQuDe Mobr's_salt anlition prepared'-100ml
Molaîy Moht salt aolufon ia D.05M
Volueoe Mohr's 20lt scÓ. taken per Aaioo =20nL

1) Molanky o kMOOy scluEbo = 0.o18G M

2) sExengh q KAAnO ealuiona 2.953gl
)Molaiy KmnOu solufon:
M Mohr's
Saut
VMon's
Sout
Soichiornenfe coîcdent Mohr's Salt
= MI(MOOu X 10.7
0.05 20

MKMnOu--0.O186 M

2) Snengt Molaity x MOIOr MasS

=0-0186 x158.
= 2.953 9l
Strength kMnOu oln. 2.983 q/L
 0ate:

21.4.23

EAPERIMENT -L
o AIM_ T0 test the prescence of cartohdrates o the guen
faod soarople..

iFenlings Test
3
(HOH)
CH0H
t
TOrtYatEcHO+In0tCU
CH0H
(Sodfum Sat
(Red

(Giucose)
2]Benedics Teat
reduciog augarut

AqNO+ NHoH’NHNO + AoDH'

Pg,0+ 2NHuOH2[Ag(NHa)\0H +34,0

(splLde)
COOH
CH,DH
1 NHAOH
CCHOH)L
CHO cOOH (Slvex MÎO)
CGluose) Caluconic Ad)

oRESUT: od sample. contaios cabchurotes.

 Expeiment 0osevoabon Inference
Fehiirg's 0u0nTest
Talke a anl osnount eA kO0d rpe Red ppt Corbohydare
in a dry, est oube.Add tnd Fehligs appeored present
sduñon A & fmA Fehing's soluho
B. Shake weu and heat che soluâon
Tolen's Reagent Test:
Add 2rnd Tollen's eeagent o arbchudale
the given sdmple and hear it Present

Benedicts Test:
Add 2nd q Benedft's Reaqent Red ppt oppeared arbchydrare
to the given sanple and Keep ît present
in the arer boh
 Date:

ExPERIMENT -IY

To test the presence of pIotÂOo he aiven food sample.

EQUATIOAJuret te :OH2
R

H Jn (Blue) N N
(iclet)

NHe
(yellos colQU)

H-NCH --0H +

-N

aRESULT Food soople cootaina protin

 Obsevafon able
Expeviment Obseroion Iference
Eyvet Test:
Add 5 drops e No soludon to tma oler eolouY Protein
Soluion qven sanple. Add oppeas prelent
copp sulphabe dropuise

Xafthaprotels Testi
To t mA e sample ooluton, add a uelo ppt Presence
Prore
feuo drops conc. HNO and heO confire

Boil 1md the sample sou§cn Blue colour Proteîn

with a few drops q ('- nînhdin oimed
onfned
solution
 ExPERIMENT-T

To rest he presceoce of tat îo the given food Sope.

RESULT food soople conts ol/at
 Qesenvafon Table
Expeinent Obsevabn Inference

MSde/pofirgy prescence
Add 2nl alcono tn the given tsoble
Sample. Snake wel.

Trarsucent/ Prescence o
Place a drop e Gt /f0t on Alter greasy spot of\/far
paper
8.4.23
ExPERIMENT-Y
To fdenfy the
TO fuoc+or group present
îo guen orgoic somple (a)
H
a eOUeTON Bronfme Watex
CH

Socfurm. hydogencortonoJe Test (colourless)

RCOOH + NoHO2RcOONO + g0+O9

RESULT: The gven orgooc cormpound contoins carboxyl

Funcâonal group.
-C-0H.
 Expeîinent Oboervaon InterenCe

SBOve orgore corngourd ND unscutahon

No obsenaton ursoroHon
ObSent

add brorine ooter dropuise

Take given cornpound in Efervescen ce Corboryl group

diy teyt tübe:Add pirch 02 is present
soofurn Bîcovbonare
(NO H03)
 Date:

28.4.23
ExeERIMENT-VIL
oAIM: [TO îdentï£y the funcfonal qroupapresent în
given oxgaic sanple (B)
olESWATQ 08ronîbe lotes Teoti
HCC-H
Coourexs)
2)Sodfum budrogencarbonate Testi
R-cOOH +NaHCOR-COONA + Ha0+CO
3) Fexfc chlonde Test:
+ Fedg
(vîolet.. complex)
Punefenal -
oRESULT: The ofuen oxgantc cornpound contoîns Phenotc group
 Expefiment Obsexvaton Inference
TeAt Ro UnsquOHon No Ooserafy unsatuaon.
D*ssolve oroprsc cornpound în 2n bsenE
e y then add bOsine uwater Doh
TetCaboy Gigup No effervescent Conibony goup
dry test
c o , SS bsent
tube.Add a pinch esodiur
bicarbonate N0gHC03O
Teatgheoote GUoup:
Taver gven cornpound in dy vielet
tedt dube. Add 2ml alcohe.
green
COlouY obrouned Phenohc group
îs presert
Sharewel. Then add 2-3md
neutr al Fedg
Fecl:
28-4.29

EXPERIMENT -VIL

To Tdenafy the funcaona group preSent în fiven

oNganic sornple ccy
H
ESUATIN: 06ronine watex Test

32)sodturn hudrogencarbonate TESL

R-cOOH + NOHCOc0ONa t Ha0 +COg
.93
l3)Ferfc Chloñde Testi
6CeHgH ++ Feclg
(Vîolex complex)
ASHOpbenyl hydrozine. Test:
NO
>ENNH

NO
(244-f§itophenyl hydoÂne) (2,4-iritoçhnyl hydrazOne)
La) socium NtOprUssde Test
[eçcadstNo]2" CHgCOCk,\e(cadsND-CHaCOCH,1
(AÎIoprussfde îan) (Red)

oRE3U1T: The gven orgonic oorpund contofDs cotbonyL

 Expefnent Orsenoon tperence
TeArJ saturaion Noobsenvionúnourofon
O73Solve organic compound în 2m obs ent
CUy tthen add bromine wate,dropwse

Take o ven cornpound 0 tesr tube. No eevesene Caboxy? gup

$s absent
Add a pînch e solu bi corboncte.. co2t
done
boreTOe gfven cornpound î0 dry test
phenolfc tube. Add
Corbony p
2, dînitropheng hydrorne Ppt observed.s preent
Shake wel.O, t o o
) Take gîven gven compou nd în Red colouY
dry teat rube. Add 1m NaOH E 2rnl is observed Carbong 9P
Sodiun itroprüsside soluñon. Shake weu Present

Take given compound în dry tesr PhenOltc 9rp

No obSeNaons obsent
tube. Add 2 ml alcohel.Shake weu
Then add 2-3ml neutral Fecl3
6.5.
23

ExPERIMENT- IX

AIM: To Tden¥Ây the funcfonal qroup presert in guen

orgaric sample (oy
(o).
oEQuATION:Bromine Watex, Test
HC=CH, +Br, Hc CH
H Br Ccolourles
2) Sodfurn hydrogencaxbonate TPAt
R-ccoH +NQHCO’R0ONa +Ho0tCO
3Fexrte Chlofde Test:

Vfoler doroplex)
)Dirtaophenul hudrazne Test: NO
NO2

ND2
(244 dîritcpheryl hydane)" (2,4 diitoneng hydazone)
Socumn NSroprusTde Test
(Nitoprusfde ion). (Rod)
5) Tollen's Reagent Test:
RCHO t+ 2[Ag (NH3),1+ g0H"’20g +9Ntg tM,0+ RaooNHa
(From Tollen's Reogent

oRESuLT The gven organic compound ontis Aldehyde Auncfonal

goup. R
Teacher's Signature:
 Expeiment Observation Interence
Teatdsgo5O0 caL NO Obgeivofonunsahurafon
în 2nd
Dfssolve orgafc compounddropseO e abset
dhen add brofine water
Test for Carboxygroup: tube.NO corbox
eeesere gr0upPs
Taxe given compDUnd tn dry test c0o( absent
socum bicorbonate
Add a pînch
Test_denoic GrOyR: Phenofc grp
Take fven cormpound t dry test tube.No observojon îs obsent
Add, 2 md u cohel-Shaxe weU. Then add
2-3 ml neutrau Fela

) Oxe fven compound

2,u-itopheny
in drY test bube,hoaor
hydrone.Shake weu.NO Carbonyg
obsevofioni9roup
Add tute. absent
Tare
) given conpound indy test
and 2 m sodun
Add 1nt NaOHsolution.
oGitroprusside nake weu.

Test or AIdehyde goup: ven o r g a n i c b

u.s)
Take snal anount of
Cornpound în o dry test tube.Hdd, mtimwboc (
Tollens Reagent.=eep the, dest tube
water bat or 2-3 minure,.
5.5.23

EXPERINMENT -X

oA TO îdenay the punconal oxoup present n guen

Cxganic somple (E)

oEQUATION: )Bromine. water Test

C-H
H Ccolaurless)
) Socfum hudrooencoooDate Test
R-coOH+NOHCO2’RcOONA + Ho0+ cog
B)fexic Chlone Test:
GCetsOH t FeclgFe(CeHs3" +3HO+3H*
(ioler cornple)
4 Test for Baue:
R-OH t HC
5) AZo dye Test:
NOND tHa -NSNO
-NH2
(Benzene diozonum
Chloride)

-N=N

B-Naphthe
azo-due
(Scarlerred)
The given oganic compound contons Arino uncRona
H
group RN
 Observafon inference
Expefnent
Tetor UsaurQino: |Ungarurofon
obsevanonS
gmpound în rm4 e obsent
Dissolve organtc dropuse
CUy hen add bromine wte
No elevescenceotoo*
9roup
Take qfven Compound, to dry tesr
bfattora 0go (o absent
tube.Adld a pinch e socum
Tet foPhenoc a1CUP: dry test Sb grp
Tawe fAven compound fn No observoson Phenolfc
tube. Add2 alcoh ol .shake weu. fs absent

Then add, 2-8nl, neutrOU Fed.

TeAt ox B00e:J Base fs
Take snal amnount e given oganic Soluble Present
Cornpound. and add diwe H tott -

oTelt or Arnine erp:

Tare sma) amount ven organfc
Cormpound în a dry test tube. AddO0ngeo ) Arioo Arîno,
md. e d). HU. ool the solution. Add red dye
2rn4 10/ aqueous NaNO) Soluton ts obtoâned present
0 t o 9t. Shave weu. Add 2m akaßnee1j
Soluion a B-naphthol. (o0 urgordh)